CN106396578A - Inorganic polymer silica gel and method for preparing same - Google Patents
Inorganic polymer silica gel and method for preparing same Download PDFInfo
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- CN106396578A CN106396578A CN201610844620.2A CN201610844620A CN106396578A CN 106396578 A CN106396578 A CN 106396578A CN 201610844620 A CN201610844620 A CN 201610844620A CN 106396578 A CN106396578 A CN 106396578A
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- parts
- powder
- inorganic polymer
- agent
- polymer silica
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00008—Obtaining or using nanotechnology related materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00017—Aspects relating to the protection of the environment
Abstract
The invention discloses inorganic polymer silica gel and a method for preparing the same. The inorganic polymer silica gel comprises gel materials and additives. The inorganic polymer silica gel and the method have the advantages that the inorganic polymer silica gel is a novel green and environment-friendly material which is developed for meeting functional requirements on foam glass materials and has integrated waterproof, anticorrosion, heat-insulation, high-performance, super-early-strength, high-temperature-resistant and freeze-thaw-resistant functions and the like; the inorganic polymer silica gel comprises foundation powder and reinforcement liquid; foundation materials can be used after being added into water and stirred according to general technological requirements and can be compounded and used with added reinforcement materials under the conditions of special technologies, specific locations and foundation treatment requirements, so that the optimal effects can be realized.
Description
Technical field
The present invention relates to Silica hydrogel preparing technical field, more particularly to a kind of inorganic polymer Silica hydrogel and its preparation side
Method.
Background technology
Foam glass is a kind of thermal insulation of superior performance（Cold insulation）, sound absorption, moistureproof, fireproof light high-strength building material and
Ornament materials, is subzero 196 degree to 450 degree using temperature range, A level does not fire the same life-span with building, moisture permeable coefficient is almost
0.Although other novel heat insulation materials emerge in an endless stream, foam glass is so that it is permanent, security, high reliability are exhausted in low-heat
The fields such as edge, tidal defense engineering, sound absorption are in occupation of increasingly consequence.Its production is waste solid Reuse of materials, is
Environmental protection simultaneously obtains the example of abundant economic interests.
When using, required adhesive glue requires to reach waterproof foam glass, anti-corrosion, heat-insulation and heat-preservation, and high-performance is super early
By force, high temperature resistant, the characteristic of freeze thawing resistance.At present, the sealant using in foam glass bonding industry mainly has diplobiont system, respectively
It is curing system and non-curing systems.
The material that non-curing systems use is thermoplastic material, such as thermoplasticity one-component hot melt butyl material.Such
Sealant meeting deliquescing in heating, prepared glass assembly will misplace when bearing heavy burden or deform, and this shortcoming is in temperature
Even more serious when higher.Therefore, it is difficult to by wanting to intensity and temperature with the foam glass assembly that hot melt butyl sealant produces
The industrial standard asking strict detects, can be only applied to less occasion of bearing a heavy burden.Additionally, such fluid sealant must be more than 100 DEG C
Temperature could apply, such operation temperature easily makes workmen injured, also increases production cost.
Curing system is divided into one-component system and bicomponent system, and the material of use is thermosetting or the material of chemical solidity
Material, such as liquid polysulphides, the material such as polyurethane and organosilicon.Curing system the more commonly used at present is typically all bi-component
They, including basic ingredient and curing agent, are mixed when using, solidify by system.Bicomponent system typically requires to set
Mixing ratio, and need normal temperature mixing at the scene.Then, by with the catalyst reaction infiltrated or reaction of moisture, solidification is slow,
Need assembly to be fixed on several hours or even a couple of days on equipment, wait sealant hardening.Simultaneously because foam glass have not close
The characteristic of water, the fluid sealant of curing system of the prior art is also not suitable for the bonding of foam glass.Such double-component system
Complicated using step, cure cycle is long, and construction cost is higher.
Therefore it provides a kind of foam glass special glue with superperformance is to solve in the urgent need to those skilled in the art
Technical problem.
