CN106345275A - Deodorant containing jasmine tea extractive - Google Patents

Deodorant containing jasmine tea extractive Download PDF

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Publication number
CN106345275A
CN106345275A CN201610810099.0A CN201610810099A CN106345275A CN 106345275 A CN106345275 A CN 106345275A CN 201610810099 A CN201610810099 A CN 201610810099A CN 106345275 A CN106345275 A CN 106345275A
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China
Prior art keywords
extract
jasmine tea
water
gained
tea
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Pending
Application number
CN201610810099.0A
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Chinese (zh)
Inventor
吴亮宇
林金科
郭雅玲
刘江洪
王艳娜
张玥
鲁静
吴命燕
林东艺
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Fujian Agriculture and Forestry University
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Fujian Agriculture and Forestry University
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Priority to CN201610810099.0A priority Critical patent/CN106345275A/en
Publication of CN106345275A publication Critical patent/CN106345275A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/84Biological processes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Molecular Biology (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Tea And Coffee (AREA)

Abstract

The invention discloses a deodorant containing jasmine tea extractive. The deodorant containing jasmine tea extractive takes the middle and low level jasmine tea with wide source and low price as the raw material; through leaching, concentration, filtering and other processes, the jasmine tea extractive is firstly obtained; the extractive reserves the fragrance of the jasmine tea soup and natural active matters in the tea; the extractive is mixed with a plant extractive, thus the prepared deodorant has the natural fragrance of jasmine, and excludes other chemical drugs; therefore, the deodorant is safe and harmless to human body.

