CN106423437B - A kind of graphene slurry dispersion grinder for generating electrostatic field - Google Patents

A kind of graphene slurry dispersion grinder for generating electrostatic field Download PDF

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Publication number
CN106423437B
CN106423437B CN201610768484.3A CN201610768484A CN106423437B CN 106423437 B CN106423437 B CN 106423437B CN 201610768484 A CN201610768484 A CN 201610768484A CN 106423437 B CN106423437 B CN 106423437B
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China
Prior art keywords
grinding pot
pyramidal structure
abrasive body
blade
grinding
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CN201610768484.3A
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Chinese (zh)
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CN106423437A (en
Inventor
沈宇栋
章钰锋
张晓�
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Wuxi Dongheng New Energy Technology Co Ltd
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Wuxi Dongheng New Energy Technology Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C18/00Disintegrating by knives or other cutting or tearing members which chop material into fragments
    • B02C18/06Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/83Mixing plants specially adapted for mixing in combination with disintegrating operations
    • B01F33/8305Devices with one shaft, provided with mixing and milling tools, e.g. using balls or rollers as working tools; Devices with two or more tools rotating about the same axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/836Mixing plants; Combinations of mixers combining mixing with other treatments
    • B01F33/8361Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating
    • B01F33/83613Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating by grinding or milling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C18/00Disintegrating by knives or other cutting or tearing members which chop material into fragments
    • B02C18/06Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
    • B02C18/16Details
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C18/00Disintegrating by knives or other cutting or tearing members which chop material into fragments
    • B02C18/06Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
    • B02C18/16Details
    • B02C18/18Knives; Mountings thereof

Abstract

It is specially a kind of graphene slurry dispersion grinder for generating electrostatic field the invention belongs to disperse field of milling, including grinding pot and abrasive body, the abrasive body is pyramidal structure, and the surface of pyramidal structure is equipped with several No.1 blades arranged along generatrix direction;The abrasive body is installed in grinding pot, and can be rotated about the axis under the drive of actuating unit in grinding pot;Abrasive body can be conductive with grinding pot, and abrasive body is connected to the positive electrode and negative electrode of supply unit with grinding pot.It can be realized to the high efficiency dispersion of graphene slurry and that graphene has been effectively ensured is completely laminar structured.

