CN106333880A - Toner with dilute emulsion substrate and preparation method thereof - Google Patents

Toner with dilute emulsion substrate and preparation method thereof Download PDF

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CN106333880A
CN106333880A CN201610917268.0A CN201610917268A CN106333880A CN 106333880 A CN106333880 A CN 106333880A CN 201610917268 A CN201610917268 A CN 201610917268A CN 106333880 A CN106333880 A CN 106333880A
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water
weight
skin
gauze
layers
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CN106333880B (en
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孙淑萍
陈滢俐
王露
王玲玲
金鑫
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Wannan Medical College
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Cosmetics (AREA)

Abstract

The invention provides a toner with a dilute emulsion substrate and a preparation method thereof. The toner comprises coix seed extracting solution, witch hazel extracting solution, licorice extracting solution, yacon extracting solution, okra squeezing liquid, aloe oil, rose hip oil, wheat-germ oil, sodium alginate, cation guar gum, 1% sodium hyaluronate solution, polyethylene glycol 400, 1,2-propylene glycol, methylparaben, self-emulsified compound emulsifier AC-402, essence, citric acid, 75% ethanol and distilled water. Compared with the prior art, the toner with the dilute emulsion substrate is light milk white, appropriate in viscosity, suitable in denseness, good in stability, fragrant in smell and fresh and cool in texture and can maintain skin moisture, reduce wrinkle, improve roughness, whiten the skin, make the skin tender and make the skin always soft, tender and white.

Description

A kind of cosmetic water of thin emulsion matrix and preparation method thereof
Technical field
The invention belongs to cosmetic field is and in particular to a kind of cosmetic water of thin emulsion matrix and preparation method thereof.
Background technology
People in the modern life experiencing intensive work for a long time, are exposed to the contour radiation of computer cell phone and ultraviolet Irradiating environment so that originally increasing becoming apparent from of day by day dim skin aging with the age, forming little microgroove, wrinkle.Wrinkle It is a kind of distinctive markss of skin aging, aging skin is insupportable for the people that each is liked to be beautiful, so skin is anti- Wrinkle whitening is most important for the people that each is liked to be beautiful.
And the generation of wrinkle sums up and has four aspect reasons: natural aging, centrifugal force, photoaging and photic damage, face The excessive contraction of portion's histrionic muscless.Wherein the most key factor is natural aging and two kinds of forms of photoaging, the former refer mainly to The growth at age, the irresistible factor existing in body, as heredity, gravity, endocrine and immunologic function etc. cause Aging;The latter, mainly due to the effect of ultraviolet, has increased the process of naturally-aged.Skin day by day become reveal lax, thinning, contain The water yield declines, it appears is dried, has squama, tarnish;Elasticity and consolidation also decline therewith;Wrinkle is formed, and gradually increases, Deepen.Additionally, the sensitivity of skin increases, pigment also increases.Skin aging interior under showing as skin cell proliferation ability Fall, epidermal renewal speed slows down, skin reconstruction reduced capability, and skin collagen synthesis slows down, and skin immunization power declines, Magnifying chromoscopy Uneven etc..
With the increasingly increase of social development, adjoint people's material life, skin care item industry is to do bigger and bigger, supplies female Property selection also get more and more, but even have not if not choosing in the skin care item of oneself skin suitable or these products The chemical substance of safety, can cause even more serious skin problem, and people are in the appearance begging safely and effectively skin-protection product.
Natural plant kind skin care item become the main trend of domestic and international skin care item research and development at present, and " Chinese herbal medicine " is then The best raw material of feature skin care item, if being added from suitable Chinese herbal medicine, can improve skin problem, making whitening skin tender Sliding, as the skin of baby, cunning is tender.It is avoided that the impact using chemical substance again.So developed new with natural plant extracts Skin care item will be the new road of having a bright future.
Content of the invention
It is an object of the invention to provide a kind of cosmetic water of thin emulsion matrix and preparation method thereof, containing Chinese medicine extraction Thing, can effectively pin the moisture in skin, can reduce wrinkle, so that skin is more added water and run through white, assume the thoroughly white U.S. of talent for swimming Beautiful.
The cosmetic water of a kind of thin emulsion matrix that the present invention provides, the raw material containing following weight portion:
Described Radix Glycyrrhizae extract is prepared by the following method:
Weigh Radix Glycyrrhizae coarse powder appropriate, soak 0.25-0.75h, be heated to 90-100 DEG C, decoct and extract 3 times, add for the 1st time sweet The water of careless 12-15 times of weight, extracts 0.5-2h, the water that the 2nd time adds 10-12 times of weight, extracts 0.5-1.5h, adds 6-8 times the 3rd time The water of weight, extracts 0.5-1.5h, every time the filtration of four layers of gauze, merging filtrate, the 10- of the volume concentration of filtrate to Radix Glycyrrhizae weight 12 times of g/ml, filter, and filtrate water-bath is heated to 80 DEG C, add 1-5% activated carbon and 0.5-3% Pulvis Talci, heat while stirring, Persistent period 30-60min, sucking filtration while hot, take filtrate to obtain final product.
