CN106360718A - Extraction technology of aloe vera gels - Google Patents
Extraction technology of aloe vera gels Download PDFInfo
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- CN106360718A CN106360718A CN201610734334.0A CN201610734334A CN106360718A CN 106360718 A CN106360718 A CN 106360718A CN 201610734334 A CN201610734334 A CN 201610734334A CN 106360718 A CN106360718 A CN 106360718A
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- China
- Prior art keywords
- aloe
- aloe vera
- extraction process
- filter
- temperature
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- 235000011399 aloe vera Nutrition 0.000 title claims abstract description 65
- 238000000605 extraction Methods 0.000 title claims abstract description 24
- 235000002961 Aloe barbadensis Nutrition 0.000 title claims abstract description 14
- 244000186892 Aloe vera Species 0.000 title claims abstract description 14
- 239000000499 gel Substances 0.000 title abstract 4
- 102000004190 Enzymes Human genes 0.000 claims abstract description 9
- 108090000790 Enzymes Proteins 0.000 claims abstract description 9
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 7
- 239000011159 matrix material Substances 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 239000000758 substrate Substances 0.000 claims abstract description 5
- 238000007710 freezing Methods 0.000 claims abstract description 4
- 230000008014 freezing Effects 0.000 claims abstract description 4
- 238000010257 thawing Methods 0.000 claims abstract description 4
- 241001116389 Aloe Species 0.000 claims description 51
- 239000000706 filtrate Substances 0.000 claims description 12
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 8
- 239000011550 stock solution Substances 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- 238000001728 nano-filtration Methods 0.000 claims description 6
- 150000005846 sugar alcohols Polymers 0.000 claims description 6
- 239000012528 membrane Substances 0.000 claims description 5
- 238000009472 formulation Methods 0.000 claims description 4
- 238000000108 ultra-filtration Methods 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000001976 enzyme digestion Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical compound ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 9
- 238000012545 processing Methods 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 4
- 239000004480 active ingredient Substances 0.000 abstract 2
- 238000002360 preparation method Methods 0.000 abstract 1
- 230000001954 sterilising effect Effects 0.000 abstract 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 235000014676 Phragmites communis Nutrition 0.000 description 5
- AFHJQYHRLPMKHU-XXWVOBANSA-N Aloin Natural products O=C1c2c(O)cc(CO)cc2[C@H]([C@H]2[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O2)c2c1c(O)ccc2 AFHJQYHRLPMKHU-XXWVOBANSA-N 0.000 description 3
- AFHJQYHRLPMKHU-OSYMLPPYSA-N aloin A Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1[C@@H]1C2=CC(CO)=CC(O)=C2C(=O)C2=C(O)C=CC=C21 AFHJQYHRLPMKHU-OSYMLPPYSA-N 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- AFHJQYHRLPMKHU-UHFFFAOYSA-N isobarbaloin Natural products OC1C(O)C(O)C(CO)OC1C1C2=CC(CO)=CC(O)=C2C(=O)C2=C(O)C=CC=C21 AFHJQYHRLPMKHU-UHFFFAOYSA-N 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 2
- 230000035614 depigmentation Effects 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000012356 Product development Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 208000019622 heart disease Diseases 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000011275 oncology therapy Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention discloses an extraction technology of aloe vera gels. The extraction technology comprises the following steps: aloe vera is peeled, the peeled aloe vera is subjected to enzymolysis, namely a gel matrix of the aloe vera is used as a substrate, under the reaction condition of the temperature of 50 DEG C-55 DEG C and the pH of 4-5.5, a biological enzyme preparation with the amount being 0.03%-0.08% of the mass of the substrate is added, the enzymolysis is conducted under a condition of stirring, and then extracting, coarse filtering, freezing, thawing, fine filtering, decolorizing, nano-filtering and ultrahigh pressure sterilizing are carried out. Compared with the existing technical schemes, the extraction technology of the aloe vera gels can greatly improve the extraction rate of the active ingredients of the aloe vera, at the same time reduces the caused loss of the active ingredients of the aloe vera in the processing processes, and improves the product added values.
Description
Technical field
The present invention relates to a kind of extraction process of Aloe gel, belong to Aloe gel extracting method field.
