CN106287265A - A kind of plug-in is except formaldehyde environmental protection LED - Google Patents
A kind of plug-in is except formaldehyde environmental protection LED Download PDFInfo
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Abstract
A kind of plug-in is except formaldehyde environmental protection LED, it is characterized in that: include LED illumination assembly and heat carrier, described LED illumination assembly apparatus is in the accommodation space by heat carrier lampshade, described heat carrier is prepared from by silicon carbide material, inner surface all even spread at described heat carrier surfaces externally and internally and described metallic sheath have heat radiation coating, the present invention not only has preferable radiating effect, also discharge negative aeroion, there is certain effect removing the finishing pollution things such as formaldehyde, toluene, TVOC simultaneously.
Description
The application is the Application No. 2016105741339 submitted to July 20 2016 applying date, invention entitled " one
Kind of plug-in is except formaldehyde environmental protection LED " the divisional application of Chinese invention patent application.
Technical field
The present invention relates to technical field of lamp ornament, be specifically related to a kind of plug-in except formaldehyde environmental protection LED.
Background technology
Along with the development and progress of society, the environmental protection idea of people is increasingly stronger, thus the illumination dress of environmental protection
Put and can more be favored by people, day by day ripe LED technology due to its have efficiently, energy-saving and environmental protection, length in service life, merit
The advantages such as rate is low, LED illumination lamp the most gradually starts to replace traditional lighting.
LED electricity-saving lamp is actually a kind of compact, carries the LED of ballast, and lamp tube ends voltage is directly over
Plasma state turns on and sends the ultraviolet of 253.7nm, and ultraviolet evokes light-emitting phosphor, due to filament during fluorescent lamp operation
Temperature at about 1160K, more much lower than temperature 2200-2700K of electric filament lamp work, thus its life-span the most significantly prolong
Long, arrive more than 5000 hours, due to the electric ballast that its operation efficiency is higher, there is not electric current as electric filament lamp simultaneously
Heat effect, the energy conversion efficiency of fluorescent material is the highest, arrives more than every watt of 50 lumens, saves energy.
On the one hand, along with the continuous rising of Global Temperature, the population of mosquito and quantity all will be greatly improved, the most day by day threaten
The health of the mankind.Mosquito, in addition to directly stining thorn and sucking blood, harass sleep, more seriously propagates multiple disease.The mosquito of China passes disease
Having malaria, Filariasis, epidemic encephalitis type B and dengue fever (or dengue hemorrhagic fever) four class, mosquito passes more important virosis
Also have yellow fever and various equine encephalitis etc..
On the other hand, by negative aeroion Technology application in electricity-saving lamp product, the electricity-saving lamp after using is long-term in indoor
Release negative aeroion, especially negative oxygen ion.Owing to it is structurally similar to ultra-oxygen anion free radical, therefore there is phase
As biological activity, it is possible to make live biological cell electronegative, so that virus loses the attacking ability to cell;Meanwhile,
Negative oxygen ion can react with the finishing pollution thing such as formaldehyde, toluene, TVOC, product be nonpoisonous and tasteless carbon dioxide and
Water, the generation of non-secondary pollution, there is certain effect purified the air of a room, such as, in artificial air's anion environment,
In air, mycete, bacterial population can reduce by more than 90% after measured.After negative oxygen ion is inhaled into human body, can regulate neural emerging
Put forth energy state, improve the ventilatory of lung, improve blood circulation, enhance metabolism, strengthen immune system ability, make people's spirit shake
Putting forth energy, improve work efficiency etc., the numerous diseases such as hypertension, asthma, influenza, insomnia, arthritis are also had certain treatment to make by it
With, so people's anion is called " vitamin in air " " long-lived element ".
So far, make conventional lamp product have the Technology design of expelling mosquito and anion releasing health care the most simultaneously
Have and see.
Summary of the invention
The deficiency existed for prior art, the technical problem to be solved is to provide a kind of plug-in except formaldehyde
Environmental protection LED, not only has preferable radiating effect, it is also possible to expelling mosquito, anion releasing, fresh air, simultaneously abnormal smells from the patient
Fragrance, character is gentle, has certain anophelifuge and antibacterial health-care effect, enriches the utilitarian function of conventional lamp.
