CN106361598A - Controllable moisture slow releasing system emulsification composition and preparing method thereof - Google Patents
Controllable moisture slow releasing system emulsification composition and preparing method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/893—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by an alkoxy or aryloxy group, e.g. behenoxy dimethicone or stearoxy dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
Abstract
The invention discloses a controllable moisture slow releasing system emulsification composition. The emulsification composition comprises 5.0%-15.0% of propylene glycol, 0.2%-1.0% of panthenol, 0.2%-2.0% of soluble collagen, 0.5%-0.8% of magnesium sulfate, 0.1%-0.3% of water soluble jojoba oil, 2.0%-7.0% of Diethylhexyl Carbonate, 0.2%-1.0% of tocopheryl acetate, 1.0%-2.5% of SSG 210SP, 3.0%-8.0% of Dow Corning 5225C, 1.0%-40.0% of phenyl trimethicone, 0.4%-0.6% of Caprylyl Glycol, 0.8%-1.5% of lactic acid, 0.01%-0.03% of essence, and the balance deionized water. The controllable moisture slow releasing system emulsification composition adopts an emulsification system with special spatial structure to form an innovative moisture storage and releasing system so that the releasing speed of aqueous active ingredients can be controlled, and has the advantages of simple operation, good stability and the like.
Description
Technical field
The present invention relates to a kind of special emulsification composition, adsorbed by Hyarogen-bonding, form unique spatial network
Structure, water composition is stored in space, can control the compositionss water speed, is widely used in all kinds of skin protection of making and produces
Product.
Background technology
Silicon oil product is due to having special water profit feel, it is to avoid the greasy thick and heavy feel of common w/o series, and
The water with o/w product moistens salubrious texture.Therefore it is popular for whole market, this kind of product covers skin care milk/frost, sleep surface
Film, bb frost, sunscreen cream, treatment etc..
At present, on the market go out aquatic products, rely primarily on ultralow emulsifier content (0.5-1.0%) formed one kind not
Stable emulsification system, because the addition of emulsifying agent is considerably less, the interface of this w/o emulsification system is very thin, rubs in external force
Under wiping, interfacial film moment ruptures, and the water composition being wrapped in interior phase pours out, thus " water outlet " or " sudden and violent water " occurs
Phenomenon, the bad control of this product stability, generally in the case of low temperature, the water composition of interior phase freezes, and volume becomes big, makes
Emulsified body is become to destroy, thus leading to the quality problems of water stratification.The technological requirement of this formula is high, mixing speed too fast or
Cross slow, all may cannot form stable emulsified body.The water speed that goes out of product is determined by formulation composition and emulsifying agent film strength
Fixed, the effect of water outlet cannot or be difficult to adjust.
Fig. 1 is the water outlet schematic diagram of traditional water outlet cream；Define a kind of form of emulsifying parcel.Fig. 2 is traditional water outlet cream
Micro-structure diagram (microscope), conventional emulsifier is a kind of linear emulsifying agent, need formed micelle, 1-2 μm of emulsion particle diameter.Figure
3 is the water outlet schematic diagram of traditional water outlet cream；Conventional emulsifier system water release principle, is tied by external force action breaks down micelle
Structure, water release is unexpected, discontinuously it is more difficult to control.
In a word, traditional go out aquatic products and have that water speed is uncontrollable, stability is not good enough, operation technological requirement is high, water outlet
The shortcomings of effect difference.
Content of the invention
In order to overcome traditional problem going out aquatic products presence, the controlled moisture storage delivery systme of the present invention, use
There is the emulsification system of special space structure, define the moisture storage delivery systme of innovation, develop there is obvious characteristic
Product, such as can control the advantages of rate of release of aqueous active ingredient, simple to operate, good stability, go out with traditional
Water frost is compared has obvious performance advantage.
Another object of the present invention is the preparation method providing fuel-displaced massage cream.
The moisture storage delivery systme of the present invention is by certain formula by ssg-210sp and dow corning 5225c
Combine.Being described below of this two raw material:
1st, ssg-210sp (25% polydimethylsiloxane peg-10/15 cross linked polymer and 75% polydimethylsiloxanes
Alkane), manufacturer: Japanese SHIN-ETSU HANTOTAI.