Described Semen Coiciss extracting solution is prepared by the following method:
Weigh Semen Coiciss appropriate, rinsed with 1-2 times amount tap water, flushing liquor is outwelled, plus the water of 12-16 times of weight of Semen Coiciss Decoct and extract 1-1.5h, four layers of filtered through gauze;Filtering residue adds the water extraction 0.5-1.5h of 10-12 times of weight of Semen Coiciss, four layers of yarn again Cloth filters;Filtering residue adds the water extraction 0.5-1.5h of 8-10 times of weight of Semen Coiciss, four layers of filtered through gauze again, and filtering residue discards, and merges three Secondary filtrate, is concentrated into 8-12 times of g/ml of Semen Coiciss weight, sucking filtration while hot, takes filtrate to obtain final product.
Described hazel extract is prepared by the following method:
Weigh Radix Hamamelidis Molliss appropriate, plus water boiling and extraction 0.5-1.5h of 14-18 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze; Filtering residue adds the water extraction 0.5-1.5h of 12-14 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze again;Filtering residue adds 10-12 times of Radix Hamamelidis Molliss again The water extraction 0.5-1.5h of weight, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, is concentrated into the 6-9 of Radix Hamamelidis Molliss weight Times g/ml, filters, and filtrate water-bath is heated to 80 DEG C, adds 1-5% activated carbon and 0.5-3% Pulvis Talci, heats while stirring, hold Continuous time 30-60min, sucking filtration while hot, take filtrate to obtain final product.
Described yacon juicing is prepared by the following method:
Weigh the yacon of constant weight, clean and be cut into bulk, plus the distilled water of 3-5 times of weight of yacon, use juice extractor After squeezing, with four layers of filtered through gauze, take filtrate standby.
Described Abelmoschus esculentus juicing is prepared by the following method:
Weigh the fresh Abelmoschus esculentus of constant weight, after being rinsed with clear water, be cut into bulk, plus 3-5 times of weight distillation of Abelmoschus esculentus Water, after being squeezed with juice extractor, with four layers of filtered through gauze, takes filtrate standby.
Described essence is Fructus Citri Limoniae essence, Bulbus Lilii essence, osmanthus flower fragrance, rose essence, Fructus Cucumidis sativi essence, flavoring pineapple essence or water Honey peach essence any one.
The preparation method of the cosmetic water of a kind of thin emulsion matrix that the present invention provides, comprises the following steps:
A) 0.01-0.05 part sodium alginate is added to naturally swelling in 10-30 part distilled water, wait swelling formed completely brilliant The transparent sodium alginate gel liquid of jade-like stone, stand-by;
B) 0.01-0.03 part cation guar gum is added to naturally swelling in 10-30 part distilled water, waits swelling complete shape Become the cation guar gum coagulant liquid of crystal clear, stand-by;
C) measure 1-3 part 75% ethanol dissolving 0.003-0.009 part Methyl p-hydroxybenzoate as antiseptic solution, stand-by;
D) weigh Rosehips oil 0.5-1 part, Semen Tritici aestivi germ oil 0.5-1 part, aloe 0.5-1 part respectively, three is stirred Mix homogeneously, adds self emulsifying mixed emulsifier ac-4021-2.5 part, heating in water bath in 70-80 DEG C, stirs in heating Mix and make its mix homogeneously, obtain the oil phase of o/w type emulsion;
E) measure 10-30 part distilled water to be placed in 70-80 DEG C of water-bath, heating obtains the aqueous phase of o/w type emulsion;
Etc. f), when oil phase, aqueous phase reach mutually synthermal, above-mentioned aqueous phase is slowly added in oil phase in thread shape, Bian Jia Hot edge same side at the uniform velocity stir, and after about 15-30min, emulsifying completes, that is, obtain the thin emulsion matrix of o/w type;
G) after emulsion matrix stirring is cooled to room temperature, then PEG400 1-3 part, 1,2-PD 1- are added to it 3 parts, 1% sodium hyaluronate solution 0.5-2 part, sodium alginate gel, cation guar gum coagulant liquid, hazel extract 1-3 Part, Semen Coiciss extracting solution 1-3 part, Radix Glycyrrhizae extract 1-3 part, Abelmoschus esculentus juicing 1-3 part, yacon juicing 1-3 part, anti-corrosion Agent solution, adding 0.01-0.25 part citric acid to adjust ph value is 6.5-7.2, adds 0.1-0.25 part essence, mix and blend is equal Even, obtain final product the cosmetic water of thin emulsion matrix.
Various composition in the present invention is as follows:
Semen Coiciss have functions that diuretic, spleen invigorating, eliminating impediment, clearing away heat and discharging pus.Multivitamin and mineral are contained in Semen Coiciss Matter can keep human body skin gloss fine and smooth, reduces wrinkle.Contained vitamin b group energy enough anti-inflammatory, oil-control, moisturizing water lock. And, acne, freckle, senile plaque can be eliminated, improve the coarse etc. of skin.And it is for the wart being caused by virus infection Etc. there being certain therapeutical effect.In addition, it also has absorbability to ultraviolet, its extractive matter adds in skin care item or cosmetics also Can reach sun-proof and anti-ultraviolet effect.Because these effects, adhere to for a long time using on the face, skin naturally can be than original light Pool is fine and smooth a lot, becomes delicate smooth.