Description

A kind of deodorizer containing Jasmine tea extract
Technical field
The invention belongs to tea product field of deep is and in particular to a kind of deodorizer containing Jasmine tea extract.
Background technology
Jasmine tea is a kind of distinctive reprocessing class tea product in Fuzhou area, and it includes the mouthfeel of Folium Camelliae sinensis and flavour, Also there is the special fragrance of Flos Jasmini Sambac, effect of refreshment, dispersing the stagnated live-QI to relieve the stagnation of QI can be reached by drinking Jasmine tea.But at present Consumer can only reach the purpose enjoying Jasmine tea product by way of boiling water brews, and lacks to Jasmine tea deep processing side The utilization in face.Based on this, this method passes through series of process method, prepares a kind of Jasmine tea extract of concentrated type, and It is raw material using this extract, produce the deodorizer with Jasmine tea fragrance and tea natural active substance, this deodorizer There is safety, to human body fanout free region, and there is good deodorizing effect.
Content of the invention
It is an object of the invention to provide a kind of deodorizer containing Jasmine tea extract, Jasmine tea extract used Remain with the natural active matter in the fragrance and Folium Camelliae sinensis of Flos Jasmini Sambac millet paste so as to the deodorizer being prepared into has the sky of Flos Jasmini Sambac So aromatic fragrance.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of deodorizer containing Jasmine tea extract, its preparation method comprises the following steps:
1) extract: cross 40 mesh sieves after the Jasmine tea being dried is pulverized, gained tea powder adds water by weight 1:50, Extract 15-30 min in 0.1mpa, 40-50 DEG C of water-bath, be filtrated to get leach at low temperature liquid;Then again by weight 1:50 in residue Middle addition water, extracts 15-30 min in 0.1mpa, 90-100 DEG C of water-bath, is filtrated to get high-temp extracting liquid, merges and extracts twice Liquid;
2) concentrate: gained lixiviating solution is concentrated under the conditions of 3-5kpa, 45-55 DEG C, is former lixiviating solution to the volume of concentrate The 10-20% of volume;
3) filter: after solution to be concentrated is cooled to room temperature, filtered with the filter membrane that aperture is 0.22 μm, obtain Jasmine tea and carry Take thing;
4) preparation of deodorizer: gained Jasmine tea extract is added to the water jointly with plant extract and stirs, heating To 35-40 DEG C and keep 30-60min, fill after cooling obtains final product.
In step 4), the addition of Jasmine tea extract accounts for the 25-30% of composition of raw materials weight.
Described plant extract includes Pericarpium Citri tangerinae extract, Pericarpium Citri grandis extract, Pericarpium Citri junoris extract, Ramulus et Folium Bauhiniae Faberi extract, winter Arbitrarily two or more in Folium Isatidis extract, Flos Caryophylli extract, orange blossom extract, Folium Menthae extract.
It is an advantage of the current invention that:
The present invention utilizes low temperature, high temperature step by step arithmetic, obtains remaining with carrying of Jasmine tea fragrance and tea natural active substance Take thing, and by being processed further being made into deodorizer.From the angle of cost control, the Jasmine tea used by the present invention Raw material can be using low and middle-grade Jasmine tea, and its wide material sources is cheap, it is possible to achieve the utilizing to greatest extent of resource.
Deodorizer provided by the present invention remains with original Jasmine tea fragrance and tea natural product, and adds without chemistry Thing, harmless and there is good deodorizing effect, can use in most of life area;And it has good stability, effect Insist on long, the various places needing clean odors can be widely used in.
Brief description
Fig. 1 is the high-efficient liquid phase chromatogram of gained Jasmine tea extract.
Specific embodiment
The preparation method of Jasmine tea extract comprises the following steps:
1) extract: cross 40 mesh sieves after the Jasmine tea being dried being pulverized using grinding machinery, gained tea powder adds by weight 1:50 Enter water, extract 15-30 min in 0.1mpa, 40-50 DEG C of water-bath, be filtrated to get leach at low temperature liquid;Then again by weight 1: 50 add water in residue, extract 15-30 min, be filtrated to get high-temp extracting liquid in 0.1mpa, 90-100 DEG C of water-bath, merge Lixiviating solution twice;
2) concentrate: gained lixiviating solution is concentrated in 3-5kpa, 45-55 DEG C of Rotary Evaporators, is former to the volume of concentrate The 10-20% of lixiviating solution volume;
3) filter: after solution to be concentrated is cooled to room temperature, filtered with the filter membrane that aperture is 0.22 μm, to remove insoluble matter And microorganism, obtain Jasmine tea extract.
After the bud of Theaceae Camellia (camellia sinensis) plant, leaf, tender stem can be harvested by Jasmine tea used, By the enzymatic activity in heating passivation fresh leaf, then by the azymic Folium Camelliae sinensis that technology obtains such as kneading, being dried, then in Folium Camelliae sinensis Add Flos Jasmini Sambac flower in full bloom to carry out scenting, weed out Flos Jasmini Sambac after scenting and be obtained;Or discard after being processed using Jasmine tea Broken leaf, old leaf.
Gained Jasmine tea extract is the powder to brown color for the sundown, and mildly bitter flavor has astringent taste, can be with hot water or cold water Dissolved each other with arbitrary proportion, also dissolve in the organic solvents such as methanol, ethanol, acetone, ethyl acetate, be slightly soluble in benzene, chloroform and oil Ether;And gained Jasmine tea extract thermostability is good, can keep steady in 250 DEG C about of ambient temperature in 1.5 hours Fixed;Its acid resistance is good, all sufficiently stable in the range of ph 2 ~ 6.Slightly moisture absorption, aqueous solution ph 3 ~ 4.