There is the unique texture of non-emulsifierses, but its can be used alone or on a small quantity cooperation emulsifying agent under conditions of, and
It readily prepares Water-In-Oil emulsified body, simple process, stable system, and outward appearance is graceful, even if under the conditions of High water cut, equally
Also highly stable emulsified body can be prepared." network structure " that ssg-210sp is formed in system, relatively conventional emulsifying dosage form
The case type micelle becoming is a semi-open system, and unique structure can be highly effective as an effective carrier
Containing and slow release from water or other active component etc..
2nd, dow corning 5225c (87.5% ring five dimethyl silicone polymer and 12.5% peg/ppg-18/18
Polydimethylsiloxane), manufacturer: Dow corning.
Dispersion in ring five dimethyl silicone polymer for the high molecular weight polyether modified organic silicon.It can be used in particular for preparing
The formula of volatile organosilicon Bao Shui.It is the transport system of a kind of non-polar component and polar compound, and non-polar component dissolves
In the organosilicon of foreign minister, polar compound is dissolved in interior phase, can form the water in oil formula of stable silicon, can be formed transparent
Emulsion system.
After polydimethylsiloxane peg-10/15 cross linked polymer and the mixing of peg/ppg-18/18 polydimethylsiloxane
The emulsifier combination being formed, under relatively low consumption, can be readily formed good stability, have the emulsified body of slow release effect.
A kind of controlled moisture slow release emulsification system compositionss that the present invention provides, comprise each group of following percentage by weight
Point:
Propylene glycol 5.0%～15.0%, pantothenylol 0.2%～1.0%, soluble collagen 0.2%～2.0%, magnesium sulfate
0.5%～0.8%, water solublity Jojoba oil 0.1%～0.3%, diethyl hexylcarbonate 2.0%～7.0%, tocopheryl acetate
Ester 0.2%～1.0%, ssg-210sp1.0%～2.5%, dow corning 5225c 3.0%～8.0%, phenyl poly- three
Methylsiloxane 1.0%～40.0%, caprylyl glycol 0.4%～0.6%, lactic acid 0.8%～1.5%, essence 0.01%～
0.03%, balance deionized water.
The preparation method of above-mentioned controlled moisture slow-releasing system emulsification composition is it is characterised in that comprise the following steps:
1) respectively deionized water, propylene glycol, pantothenylol, soluble collagen, magnesium sulfate, water solublity Jojoba oil are sequentially added
In aqueous phase pot, open stirring, directly stir；
2) respectively by diethyl hexylcarbonate, tocopherol acetass, ssg-210sp, dow corning 5225c, phenyl
Poly- trimethicone sequentially adds in emulsifying pot, opens stirring, mix homogeneously；
3) mixing speed of emulsifying pot is adjusted to 200 revs/min, and a component is slowly sucked by vacuum, inhales within about 10 minutes
Complete, open low speed homogenizing, homogenizing 10 minutes；
4) by caprylyl glycol, lactic acid, essence mix homogeneously, it is then slowly added in emulsifying pot, stirs；Low speed homogenizing 10
Minute.
5) check qualified, fill.
The controlled moisture storage delivery systme of the present invention, can overcome the defect of traditional water outlet cream product, energy well
For consumer provide a kind of brand-new " water outlet " sensation and stability high go out aquatic products.This product of our exploitations,
Due to using the controlled water release system of innovation, there is following clear advantage:
1st, this moisture stores releasing effect and the speed that delivery systme can control moisture content completely, can allow active component
Continuous action to skin, expands the range of application of product.
2nd, the stability of this system will be substantially better than traditional w/o product and common " water outlet cream ".
3rd, there is very wide ph toleration, can be compatible with composition between 2～11 for the ph, can add including bigcatkin willow
Acid, in interior active component, forms slow-releasing system, and reduces skin irritation and provide long-acting.
4th, this is a kind of emulsification system in silicon source, lasting refrigerant comfortable silk can be provided to slide skin sense for skin.
5th, this delivery systme manufacturing technique requirent low it is not necessary to can be prepared by heating, energy consumption can be greatlyd save
And improve production efficiency.
6th, do not need to add traditional thickening agent and will not go out during smearing increasing the stability of system, therefore product
The sticky texture now brought due to thickening agent.
Brief description
Fig. 1 is the water outlet schematic diagram of traditional water outlet cream.
Fig. 2 is the structure chart of traditional water outlet cream.
Fig. 3 is the schematic diagram of traditional water outlet cream.
Fig. 4 is controlled moisture storage delivery systme schematic diagram.
Fig. 5 is the micro-structure diagram that controlled moisture stores delivery systme.
Fig. 6 is the water outlet schematic diagram that controlled moisture stores delivery systme.