Radix Hamamelidis Molliss can adjust sebum secretion, has moisturizing and Milk Protein.Lymph blood circulation can be promoted, specially overcome Cracking, sunburn, acne are had improvement by morning eye bladder and black eye.The regeneration capacity at skin night can effectively be helped.Remove Eye pouch, loosen and relax and have very excellent effect for oily skin or the skin of allergy.Releive, restrain, antibacterial Effect, because have convergence oil-control, sterilization significant curative effect.Skin can be rapidly permeated into, adjust skin, balance from inside to outside comprehensively Skin ph value and fat secretion, purify pore, repair impaired skin, effectively adjust the pore of diastole hence it is evident that restraining enlarged pores, Prevent blackhead, acne from producing, make skin quickly assume fine and smooth, smooth, tight.Radix Hamamelidis Molliss have deep layer cleaning and resist certainly By effect of base, skin can be made anti-ageing.General in skin care item and cosmetics, for antiinflammatory and the skin that relaxes irriate but not Xerosis cutiss can be caused, and have effect of healing of wound.
Yacon has good effect to small pox skin.Due to containing substantial amounts of volatile oil, alkaloid, flavone in yacon The nutritions such as class, phenols, saccharide, tannin.Can accelerate the metabolism of skin, reduce wrinkle, make skin keep gloss, rich Full, slow down aging, has good curative effect to facial freckle, chloasma hepaticum etc., has the effect of stronger whitening and softening skin simultaneously.
The Abelmoschus esculentus place more special with respect to other vegetables is the mucus that the inside of Abelmoschus esculentus is contained.This rare Emplastic (sugared polymer) in main component contain pectin, viscous glycoprotein, vitamin a and vitamin c.Vitamin c and Soluble fiber can be with facilitating digestion and beauty treatment, and both combination has necessarily gentle protective effect to skin.
Radix Glycyrrhizae is described as " plant whitening queen ", because containing protein and several amino acids, lipid, polysaccharide in Radix Glycyrrhizae Class, fruit acid, vitamin and trace element etc..The coordinative role of many kinds of substance nutritious moisture-keeping function to skin.Can eliminate black Speckle, prevent pachylosiies.In Radix Glycyrrhizae, contained flavones ingredient has obvious antioxidation, and it is mainly lived to tyrosine Property suppression and the suppression to dopa pigment tautomerase activity and indole5.6quinone polymerization obstruction, thus effectively Suppress melanic generation, so that skin is bleached.The oxidation resistance of Radix Glycyrrhizae with vitamin e relatively, can remove multiple freedom Base and suppression lipofuscin generate, and promote the several functions such as Antioxidative Defense System.There is slow down aging, mitigate Pigmented work With etc..Liquorice whitening effect is good, action temperature and, safe without toxic side effect, be widely used in various skin care item as whitening agent.
Semen Tritici aestivi germ oil is referred to as " vitamin of skin ".Wherein it is rich in vitamin e, b, protein, mineral, fresh coconut palm Seed oil, also multiple unsaturated fatty acid such as linolenic acid, linoleic acid.Can vitimin supplement e and have and improve pigment on skin Precipitation, xerodermatic effect, protect the skin from the interference of ultraviolet.Good anti-of it or a kind of natural and performance simultaneously Rotten agent.
It is rich in Rosehips oil and have γ-linoleic acid, unsaturated fatty acid, Palmic acid, citric acid, vitamin a, c, class recklessly Radix Raphani element etc..Rosehips oil is all effective to the skin injury cicatrix leading to because of acne, operation, burn, chickenpox, wound and otch.Molten Solution blackhead, pore refining, the red and swollen erythema of elimination.The strong cell regeneration of Rosehips oil and wound healing function contribute to being good for Health, the growth of normal skin, substitute scar tissue.It can not only reconfigure damaged skin texture, and can also improve The color of skin and elasticity.Rosehips oil can improve skin regeneration and updating ability by promoting the activity of epidermis cell, from And stop and reverse the classical symptom such as wrinkle, canthus wrinkle of skin aging generation and relax.With the disappearance of catabiosis, face Portion's skin will become consolidation and more smooth.Rosehips oil can be repaired and substitute the skin histology having been torn, and efficiently reduce The appearance of striae atrophicae.Adhere to using Rosehips oil for a long time, pigmentation speckle will gradually mitigate can also repair sun-damaged skin, light Change black speck freckle, recover tender flour hole.
Hyaluronate sodium also known as Sodium Hyaluronate, hyaluronic acid sodium, are a kind of acid mucopolysaccharide.Hyaluronic acid is from buphthalmos, chicken Extract in the special materials such as hat, the umbilical cord of people, recently also have and extract from some antibacterials such as actinomycetes.Hyaluronate sodium is in itself One of composition of human body skin, is distribution a kind of acid mucopolysaccharide the widest in human body, is present in the substrate of connective tissue, tool There is good moisture-keeping function.Contain substantial amounts of carboxyl and hydroxyl in hyaluronan molecule, form intramolecular in aqueous and divide Hydrogen bond between son, this makes it have powerful water retention, can be the nature having now been found that in conjunction with itself more than 400 times of water The best material of moisture retention in boundary, is referred to as preferable nature moisturizing factor.The 2% water-soluble liquid energy of pure hyaluronic acid is protected securely Hold 98% moisture.
