CN106362628B - A kind of non-contact high-frequency ultrasonic dispersers - Google Patents

A kind of non-contact high-frequency ultrasonic dispersers Download PDF

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Publication number
CN106362628B
CN106362628B CN201611006761.3A CN201611006761A CN106362628B CN 106362628 B CN106362628 B CN 106362628B CN 201611006761 A CN201611006761 A CN 201611006761A CN 106362628 B CN106362628 B CN 106362628B
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dispersion tube
tube
ultrasonic
dispersion
inner cavity
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CN106362628A (en
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方泽波
龚恒翔
谭永胜
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University of Shaoxing
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University of Shaoxing
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/80Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/55Mixing liquids with solids the mixture being submitted to electrical, sonic or similar energy
    • B01F23/551Mixing liquids with solids the mixture being submitted to electrical, sonic or similar energy using vibrations

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention discloses a kind of non-contact high-frequency ultrasonic dispersers, the inner cavity of dispersion tube is same as filling with liquid to be dispersed, and the outer wall of the dispersion tube is equipped with an inlet tube and an outlet tube, this two root canals road is connected to the inner cavity of dispersion tube, and one, this two root canals road, upper, one under;Ultrasonic generator number is two, the two ultrasonic generators are respectively by the upper and lower port closed of dispersion tube, the ultrasonic wave that the ultrasonic generator issues passes in the inner cavity of dispersion tube through poly- four ethylene diaphragm, and the liquid in dispersion tube is directly contacted with the poly- four ethylene diaphragm of two ultrasonic generators, and spacing >=40mm between the poly- four ethylene diaphragm of two panels.The present invention connects in pipeline is continuously conveyed, the little particle of transport flow liquid in pipeline can be continued for dispersing, so that little particle is evenly distributed in working fluid, avoid generating aggregate, precipitating, the present invention is contactless structure, can effectively avoid pollution working fluid.