Background technology
In recent years, because Aloe gel obtains consumer's accreditation, reed in effect of the aspects such as beauty treatment, health food, medicine
Luxuriant growth gel industry is also flourishing.The developing mechanism of external Aloe industry is fairly perfect, has evolved into plantation, processing, sells
Integration, the exploitation of the suitability extensive aloe product is increasingly complete, and progressively turns to the high in technological content and high reed of added value
The exploitation of luxuriant growth product.Aloe product from initial Aloe cosmetics, health product, medicine, the food containing Aloe miscellaneous,
To nowadays high-end treatment diabetes, heart disease and cancer therapy drug etc..
China's aloe industry is started in late 1980s, and the aloe industry of China is scarcely out of swaddling-clothes.With reed
The health keeping and medical function of luxuriant growth is recognized, and China has started " Aloe heat ", also advances the development of China's aloe industry.At present,
Come in terms of the cultivated area of Aloe, process technology, product development ability, market development degree and research strength and level etc.
See, the development of China's aloe industry still belongs to the primary stage, and the technical merit of processing Aloe is relatively low, and scientific and technological content is not also high, but
It is that China Aloe market also expands continuous, the market potential of China's aloe product is big indubitable.
The extracting method of Aloe gel mainly has solvent extraction method and ultrasonic extraction at present, but these traditional extraction sides
Method yield is relatively low, seriously polluted, is not easy to industrialization.Meanwhile, although traditional Technology for Heating Processing can sterilize, enzyme denaturing, meeting
Destroying the heat-sensitive ingredients such as barbaloin, will also result in the change of Aloe gel color and luster, fragrance, so needing to be invented new extraction side
Method is solving the above problems.
Content of the invention
(1) technical problem to be solved
For solving the above problems, the present invention proposes a kind of extraction process of Aloe gel.
(2) technical scheme
The extraction process of the Aloe gel of the present invention, including below scheme:
(1) Aloe peeling: take fresh aloe to be raw material, automatically stripped with machine and obtain Aloe vera inner gel matrix after leaf skin；
(2) digest: with Aloe vera inner gel matrix as substrate, be 50 DEG C -55 DEG C in temperature, ph is the reaction condition of 4-5.5
Under, add the biological enzyme formulation of the 0.03%-0.08% of bottom quantity of material amount to carry out enzyme digestion reaction under conditions of stirring, reach
Higher rational enzymolysis yield value；
(3) extract: under the conditions of temperature is 10 DEG C -20 DEG C, using polyhydric alcohol extraction, the time is 60min；
(4) coarse filtration: extract is carried out on filter primary filter；
(5) freeze；
(6) thaw；
(7) fine straining: by thaw after primary filtrate secondary filter is carried out on filter, remove further chilled and
Precipitation of thawing or the impurity of polymerization, obtain the higher Aloe gel stock solution of purity；
(8) decolour: at ambient temperature, add active carbon powder to pass through stirring in the Aloe gel stock solution after fine straining
Decolouring, removes depigmentation thoroughly, good decolorizing effect；
(9) nanofiltration: under normal temperature condition, first organic from molecular cut off 4000da in airtight concentration systems
Aloe gel stock solution is filtered by ultrafilter membrane, then from the nanofiltration membrane of molecular cut off 300da, the filtrate of ultrafiltration is carried out
Concentrate so that the molecular weight of active component is maintained between 300da-4000da in solution, be concentrated into and slough 90% moisture, obtain
10:1 concentrated solution；
(10) supertension sterilize: be 400mpa in pressure, collaborative temperature be 30 DEG C under the conditions of ultrahigh pressure vessel in will be dense
After contracting liquid pressurize 15min, deaerate after pressure is reduced to 0 20min, can sterilize, enzyme denaturing, can preferably keep reed in concentrated solution again
Luxuriant growth polysaccharide, the quality of barbaloin isoreactivity composition.
As preferred technical scheme, described polyhydric alcohol is mixed with 1:1 ratio by ethylene glycol and glycerol, extraction effect
Really good, purity is high.
As preferred technical scheme, described Aloe is U.S. Curacao kind Aloe.
As preferred technical scheme, described filter adopts horizontal vacuum belt filter.
As preferred technical scheme, the temperature of described freezing is -10 DEG C -15 DEG C, and cooling time is 40min-80min,
On the one hand can ensure that original quality of the active component in primary filtrate, on the other hand can allow miscellaneous in primary filtrate
Matter preferably precipitates or aggregates into macromole, is easy to the carrying out of fine straining process.