Specific embodiment
The moisture storage delivery systme of the present invention is by certain formula by ssg-210sp and dow corning 5225c
Combine.
Being described below of this two raw material:
1st, ssg-210sp (25% polydimethylsiloxane peg-10/15 cross linked polymer and 75% polydimethylsiloxanes
Alkane), manufacturer: Japanese SHIN-ETSU HANTOTAI.
There is the unique texture of non-emulsifierses, but its can be used alone or on a small quantity cooperation emulsifying agent under conditions of, and
It readily prepares Water-In-Oil emulsified body, simple process, stable system, and outward appearance is graceful, even if under the conditions of High water cut, equally
Also highly stable emulsified body can be prepared." network structure " that ssg-210sp is formed in system, relatively conventional emulsifying dosage form
The case type micelle becoming is a semi-open system, and unique structure can be highly effective as an effective carrier
Containing and slowly release water or other active component etc..
2nd, dow corning 5225c (87.5% ring five dimethyl silicone polymer and 12.5% peg/ppg-18/18
Polydimethylsiloxane), manufacturer: Dow corning.
Dispersion in ring five dimethyl silicone polymer for the high molecular weight polyether modified organic silicon.It can be used in particular for preparing
The formula of volatile organosilicon Bao Shui.It is the transport system of a kind of non-polar component and polar compound, and non-polar component dissolves
In the organosilicon of foreign minister, polar compound is dissolved in interior phase, can form stable silicon oil packed water formulation, can be formed transparent
Emulsion system.
After polydimethylsiloxane peg-10/15 cross linked polymer and the mixing of peg/ppg-18/18 polydimethylsiloxane
The emulsifier combination being formed, under relatively low consumption, can be readily formed good stability, have the emulsified body of slow release effect.
Refer to shown in Fig. 1, be a kind of controlled moisture storage delivery systme schematic diagram of the present invention, moisture is by hydrogen bond
Active force adsorbs, and is stored in space.Fig. 2 is the micro-structure diagram that controlled moisture stores delivery systme, is shown that 3d is three-dimensional
Emulsifying agent, not necessarily forms micelle, 5-20 μm of emulsion particle diameter.Fig. 3 is the water outlet schematic diagram that controlled moisture stores delivery systme, shows
Show is to be adsorbed by Hyarogen-bonding, is stored in space.Water release is continuous, natural, controlled.
In addition, controlled moisture storage delivery systme is as shown in table 1 below with traditional water outlet cream performance comparison.
The controlled moisture storage delivery systme of table 1 and traditional water outlet cream performance comparison
Compared with prior art, the controlled slow-releasing system of the present invention overcomes the presence of traditional silicon Water-In-Oil and water outlet cream
Shortcoming, selected two kinds of emulsifying agents with special construction to constitute the slow-releasing system of innovation so that the moisture of product and work
Property composition has the effect of controlled, intelligent slow release, it is possible to reduce the zest to skin for the active component, increased active component
Action time, improve effect of product.
This formula system, has the stability of height, overcomes tradition and goes out resist cold out the quality of water stratification of aquatic products and asks
Topic；The preparation of product can be completed by conventional stirring, reduce the difficulty of production, improve production efficiency.This characteristic
" water outlet cream " fast-selling with market is similar, has very high market popularization value and good demonstrating effect.
The present invention is described in further detail with reference to effete test embodiment below by way of concrete preferred embodiment, but the present invention
It is not limited in below example.
Embodiments of the invention 1-3 is as shown in table 2 below with the raw material components of reference examples 1-2.
Table 2 embodiments of the invention 1-3 and the raw material components of reference examples 1-2
The preparation method of the controlled delivery systme compositionss described in table 2, its processing step can be expressed as follows:
1) by the deionized water in a component, propylene glycol, pantothenylol, soluble collagen, magnesium sulfate, water solublity Jojoba oil according to
In secondary addition aqueous phase pot, open stirring (60 revs/min), directly stir；
2) by the diethyl hexylcarbonate of b component, tocopherol acetass, ssg-210sp, dow corning 5225c, benzene
The poly- trimethicone of base sequentially adds in emulsifying pot, opens stirring (50 revs/min), mix homogeneously；
3) mixing speed of emulsifying pot is adjusted to 200 revs/min, and a component is slowly sucked by vacuum, inhales within about 10 minutes
Complete, open low speed homogenizing (1000 revs/min), homogenizing 10 minutes；
4) by c component caprylyl glycol, lactic acid, essence mix homogeneously, it is then slowly added in emulsifying pot, stir (200 revs/min
Clock) uniformly；Low speed homogenizing (1000 revs/min) 10 minutes.