Content of the invention
The invention provides a kind of inorganic polymer Silica hydrogel and preparation method thereof.
The invention provides following scheme：
A kind of inorganic polymer Silica hydrogel, including gel rubber material and additive；
Described gel rubber material includes the raw material of following weight portion：31.5～33.1 parts of low alkalinity aluminate cement, wollastonite powder 1.5～
1.7 parts, 6.1～6.6 parts of one-level flyash；
Described additive includes the raw material of following weight portion：31.5～33.1 parts of silicon dioxide powder, 7～9 parts of diamond dust, polycarboxylic acids
0.15～0.18 part of based water reducer, 0.01～0.03 part of retarder, 1.5～1.7 parts of reinforcing agent antifreezing agent, hydroxypropyl methyl fiber
0.22～0.26 part of element, 7～9 parts of insulation powder, 1.5～1.7 parts of kaolin, 1.5～1.7 parts of stabilizer, anti-crack water-proof agent
1.1～1.3 parts, 0.3～0.5 part of preservative, 1.5～2.5 parts of colouring agent, resistance to 0.06～0.09 part of dimension, the lignocellulosic of towing
0.15～0.17 part, 1.1～1.3 parts of polymer dispersion powder, 1.1～1.3 parts of nanoscale airsetting rubber powder.
Preferably：Described gel rubber material includes the raw material of following weight portion：322.2 parts of low alkalinity aluminate cement, silicon ash
1.6 parts of powder, 6.4 parts of one-level flyash.
Preferably：Described additive includes the raw material of following weight portion：32.2 parts of silicon dioxide powder, 8 parts of diamond dust, poly- carboxylic
0.16 part of sour based water reducer, 0.02 part of retarder, 1.6 parts of reinforcing agent antifreezing agent, 0.24 part of hydroxypropyl methyl cellulose, thermal insulation separation
8 parts of hot powder, 1.6 parts of kaolin, 11.6 parts of stabilizer, 1.2 parts of anti-crack water-proof agent, 0.4 part of preservative, 2 parts of colouring agent, resistance to tow
0.08 part of dimension, 0.16 part of lignocellulosic, 1.2 parts of polymer dispersion powder, 1.2 parts of nanoscale airsetting rubber powder.
Preferably：Described insulation powder includes vermiculite mica.
Preferably：Described stabilizer is bentonite.
A kind of preparation method of described inorganic polymer Silica hydrogel, methods described includes：
Take each raw material according to described weight portion；
By described poly carboxylic acid series water reducer, retarder, reinforcing agent antifreezing agent, insulation powder, kaolin, stabilizer, ZY cracking resistance
Waterproofing agent, preservative, colouring agent are put into and are ground in pulverizer obtaining the first masterbatch；
By described low alkalinity aluminate cement, wollastonite powder, one-level flyash, silicon dioxide powder, diamond dust, hydroxypropyl methyl fiber
Shearing put in the lump by plain, resistance to dimension of towing, lignocellulosic, polymer dispersion powder, nanoscale airsetting rubber powder and described first masterbatch
Be sufficiently stirred in type dispersion machine 28～32 minutes, shutdown static 5 minutes both described inorganic polymer Silica hydrogel.
Preferably：Described pulverizer is winnowing type pulverizer.
Preferably：Described pulverizer covers flour mill for thunder.