Sodium alginate also known as sodium alginate, seaweed gel, Algin, alginate, are by the natural polysaccharide carbon extracting in Thallus Laminariae (Thallus Eckloniae) Hydrate.Sodium alginate has natural moisture preserving effect, is also a kind of thickening agent of good performance simultaneously.
Cation guar gum is in skin-protection product, it is possible to decrease chemical substance to the zest of skin and protects keratoprotein not Damaged.So that skin is smoothed, reduce the loss of natural lipid in skin, increase the pliability of skin.Simultaneously can be with anion, non- Ion and dual character ion combine, and are a kind of surfactants of better performances.
Experiments verify that, Semen Coiciss extracting solution, hazel extract, Radix Glycyrrhizae extract, yacon juicing, Abelmoschus esculentus squeeze Take liquid, Semen Tritici aestivi germ oil, Rosehips oil, aloe etc. whitening, speckle dispelling, crease-resistant, moisturizing, moisten, the aspect such as skin care has very well Synergy, it is soft that skin and muscles are fair.
Compared with prior art, the cosmetic water of present invention preparation is in light milky, and viscosity is suitable, denseness is suitable, steady Qualitative good, high safety fragrant odour, texture are salubrious, can keep skin moisture.Wrinkle can be reduced, improve coarse skin, U.S. Delicate skin, maintain skin softness bullet slide, make skin soft pale as baby skin.The addition of multiple natural Chinese medicines, one Aspect can avoid adding excessive chemical substance to the stimulation of skin and injury;On the other hand can effectively pin in skin Moisture, can reduce wrinkle, so that skin is more added water and run through white, assume the thoroughly white beauty of talent for swimming.Utilize thin emulsion matrix simultaneously Way, can preferably be absorbed by skin, have stronger whitening skin and preserving moisture effect.Simple and elegant fragrance, refreshing, more allow people fill Share the infinite enjoyment by skin protection.
Specific embodiment
With reference to embodiment, the present invention will be further described.
The Semen Tritici aestivi germ oil of the present invention, Rosehips oil, aloe etc. are commercially available;The concentration of ethanol is volumetric concentration.
Embodiment 1
A kind of cosmetic water of thin emulsion matrix, containing following raw material:
A kind of preparation method of the cosmetic water of thin emulsion matrix, comprises the following steps:
The preparation of 1.1 Radix Glycyrrhizae extract:
Weigh Radix Glycyrrhizae coarse powder 20g, soak 0.5h, be heated to 90 DEG C, decoct and extract 3 times, add 12 times of weight of Radix Glycyrrhizae the 1st time Water, extracts 1.5h, the water that the 2nd time adds 10 times of weight of Radix Glycyrrhizae, extracts 1h, the water that the 3rd time adds 6 times of weight of Radix Glycyrrhizae, extracts 1h, every time Four layers of gauze filtration, merging filtrate, the volume concentration of filtrate, to 12 times (g/ml) of Radix Glycyrrhizae weight, filters, filtrate heating in water bath To 80 DEG C, add filtrate weight 2.5% activated carbon and 1% Pulvis Talci, heat while stirring, persistent period 40min, takes out while hot Filter, takes filtrate to obtain final product.
The preparation of 1.2 Semen Coiciss extracting solution:
Weigh Semen Coiciss 25g, rinsed with the tap water of 1 times of weight, flushing liquor is outwelled, plus the decocting of 12 times of weight of Semen Coiciss Boil extraction 1.5h, four layers of filtered through gauze;Filtering residue adds the water extraction 1h of 10 times of weight of Semen Coiciss, four layers of filtered through gauze again;Filtering residue is again Plus the water extraction 1h of 8 times of weight of Semen Coiciss, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, is concentrated into Semen Coiciss weight 12 times (g/ml), filtration obtains final product.
The preparation of 1.3 hazel extracts:
Weigh Radix Hamamelidis Molliss 20g, plus water boiling and extraction 1.5h of 14 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze;Filtering residue adds again The water extraction 1h of 12 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze;Filtering residue adds the water extraction 1h of 10 times of weight of Radix Hamamelidis Molliss, four layers of yarn again Cloth filters, and filtering residue discards, and merges three filtrates, is concentrated into 9 times (g/ml) of Radix Hamamelidis Molliss weight, filters, and filtrate water-bath is heated to 80 DEG C, add filtrate weight 2.5% activated carbon and 1% Pulvis Talci, heat while stirring, persistent period 40min, sucking filtration while hot, Filtrate is taken to obtain final product.
The preparation of 1.4 yacon juicings
Weigh yacon 20g, clean and be cut into bulk, add the distilled water of 100ml.After being squeezed with juice extractor, with four layers of yarn Cloth filters, and takes filtrate standby.
The preparation of 1.5 Abelmoschus esculentus juicings
Weigh fresh Abelmoschus esculentus 20g, after being rinsed with clear water, be cut into bulk, add the distilled water of 100ml.Use juice extractor After squeezing, with four layers of filtered through gauze, take filtrate standby.