Description

A kind of graphene slurry dispersion grinder for generating electrostatic field
Technical field
It is specially that a kind of graphene slurry for generating electrostatic field disperses grinding dress the invention belongs to disperse field of milling It puts.
Background technology
Graphene is the two dimension crystalline substance for the only one layer atomic thickness for being stripped out from graphite material, being made of carbon atom Body.Graphene is both most thin material and most tough material, 200 times more taller than best steel of fracture strength;Simultaneously It has good elasticity again, and stretch range can reach the 20% of own dimensions.Graphene characteristic possessed by itself, The various fields such as new energy, new material, derived energy chemical, electronic information, aerospace and defence and military realize extensive use.
Since graphene is laminar structured, in order to enable graphene can preserve it preferably during concrete application Characteristic needs to have kept the laminated structure of graphene during graphene is prepared.And the synthetic method of graphene mainly has Two kinds:Mechanical means and chemical method.Mechanical means includes micromechanics partition method, epitaxy method and the method for heating SiC;Change Method is chemical reduction method and chemical dissociation method.It is micromechanics partition method that wherein application is most common, directly by graphene Thin slice is cut down from larger crystal, and gained sheet graphene can be stabilized under external environment.Typical case's system Preparation Method be with another material it is puffing or introduce defect pyrolytic graphite rub, the surface of body phase graphite can generate The crystal of flocculus shape, the graphene containing individual layer in the crystal of these flocculus shapes.But shortcoming is that this method is to utilize the graphite that rubs The thin slice that surface obtains filters out the graphene platelet of individual layer, and size is difficult to control, and can not reliably factory length supply enough The graphite flake sample of application.It is carried out in the prior art using the mode of most preferably mechanical lapping, as Chinese patent CN is a kind of Wet grinding mill, including motor, cylinder, rotation axis and stirring blade, stirring blade is fixed in rotation axis, and rotation axis is threaded through In cylinder, the both ends of cylinder are respectively equipped with preceding connecting plate and rear connecting plate, and inlet port and outlet port, rotation axis are offered on cylinder One end be connected by the first connector with motor, the other end of rotation axis is connected with the second connector.The both ends of rotation axis point It is not threaded through in fore bearing and rear bearing, there is support at the both ends of rotation axis, make rotation axis more stable when rotating, safety coefficient It is high.First lip-type packing, the second lip-type packing and the first oil immersion asbestos packing are sealed processing to one end of rotation axis, 3rd lip-type packing and the second oil immersion asbestos packing are sealed processing to the other end of rotation axis, extend wet grinding mill Service life.For another example Chinese patent CN201366369 discloses a kind of nano dispersion mill, and lateral rotation is set up on babinet There is main shaft, be equipped with fixed seat in wall box, mechanical seal fixed seat is equipped in fixed seat, is set in mechanical seal fixed seat There is upper and lower mechanical seal, grinding chamber flange is equipped in fixed seat side wall, isolation ring is equipped in grinding chamber flange, is being ground Cavity cover board is fixed with by grinding cavity inner sleeve on cell method orchid, in grinding cavit there is grinding microballon, lead in main shaft one end It crosses hubcap sleeve-board and is fixed with grinding grading wheel, feed pipe is fixed in grinding cavity inner sleeve bottom side of the wall, in grinding chamber Grinding microballon charge pipe is fixed on the side wall of set upper side, has charge door cover in the input end buckle closure of grinding microballon charge pipe, Cavity cover board is equipped with sewage draining exit, and buckle closure has sewage draining exit cover on sewage draining exit, ball-cock assembly is equipped on feed pipe, in main shaft Discharge hole is inside offered, the fines outlet connected with discharge hole is equipped at grinding grading wheel center.But the above method only carries To how the method for effective dispersing and disintegrating abrasive material, but when being specifically applied to graphene slurry then there are it is larger the problem of, how The preferable lamellar structure for preserving graphene.
The content of the invention
In order to solve the above technical problem, the present invention provides a kind of graphene slurries for generating electrostatic field to disperse grinding dress It puts, can realize to the high efficiency dispersion of graphene slurry and that graphene has been effectively ensured is completely laminar structured.
To realize above-mentioned technical purpose, the specific technical solution that the present invention takes is a kind of stone for generating electrostatic field Black alkene slurry dispersion grinder, including grinding pot and abrasive body, the abrasive body is pyramidal structure, and the surface of pyramidal structure is set There are several No.1 blades arranged along generatrix direction, the angle between each No.1 blade and pyramidal structure surface is from top to bottom It is sequentially reduced, and at the upper end of pyramidal structure, No.1 blade is vertical with the surface of pyramidal structure, in the lower end of pyramidal structure When No.1 blade it is parallel with the tangential direction on pyramidal structure surface;The abrasive body is installed in grinding pot, and can be in engine It is rotated about the axis under the drive of structure in grinding pot;Abrasive body can be conductive with grinding pot, and abrasive body is connected respectively with grinding pot In the positive electrode and negative electrode of supply unit.
As the improved technical solution of the present invention, the inner wall of the grinding pot is being equipped with several along the axial direction of tank body No. two blades.
