CN106381457A - Preparation method of anti-fatigue spring steel - Google Patents

Preparation method of anti-fatigue spring steel Download PDF

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Publication number
CN106381457A
CN106381457A CN201610797453.0A CN201610797453A CN106381457A CN 106381457 A CN106381457 A CN 106381457A CN 201610797453 A CN201610797453 A CN 201610797453A CN 106381457 A CN106381457 A CN 106381457A
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CN
China
Prior art keywords
spring steel
preparation
resisting fatigue
refine
cooling
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Pending
Application number
CN201610797453.0A
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Chinese (zh)
Inventor
赖世权
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Shenzhen step Technology Transfer Center Co., Ltd.
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赖世权
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Priority to CN201610797453.0A priority Critical patent/CN106381457A/en
Publication of CN106381457A publication Critical patent/CN106381457A/en
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/60Ferrous alloys, e.g. steel alloys containing lead, selenium, tellurium, or antimony, or more than 0.04% by weight of sulfur
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/02Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
    • C21D8/0247Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips characterised by the heat treatment
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C33/00Making ferrous alloys
    • C22C33/04Making ferrous alloys by melting
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/14Ferrous alloys, e.g. steel alloys containing titanium or zirconium
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16FSPRINGS; SHOCK-ABSORBERS; MEANS FOR DAMPING VIBRATION
    • F16F1/00Springs
    • F16F1/02Springs made of steel or other material having low internal friction; Wound, torsion, leaf, cup, ring or the like springs, the material of the spring not being relevant
    • F16F1/021Springs made of steel or other material having low internal friction; Wound, torsion, leaf, cup, ring or the like springs, the material of the spring not being relevant characterised by their composition, e.g. comprising materials providing for particular spring properties

Abstract

The invention discloses a preparation method of anti-fatigue spring steel. The preparation method comprises the following steps: (1) mixing of raw materials of the anti-fatigue spring steel, which comprise the following components in percentage by mass: 0.71%-0.82% of C, 3.1%-3.5% of Si, 0.3%-0.5% of Mn, 0.012%-0.013% of Ti, 0.1%-0.2% of S and 0.3%-0.5% of Al; (2) primary smelting; (3) refining; (4) cooling forming, including cooling refined anti-fatigue spring steel to 1,100 DEG C with the cooling rate controlled at 3-5 DEG C/min, keeping the refined anti-fatigue spring steel at 1,100 DEG C for 16-18 min, and then continuing to cool the refined anti-fatigue spring steel to normal temperature with the cooling rate controlled at 15-19 DEG C/min; (5) rolling; (6) quenching; and (7) tempering. The preparation method provided by the invention improves the anti-fatigue property of the anti-fatigue spring steel.