As preferred technical scheme, described thaw point is 25 DEG C -30 DEG C, the quality of primary filtrate will not be caused
Destroy.
(3) beneficial effect
Compared with prior art, it has the advantages that the extraction process of the Aloe gel of the present invention to the present invention,
The extraction ratio of active aloe composition can be greatly improved, reduce the loss of the active aloe composition that the course of processing causes simultaneously, improve
Added value of product.
Specific embodiment
By the following examples the present invention is further detailed.
(1) Aloe peeling: take fresh aloe to be raw material, automatically stripped with machine and obtain Aloe vera inner gel matrix after leaf skin；
(2) digest: with Aloe vera inner gel matrix as substrate, be 50 DEG C -55 DEG C in temperature, ph is the reaction condition of 4-5.5
Under, add the biological enzyme formulation of the 0.03%-0.08% of bottom quantity of material amount to carry out enzyme digestion reaction under conditions of stirring, reach
Higher rational enzymolysis yield value；
(3) extract: under the conditions of temperature is 10 DEG C -20 DEG C, using polyhydric alcohol extraction, the time is 60min；
(4) coarse filtration: extract is carried out on filter primary filter；
(5) freeze；
(6) thaw；
(7) fine straining: by thaw after primary filtrate secondary filter is carried out on filter, remove further chilled and
Precipitation of thawing or the impurity of polymerization, obtain the higher Aloe gel stock solution of purity；
(8) decolour: at ambient temperature, add active carbon powder to pass through stirring in the Aloe gel stock solution after fine straining
Decolouring, removes depigmentation thoroughly, good decolorizing effect；
(9) nanofiltration: under normal temperature condition, first organic from molecular cut off 4000da in airtight concentration systems
Aloe gel stock solution is filtered by ultrafilter membrane, then from the nanofiltration membrane of molecular cut off 300da, the filtrate of ultrafiltration is carried out
Concentrate so that the molecular weight of active component is maintained between 300da-4000da in solution, be concentrated into and slough 90% moisture, obtain
10:1 concentrated solution；
(10) supertension sterilize: be 400mpa in pressure, collaborative temperature be 30 DEG C under the conditions of ultrahigh pressure vessel in will be dense
After contracting liquid pressurize 15min, deaerate after pressure is reduced to 0 20min, can sterilize, enzyme denaturing, can preferably keep reed in concentrated solution again
Luxuriant growth polysaccharide, the quality of barbaloin isoreactivity composition.
Further, described polyhydric alcohol is mixed with 1:1 ratio by ethylene glycol and glycerol, and effect of extracting is good, purity
High.
Further, described Aloe is U.S. Curacao kind Aloe.
Further, described filter adopts horizontal vacuum belt filter, good filtration effect.
Further, the temperature of described freezing is -10 DEG C -15 DEG C, and cooling time is 40min-80min, on the one hand permissible
Ensure original quality of the active component in primary filtrate, the impurity in primary filtrate on the other hand can be allowed preferably to sink
Form sediment or aggregate into macromole, be easy to the carrying out of fine straining process.
Further, described thaw point is 25 DEG C -30 DEG C, and the quality of primary filtrate will not be damaged.
Embodiment described above is only that the preferred embodiment of the present invention is described, the not structure to the present invention
Think and scope is defined.On the premise of without departing from design concept of the present invention, the technology to the present invention for this area ordinary person
Various modifications and improvement that scheme is made, all should drop into protection scope of the present invention, the technology contents that the present invention is claimed,
All record in detail in the claims.
Claims (7)
1. a kind of extraction process of Aloe gel, including below scheme:
(1) Aloe peeling: take fresh aloe to be raw material, automatically stripped with machine and obtain Aloe vera inner gel matrix after leaf skin；
(2) digest: with Aloe vera inner gel matrix as substrate, it is 50 DEG C -55 DEG C in temperature, ph is under the reaction condition of 4-5.5, plus
The biological enzyme formulation entering the 0.03%-0.08% of bottom quantity of material amount carries out enzyme digestion reaction under conditions of stirring；
(3) extract: under the conditions of temperature is 10 DEG C -20 DEG C, using polyhydric alcohol extraction, the time is 60min；
(4) coarse filtration: extract is carried out on filter primary filter；
(5) freeze；
(6) thaw；
(7) fine straining: the primary filtrate after thawing is carried out secondary filter on filter；
(8) decolour: at ambient temperature, add active carbon powder to pass through stirring in the Aloe gel stock solution after fine straining de-
Color；
(9) nanofiltration: under normal temperature condition, first select organic ultrafiltration of molecular cut off 4000da in airtight concentration systems
Aloe gel stock solution is filtered by film, then from the nanofiltration membrane of molecular cut off 300da, the filtrate of ultrafiltration is concentrated；
(10) supertension sterilize: be 400mpa in pressure, collaborative temperature be 30 DEG C under the conditions of ultrahigh pressure vessel in by concentrated solution
After pressurize 15min, deaerate after pressure is reduced to 0 20min.
