CN106421747A - Fibroin moisturizing eye drop and preparation method thereof - Google Patents
Fibroin moisturizing eye drop and preparation method thereof Download PDFInfo
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- CN106421747A CN106421747A CN201611053140.0A CN201611053140A CN106421747A CN 106421747 A CN106421747 A CN 106421747A CN 201611053140 A CN201611053140 A CN 201611053140A CN 106421747 A CN106421747 A CN 106421747A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K38/00—Medicinal preparations containing peptides
- A61K38/04—Peptides having up to 20 amino acids in a fully defined sequence; Derivatives thereof
- A61K38/10—Peptides having 12 to 20 amino acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/16—Ginkgophyta, e.g. Ginkgoaceae (Ginkgo family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/287—Chrysanthemum, e.g. daisy
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/42—Cucurbitaceae (Cucumber family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/482—Cassia, e.g. golden shower tree
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/738—Rosa (rose)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8984—Dendrobium
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
- A61K47/14—Esters of carboxylic acids, e.g. fatty acid monoglycerides, medium-chain triglycerides, parabens or PEG fatty acid esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0048—Eye, e.g. artificial tears
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/08—Solutions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
Abstract
The invention discloses fibroin moisturizing eye drop and a preparation method thereof. The eye drop is prepared from the following raw materials in parts by weight: 20 to 34 parts of fibroin, 12 to 19 parts of caulis dendrobii extracting liquid, 2 to 8 parts of honeysuckle flower extracting liquid, 3 to 8 parts of borneol, 12 to 22 parts of white chrysanthemum flower, 4 to 12 parts of folium ginkgo, 2 to 4 parts of propyl hydroxybenzoate, 9 to 13 parts of rose flower extracting liquid, 2 to 4 parts of sorbitol, 3 to 7 parts of water, 3 to 5 parts of watermelon peel extracting liquid and 4 to 10 parts of semen cassiae. The preparation method comprises: feeding the white chrysanthemum flowers, the folium ginkgo and the semen cassiae into an earthenware cooking pot filled with water; decocting by small fire for 4 hours to 6 hours; after cooling, filtering and collecting filtrate for later use; adding the caulis dendrobii extracting liquid, the honeysuckle flower extracting liquid, the rose flower extracting liquid and the watermelon peel extracting liquid into the filtrate in the step 1; heating to 50 DEG C to 60 DEG C; adding the fibroin, the borneol, the propyl hydroxybenzoate, the sorbitol and the water and uniformly stirring; adjusting the pH (Potential of Hydrogen) value to 6 to 7, and sterilizing to obtain the eye drop. The eye drop provided by the invention is long in moisturizing time and good in anti-fatigue effect; the preparation method is simple so that the eye drop is suitable for industrialized production.
Description
Technical field
This area belongs to daily necessities field and in particular to a kind of fibroin moisturizing eyedrops and preparation method thereof.
Background technology
With growth in the living standard, people's operating pressure is big, and the time with eye is also more and more longer, especially uses now
Electronic product many, eye strain has been universal phenomenon.
Eye fatigue arises that dry and astringent, itch, the phenomenon such as eye-blurred, and severe patient can cause intraocular pressure to raise, and causes
More complication.Although existing eyedrops kind is a lot, mostly contain preservative, Long-Time Service has secondary work to eyes
With, in addition the effect of existing liquid medicine relieving eye strain poor it is impossible to alleviate that one's eyes became bloodshot waits other problems.It is thus desirable to
Research and develop that a kind of moisture preserving time is long, antifatigue effect substantially, the life requirement to meet people for the eyedrops of preservative free.
Content of the invention
For the deficiencies in the prior art, it is an object of the invention to provide a kind of fibroin moisturizing eyedrops and its preparation side
Method, this eyedrops moistening effect is good, effectively alleviates eye strain, reduces the risk of eye disease morbidity.
For solving prior art problem, the technical scheme that the present invention takes is：
A kind of fibroin moisturizing eyedrops, including the raw material of following meter by weight：Fibroin 20-34 part, dendrobium extract 12-19
Part, Flos Lonicerae extractive solution 2-8 part, borneol 3-8 part, feverfew 12-22 part, ginkgo leaf 4-12 part, Nipasol 2-4 part, rose
Flower extract 9-13 part, sorbierite 2-4 part, water 3-7 part, watermelon peel extract 3-5 part, cassia seed 4-10 part.