5) check qualified, fill.
It is below effete test embodiment content.
First, outlet effect evaluation methodology:
1st, tested material: embodiment 1-3, reference examples 1-2, commercially available well-known water outlet cream.
2nd, volunteer: totally 40 people, male 15 people, female 25 people, 18～35 years old age.
Test method: pick the mastic of (about 0.3 gram) in right amount with handss amount, equably smear counterclockwise on the back of the hand, and remember
Record the number of turns smeared, observe the situation of water outlet, and make a record, pass judgment on as follows:
A, water outlet are very fast: smear less than 5 times it was observed that obvious outlet effect.
B, water outlet speed: smear more than 5 times, less than 15 times it was observed that obvious outlet effect.
C, to go out water speed general: smears more than 15 times, less than 30 times it may be observed that outlet effect.
D, water outlet are inconspicuous: smear more than 30 times, do not observe outlet effect.
3rd, evaluation of result: by above standard recording outlet effect, as shown in table 3 below.
Table 3 embodiments of the invention 1-3 is compareed with the outlet effect of reference examples 1-2, commercially available water outlet cream
Embodiment 1-3 be can be seen that due to employing slow release emulsification system by the experimental result of table 3, can control better
Mastic processed go out water speed and effect；And reference examples 1 use single emulsifying agent, its outlet effect too fast it is difficult to control
System；Reference examples 2 use single emulsifying agent, and its outlet effect is too poor, cannot provide a kind of good outlet effect.City
The water outlet cream product sold also is the use of the emulsification system of similar reference examples 1, equally show outlet effect too fast it is difficult to control
Situation.
2nd, Product Safety assessment (human skin patch result)
Tested material: embodiment 1, embodiment 2, embodiment 3, reference examples 1, reference examples 2.
Negative control: blank.
Experimenter: totally 40 people, male 15 people, female 25 people, 18～30 years old age, meet experimenter's aspiration inclusion criteria.
Speckle method for testing: try device from qualified speckle, with closed patch test method, by tested material about 0.02ml～
0.025ml is applied in speckle examination device, and external special adhesive tape is pasted on experimenter's forearm song side, removes tested material, in going after 24 hours
Except tested material speckle tries 30min after device, observe dermoreaction after impression disappears, by " cosmetics health specification " (version in 2007)
Dermoreaction grade scale records its result.
Evaluation of result: record reaction result by table 4 (skin adverse reaction grade scale), as shown in table 4 below.
Table 4 embodiments of the invention 1-3 and reference examples 1-2, the dermoreaction effect comparison of commercially available water outlet cream
Result of the test:
Cosmetics human skin patch result, as shown in table 5 below.
Table 5 embodiments of the invention 1-3 and reference examples 1-2, the human body skin patch effect comparison of commercially available water outlet cream
The human skin patch result of table 5 shows:
1) in embodiment 1,2,3 (this patent formula), all negative (grading system: 0 of 40 subjects skin
Level).According to " cosmetics health specification " (version in 2007) human body skin class patch test criterion, sample is to human body no skin not
Good reaction.
2) reference examples 1, reference examples 2 (commercially available domestic famous brand name emulsion) respectively have 2 experimenters 1 order reaction.
Experiment conclusion: embodiment employs controlled slow delivery systme, can lentamente control the release of lactic acid in product,
Reduce the zest of skin；And reference examples employ single emulsifying agent it is impossible to control the rate of release of lactic acid, thus respectively
Occur in that 1 order reaction in 2 experimenters.
3rd, product stability assessment
The sample of test: embodiment 1, embodiment 2, embodiment 3, reference examples 1, reference examples 2, commercially available water outlet cream.
2.1.1 temperature stability test
2.1.1.1 48 DEG C of stability tests:
Test sample: 1 or more.Testing time: 4 weeks.
Method of testing: product (content) is loaded in the pet bottle of 30ml, labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in the heat-resistant stability of test product in 48 DEG C of biochemical cultivation case, exist respectively
24 hours, 1 week, 2 weeks, 4 weeks when (recover to room temperature) to observe the outward appearance of product, abnormal smells from the patient, ph, the change of viscosity, and by day part
Change, be recorded in report.
2.1.1.2 40 DEG C of stability tests:
Test sample: 1 or more.Testing time: 12 weeks.