As the improved technical solution of the present invention, the width of No. two blades is less than 0.1mm.
As the improved technical solution of the present invention, No. two blades are with perpendicular to the direction setting of grinding top tank structure.
As the improved technical solution of the present invention, the grinding pot offers discharge port in bottom.
As the improved technical solution of the present invention, the width of the No.1 blade is less than 2mm.
Beneficial effects of the present invention
By setting No.1 blade on the surface of abrasive body so that No.1 blade can be 360 ° during rotation for abrasive body Graphene slurry is cut, and the graphene slurry to being sunken to grinding pot lower end after cutting is put down beneficial to the blade of No.1 blade Row carries out cutting and grinding simultaneously in the characteristics of abrasive body surface;
Supply unit is opened in process of lapping, improves slurry to graphene using the electric humidification of graphene and slurry Adhesiving effect, the turbulence that then graphene slurry generates when abrasive body and grinding pot carry out the relative rotation of high speed, in rapids Under dynamic effect and the collective effect of blade, realize the high efficiency dispersion to graphene slurry, and ensure scattered graphite system slurry The complete sheet-shaped of middle graphene.
Description of the drawings
The structure of abrasive body is shown in a kind of graphene slurry dispersion grinder for generating electrostatic field of Fig. 1 present invention It is intended to;
A kind of top view of the grinding pot of graphene slurry dispersion grinder for generating electrostatic field of Fig. 2 present invention;
In figure:1st, abrasive body;2nd, No.1 blade;3rd, grinding pot;4th, No. two blades.
Specific embodiment
To make the purpose of the embodiment of the present invention and technical solution clearer, below in conjunction with the attached of the embodiment of the present invention Figure, is clearly and completely described the technical solution of the embodiment of the present invention.Obviously, described embodiment is of the invention Part of the embodiment, instead of all the embodiments.Based on described the embodiment of the present invention, those of ordinary skill in the art The all other embodiments obtained on the premise of without creative work, belong to the scope of protection of the invention.
Those skilled in the art of the present technique are appreciated that unless otherwise defined, all terms used herein(Including technology art Language and scientific terminology)With the identical meaning of the general understanding with the those of ordinary skill in fields of the present invention.Should also Understand, those terms such as defined in the general dictionary, which should be understood that, to be had and the meaning in the context of the prior art The consistent meaning of justice, and unless defined as here, will not be with idealizing or the meaning of overly formal be explained.
The meaning of heretofore described " inside and outside " referred to compared with equipment itself, the side inside sensing equipment To be interior, on the contrary is specific restriction outer rather than to the device of the invention mechanism.
A kind of graphene slurry dispersion grinder for generating electrostatic field, it is described to grind including grinding pot 3 and abrasive body 1 Mill body 1 is pyramidal structure(As shown in Figure 1), the surface of pyramidal structure is equipped with several No.1 blades 2, each No.1 blade 2 To be arranged along generatrix direction, the angle between each No.1 blade 2 and pyramidal structure surface is sequentially reduced from top to bottom, and No.1 blade 2 is vertical with the surface of pyramidal structure during the upper end of pyramidal structure(No.1 blade 2 and the angle on pyramidal structure surface are 90°), it is therefore intended that for the solid phase graphene that ablation volume is larger, and cause solid phase graphene in grinding pot and abrasive body When under relative rotation when under the action of electric field along lower end of the optimized cutting face in pyramidal structure No.1 blade 2 and pyramidal structure table The tangential direction in face is parallel(No.1 blade 2 and the angle on pyramidal structure surface are 0 °);The abrasive body 1 is installed on grinding pot 3 In, and can be rotated about the axis under the drive of actuating unit in grinding pot 3;Abrasive body 1 can be conductive with grinding pot 3, grinding Body 1 is connected to the positive electrode and negative electrode of supply unit with grinding pot 3;It is electric wet for generate between graphene and slurry Profit;
As preference, abrasive body 1 can generate electric field of the electric field strength less than 1V/nm after powered up with grinding pot 3.
As shown in Figure 2, the inner wall of the grinding pot 3 is being equipped with several No. two blades 4 along the axial direction of tank body;For Ensure the dispersion effect of graphene, the width of No. two blades 4 is less than 0.1mm;No. two blades 4 are with perpendicular to grinding The direction of 3 inner wall of tank is set;The width of the No.1 blade 2 is less than 2mm.
In order to facilitate discharging, the grinding pot 3 offers discharge port in bottom.
As another arrangement of No.1 blade 2, No.1 blade 2 is set along the length direction on the surface of pyramidal structure It puts, and each No.1 blade 2 is along the distribution that rotates in a circumferential direction of abrasive body 1;No.1 blade 2 and pyramidal structure surface angle are from upper It is sequentially reduced under, and at the upper end of pyramidal structure, No.1 blade 2 is vertical with the surface of pyramidal structure, in pyramidal structure No.1 blade 2 is parallel with the tangential direction on pyramidal structure surface during lower end(No.1 blade 2 and the surface angle of pyramidal structure are 0°).
It these are only embodiments of the present invention, description is more specific and in detail, but can not therefore be interpreted as pair The limitation of the scope of the claims of the present invention.It should be pointed out that for those of ordinary skill in the art, the present invention is not being departed from On the premise of design, various modifications and improvements can be made, these are all belonged to the scope of protection of the present invention.