The cosmetic water preparation of 1.6 thin emulsion matrixes
A) 0.01g sodium alginate is added to naturally swelling in 10g distilled water, wait swelling completely formed crystal clear sea Sodium alginate gel liquid, stand-by;
B) 0.01g cation guar gum is added to naturally swelling in 15g distilled water, wait swelling completely formed crystal clear Cation guar gum coagulant liquid, stand-by;
C) measure 1g 75% ethanol dissolving 0.003g Methyl p-hydroxybenzoate as antiseptic solution, stand-by;
D) weigh Rosehips oil 0.5g, Semen Tritici aestivi germ oil 0.5g, aloe 0.5g respectively, three be uniformly mixed, Add self emulsifying mixed emulsifier ac-402 1.5g, heating in water bath in 70 DEG C, heat while stirring and so that it is mixed all Even, obtain the oil phase of o/w type emulsion;
E) measuring 10g distilled water is placed on heating in water-bath to obtain the aqueous phase of o/w type emulsion;
F), in 70 DEG C of water-baths, when waiting oil phase, aqueous phase to reach mutually synthermal, above-mentioned aqueous phase is in thread shape along walls of beaker It is slowly added in oil phase, side heating edge same side at the uniform velocity stir, and after about 15min, emulsifying completes, that is, obtain o/w type thin Emulsion matrix;
G) add PEG400 1g, 1,2- propylene glycol 1g, 1% transparent to it again after emulsion stirring is cooled to room temperature Matter acid sodium 1.5g, sodium alginate gel, cation guar gum coagulant liquid, hazel extract 1g, Semen Coiciss extracting solution 1g, Radix Glycyrrhizae Extracting solution 1g, Abelmoschus esculentus juicing 1g, yacon juicing 1g, antiseptic solution, adding 0.1g citric acid to adjust ph value is 7.2, Add 0.1g essence, mixing and stirring, obtain final product the cosmetic water of thin emulsion matrix.
Embodiment 2
A kind of cosmetic water of thin emulsion matrix, containing following raw material:
A kind of preparation method of the cosmetic water of thin emulsion matrix, comprises the following steps:
The preparation of 2.1 Radix Glycyrrhizae extract:
Weigh Radix Glycyrrhizae 25g appropriate, soak 0.5h, be heated to 100 DEG C, decoct and extract 3 times, the 1st time plus 13 times of weight of Radix Glycyrrhizae Water, extract 1.5h, the water of the 2nd time plus 11 times of weight of Radix Glycyrrhizae, extract 1h, the water of the 3rd time plus 7 times of weight of Radix Glycyrrhizae, extract 1h, often Secondary four layers of gauze filtration, merging filtrate, the volume concentration of filtrate, to 11 times (g/ml) of Radix Glycyrrhizae weight, filters, filtrate water-bath adds Heat, to 80 DEG C, adds filtrate weight 4% activated carbon and 2% Pulvis Talci, heats while stirring, and persistent period 50min takes out while hot Filter, takes filtrate to obtain final product.
The preparation of 2.2 Semen Coiciss extracting solution:
Weigh Semen Coiciss 30g, rinsed with the tap water of 1.5 times of weight, flushing liquor is outwelled, plus the water of 14 times of weight of Semen Coiciss Decoct and extract 1.5h, four layers of filtered through gauze;Filtering residue adds the water extraction 1h of 11 times of weight of Semen Coiciss, four layers of filtered through gauze again;Filtering residue Again plus 9 times of weight of Semen Coiciss water extraction 1h, four layers of filtered through gauze, filtering residue discards, merge three filtrates, be concentrated into Semen Coiciss weight 10 times (g/ml) of amount, filtration obtains final product.
The preparation of 2.3 hazel extracts:
Weigh Radix Hamamelidis Molliss 25g, plus water boiling and extraction 1.5h of 16 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze;Filtering residue adds again The water extraction 1h of 13 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze;Filtering residue adds the water extraction 1h of 11 times of weight of Radix Hamamelidis Molliss, four layers of yarn again Cloth filters, and filtering residue discards, and merges three filtrates, is concentrated into 8 times (g/ml) of Radix Hamamelidis Molliss weight, filters, and filtrate water-bath is heated to 80 DEG C, add 4% activated carbon and 2% Pulvis Talci, heat while stirring, persistent period 50min, sucking filtration while hot, take filtrate to obtain final product.
The preparation of 2.4 yacon juicings:
Weigh yacon 25g, clean and be cut into bulk, add the distilled water of 100ml, after being squeezed with juice extractor, with four layers of yarn Cloth filters, and takes filtrate standby.
The preparation of 2.5 Abelmoschus esculentus juicings:
Weigh necessarily fresh Abelmoschus esculentus 25g, after being rinsed with clear water, be cut into bulk, add the distilled water of 100ml, with squeezing After juice machine squeezes, with four layers of filtered through gauze, take filtrate standby.