The specific embodiment being provided according to the present invention, the invention discloses following technique effect：
By the invention it is possible to realize a kind of inorganic polymer Silica hydrogel and preparation method thereof, under a kind of implementation, this is no
Machine polymer silicon gel includes gel rubber material and additive；Described gel rubber material includes the raw material of following weight portion：Low alkalinity
31.5～33.1 parts of aluminate cement, 1.5～1.7 parts of wollastonite powder, 6.1～6.6 parts of one-level flyash；Described additive include as
The raw material of lower weight portion：31.5～33.1 parts of silicon dioxide powder, 7～9 parts of diamond dust, poly carboxylic acid series water reducer 0.15～0.18
Part, 0.01～0.03 part of retarder, 1.5～1.7 parts of reinforcing agent antifreezing agent, 0.22～0.26 part of hydroxypropyl methyl cellulose, guarantor
7～9 parts of warm heat-insulating powder, 1.5～1.7 parts of kaolin, 1.5～1.7 parts of stabilizer, 1.1～1.3 parts of anti-crack water-proof agent, preservative
0.3～0.5 part, 1.5～2.5 parts of colouring agent, resistance to 0.06～0.09 part of dimension of towing, 0.15～0.17 part of lignocellulosic, can divide
1.1～1.3 parts of scattered latex powder, 1.1～1.3 parts of nanoscale airsetting rubber powder.This inorganic polymer Silica hydrogel is to combine foam glass
The functional requisite of material, a kind of collection waterproof of research and development, anti-corrosion, heat-insulation and heat-preservation, high-performance, super hardening, high temperature resistant, freeze thawing resistance etc.
The multi-functional new green environment protection material in one.It is made up of basic powder and strengthening liquid material two parts.General technology will
Ask the basestocks stirring that adds water can use, special process, specific portions and need the need of based process to add strengthening material compound
Use, to reach optimal perfect effect.
Certainly, the arbitrary product implementing the present invention it is not absolutely required to reach all the above advantage simultaneously.
Specific embodiment
The enforcement it is clear that described will be clearly and completely described to the technical scheme in the embodiment of the present invention below
Example is only a part of embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, this area is common
The every other embodiment that technical staff is obtained, broadly falls into the scope of protection of the invention.
Embodiment one
The embodiment of the present invention one provides a kind of inorganic polymer Silica hydrogel, and this Silica hydrogel includes gel rubber material and additive；
Described gel rubber material includes the raw material of following weight portion：31.5～33.1 parts of low alkalinity aluminate cement, wollastonite powder 1.5～
1.7 parts, 6.1～6.6 parts of one-level flyash；In actual applications, described gel rubber material can include the raw material of following weight portion：
322.2 parts of low alkalinity aluminate cement, 1.6 parts of wollastonite powder, 6.4 parts of one-level flyash.
Described additive includes the raw material of following weight portion：31.5～33.1 parts of silicon dioxide powder, 7～9 parts of diamond dust, poly-
0.15～0.18 part of carboxylic acid water reducing agent, 0.01～0.03 part of retarder, 1.5～1.7 parts of reinforcing agent antifreezing agent, hydroxypropyl methyl
0.22～0.26 part of cellulose, 7～9 parts of insulation powder, 1.5～1.7 parts of kaolin, 1.5～1.7 parts of stabilizer, cracking resistance are prevented
1.1～1.3 parts of aqua, 0.3～0.5 part of preservative, 1.5～2.5 parts of colouring agent, resistance to 0.06～0.09 part of dimension, the wooden fibre of towing
0.15～0.17 part of dimension element, 1.1～1.3 parts of polymer dispersion powder, 1.1～1.3 parts of nanoscale airsetting rubber powder.In practical application
In, described additive includes the raw material of following weight portion：32.2 parts of silicon dioxide powder, 8 parts of diamond dust, poly carboxylic acid series water reducer
0.16 part, 0.02 part of retarder, 1.6 parts of reinforcing agent antifreezing agent, 0.24 part of hydroxypropyl methyl cellulose, 8 parts of insulation powder, high
Ridge soil 1.6 parts, 11.6 parts of stabilizer, 1.2 parts of anti-crack water-proof agent, 0.4 part of preservative, 2 parts of colouring agent, resistance to tow dimension 0.08 part,
0.16 part of lignocellulosic, 1.2 parts of polymer dispersion powder, 1.2 parts of nanoscale airsetting rubber powder.Further, described insulation
Powder includes vermiculite mica.Further, described stabilizer can be bentonite.