Claims (4)

1. a kind of graphene slurry dispersion grinder for generating electrostatic field, which is characterized in that including grinding pot and abrasive body, The abrasive body is pyramidal structure, and the surface of pyramidal structure is equipped with several No.1 blades arranged along generatrix direction, Mei Geyi Angle number between blade and pyramidal structure surface is sequentially reduced from top to bottom, and the No.1 blade at the upper end of pyramidal structure Vertical with the surface of pyramidal structure, at the lower end of pyramidal structure, No.1 blade is parallel with the tangential direction on pyramidal structure surface; The abrasive body is installed in grinding pot, and can be rotated about the axis under the drive of actuating unit in grinding pot;Abrasive body with Grinding pot can be conductive, and abrasive body is connected to the positive electrode and negative electrode of supply unit with grinding pot;The grinding pot is in bottom Offer discharge port;The width of the No.1 blade is less than 2mm.
2. a kind of graphene slurry dispersion grinder for generating electrostatic field according to claim 1, which is characterized in that The inner wall of the grinding pot is being equipped with several No. two blades along the axial direction of tank body.
3. a kind of graphene slurry dispersion grinder for generating electrostatic field according to claim 2, which is characterized in that The width of No. two blades is less than 0.1mm.
4. a kind of graphene slurry dispersion grinder for generating electrostatic field according to claim 2, which is characterized in that No. two blades are with perpendicular to the direction setting of grinding top tank structure.
CN201610768484.3A 2016-08-31 2016-08-31 A kind of graphene slurry dispersion grinder for generating electrostatic field Active CN106423437B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107470007A (en) * 2017-08-28 2017-12-15 无锡厚发自动化设备有限公司 A kind of lapping device of magnetic

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0011765A1 (en) * 1978-12-05 1980-06-11 Friedrich Wilh. Schwing GmbH Mixer for thick materials, for example filter cakes, slurries or the like, and its use
CN201092635Y (en) * 2007-09-04 2008-07-30 陕西科技大学 Grinding disc of high consistency refining machine
CN201366369Y (en) * 2009-02-20 2009-12-23 边浩光 Nanometer dispersion mill
CN203342727U (en) * 2013-05-08 2013-12-18 淮北龙盘工贸有限责任公司 Cutting and dispersing disc for material mixing and stirring
CN104477882A (en) * 2014-10-23 2015-04-01 江阴碳谷科技有限公司 A vortex graphene stripping device, a graphene producing system and a producing method
CN205056165U (en) * 2015-07-22 2016-03-02 江阴市东仁机械有限公司 Wet -process grinder
CN206082708U (en) * 2016-08-31 2017-04-12 无锡东恒新能源科技有限公司 Can produce graphite alkene paste grinder device of electrostatic field

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0011765A1 (en) * 1978-12-05 1980-06-11 Friedrich Wilh. Schwing GmbH Mixer for thick materials, for example filter cakes, slurries or the like, and its use
CN201092635Y (en) * 2007-09-04 2008-07-30 陕西科技大学 Grinding disc of high consistency refining machine
CN201366369Y (en) * 2009-02-20 2009-12-23 边浩光 Nanometer dispersion mill
CN203342727U (en) * 2013-05-08 2013-12-18 淮北龙盘工贸有限责任公司 Cutting and dispersing disc for material mixing and stirring
CN104477882A (en) * 2014-10-23 2015-04-01 江阴碳谷科技有限公司 A vortex graphene stripping device, a graphene producing system and a producing method
CN205056165U (en) * 2015-07-22 2016-03-02 江阴市东仁机械有限公司 Wet -process grinder
CN206082708U (en) * 2016-08-31 2017-04-12 无锡东恒新能源科技有限公司 Can produce graphite alkene paste grinder device of electrostatic field

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