The cosmetic water preparation of 2.6 thin emulsion matrixes
A) 0.03g sodium alginate is added to naturally swelling in 20g distilled water, wait swelling completely formed crystal clear sea Sodium alginate gel liquid, stand-by;
B) 0.02g cation guar gum is added to naturally swelling in 20g distilled water, wait swelling completely formed crystal clear Cation guar gum coagulant liquid, stand-by;
C) measure 3g 75% ethanol dissolving 0.009g Methyl p-hydroxybenzoate as antiseptic solution, stand-by;
D) weigh Rosehips oil 0.8g, Semen Tritici aestivi germ oil 0.8g, aloe 0.8g respectively, three be uniformly mixed, Add self emulsifying mixed emulsifier ac-402 2g, heating in water bath in 70 DEG C, heat while stirring and make its mix homogeneously, Obtain the oil phase of o/w type emulsion;
E) measuring 20g distilled water is placed on heating in water-bath to obtain the aqueous phase of o/w type emulsion;
F), in 70-80 DEG C of water-bath, when waiting oil phase, aqueous phase to reach mutually synthermal, above-mentioned aqueous phase is in thread shape along burning Wall of cup is slowly added in oil phase, and side heating edge same side at the uniform velocity stir, and after about 20min, emulsifying completes, that is, obtain o/w type Thin emulsion matrix;
G) add PEG400 2g, 1,2- propylene glycol 2g, 1% transparent to it again after emulsion stirring is cooled to room temperature Matter acid sodium 1g, sodium alginate gel, cation guar gum coagulant liquid, hazel extract 2g, Semen Coiciss extracting solution 2g, Radix Glycyrrhizae carry Take liquid 2g, Abelmoschus esculentus juicing 2g, yacon juicing 2g, antiseptic solution, adding 0.18g citric acid to adjust ph value is 6.8, then Add 0.18g essence, mixing and stirring, obtain final product the cosmetic water of thin emulsion matrix.
Embodiment 3
A kind of cosmetic water of thin emulsion matrix, containing following raw material:
A kind of preparation method of the cosmetic water of thin emulsion matrix, comprises the following steps:
The preparation of 3.1 Radix Glycyrrhizae extract:
Weigh Radix Glycyrrhizae 30g appropriate, soak 0.75h, be heated to 100 DEG C, decoct and extract 3 times, the 1st time plus 15 times of weight of Radix Glycyrrhizae Water, extract 2h, the water of the 2nd time plus 12 times of weight of Radix Glycyrrhizae, extract 1.5h, the water of the 3rd time plus 8 times of weight of Radix Glycyrrhizae, extract 1h, often Secondary four layers of gauze filtration, merging filtrate, the volume concentration of filtrate, to 10 times (g/ml) of Radix Glycyrrhizae weight, filters, filtrate water-bath adds Heat, to 80 DEG C, adds filtrate weight 5% activated carbon and 3% Pulvis Talci, heats while stirring, and persistent period 60min takes out while hot Filter, takes filtrate to obtain final product.
The preparation of 3.2 Semen Coiciss extracting solution:
Weigh Semen Coiciss 35g, rinsed with the tap water of 2 times of weight, flushing liquor is outwelled, plus the decocting of 16 times of weight of Semen Coiciss Boil extraction 1.5h, four layers of filtered through gauze;Filtering residue adds the water extraction 1h of 12 times of weight of Semen Coiciss, four layers of filtered through gauze again;Filtering residue is again Plus the water extraction 1h of 10 times of weight of Semen Coiciss, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, is concentrated into Semen Coiciss weight 8 times (g/ml) of amount, filtration obtains final product.
The preparation of 3.3 hazel extracts:
Weigh Radix Hamamelidis Molliss 30g, plus water boiling and extraction 1.5h of 18 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze;Filtering residue adds again The water extraction 1.5h of 14 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze;Filtering residue adds the water extraction 1.5h of 12 times of weight of Radix Hamamelidis Molliss again, and four Layer filtered through gauze, filtering residue discards, and merges three filtrates, is concentrated into 6 times (g/ml) of Radix Hamamelidis Molliss weight, filters, and filtrate water-bath adds Heat, to 80 DEG C, adds filtrate weight 5% activated carbon and 3% Pulvis Talci, heats while stirring, and persistent period 60min takes out while hot Filter, takes filtrate to obtain final product.
The preparation of 2.4 yacon juicings:
Weigh yacon 30g, clean and be cut into bulk, add 90ml distilled water, after being squeezed with juice extractor, with four layers of gauze mistake Filter, takes filtrate standby.
The preparation of 2.5 Abelmoschus esculentus juicings:
Weigh necessarily fresh Abelmoschus esculentus 30g, after being rinsed with clear water, be cut into bulk, add 90ml distilled water, use juice extractor After squeezing, with four layers of filtered through gauze, take filtrate standby.
The cosmetic water preparation of 2.6 thin emulsion matrixes
A) 0.05g sodium alginate is added to naturally swelling in 30g distilled water, wait swelling completely formed crystal clear sea Sodium alginate gel liquid, stand-by;
B) 0.03g cation guar gum is added to naturally swelling in 30g distilled water, wait swelling completely formed crystal clear Cation guar gum coagulant liquid, stand-by;
C) measure 3g75% ethanol dissolving 0.009g Methyl p-hydroxybenzoate as antiseptic solution, stand-by;
D) weigh Rosehips oil 1g, Semen Tritici aestivi germ oil 1g, aloe 1g respectively, three is uniformly mixed, adds Self emulsifying mixed emulsifier ac-402 2.5g, heating in water bath in 80 DEG C, heat while stirring and make its mix homogeneously, obtain The oil phase of o/w type emulsion;
E) measuring 30g distilled water is placed on heating in water-bath to obtain the aqueous phase of o/w type emulsion;
F), in 80 DEG C of water-baths, when waiting oil phase, aqueous phase to reach mutually synthermal, above-mentioned aqueous phase is in thread shape along walls of beaker It is slowly added in oil phase, side heating edge same side at the uniform velocity stir, and after about 30min, emulsifying completes, that is, obtain o/w type thin Emulsion matrix;
G) add PEG400 3g, 1,2- propylene glycol 3g, 1% transparent to it again after emulsion stirring is cooled to room temperature Matter acid sodium solution 2g, sodium alginate gel, cation guar gum coagulant liquid, hazel extract 3g, Semen Coiciss extracting solution 3g, sweet Careless extracting solution 3g, Abelmoschus esculentus juicing 3g, yacon juicing 3g, antiseptic solution, add 0.25g citric acid adjust ph value be 6.5, add 0.25g essence, mixing and stirring, obtain final product the cosmetic water of thin emulsion matrix.