2. Aloe gel according to claim 1 extraction process it is characterised in that: described polyhydric alcohol is by ethylene glycol and third
Triol is mixed with 1:1 ratio.
3. Aloe gel according to claim 1 extraction process it is characterised in that: described Aloe be U.S.'s Curacao product
Plant Aloe.
4. Aloe gel according to claim 1 extraction process it is characterised in that: described biological enzyme formulation be cellulose
Enzyme.
5. Aloe gel according to claim 1 extraction process it is characterised in that: described filter adopts horizontal belt
Vacuum filter.
6. Aloe gel according to claim 1 extraction process it is characterised in that: the temperature of described freezing be -10 DEG C -
15 DEG C, cooling time is 40min-80min.
7. Aloe gel according to claim 1 extraction process it is characterised in that: described thaw point be 25 DEG C -30
℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610734334.0A CN106360718A (en) | 2016-08-26 | 2016-08-26 | Extraction technology of aloe vera gels |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610734334.0A CN106360718A (en) | 2016-08-26 | 2016-08-26 | Extraction technology of aloe vera gels |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106360718A true CN106360718A (en) | 2017-02-01 |
Family
ID=57902728
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610734334.0A Pending CN106360718A (en) | 2016-08-26 | 2016-08-26 | Extraction technology of aloe vera gels |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106360718A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107050217A (en) * | 2017-06-26 | 2017-08-18 | 湖州知维技术服务有限公司 | A kind of preparation method of aloe gel |
| CN109487543A (en) * | 2018-11-12 | 2019-03-19 | 北京阿尔法针织有限公司 | A kind of knitting of knitted fabric |
| CN109498732A (en) * | 2018-11-26 | 2019-03-22 | 郑州吉尔康消毒制品有限公司 | Hand-wrist bones gel and preparation method thereof |
| CN110393692A (en) * | 2019-09-04 | 2019-11-01 | 广东丸美生物技术股份有限公司 | Wire drawing plant thickener and its preparation method and application |
| CN112189847A (en) * | 2020-09-08 | 2021-01-08 | 武汉金绿谷生物科技有限公司 | Preparation process of herbal gel |
| CN114917170A (en) * | 2022-05-25 | 2022-08-19 | 科玛化妆品(无锡)有限公司 | Aloe gel frosted particles and preparation method and application thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107050217A (en) * | 2017-06-26 | 2017-08-18 | 湖州知维技术服务有限公司 | A kind of preparation method of aloe gel |
| CN109487543A (en) * | 2018-11-12 | 2019-03-19 | 北京阿尔法针织有限公司 | A kind of knitting of knitted fabric |
| CN109487543B (en) * | 2018-11-12 | 2021-05-11 | 北京阿尔法针织有限公司 | Knitting process of knitted fabric |
| CN109498732A (en) * | 2018-11-26 | 2019-03-22 | 郑州吉尔康消毒制品有限公司 | Hand-wrist bones gel and preparation method thereof |
| CN110393692A (en) * | 2019-09-04 | 2019-11-01 | 广东丸美生物技术股份有限公司 | Wire drawing plant thickener and its preparation method and application |
| CN110393692B (en) * | 2019-09-04 | 2023-03-31 | 广东丸美生物技术股份有限公司 | Wiredrawing plant thickening agent and preparation method and application thereof |
| CN112189847A (en) * | 2020-09-08 | 2021-01-08 | 武汉金绿谷生物科技有限公司 | Preparation process of herbal gel |
| CN114917170A (en) * | 2022-05-25 | 2022-08-19 | 科玛化妆品(无锡)有限公司 | Aloe gel frosted particles and preparation method and application thereof |
| CN114917170B (en) * | 2022-05-25 | 2023-10-13 | 科玛化妆品(无锡)有限公司 | Aloe gel frosted particles and preparation method and application thereof |
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