Description

The preparation method of resisting fatigue spring steel
Technical field
The present invention relates to a kind of preparation method of resisting fatigue spring steel.
Background technology
The performance indications such as intensity, toughness and grain size are only capable of indirectly evaluating spring steel, and anti-fatigue performance is only reflection bullet The most important index of spring steel, it not only can reflect the quality of the property indices such as intensity, toughness and the grain size of spring steel, Can also reflect best match between above-mentioned each performance and by the coupling between this performance the shadow to spring steel service life Ring.And the inherent quality of spring steel has very big associating with the fatigue resistance of spring steel.Therefore, no matter spring steel kind also It is the research of production technology aspect, all with the fatigue behaviour of raising spring steel as final purpose.
Content of the invention
For above-mentioned technical problem, the present invention has designed and developed a kind of system of the excellent resisting fatigue spring steel of anti-fatigue performance Preparation Method.
The present invention provides technical scheme below:
A kind of preparation method of resisting fatigue spring steel, including:
Step (1) by the raw material mix homogeneously of spring steel, the raw material of spring steel include by mass percentage with the following group Point:0.71~0.82% C, 3.1~3.5% Si, 0.3~0.5% Mn, 0.012~0.013% Ti, 0.1~ 0.2% S and 0.3~0.5% Al, balance of Fe;
Step (2) is just refined, and just refines and continues 5~10min at 1300 DEG C, starts from 1300 DEG C with 10~15 DEG C/min afterwards Speed rise to 1700 DEG C, and continue 5~10min at 1700 DEG C again;
Step (3) refine, the temperature of refine is 1550~1600 DEG C, after refine carries out 10~15min, sends into temperature and exists 1550~1600 DEG C of hot nitrogen, blows lasting 5min and stops, and the concise persistent period altogether is 30~35min;
Step (4) cooling shaping, control rate of cooling is 3~5 DEG C/min, is cooled to 1100 DEG C, keeps 16 at 1100 DEG C ~18min, proceeds to cool down, control rate of cooling is 15~19 DEG C/min, until being cooled to room temperature afterwards;
Step (5) rolls;
Step (6) quenches;
Step (7) is tempered.
Preferably, in the described preparation method of resisting fatigue spring steel, the raw material of spring steel is included by mass percentage The following components of meter:0.82% C, 3.1% Si, 0.33% Mn, 0.012% Ti, 0.15% S and 0.34% Al, balance of Fe.
Preferably, in the described preparation method of resisting fatigue spring steel, in described step (2), just refine at 1300 DEG C Continue 10min, continue 10min at 1700 DEG C again.
Preferably, in the described preparation method of resisting fatigue spring steel, in described step (2), from 1300 DEG C start with The speed of 12 DEG C/min rises to 1700 DEG C.
Preferably, in the described preparation method of resisting fatigue spring steel, in described step (3), concise temperature is 1550℃.
The present invention improves the anti-fatigue performance of spring steel.
Specific embodiment
The present invention is described in further detail below, with make those skilled in the art with reference to specification word being capable of evidence To implement.
The present invention provides a kind of preparation method of resisting fatigue spring steel, including:
Step (1) by the raw material mix homogeneously of spring steel, the raw material of spring steel include by mass percentage with the following group Point:0.71~0.82% C, 3.1~3.5% Si, 0.3~0.5% Mn, 0.012~0.013% Ti, 0.1~ 0.2% S and 0.3~0.5% Al, balance of Fe;
Step (2) is just refined, and just refines and continues 5~10min at 1300 DEG C, starts from 1300 DEG C with 10~15 DEG C/min afterwards Speed rise to 1700 DEG C, and continue 5~10min at 1700 DEG C again;
Step (3) refine, the temperature of refine is 1550~1600 DEG C, after refine carries out 10~15min, sends into temperature and exists 1550~1600 DEG C of hot nitrogen, blows lasting 5min and stops, and the concise persistent period altogether is 30~35min;
Step (4) cooling shaping, control rate of cooling is 3~5 DEG C/min, is cooled to 1100 DEG C, keeps 16 at 1100 DEG C ~18min, proceeds to cool down, control rate of cooling is 15~19 DEG C/min, until being cooled to room temperature afterwards;
Step (5) rolls;
Step (6) quenches;
Step (7) is tempered.
The present invention accurately sets the condition of just refining, carries out certain time at relatively low temperature first, makes Raw mixture partly first changing with respect to outside, is being risen under higher temperature with certain speed afterwards, is making raw material The change of mixture diffuses to inner side by outside.This contributes to improving the organizational structure in the outside of spring steel, so that spring steel The mechanical property in outside is more excellent.
Secondly, the present invention goes back the concise condition of careful design, after concise carrying out to certain time, sends into temperature and also exists 1550~1600 DEG C of hot nitrogen, blows lasting 5min, continues refine.Aforesaid operations contribute to the upper surface to liquation provides guarantor Shield, and make the mechanical property outside spring steel more preferable.
Cooling shaping is carried out in two stages, and first stage is more than 1100 DEG C, with the cooling of slow speed, so that It is internally formed the tissue of densification in spring steel in cooling procedure;Second stage is to arrive room temperature at 1100 DEG C, with respect to relatively Fast speed cooling, reduces the brittle inclusion of aluminium sesquioxide, to improve the anti-fatigue performance of spring steel.
The fatigue limit of the spring steel that the present invention prepares can reach 990MPa, compared to traditional handicraft 800MPa, has increased significantly.The tensile strength of the spring steel of the present invention can reach 2301MPa, and elongation after fracture is 10.4%.
In the raw material composition of spring steel, C can improve intensity and the hardness of spring steel;Si can improve the bullet of spring steel Property, and acid resistance can be improved;Mn can improve the intensity of spring steel.
Preferably, in the described preparation method of resisting fatigue spring steel, the raw material of spring steel is included by mass percentage The following components of meter:0.82% C, 3.1% Si, 0.33% Mn, 0.012% Ti, 0.15% S and 0.34% Al, balance of Fe.
Preferably, in the described preparation method of resisting fatigue spring steel, in described step (2), just refine at 1300 DEG C Continue 10min, continue 10min at 1700 DEG C again.
Preferably, in the described preparation method of resisting fatigue spring steel, in described step (2), from 1300 DEG C start with The speed of 12 DEG C/min rises to 1700 DEG C.
Preferably, in the described preparation method of resisting fatigue spring steel, in described step (3), concise temperature is 1550℃.
Although embodiment of the present invention is disclosed as above, it is not restricted to listed in description and embodiment With, it can be applied to various suitable the field of the invention completely, for those skilled in the art, can be easily Realize other modification, therefore under the general concept being limited without departing substantially from claim and equivalency range, the present invention does not limit In specific details.