As improved it is, above-mentioned fibroin moisturizing eyedrops, including the raw material of following meter by weight：32 parts of fibroin,
14 parts of dendrobium extract, 6 parts of Flos Lonicerae extractive solution, 5 parts of borneol, 20 parts of feverfew, 10 parts of ginkgo leaf, 3 parts of Nipasol, rose
10 parts of extract of flower, 3 parts of sorbierite, 5 parts of water, 4 parts of watermelon peel extract, 8 parts of cassia seed.
The preparation method of above-mentioned fibroin eyedrops, comprises the following steps：
Step 1, feverfew, ginkgo leaf, cassia seed is incorporated with the marmite of water, fries 4-6 hour by slow fire, be collected by filtration after cooling
Filtrate is standby；
Step 2, the filtrate in step 1 is added dendrobium extract, Flos Lonicerae extractive solution, rose extract and watermelon peel to extract
Liquid, is heated to 50-60 DEG C, adds fibroin, after borneol, Nipasol, sorb alcohol and water stir, after adjusting pH to 6-7
Sterilize to obtain eyedrops.
It is that in step 1, slow fire temperature is 30 DEG C as improved.
It is that in step 2, mixing speed is 200-380rpm as improved.
Beneficial effect
The present invention prepares eyedrops using the good fibroin of performance of keeping humidity for raw material, effectively alleviate excessively with eye cause dry and astringent,
The symptoms such as itch, fibroin and dendrobium extract collocation nourishing eyes cell effectively, therefore Long-Time Service can improve eyesight.
Specific embodiment
Embodiment 1
A kind of fibroin moisturizing eyedrops, including the raw material of following meter by weight：Fibroin 20-34 part, dendrobium extract 12-19
Part, Flos Lonicerae extractive solution 2-8 part, borneol 3-8 part, feverfew 12-22 part, ginkgo leaf 4-12 part, Nipasol 2-4 part, rose
Flower extract 9-13 part, sorbierite 2-4 part, water 3-7 part, watermelon peel extract 3-5 part, cassia seed 4-10 part.
The preparation method of above-mentioned fibroin eyedrops, comprises the following steps：
Step 1, feverfew, ginkgo leaf, cassia seed are incorporated with the marmite of water, and 30 DEG C fry by slow fire 4 hours, filter and receive after cooling
Collection filtrate is standby；
Step 2, the filtrate in step 1 is added dendrobium extract, Flos Lonicerae extractive solution, rose extract and watermelon peel to extract
Liquid, is heated to 50-60 DEG C, adds fibroin, after borneol, Nipasol, sorb alcohol and water stir with the speed of 200rpm,
Sterilize to obtain after adjusting pH to 6-7 eyedrops.
Patient's use that the eyedrops of embodiment 1 is stayed up late congested to eye, about 3-4 hour, the eye trace of blood disappears
Lose, eye MEBO ribbon gauze can keep 15 hours, adhere to dripping and use January, still daily with eye more than 20 hours, eyes all do not have dry and astringent
With symptoms such as hyperemia.
Embodiment 2
A kind of fibroin moisturizing eyedrops, including the raw material of following meter by weight：32 parts of fibroin, 14 parts of dendrobium extract, gold
6 parts of honeysuckle flower extract, 5 parts of borneol, 20 parts of feverfew, 10 parts of ginkgo leaf, 3 parts of Nipasol, 10 parts of rose extract, sorb
3 parts of alcohol, 5 parts of water, 4 parts of watermelon peel extract, 8 parts of cassia seed.
The preparation method of above-mentioned fibroin eyedrops, comprises the following steps：
Step 1, feverfew, ginkgo leaf, cassia seed are incorporated with the marmite of water, and 30 DEG C fry by slow fire 5 hours, filter and receive after cooling
Collection filtrate is standby；
Step 2, the filtrate in step 1 is added dendrobium extract, Flos Lonicerae extractive solution, rose extract and watermelon peel to extract
Liquid, is heated to 50-60 DEG C, adds fibroin, after borneol, Nipasol, sorb alcohol and water stir with the speed of 300rpm,
Sterilize to obtain after adjusting pH to 6-7 eyedrops.