Description

A kind of non-contact high-frequency ultrasonic dispersers
Technical field
The invention belongs to disperser field more particularly to a kind of non-contact high-frequency ultrasonic dispersers.
Background technique
Disperser avoids the formation of aggregate, precipitating for the little particle dispersion in dispersing liquid.Existing disperser type More, the immediate prior art is ultrasonic dispersers, it is used to contain the container of liquid using one, and in bulk container interpolation Enter a hollow bar, is provided with ultrasonic generator in hollow bar.Ultrasonic wave occurs for ultrasonic generator, and passes to appearance by hollow bar In device, and then ultrasonic vibration is generated to the liquid in container, with the little particle in dispersing liquid, avoids the formation of aggregate, precipitating, After completing dispersion, then that liquid poured out container is spare.
There are two the main disadvantages of this ultrasonic dispersers: one, be contact type structure, i.e., hollow bar can in container Liquid contact, and hollow bar may be chemically reacted with liquid, thus can contaminated fluid, can not make so as to cause liquid With.Two, after completing dispersion, then liquid is poured out to little particle after container is spare, and the liquid after dispersing stands a period of time and is held very much Easily assemble again, forms aggregate, precipitating again, the meaning of dispersion is thus lost, because there is the liquid of aggregate, precipitating It can not be available completely in some industries.Three, can not be within certain working range to the liquid insulating after dispersion, this is asked Topic is unable to satisfy some workplaces.
In addition, carrying out the short grained liquid of continuous conveyor frequently with pipeline in medical treatment and scientific research.However, little particle all can Non-uniform distribution occurs, forms aggregate, precipitating etc., neck is continuously conveyed in pipeline in the non-uniform Distribution of this mixing liquid The problem of domain may result in serious consequence, and the prior art not can solve always this respect.
Summary of the invention
Technical problem to be solved by the present invention lies in a kind of contactless high frequency ultrasound disperser is provided, it is intended to through this Disperser disperses the little particle being continuously conveyed in pipeline in working fluid, avoids the formation of aggregate, precipitating.
Technical scheme is as follows: a kind of non-contact high-frequency ultrasonic dispersers, it is characterised in that: including dispersion tube (1) and ultrasonic generator, wherein the inner cavity of dispersion tube (1) is same as filling with liquid to be dispersed, on the outer wall of the dispersion tube Equipped with inlet tube (2) He Yigen outlet tube (3), this two root canals road is connected to the inner cavity of dispersion tube (1), and this two root canal One, road is upper, and one under;The ultrasonic generator number is two, the two ultrasonic generators are respectively by institute The upper and lower port closed of dispersion tube (1) is stated, the ultrasonic wave which issues penetrates poly- four ethylene diaphragm (4) It passes in the inner cavity of the dispersion tube (1), and poly- four ethylene of the liquid in dispersion tube (1) and two ultrasonic generators is thin Diaphragm (4) directly contacts, and spacing (H) >=40mm between the poly- four ethylene diaphragm (4) of two panels;
The ultrasonic generator includes connector sleeve (5) and coolant liquid inlet pipe (11), and wherein connector sleeve (5) is tightly connected At the port of the dispersion tube (1), which is equipped with diaphragm seal circle (6) close to the position of dispersion tube (1) port With the poly- four ethylene diaphragm (4), and poly- four ethylene diaphragm (4) is pressed on connector sleeve (5) inner wall by diaphragm seal circle (6) Annular stop step on;Connector sleeve (5) inner hole is equipped with end cap (7) far from the position of dispersion tube (1) port, in the end cap Equipped with high-frequency piezoelectric ceramic piece (8), fixed card ring (9) and positioning steel ring (10), wherein fixed card ring (9) and positioning steel ring (10) For fixing high-frequency piezoelectric ceramic piece (8), and the corresponding pole of the positive and negative electrode of high-frequency piezoelectric ceramic piece (8) and ultrasonic atomizatio circuit It is connected, and spacing (L)≤10mm between high-frequency piezoelectric ceramic piece (8) and the poly- four ethylene diaphragm (4);The high frequency pressure Connector sleeve (5) inner cavity between electroceramics piece (8) and poly- four ethylene diaphragm (4) is the cooling chamber for containing cooling water, described cold But liquid inlet pipe (11) and coolant liquid outlet pipe (12) are mounted in connector sleeve (5) outside, and are connected to the cooling chamber;
The dispersion tube (1) is hollow structure, and the hollow cavity of the dispersion tube is incubation cavity, and dispersion tube (1) is circumscribed with one Root heat preservation liquid inlet pipe (13) and a heat preservation liquid outlet pipe (14), this two root canals road are connected to the incubation cavity.