Gained Jasmine tea extract is carried out with efficient liquid phase chromatographic analysis, method is with reference to gb/t 8313-2008, chromatograph Result is shown in Fig. 1, and in extract, caffeine and each catechin component content are shown in Table 1.
Caffeine and catechin component content in table 1 extract
From testing result, gained Jasmine tea extract is rich in caffeine and catechin composition, and these compositions have suppression The effect of glucose polymerisation enzymatic activity processed, has significant anti-proliferative effect to lactic acid bacteria and other noxious bacteria, it is possible to reduce have The attachment of evil flora and breeding, it is to avoid a large amount of unpleasant smells that flora is assembled and produced.
In order that content of the present invention easily facilitates understanding, with reference to specific embodiment to of the present invention Technical scheme is described further, but the present invention is not limited only to this.
Embodiment 1
1) extract: cross 40 mesh sieves after the Jasmine tea being dried being pulverized using grinding machinery, gained tea powder adds by weight 1:50 Enter water, extract 30 min in 0.1mpa, 40 DEG C of water-baths, be filtrated to get leach at low temperature liquid;Then again by weight 1:50 residual Add water in slag, in 0.1mpa, 90 DEG C of water-baths, extract 30 min, be filtrated to get high-temp extracting liquid, merge lixiviating solution twice;
2) concentrate: gained lixiviating solution is concentrated in 3kpa, 55 DEG C of Rotary Evaporators, is former lixiviating solution to the volume of concentrate The 10% of volume;
3) filter: after solution to be concentrated is cooled to room temperature, filtered with the filter membrane that aperture is 0.22 μm, to remove insoluble matter And microorganism, obtain Jasmine tea extract;
4) preparation of plant extract: after Pericarpium Citri tangerinae, pomelo peel, Pericarpium Citri junoriss are pulverized respectively, add water by weight 1:5, distillation extraction 4h, obtains Pericarpium Citri tangerinae extract, Pericarpium Citri grandis extract and Pericarpium Citri junoris extract;
5) preparation of deodorizer: gained Jasmine tea extract and Pericarpium Citri tangerinae extract, Pericarpium Citri grandis extract, Pericarpium Citri junoris extract are added Enter in water and stir, be heated to 40 DEG C and keep 30min, fill after cooling obtains final product.
Weight percent sum is 100% meter, and percetage by weight shared by each raw material in step 5) is: Jasmine tea extracts Thing 30%, Pericarpium Citri tangerinae extract 20%, Pericarpium Citri grandis extract 15%, Pericarpium Citri junoris extract 5%, balance of water.
Embodiment 2
1) extract: cross 40 mesh sieves after the Jasmine tea being dried being pulverized using grinding machinery, gained tea powder adds by weight 1:50 Enter water, extract 20 min in 0.1mpa, 50 DEG C of water-baths, be filtrated to get leach at low temperature liquid;Then again by weight 1:50 residual Add water in slag, in 0.1mpa, 100 DEG C of water-baths, extract 20 min, be filtrated to get high-temp extracting liquid, merge lixiviating solution twice;
2) concentrate: gained lixiviating solution is concentrated in 5kpa, 45 DEG C of Rotary Evaporators, is former lixiviating solution to the volume of concentrate The 20% of volume;
3) filter: after solution to be concentrated is cooled to room temperature, filtered with the filter membrane that aperture is 0.22 μm, to remove insoluble matter And microorganism, obtain Jasmine tea extract;
4) preparation of plant extract: after Ramulus et Folium Bauhiniae Faberi, Pericarpium Citri junoriss, Folium Ilicis Purpureae are pulverized respectively, add water by weight 1:5, distillation carries Take 3h, obtain Ramulus et Folium Bauhiniae Faberi extract, Pericarpium Citri junoris extract and Ilicis Purpureae leaf extract;
5) preparation of deodorizer: by gained Jasmine tea extract and Ramulus et Folium Bauhiniae Faberi extract, Pericarpium Citri junoris extract, Ilicis Purpureae leaf extract It is added to the water and stirs, be heated to 40 DEG C and keep 30min, fill after cooling obtains final product.
Weight percent sum is 100% meter, and percetage by weight shared by each raw material in step 5) is: Jasmine tea extracts Thing 30%, Ramulus et Folium Bauhiniae Faberi extract 10%, Pericarpium Citri junoris extract 10%, Ilicis Purpureae leaf extract 5%, balance of water.
Embodiment 3
1) extract: cross 40 mesh sieves after the Jasmine tea being dried being pulverized using grinding machinery, gained tea powder adds by weight 1:50 Enter water, extract 15 min in 0.1mpa, 45 DEG C of water-baths, be filtrated to get leach at low temperature liquid;Then again by weight 1:50 residual Add water in slag, in 0.1mpa, 95 DEG C of water-baths, extract 15 min, be filtrated to get high-temp extracting liquid, merge lixiviating solution twice;
2) concentrate: gained lixiviating solution is concentrated in 4kpa, 40 DEG C of Rotary Evaporators, is former lixiviating solution to the volume of concentrate The 15% of volume;
3) filter: after solution to be concentrated is cooled to room temperature, filtered with the filter membrane that aperture is 0.22 μm, to remove insoluble matter And microorganism, obtain Jasmine tea extract;
4) preparation of plant extract: after Flos Caryophylli, Herba Menthae, orange blossom are pulverized respectively, add water by weight 1:5,50 DEG C of extraction 2h, Obtain Flos Caryophylli extract, Folium Menthae extract and orange blossom extract;
5) preparation of deodorizer: gained Jasmine tea extract is added with Flos Caryophylli extract, Folium Menthae extract, orange blossom extract Stir in water, be heated to 35 DEG C and keep 60min, fill after cooling obtains final product.
Weight percent sum is 100% meter, and percetage by weight shared by each raw material in step 5) is: Jasmine tea extracts Thing 25%, Flos Caryophylli extract 10%, Folium Menthae extract 15%, orange blossom extract 15%, balance of water.
The foregoing is only presently preferred embodiments of the present invention, all impartial changes done according to scope of the present invention patent with Modify, all should belong to the covering scope of the present invention.