The eyedrops of embodiment 2 is used for putting into practice, with embodiment 1, effect is using 2-3 hour, eye blood to practice condition
Silk disappears, and eye MEBO ribbon gauze keeps 17 hours, adheres to dripping and uses January, the symptom such as eyes are no dry and astringent and congested.
Embodiment 3
A kind of fibroin moisturizing eyedrops, including the raw material of following meter by weight：Fibroin 20-34 part, dendrobium extract 12-19
Part, Flos Lonicerae extractive solution 2-8 part, borneol 3-8 part, feverfew 12-22 part, ginkgo leaf 4-12 part, Nipasol 2-4 part, rose
Flower extract 9-13 part, sorbierite 2-4 part, water 3-7 part, watermelon peel extract 3-5 part, cassia seed 4-10 part.
The preparation method of above-mentioned fibroin eyedrops, comprises the following steps：
Step 1, feverfew, ginkgo leaf, cassia seed are incorporated with the marmite of water, and 30 DEG C fry by slow fire 6 hours, filter and receive after cooling
Collection filtrate is standby；
Step 2, the filtrate in step 1 is added dendrobium extract, Flos Lonicerae extractive solution, rose extract and watermelon peel to extract
Liquid, is heated to 50-60 DEG C, adds fibroin, after borneol, Nipasol, sorb alcohol and water stir with the speed of 380rpm,
Sterilize to obtain after adjusting pH to 7 eyedrops.
The eyedrops of embodiment 3 is used for putting into practice, with embodiment 1, effect is using 3-3.5 hour, eye to practice condition
The trace of blood disappears, and eye MEBO ribbon gauze keeps 16 hours, adheres to dripping and uses January, the symptom such as eyes are no dry and astringent and congested.
Comparative example 1
A kind of fibroin moisturizing eyedrops, including the raw material of following meter by weight：32 parts of fibroin, 6 parts of Flos Lonicerae extractive solution, ice
5 parts of piece, 20 parts of feverfew, 10 parts of ginkgo leaf, 3 parts of Nipasol, 10 parts of rose extract, 3 parts of sorbierite, 5 parts of water, watermelon
4 parts of skin extract, 8 parts of cassia seed.
The preparation method of above-mentioned fibroin eyedrops, comprises the following steps：
Step 1, feverfew, ginkgo leaf, cassia seed are incorporated with the marmite of water, and 30 DEG C fry by slow fire 5 hours, filter and receive after cooling
Collection filtrate is standby；
Step 2, the filtrate in step 1 is added Flos Lonicerae extractive solution, rose extract and watermelon peel extract, is heated to
50-60 DEG C, add fibroin, after borneol, Nipasol, sorb alcohol and water stir with the speed of 300rpm, adjust pH to
Sterilize after 6-7 to obtain eyedrops.
The eyedrops of comparative example 1 is used for putting into practice, with embodiment 1, effect is using 3-3.5 hour, eye to practice condition
The trace of blood disappears, and eye MEBO ribbon gauze keeps 10 hours, adheres to dripping and uses January, the symptom such as eyes are no dry and astringent and congested.
Comparative example 2
A kind of fibroin moisturizing eyedrops, including the raw material of following meter by weight：14 parts of dendrobium extract, Flos Lonicerae extractive solution
6 parts, 5 parts of borneol, 20 parts of feverfew, 10 parts of ginkgo leaf, 3 parts of Nipasol, 10 parts of rose extract, 3 parts of sorbierite, water 5
Part, 4 parts of watermelon peel extract, 8 parts of cassia seed.
The preparation method of above-mentioned fibroin eyedrops, comprises the following steps：
Step 1, feverfew, ginkgo leaf, cassia seed are incorporated with the marmite of water, and 30 DEG C fry by slow fire 5 hours, filter and receive after cooling
Collection filtrate is standby；
Step 2, the filtrate in step 1 is added dendrobium extract, Flos Lonicerae extractive solution, rose extract and watermelon peel to extract
Liquid, is heated to 50-60 DEG C, adds borneol, after Nipasol, sorb alcohol and water stir with the speed of 300rpm, adjusts
Sterilize after pH to 6-7 to obtain eyedrops.