Method of testing: product (content) is loaded in the pet bottle of 30ml, labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in the heat-resistant stability of test product in 40 DEG C of biochemical cultivation case, exist respectively
(recover to room temperature) when 24 hours, 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks to observe the outward appearance of product, abnormal smells from the patient, ph, the change of viscosity,
And the change by day part, it is recorded in report.
2.1.1.3 room temperature (ambient) stability test:
Test sample: 1 or more.Testing time: 12 weeks.
Method of testing: product (content) is loaded in the pet bottle of 30ml, labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in sample cabinet, respectively 24 hours (survey ph value, viscosimetric), 1 week, 2 weeks, 4
The outward appearance of observation product, abnormal smells from the patient, ph, the change of viscosity, and the change by day part, record during week, 8 weeks and 12 weeks (surveying ph value)
Enter in report.
2.1.1.4-18 DEG C stability test:
Test sample: 1 or more.Testing time: 12 weeks.
Method of testing: product (content) is loaded in the pet bottle of 30ml, labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in the cold-resistant stability of test product in -18 DEG C of refrigerators, respectively 24 hours, 1
Week, 2 weeks, 4 weeks, 8 weeks and (recover to room temperature) outward appearance of observation product, abnormal smells from the patient, ph, the change of viscosity when 12 weeks, and when will be each
The change of section, is recorded in report.
Stability result: embodiment 1,2,3 has passed through the stability test of 12 weeks, product shows the stability of height.
In the cold-resistant test when 2 weeks for the reference examples 1,2, occur in that out the phenomenon of water stratification；When 1 week, product commercially available water outlet cream occurred
The resistance to phenomenon giving the best account of water stratification.
The above, be only presently preferred embodiments of the present invention, not the present invention is made with any pro forma restriction, therefore
Every without departing from technical solution of the present invention content, any simply repaiied according to what the technical spirit of the present invention made to above example
Change, equivalent variations and modification, all still fall within the range of technical solution of the present invention.
Claims (3)
1. a kind of controlled moisture slow-releasing system emulsification composition it is characterised in that: by weight percentage, described moisture slow release
System combination comprises:
1.0%～2.5% ssg-210sp, described ssg-210sp are polydimethylsiloxane peg-10/15 cross linked polymers
The mixture forming by weight 1:3 with polydimethylsiloxane；
3.0%～8.0% dow corning 5225c, described dow corning 5225c is ring five dimethyl silicone polymer
The mixture forming by weight 1:7 with peg/ppg-18/18 polydimethylsiloxane.
2. controlled moisture slow-releasing system emulsification composition according to claim 1 is it is characterised in that also comprise following a
Component, b component and c component:
Described a component comprises: propylene glycol 5.0%～15.0%, pantothenylol 0.2%～1.0%, soluble collagen 0.2%～
2.0%th, Pyrusussuriensiss (sugared) alcohol 5.0%-10.0%, magnesium sulfate 0.5%～0.8%, water solublity Jojoba oil 0.1%～0.3%, remaining
Amount deionized water；
Described b component comprises: diethyl hexylcarbonate 2.0%～7.0%, tocopherol acetass 0.2%～1.0%, phenyl gather
Trimethicone 1.0%～40.0%；
Described c component comprises: caprylyl glycol 0.4%～0.6%, lactic acid 0.8%～1.5%, essence 0.01%～0.03%.
3. the controlled moisture slow-releasing system emulsification composition described in claim 2 preparation method it is characterised in that include with
Lower step:
1) deionized water in a component, propylene glycol, pantothenylol, soluble collagen, magnesium sulfate, water solublity Jojoba oil are added successively
Enter in aqueous phase pot, open stirring, directly stir；
2) diethyl hexylcarbonate of b component, tocopherol acetass, ssg-210sp, dow corning 5225c, phenyl are gathered
Trimethicone sequentially adds in emulsifying pot, opens stirring, mix homogeneously；
3) mixing speed of emulsifying pot is adjusted to 200 revs/min, and a component is slowly sucked by vacuum, sucks within about 10 minutes,
Open low speed homogenizing, homogenizing 10 minutes；
4) by the caprylyl glycol of c component, lactic acid, essence mix homogeneously, it is then slowly added in emulsifying pot, stirs；Low speed is equal
Matter 10 minutes.
5) check qualified, fill.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107536718A (en) * | 2017-09-29 | 2018-01-05 | 广东馨柯生命科学有限公司 | A kind of long-acting slow-release whitening snow defrosting and preparation method thereof |
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