Claims (5)

1. a kind of preparation method of resisting fatigue spring steel is it is characterised in that include:
By the raw material mix homogeneously of spring steel, the raw material of spring steel includes following components by mass percentage to step (1): 0.71~0.82% C's, 3.1~3.5% Si, 0.3~0.5% Mn, 0.012~0.013% Ti, 0.1~0.2% S and 0.3~0.5% Al, balance of Fe;
Step (2) is just refined, and just refines and continues 5~10min at 1300 DEG C, starts from 1300 DEG C with the speed of 10~15 DEG C/min afterwards Degree rises to 1700 DEG C, and continues 5~10min at 1700 DEG C again;
Step (3) refine, the temperature of refine is 1550~1600 DEG C, after refine carries out 10~15min, sends into temperature 1550 ~1600 DEG C of hot nitrogen, blows lasting 5min and stops, and the concise persistent period altogether is 30~35min;
Step (4) cooling shaping, control rate of cooling be 3~5 DEG C/min, be cooled to 1100 DEG C, 1100 DEG C keep 16~ 18min, proceeds to cool down, control rate of cooling is 15~19 DEG C/min, until being cooled to room temperature afterwards;
Step (5) rolls;
Step (6) quenches;
Step (7) is tempered.
2. the preparation method of resisting fatigue spring steel as claimed in claim 1 is it is characterised in that the raw material of spring steel is included by matter The following components of amount percentages:0.82% C, 3.1% Si, 0.33% Mn, 0.012% Ti, 0.15% S and 0.34% Al, balance of Fe.
3. the preparation method of resisting fatigue spring steel as claimed in claim 1 is it is characterised in that in described step (2), just refine Continue 10min at 1300 DEG C, continue 10min at 1700 DEG C again.
4. the preparation method of resisting fatigue spring steel as claimed in claim 3 is it is characterised in that in described step (2), from 1300 DEG C beginning rises to 1700 DEG C with the speed of 12 DEG C/min.
5. the preparation method of resisting fatigue spring steel as claimed in claim 1 is it is characterised in that in described step (3), concise Temperature is 1550 DEG C.
CN201610797453.0A 2016-08-31 2016-08-31 Preparation method of anti-fatigue spring steel Pending CN106381457A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116590628A (en) * 2023-07-18 2023-08-15 南通多邦机械有限公司 Preparation method of high-elasticity anti-fatigue horseshoe

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101671792A (en) * 2008-09-12 2010-03-17 攀钢集团研究院有限公司 Spring steel and preparation method thereof
CN103614634A (en) * 2013-11-28 2014-03-05 柳城县鼎铭金属制品有限公司 Alloy spring wire and preparation method thereof
CN105838980A (en) * 2015-12-09 2016-08-10 苏州市吴中区胥口丰收机械配件厂 High-strength spring steel and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101671792A (en) * 2008-09-12 2010-03-17 攀钢集团研究院有限公司 Spring steel and preparation method thereof
CN103614634A (en) * 2013-11-28 2014-03-05 柳城县鼎铭金属制品有限公司 Alloy spring wire and preparation method thereof
CN105838980A (en) * 2015-12-09 2016-08-10 苏州市吴中区胥口丰收机械配件厂 High-strength spring steel and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
付广艳 主编: "《机械工程材料》", 28 February 2014, 北京理工大学出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116590628A (en) * 2023-07-18 2023-08-15 南通多邦机械有限公司 Preparation method of high-elasticity anti-fatigue horseshoe

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Effective date of registration: 20180619

Address after: 518000 Guangdong Shenzhen Longhua New District big wave street Longsheng community Tenglong road gold rush e-commerce incubation base exhibition hall E commercial block 706

Applicant after: Shenzhen step Technology Transfer Center Co., Ltd.

Address before: 536000 South Asia building, 66 North Bay West Road, Yinhai, Beihai, the Guangxi Zhuang Autonomous Region

Applicant before: Lai Shiquan

RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170208