Embodiment two
The embodiment of the present invention two provides a kind of preparation method of inorganic polymer Silica hydrogel, and the method includes：
Take each raw material according to described weight portion；In concrete this raw material of acquisition, can divide according to the weight described in embodiment one
Number weighs, and that is, described gel rubber material includes the raw material of following weight portion：31.5～33.1 parts of low alkalinity aluminate cement, wollastonite powder
1.5～1.7 parts, 6.1～6.6 parts of one-level flyash；
Described additive includes the raw material of following weight portion：31.5～33.1 parts of silicon dioxide powder, 7～9 parts of diamond dust, polycarboxylic acids
0.15～0.18 part of based water reducer, 0.01～0.03 part of retarder, 1.5～1.7 parts of reinforcing agent antifreezing agent, hydroxypropyl methyl fiber
0.22～0.26 part of element, 7～9 parts of insulation powder, 1.5～1.7 parts of kaolin, 1.5～1.7 parts of stabilizer, anti-crack water-proof agent
1.1～1.3 parts, 0.3～0.5 part of preservative, 1.5～2.5 parts of colouring agent, resistance to 0.06～0.09 part of dimension, the lignocellulosic of towing
0.15～0.17 part, 1.1～1.3 parts of polymer dispersion powder, 1.1～1.3 parts of nanoscale airsetting rubber powder.
By described poly carboxylic acid series water reducer, retarder, reinforcing agent antifreezing agent, insulation powder, kaolin, stabilizer, ZY
Anti-crack water-proof agent, preservative, colouring agent are put into and are ground in pulverizer obtaining the first masterbatch；This reinforcing agent antifreezing agent has very
Good freeze thawing resistance effect.In actual applications, described pulverizer can be winnowing type pulverizer.Described pulverizer can also be thunder
Cover flour mill.
By described low alkalinity aluminate cement, wollastonite powder, one-level flyash, silicon dioxide powder, diamond dust, hydroxypropyl methyl
Cellulose, resistance to dimension of towing, lignocellulosic, polymer dispersion powder, nanoscale airsetting rubber powder are put in the lump with described first masterbatch
Be sufficiently stirred in shearing-type dispersion machine 28～32 minutes, shutdown static 5 minutes both described inorganic polymer Silica hydrogel.This silicon ash
Powder, when selecting, needs to select superfine ultra-fine wollastonite powder.
In a word, the embodiment of the present application provides a kind of inorganic polymer Silica hydrogel and preparation method thereof, this inorganic polymer
Silica hydrogel is the functional requisite with reference to foam glass material, a kind of collection waterproof of research and development, anti-corrosion, heat-insulation and heat-preservation, and high-performance surpasses
Early strong, high temperature resistant, the multi-functional new green environment protection material in one such as freeze thawing resistance.It is by basic powder and strengthening liquid material two
Part forms.General technology requires the basestocks stirring that adds water can use, special process, specific portions and need based process
Need add strengthening material compound use, to reach optimal perfect effect.This Silica hydrogel effectively solve foam glass due to
Not hydrophilic, the corrosion-resistant and difficult problem that should not bond, worth spread uses.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation are made a distinction with another entity or operation, and not necessarily require or imply these entities or deposit between operating
In any this actual relation or order.And, term " inclusion ", "comprising" or its any other variant are intended to
Comprising of nonexcludability, wants so that including a series of process of key elements, method, article or equipment and not only including those
Element, but also include other key elements being not expressly set out, or also include for this process, method, article or equipment
Intrinsic key element.In the absence of more restrictions, the key element that limited by sentence "including a ..." it is not excluded that
Also there is other identical element including in the process of described key element, method, article or equipment.
The foregoing is only presently preferred embodiments of the present invention, be not intended to limit protection scope of the present invention.All
Any modification, equivalent substitution and improvement made within the spirit and principles in the present invention etc., are all contained in protection scope of the present invention
Interior.