In the above-mentioned technical solutions, the access of this disperser is continuously conveyed by pipeline by inlet tube (2) and outlet tube (3) In, enter in the inner cavity of dispersion tube (1) with short grained liquid, and inlet tube (2) and outlet tube (3) are arranged one on the other Enough discrete areas are left, sufficiently, effectively to carry out ultrasonic disperse to the working fluid being continuously conveyed in pipeline;And And the liquid in dispersion tube (1) is directly contacted with the poly- four ethylene diaphragm (4) of upper and lower side, and poly- four ethylene diaphragm (4) Chemical stability it is fine, in dispersion tube (1) liquid occur chemical reaction possibility it is minimum.Two ultrasonic generators When work, ultrasonic wave enters in dispersion tube (1);Since the intensity of ultrasonic wave can gradually decay with the increase of propagation distance, Therefore two ultrasonic generator settings symmetrical above and below, it can guarantee the ultrasonic power density in dispersion tube (1) effectively, as best one can It is uniformly distributed, when ultrasonic oscillation disperses little particle, so that little particle be allowed to be uniformly distributed in a liquid, constantly avoids the group of generation Aggressiveness, precipitating.In addition, spacing (H) needs >=40mm between the poly- four ethylene diaphragm (4) of two panels, we test proves that The main function form of spacing (H) < 35mm ultrasonic wave is exactly cavitation effect, at this moment just will form and hazes, and cannot play ultrasound Peptizaiton.
Meanwhile the ultrasonic generator includes connector sleeve (5) and coolant liquid inlet pipe (11), wherein connector sleeve (5) is close Envelope is connected at the port of the dispersion tube (1), which is equipped with diaphragm seal close to the position of dispersion tube (1) port (6) and the poly- four ethylene diaphragm (4) are enclosed, and poly- four ethylene diaphragm (4) is pressed on connector sleeve by diaphragm seal circle (6) (5) on the annular stop step of inner wall;Connector sleeve (5) inner hole is equipped with end cap (7) far from the position of dispersion tube (1) port, The end cap is provided with high-frequency piezoelectric ceramic piece (8), fixed card ring (9) and positioning steel ring (10), wherein fixed card ring (9) and positioning Steel ring (10) is for fixing high-frequency piezoelectric ceramic piece (8), and the positive and negative electrode of high-frequency piezoelectric ceramic piece (8) and ultrasonic atomizatio circuit Correspondence be extremely connected, and spacing (L)≤10mm between high-frequency piezoelectric ceramic piece (8) and the poly- four ethylene diaphragm (4);Institute Stating connector sleeve (5) inner cavity between high-frequency piezoelectric ceramic piece (8) and poly- four ethylene diaphragm (4) is the cooling for containing cooling water Chamber, the coolant liquid inlet pipe (11) and coolant liquid outlet pipe (12) are mounted in connector sleeve (5) outside, and are connected to the cooling chamber.
In addition, the dispersion tube (1) is hollow structure, the hollow cavity of the dispersion tube is incubation cavity, and dispersion tube (1) is external There are a heat preservation liquid inlet pipe (13) and a heat preservation liquid outlet pipe (14), this two root canals road is connected to the incubation cavity.Use with Upper structure design, can thus keep the temperature the liquid filled in dispersion tube (1) inner cavity, to make in dispersion tube (1) inner cavity Liquid keep the temperature in a certain range, to meet the requirement of all occasions.
It designs using the above structure, high-frequency piezoelectric ceramic piece generates ultrasonic wave when working, ultrasonic wave is thin through poly- four ethylene Diaphragm (4) passes in dispersion tube (1), and liquid and little particle in dispersion tube (1) is made to generate ultrasonic vibration, to make little particle It is evenly dispersed in a liquid.It can generate heat in ultrasonic wave communication process, cooling chamber just can be carried out cooling, and cooling chamber can also be to high frequency Piezoelectric ceramic piece (8) cooling down, to guarantee that high-frequency piezoelectric ceramic piece (8) works normally in operating temperature range.At this In structure, spacing (L)≤10mm be play peptizaiton to guarantee the more energy of ultrasonic wave for ultrasonic vibration, and It is preferably 8-10mm away from (L).
Using above technical scheme, the present invention is connect in pipeline is continuously conveyed, can in pipeline transport flow liquid it is small Particle is continued for dispersing, so that little particle is evenly distributed in working fluid, avoids generating aggregate, precipitating, and The present invention is contactless structure, can effectively avoid pollution working fluid, guarantees the purity of working fluid, and ultrasonic wave occurs The structure of device is simple, high reliablity, can effectively generate ultrasonic wave, and the configuration of the present invention is simple, compact, easily fabricated, very Solves the still unsolved problem of the prior art well.
Preferably, the spacing (H) between poly- four ethylene diaphragm (4) described in two panels is 45mm.It is set using above-mentioned parameter Meter, can be such that the ultrasonic power density in dispersion tube (1) inner cavity is uniformly distributed, preferably thus so as to improve dispersion effect.