Claims (3)

1. a kind of deodorizer containing Jasmine tea extract it is characterised in that: its preparation method comprises the following steps:
1) extract: cross 40 mesh sieves after the Jasmine tea being dried is pulverized, gained tea powder adds water by weight 1:50, Extract 15-30 min in 0.1mpa, 40-50 DEG C of water-bath, be filtrated to get leach at low temperature liquid;Then again by weight 1:50 in residue Middle addition water, extracts 15-30 min in 0.1mpa, 90-100 DEG C of water-bath, is filtrated to get high-temp extracting liquid, merges and extracts twice Liquid;
2) concentrate: gained lixiviating solution is concentrated under the conditions of 3-5kpa, 45-55 DEG C, is former lixiviating solution to the volume of concentrate The 10-20% of volume;
3) filter: after solution to be concentrated is cooled to room temperature, filtered with the filter membrane that aperture is 0.22 μm, obtain Jasmine tea and carry Take thing;
4) preparation of deodorizer: gained Jasmine tea extract is added to the water jointly with plant extract and stirs, heating To 35-40 DEG C and keep 30-60min, fill after cooling obtains final product.
2. according to claim 1 the deodorizer containing Jasmine tea extract it is characterised in that: Jasmine tea in step 4) The addition of extract accounts for the 25-30% of composition of raw materials weight.
3. according to claim 1 the deodorizer containing Jasmine tea extract it is characterised in that: described plant extract bag Include Pericarpium Citri tangerinae extract, Pericarpium Citri grandis extract, Pericarpium Citri junoris extract, Ramulus et Folium Bauhiniae Faberi extract, Ilicis Purpureae leaf extract, Flos Caryophylli extract, orange Arbitrarily two or more in flower extract, Folium Menthae extract.
CN201610810099.0A 2016-09-08 2016-09-08 Deodorant containing jasmine tea extractive Pending CN106345275A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108578519A (en) * 2018-04-11 2018-09-28 福建农林大学 A kind of anti-oxidant eyedrops and preparation method thereof containing jasmine tea extract
CN111528228A (en) * 2020-04-30 2020-08-14 吴端表 Antibacterial and deodorant compound

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102763743A (en) * 2012-08-06 2012-11-07 福建农林大学 Process for processing instant tea with high content of ester-type catechin
CN103418009A (en) * 2013-08-16 2013-12-04 马健 Grapefruit freshening deodorant
CN103751829A (en) * 2014-01-27 2014-04-30 北京戴斯科技有限公司 Deodorizer and preparation method thereof
CN105053030A (en) * 2015-08-11 2015-11-18 无锡桥阳机械制造有限公司 Preparation method of jasmine tea spray

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102763743A (en) * 2012-08-06 2012-11-07 福建农林大学 Process for processing instant tea with high content of ester-type catechin
CN103418009A (en) * 2013-08-16 2013-12-04 马健 Grapefruit freshening deodorant
CN103751829A (en) * 2014-01-27 2014-04-30 北京戴斯科技有限公司 Deodorizer and preparation method thereof
CN105053030A (en) * 2015-08-11 2015-11-18 无锡桥阳机械制造有限公司 Preparation method of jasmine tea spray

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108578519A (en) * 2018-04-11 2018-09-28 福建农林大学 A kind of anti-oxidant eyedrops and preparation method thereof containing jasmine tea extract
CN111528228A (en) * 2020-04-30 2020-08-14 吴端表 Antibacterial and deodorant compound

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