Claims (8)
1. a kind of inorganic polymer Silica hydrogel is it is characterised in that include gel rubber material and additive；
Described gel rubber material includes the raw material of following weight portion：31.5～33.1 parts of low alkalinity aluminate cement, wollastonite powder 1.5～
1.7 parts, 6.1～6.6 parts of one-level flyash；
Described additive includes the raw material of following weight portion：31.5～33.1 parts of silicon dioxide powder, 7～9 parts of diamond dust, polycarboxylic acids
0.15～0.18 part of based water reducer, 0.01～0.03 part of retarder, 1.5～1.7 parts of reinforcing agent antifreezing agent, hydroxypropyl methyl fiber
0.22～0.26 part of element, 7～9 parts of insulation powder, 1.5～1.7 parts of kaolin, 1.5～1.7 parts of stabilizer, anti-crack water-proof agent
1.1～1.3 parts, 0.3～0.5 part of preservative, 1.5～2.5 parts of colouring agent, resistance to 0.06～0.09 part of dimension, the lignocellulosic of towing
0.15～0.17 part, 1.1～1.3 parts of polymer dispersion powder, 1.1～1.3 parts of nanoscale airsetting rubber powder.
2. inorganic polymer Silica hydrogel according to claim 1 is it is characterised in that described gel rubber material includes following weight
The raw material of part：322.2 parts of low alkalinity aluminate cement, 1.6 parts of wollastonite powder, 6.4 parts of one-level flyash.
3. inorganic polymer Silica hydrogel according to claim 1 is it is characterised in that described additive includes following weight portion
Raw material：32.2 parts of silicon dioxide powder, 8 parts of diamond dust, 0.16 part of poly carboxylic acid series water reducer, 0.02 part of retarder, reinforcing agent are prevented
Freeze 1.6 parts of agent, 0.24 part of hydroxypropyl methyl cellulose, 8 parts of insulation powder, 1.6 parts of kaolin, 11.6 parts of stabilizer, cracking resistance
1.2 parts of waterproofing agent, 0.4 part of preservative, 2 parts of colouring agent, resistance to 0.08 part of dimension of towing, 0.16 part of lignocellulosic, dispersible latex
1.2 parts of powder, 1.2 parts of nanoscale airsetting rubber powder.
4. inorganic polymer Silica hydrogel according to claim 3 is it is characterised in that described insulation powder includes vermiculite cloud
Female.
5. inorganic polymer Silica hydrogel according to claim 3 is it is characterised in that described stabilizer is bentonite.
6. a kind of preparation method of the inorganic polymer Silica hydrogel described in claim 1 to 5 any one is it is characterised in that institute
The method of stating includes：
Take each raw material according to described weight portion；
By described poly carboxylic acid series water reducer, retarder, reinforcing agent antifreezing agent, insulation powder, kaolin, stabilizer, ZY cracking resistance
Waterproofing agent, preservative, colouring agent are put into and are ground in pulverizer obtaining the first masterbatch；
By described low alkalinity aluminate cement, wollastonite powder, one-level flyash, silicon dioxide powder, diamond dust, hydroxypropyl methyl fiber
Shearing put in the lump by plain, resistance to dimension of towing, lignocellulosic, polymer dispersion powder, nanoscale airsetting rubber powder and described first masterbatch
Be sufficiently stirred in type dispersion machine 28～32 minutes, shutdown static 5 minutes both described inorganic polymer Silica hydrogel.
7. method according to claim 6 is it is characterised in that described pulverizer is winnowing type pulverizer.
8. method according to claim 6 is it is characterised in that described pulverizer covers flour mill for thunder.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610844620.2A CN106396578A (en) | 2016-09-23 | 2016-09-23 | Inorganic polymer silica gel and method for preparing same |
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| CN201610844620.2A CN106396578A (en) | 2016-09-23 | 2016-09-23 | Inorganic polymer silica gel and method for preparing same |
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Cited By (1)
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Wan Guanghui Inventor after: Han Song Inventor after: Fu Zenghui Inventor before: Fu Zenghui |
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| CB03 | Change of inventor or designer information | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170215 |
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| RJ01 | Rejection of invention patent application after publication |