The utility model has the advantages that the present invention connects in pipeline is continuously conveyed, the little particle of transport flow liquid in pipeline can be continued Ground is dispersed, so that little particle is evenly distributed in working fluid, avoids generating aggregate, precipitating, and the present invention is Contactless structure can effectively avoid pollution working fluid, guarantee the purity of working fluid, and the knot of ultrasonic generator Structure is simple, high reliablity, can effectively generate ultrasonic wave, and the configuration of the present invention is simple, compact, easily fabricated, well solves The prior art still unsolved problem.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the cross section view of Fig. 1.
Fig. 3 is the sectional view along A-A of Fig. 2.
Specific embodiment
Present invention will be further explained below with reference to the attached drawings and examples:
As shown in Fig. 1,2 and 3, a kind of non-contact high-frequency ultrasonic dispersers, mainly by dispersion tube 1, inlet tube 2, out liquid Pipe 3, poly- four ethylene diaphragm 4 and ultrasonic generator are constituted.Wherein, the inner cavity of dispersion tube 1 is same as filling with liquid to be dispersed The outer wall of body, the dispersion tube 1 is equipped with an inlet tube 2 and an outlet tube 3, this inner cavity of two root canals road with dispersion tube 1 Connection, and one, this two root canals road, upper, one under.When it is implemented, can be inlet tube 2 upper, outlet tube 3 under, It is also possible to inlet tube 2 under, outlet tube 3 is upper.In the present case, ultrasonic generator number is two, the two ultrasounds Wave generating device is symmetrical arranged, and respectively by the upper and lower port closed of dispersion tube 1.The ultrasonic wave that ultrasonic generator issues It is passed in the inner cavity of dispersion tube 1 through poly- four ethylene diaphragm 4, and liquid and two ultrasonic generators in dispersion tube 1 Poly- four ethylene diaphragm 4 directly contact.Spacing H >=40mm between the poly- four ethylene diaphragm 4 of two panels, in the accompanying drawings with above One strata, four ethylene diaphragm, 4 lower surface indicates spacing H at a distance from following one poly- four ethylene diaphragm, 4 upper surface.Also, The thickness of poly- four ethylene diaphragm 4 is in 0.05mm hereinafter, thus propagating convenient for ultrasonic wave.In the present case, poly- four ethylene of two panels Spacing H between diaphragm 4 is 45mm.
As shown in Fig. 1,2 and 3, ultrasonic generator includes connector sleeve 5 and coolant liquid inlet pipe 11, and wherein connector sleeve 5 is close Envelope is connected at the port of dispersion tube 1, which equipped with diaphragm seal circle 6 and gathers close to the position of 1 port of dispersion tube Four ethylene diaphragms 4, and poly- four ethylene diaphragm 4 is pressed on the annular stop step of 5 inner wall of connector sleeve by diaphragm seal circle 6 On.5 inner hole of connector sleeve is equipped with end cap 7 far from the position of 1 port of dispersion tube, and the end cap 7 is interior to be equipped with high frequency piezoelectric ceramic along axial Piece 8, fixed card ring 9 and positioning steel ring 10, wherein fixed card ring 9 and positioning steel ring 10 are for fixing high-frequency piezoelectric ceramic piece 8.It is high The positive and negative electrode of frequency piezoelectric ceramic piece 8 is corresponding with ultrasonic atomizatio circuit (being not drawn into this case) to be extremely connected, and high frequency piezoelectric ceramic The connection type and working principle of piece 8 and ultrasonic atomizatio circuit are the prior art, are known to the staff of this field.This case institute The high frequency of meaning refer to the working frequency of high-frequency piezoelectric ceramic piece 8 in 1.7MHz or more, and in this field working frequency 1MHz with It is upper just to refer to high frequency.
Spacing L≤10mm between high-frequency piezoelectric ceramic piece 8 and poly- four ethylene diaphragm 4, uses high frequency piezo in the accompanying drawings 8 lower surface of potsherd indicates spacing L at a distance from poly- four ethylene diaphragm, 4 upper surface.
5 inner cavity of connector sleeve between high-frequency piezoelectric ceramic piece 8 and poly- four ethylene diaphragm 4 is the cooling for containing cooling water Chamber, coolant liquid inlet pipe 11 and coolant liquid outlet pipe 12 are connected on the outer wall of connector sleeve 5 with cooling chamber.In the present case, cooling Liquid uses cooling water.In addition, dispersion tube 1 is hollow structure, the hollow cavity of the dispersion tube 1 is incubation cavity, and dispersion tube 1 is circumscribed with A piece heat preservation liquid inlet pipe 13 and a heat preservation liquid outlet pipe 14, this two root canals road are connected to incubation cavity.In addition, inlet tube 2 and go out After liquid pipe 3 passes through incubation cavity, in the inner cavity that reaches dispersion tube 1 respectively.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not limitation with the present invention, all in essence of the invention Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.