Embodiment 4
The physical and chemical index of embodiment 1,2,3 is as follows:
1st, character
This product is that viscosity is suitable, good stability, and uniformity is good, and texture is salubrious, and in light milky, abnormal smells from the patient is pure and fresh simple and elegant Thin emulsion matrix solution.
2nd, ph value checks
This product is taken to record ph value for 6.5-7.2.
3rd, caloric test
Cosmetic water is packaged in transparence cosmetic bottle, observes no denaturalization phenomenon within one month in 4 DEG C of refrigerator cold-storages.In 55 DEG C calorstat in 24h, the phenomenon such as cosmetic water is no spoiled, rotten.
4th, room temperature places experiment
The made cosmetic water of embodiment 1,2,3 is placed in bottle for cosmetics, room temperature standing is investigated 6 months, no lamination, With after feel unchanged, abnormal smells from the patient is unchanged, no denaturalization phenomenon.
5th, irritation test
White mice back cuts off hair, and Example 1,2,3 skin smoothing appropriate amount of water is applied to cuts plucked position, and no painting position is not entered Row compares, and result does not have zest and anaphylaxiss.
Example 1,2,3 skin smoothing appropriate amount of water is applied in volunteer (16-65 year, 100 people) gesture and facial expression, observes after spending 30 minutes No rubescent, dermexanthesis, foaming phenomena.Compare water profit with rear sensation skin, soft, fine and smooth, there is the sensation that comparison is comfortable.
6th, the cosmetic water resultant effect of thin emulsion matrix is investigated
Following with effect feeling the cosmetic water to evaluate the thin emulsion matrix that embodiment 1,2,3 produces on probation. Using public-opinion poll point system, choose 90 25-55 year age bracket women as object on probation, be arbitrarily divided into three groups, point Do not put arm on the skin with the cosmetic water of embodiment 1,2,3 preparation.Daily using twice, use time two months.Every using effect is total It is divided into 5 points: five to be divided into best result, represent very well, very satisfied;4 are divided into preferably;3 are divided into and can accept;Less than 3 points is bad, Can not accept.It is below every average.Knot
Fruit is shown in Table:
In sum, the cosmetic water of the made thin emulsion matrix of the present invention have good whitening and softening skin, moisturizing, nourishing and The effect of anti-microgroove.

Claims (8)

1. a kind of cosmetic water of thin emulsion matrix it is characterised in that the cosmetic water of described thin emulsion matrix contain following The raw material of weight portion:
2. the cosmetic water of thin emulsion matrix according to claim 1 is it is characterised in that described Radix Glycyrrhizae extract passes through Prepared by following methods:
Weigh Radix Glycyrrhizae coarse powder appropriate, soak 0.25-0.75h, be heated to 90-100 DEG C, decoct and extract 3 times, add Radix Glycyrrhizae 12- the 1st time The water of 15 times of weight, extracts 0.5-2h, the water that the 2nd time adds 10-12 times of weight, extracts 0.5-1.5h, the 3rd time plus 6-8 times of weight Water, extract 0.5-1.5h, every time the filtration of four layers of gauze, merging filtrate, 10-12 times of the volume concentration of filtrate to Radix Glycyrrhizae weight G/ml, filters, and filtrate water-bath is heated to 80 DEG C, adds 1-5% activated carbon and 0.5-3% Pulvis Talci, heats while stirring, and continues Time 30-60min, sucking filtration while hot, take filtrate to obtain final product.
3. the cosmetic water of thin emulsion matrix according to claim 1 is it is characterised in that described Semen Coiciss extracting solution leads to Cross following methods to prepare:
Weigh Semen Coiciss appropriate, rinsed with 1-2 times amount tap water, flushing liquor is outwelled, plus the decocting of 12-16 times of weight of Semen Coiciss boils Extract 1-1.5h, four layers of filtered through gauze;Filtering residue adds the water extraction 0.5-1.5h of 10-12 times of weight of Semen Coiciss, four layers of gauze mistake again Filter;Filtering residue adds the water extraction 0.5-1.5h of 8-10 times of weight of Semen Coiciss, four layers of filtered through gauze again, and filtering residue discards, and merges three filters Liquid, is concentrated into 8-12 times of g/ml of Semen Coiciss weight, sucking filtration while hot, takes filtrate to obtain final product.