The eyedrops of comparative example 2 is used for putting into practice, with embodiment 1, effect is using 3.5-4 hour, eye to practice condition
The trace of blood disappears, and eye MEBO ribbon gauze keeps 13 hours, adheres to dripping and uses January, eyes are no dry and astringent, but congestive symptom often occurs.
Compared by above-mentioned, eyedrops moisture preserving time of the present invention is long, and antifatigue effect is good, adhere to dripping and use, can alleviate
Eye problems, when fibroin and dendrobium candidum are together as raw material, moistening effect is more preferably obvious.The medicament for the eyes depth of water therefore of the present invention is subject to
With eye, race is liked.
Claims (5)
1. a kind of fibroin moisturizing eyedrops is it is characterised in that include the raw material of following meter by weight：Fibroin 20-34 part, stone
Dry measure used in former times extract 12-19 part, Flos Lonicerae extractive solution 2-8 part, borneol 3-8 part, feverfew 12-22 part, ginkgo leaf 4-12 part, oxybenzene third
Ester 2-4 part, rose extract 9-13 part, sorbierite 2-4 part, water 3-7 part, watermelon peel extract 3-5 part, cassia seed 4-10
Part.
2. fibroin moisturizing eyedrops according to claim 1 is it is characterised in that include the former of following meter by weight
Material：32 parts of fibroin, 14 parts of dendrobium extract, 6 parts of Flos Lonicerae extractive solution, 5 parts of borneol, 20 parts of feverfew, 10 parts of ginkgo leaf, oxybenzene
3 parts of propyl ester, 10 parts of rose extract, 3 parts of sorbierite, 5 parts of water, 4 parts of watermelon peel extract, 8 parts of cassia seed.
3. the preparation method based on the fibroin moisturizing eyedrops described in claim 1 is it is characterised in that comprise the following steps：
Step 1, feverfew, ginkgo leaf, cassia seed is incorporated with the marmite of water, fries 4-6 hour by slow fire, be collected by filtration after cooling
Filtrate is standby；
Step 2, the filtrate in step 1 is added dendrobium extract, Flos Lonicerae extractive solution, rose extract and watermelon peel to extract
Liquid, is heated to 50-60 DEG C, adds fibroin, after borneol, Nipasol, sorb alcohol and water stir, after adjusting pH to 6-7
Sterilize to obtain eyedrops.
4. the preparation method of fibroin moisturizing eyedrops according to claim 3 is it is characterised in that slow fire temperature in step 1
For 30 DEG C.
5. the preparation method of fibroin moisturizing eyedrops according to claim 3 is it is characterised in that mixing speed in step 2
For 200-380rpm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611053140.0A CN106421747A (en) | 2016-11-25 | 2016-11-25 | Fibroin moisturizing eye drop and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611053140.0A CN106421747A (en) | 2016-11-25 | 2016-11-25 | Fibroin moisturizing eye drop and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106421747A true CN106421747A (en) | 2017-02-22 |
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ID=58218847
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611053140.0A Pending CN106421747A (en) | 2016-11-25 | 2016-11-25 | Fibroin moisturizing eye drop and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101642505A (en) * | 2008-08-04 | 2010-02-10 | 刘燕超 | Eye drop for treating myopic eyes |
| CN102319323A (en) * | 2011-10-08 | 2012-01-18 | 贾飞 | Eyedrop for reducing intraocular pressure and treating glaucoma and preparation method thereof |
| CN102579599A (en) * | 2012-03-27 | 2012-07-18 | 江西珍视明药业有限公司 | Decumbent corydalis tuber eye drop and preparation method thereof |
-
2016
- 2016-11-25 CN CN201611053140.0A patent/CN106421747A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101642505A (en) * | 2008-08-04 | 2010-02-10 | 刘燕超 | Eye drop for treating myopic eyes |
| CN102319323A (en) * | 2011-10-08 | 2012-01-18 | 贾飞 | Eyedrop for reducing intraocular pressure and treating glaucoma and preparation method thereof |
| CN102579599A (en) * | 2012-03-27 | 2012-07-18 | 江西珍视明药业有限公司 | Decumbent corydalis tuber eye drop and preparation method thereof |
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Application publication date: 20170222 |