Claims (2)

1. a kind of non-contact high-frequency ultrasonic dispersers, it is characterised in that: including dispersion tube (1) and ultrasonic generator, The inner cavity of middle dispersion tube (1) is equipped with inlet tube (2) He Yigen for filling with liquid to be dispersed, the outer wall of the dispersion tube Outlet tube (3), this two root canals road are connected to the inner cavity of dispersion tube (1), and one, this two root canals road, upper, one under;Institute Inlet tube (2) and outlet tube (3) are stated after incubation cavity, in the inner cavity for reaching dispersion tube (1) respectively;The ultrasonic wave occurs Device number is two, the two ultrasonic generators are respectively by the upper and lower port closed of the dispersion tube (1), the ultrasound The ultrasonic wave that wave generating device issues passes in the inner cavity of the dispersion tube (1) through polytetrafluoroethylene film piece (4), and disperses Liquid in cylinder (1) is directly contacted with the polytetrafluoroethylene film piece (4) of two ultrasonic generators, and two panels polytetrafluoroethyl-ne Spacing (H) >=40mm between alkene diaphragm (4), the thickness of polytetrafluoroethylene film piece is in 0.05mm or less;
The ultrasonic generator includes connector sleeve (5) and coolant liquid inlet pipe (11), and wherein connector sleeve (5) is sealedly connected on institute At the port for stating dispersion tube (1), which is equipped with diaphragm seal circle (6) and institute close to the position of dispersion tube (1) port It states polytetrafluoroethylene film piece (4), and polytetrafluoroethylene film piece (4) is pressed on connector sleeve (5) inner wall by diaphragm seal circle (6) Annular stop step on;Connector sleeve (5) inner hole is equipped with end cap (7) far from the position of dispersion tube (1) port, in the end cap Equipped with high-frequency piezoelectric ceramic piece (8), fixed card ring (9) and positioning steel ring (10), wherein fixed card ring (9) and positioning steel ring (10) For fixing high-frequency piezoelectric ceramic piece (8), and the corresponding pole of the positive and negative electrode of high-frequency piezoelectric ceramic piece (8) and ultrasonic atomizatio circuit It is connected, and spacing (L)≤10mm between high-frequency piezoelectric ceramic piece (8) and the polytetrafluoroethylene film piece (4);The high frequency Connector sleeve (5) inner cavity between piezoelectric ceramic piece (8) and polytetrafluoroethylene film piece (4) is the cooling chamber for containing cooling water, institute It states coolant liquid inlet pipe (11) and coolant liquid outlet pipe (12) is mounted in connector sleeve (5) outside, and be connected to the cooling chamber;
The dispersion tube (1) is hollow structure, and the hollow cavity of the dispersion tube is incubation cavity, and dispersion tube (1) is circumscribed with a guarantor Warm liquid inlet pipe (13) and a heat preservation liquid outlet pipe (14), this two root canals road are connected to the incubation cavity.
2. non-contact high-frequency ultrasonic dispersers according to claim 1, it is characterised in that: polytetrafluoroethylene (PTFE) described in two panels Spacing (H) between diaphragm (4) is 45mm.
CN201611006761.3A 2016-11-01 2016-11-01 A kind of non-contact high-frequency ultrasonic dispersers Active CN106362628B (en)

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Publication number Priority date Publication date Assignee Title
CN113740127A (en) * 2021-08-09 2021-12-03 宁波新芝生物科技股份有限公司 Non-contact refrigeration type ultrasonic pulverizer

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105032679A (en) * 2015-08-14 2015-11-11 重庆理工大学 Ultrasonic atomization source
CN205008171U (en) * 2015-08-14 2016-02-03 重庆理工大学 Atomizing piece mounting structure in ultrasonic atomization source
CN206240416U (en) * 2016-11-01 2017-06-13 重庆理工大学 Non-contact high-frequency ultrasonic dispersers

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105032679A (en) * 2015-08-14 2015-11-11 重庆理工大学 Ultrasonic atomization source
CN205008171U (en) * 2015-08-14 2016-02-03 重庆理工大学 Atomizing piece mounting structure in ultrasonic atomization source
CN206240416U (en) * 2016-11-01 2017-06-13 重庆理工大学 Non-contact high-frequency ultrasonic dispersers

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