4. the cosmetic water of thin emulsion matrix according to claim 1 is it is characterised in that described hazel extract is led to Cross following methods to prepare:
Weigh Radix Hamamelidis Molliss appropriate, plus water boiling and extraction 0.5-1.5h of 14-18 times of weight of Radix Hamamelidis Molliss, four layers of filtered through gauze;Filtering residue Again plus 12-14 times of weight of Radix Hamamelidis Molliss water extraction 0.5-1.5h, four layers of filtered through gauze;Filtering residue adds 10-12 times of weight of Radix Hamamelidis Molliss again Water extraction 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, merge three filtrates, be concentrated into 6-9 times of g/ of Radix Hamamelidis Molliss weight Ml, filters, and filtrate water-bath is heated to 80 DEG C, adds 1-5% activated carbon and 0.5-3% Pulvis Talci, heats while stirring, when continuing Between 30-60min, sucking filtration while hot, take filtrate to obtain final product.
5. the cosmetic water of thin emulsion matrix according to claim 1 is it is characterised in that described yacon juicing leads to Cross following methods to prepare:
Weigh the yacon of constant weight, clean and be cut into bulk, plus the distilled water of 3-5 times of weight of yacon, squeezed with juice extractor Afterwards, with four layers of filtered through gauze, take filtrate standby.
6. the cosmetic water of thin emulsion matrix according to claim 1 is it is characterised in that described Abelmoschus esculentus juicing leads to Cross following methods to prepare:
Weigh the fresh Abelmoschus esculentus of constant weight, after being rinsed with clear water, be cut into bulk, plus 3-5 times of weight distilled water of Abelmoschus esculentus, use After juice extractor squeezes, with four layers of filtered through gauze, take filtrate standby.
7. the cosmetic water of thin emulsion matrix according to claim 1 is it is characterised in that described essence is NINGMENGXIANG Essence, Bulbus Lilii essence, osmanthus flower fragrance, rose essence, Fructus Cucumidis sativi essence, flavoring pineapple essence or peach flavor any one.
8. a kind of preparation method of the cosmetic water of thin emulsion matrix described in any one of claim 1-7 is it is characterised in that institute State preparation method to comprise the following steps:
A) 0.01-0.05 part sodium alginate is added to naturally swelling in 10-30 part distilled water, wait swelling formed completely sparkling and crystal-clear Bright sodium alginate gel liquid, stand-by;
B) 0.01-0.03 part cation guar gum is added to naturally swelling in 10-30 part distilled water, wait swelling formed completely brilliant The transparent cation guar gum coagulant liquid of jade-like stone, stand-by;
C) measure 1-3 part 75% ethanol dissolving 0.003-0.009 part methyl hydroxybenzoate as antiseptic solution, stand-by;
D) weigh Rosehips oil 0.5-1 part, Semen Tritici aestivi germ oil 0.5-1 part, aloe 0.5-1 part respectively, three is stirred mixing Uniformly, add self emulsifying mixed emulsifier ac-4020.5-2.5 part, heating in water bath in 70-80 DEG C, heat while stirring Make its mix homogeneously, obtain the oil phase of o/w type emulsion;
E) measure 10-30 part distilled water to be placed in 70-80 DEG C of water-bath, heating obtains the aqueous phase of o/w type emulsion;
Etc. f), when oil phase, aqueous phase reach mutually synthermal, above-mentioned aqueous phase is slowly added in oil phase in thread shape, in heating At the uniform velocity stir along same side, after about 15-30min, emulsifying completes, that is, obtain the thin emulsion matrix of o/w type;
G) after emulsion matrix stirring be cooled to room temperature after, then to its add PEG400 1-3 part, 1,2-PD 1-3 part, 1% sodium hyaluronate solution 0.5-2 part, sodium alginate gel liquid, cation guar gum coagulant liquid, hazel extract 1-3 part, Semen Coiciss extracting solution 1-3 part, Radix Glycyrrhizae extract 1-3 part, Abelmoschus esculentus juicing 1-3 part, yacon juicing 1-3 part, preservative Solution, adding 0.01-0.25 part citric acid to adjust ph value is 6.5-7.2, adds 0.1-0.25 part essence, mixing and stirring, Obtain final product the cosmetic water of thin emulsion matrix.
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CN107375132A (en) * 2017-07-24 2017-11-24 皖南医学院 Compact light scar of one kind repairs emulsion and preparation method thereof after the thin type palpus of anti-inflammatory
CN107823048A (en) * 2017-11-24 2018-03-23 储成玲 A kind of skin whitening, moisturizing toner and preparation method thereof
CN108338945A (en) * 2018-03-01 2018-07-31 玫研(上海)生物科技有限公司 A kind of high-quality sodium hyaluronate magma and preparation method thereof
CN118001204A (en) * 2024-04-09 2024-05-10 广州旭妆生物科技有限公司 Temperature-sensitive gel and preparation method thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375132A (en) * 2017-07-24 2017-11-24 皖南医学院 Compact light scar of one kind repairs emulsion and preparation method thereof after the thin type palpus of anti-inflammatory
CN107823048A (en) * 2017-11-24 2018-03-23 储成玲 A kind of skin whitening, moisturizing toner and preparation method thereof
CN108338945A (en) * 2018-03-01 2018-07-31 玫研(上海)生物科技有限公司 A kind of high-quality sodium hyaluronate magma and preparation method thereof
CN118001204A (en) * 2024-04-09 2024-05-10 广州旭妆生物科技有限公司 Temperature-sensitive gel and preparation method thereof

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