It is an object of the invention to be achieved through the following technical solutions:
A kind of plug-in is except formaldehyde environmental protection LED, it is characterised in that: include that lampshade, LED illumination assembly are mutually socketed with lampshade
Metallic sheath and heat carrier between lampshade and metallic sheath, described LED illumination assembly apparatus is by described heat carrier and lamp
Cover is coated with in the accommodation space formed, and the surface of described lampshade is provided with multiple louvre, and described metallic sheath has some heat radiations
Hole, described heat carrier has some louvres, and described heat carrier is prepared from by silicon carbide material, wherein, in described heat conduction
The inner surface of surface, inside and outside and described metallic sheath all even spread have heat radiation coating, and described heat radiation coating is by following component
It is prepared from according to parts by weight: hybrid resin 60-75 weight portion, sodium-based montmorillonite 3-4.5 weight portion, carboxylic styrene butadiene latex 4-
6.5 weight portions, silicones metlyl branching silicone oil 1.5-2 weight portion, Polyethylene Glycol 0.7-1.2 weight portion, pentane 0.7-1.8 weight
Amount part, nano silicon 1-2.5 weight portion, polyacrylonitrile-based carbon fibre 7-9 weight portion, Graphene 5-6.5 weight portion, gas phase
Silica 1-2 weight portion, fire retardant 5.5-7 weight portion, curing agent 4-6 weight portion, solvent 15-20 weight
Part, ceria 0.1-0.15 weight portion, active mineral matter powder 1.5-2 weight portion, essential oil of traditional Chinese medicine 1.5-2.5 weight portion;Wherein,
Described hybrid resin be the mass ratio of the mixture of phenolic resin and epoxy resin, phenolic resin and epoxy resin be 2:1-3:1;
The a length of 0.01mm of described polyacrylonitrile-based carbon fibre;Described fire retardant is APP, tripolycyanamide and expanded graphites
Mixture, the mass ratio 2:1.5:1.3 of described APP, tripolycyanamide and expanded graphites;Described solvent is two
Pyruvic alcohol and the mixture of butyl ester, the mass ratio of described DAA and butyl ester is 3:1-3:2;Described active mineral matter powder is
Germanite, fluorite, tourmaline, gahnite by weight the mixture of 2.5:3:3.5:1.7, wherein tourmaline be dravite and
Elbaite is by weight the mixture of 4:3, particle diameter≤15 μm of described active mineral matter powder, and described heat radiation coating is by as follows
Step is prepared from:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight
Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put
In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender
Go out, i.e. prepare mixture A, standby;
S2, by material Aloe 70-80 weight portion, fly expelling plum 20-25 weight portion, Pericarpium Citri Reticulatae 15-18 weight portion, lavandula angustifolia 15-20 weight
Amount part, Herba Anemones Hupehensis 3-5 weight portion, Rhizoma Acori Graminei 3-5 weight portion, Herba Menthae 1-3 weight portion, XIAONIE 1-3 weight portion, Radix Salviae Miltiorrhizae 3-4 weight
Amount part, Herba polygoni hydropiperis 3-4 weight portion, Radix Stemonae 5-8 weight portion decontamination, it is placed in vacuum still 2-3 hour of-20 DEG C together, the most again
Being placed in microwave dryer and carry out pretreatment, wherein drying time is 30-40 minute, and microwave power is 17kw;
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby
With;
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still
Crude oil is collected with triangular flask, standby;
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is
The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e.
Prepare volatile oil B, standby;
S6, by Fructus Schisandrae Chinensis 1-3 weight portion, Origanum majorana 1.5-2.5 weight portion, Herba Portulacae 3-4 weight portion, Herba Pogostemonis 3-4 weight portion,
Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Artemisia argyi Levl. et Van. var. argyi cv. Qiai 3-4 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, then add from
Sub-water soaking 5 hours, amount of water by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby;
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.13-0.2 weight portion and be dried place
Reason, i.e. prepares volatile oil C, standby;
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points
Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon
The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5;
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 70-80 DEG C, concentrates in blender
Stirring mixing 15 minutes, obtains premix material, standby;
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change
Property aromatic amine curing agent, at 70-80 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity
Agent 3-5 weight portion, diethyltoluamide 0.1-0.2, butyl butyrate 9-15 weight portion, Eucalyptus oil 10-13 weight portion, isopropyl myristate
1-2 weight portion, polyoxyethylenated alcohol sodium sulfate 10-15 weight portion and sodium benzoate 0.1-0.3 weight portion.
It should be noted that the experiment proved that, active mineral matter powder adds appropriate ceria (CeO2), utilize
The emittance of this rare earth element is high, the feature of half degradation period limit for length, and the anion that active mineral matter powder can be significantly increased produces
Rate, its principle is as follows: the Ce in ceria4+Ce is changed under photoenvironment3+, in conversion process, electron-hole
Recombination probability reduces, then in active mineral matter powder under the effect of the material electric field such as tourmaline, part electronics is passively with electric field side
To displacement, electron-hole recombination probability reduces, thus at tourmaline/CeO2Substantial amounts of electricity has been gathered on composite powder surface
The energy of solution air molecule, and then create the negative aeroion of high concentration, Ce simultaneously3+It is oxidized into again Ce4+, then repeat
Aforesaid conversion process;Meanwhile, through practice detection, be combined through the present invention active mineral matter powder of proportioning adds appropriate
Ceria component, higher more than 10 times than without the concentration of active mineral matter powder anion adding ceria, r ray with from
So environment is identical.
The present invention is based on motherland's traditional medicine, with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine with anti-
Reviewing card, give full play to each group of weight portion synergism, the effect brief introduction of the most each raw material is as follows.
Aloe: " Bencao Jingshu ": Aloe, cold can heat extraction, hardship can expel the heat-evil dampness, bitter can parasite killing, to bitter to cold, therefore be heat extraction
The key medicine of parasite killing.Its main hot blast is unhappy, steam between the breast side of body, improving eyesight, relieving palpitation, and children epilepsy cool breeze is treated five kinds of child malnutrition, killed three worm persons, heat
Then giving birth to wind, heat energy makes people unhappy, and between evanescence of heat then wind heat unhappiness and chest and diaphragm, steam is explained by oneself.
Fly expelling plum: Verenaceae Lantana, belongs to perennial plant, evergreen half climing property shrub, sprig four prismatic, long and under
Hang down and there is reverse sharp thorn, its branch and leaf and flower volatilize the abnormal smells from the patient that mosquitos and flies is sensitive, there is the strongest expulsion mosquitos and flies effect,
And to human body without any injury, have " anophelifuge seven becomes flower " good reputation.
Pericarpium Citri Reticulatae: be the dry mature skin of rutaceae orange and variety thereof, have appetizing of regulating the flow of vital energy, drying dampness to eliminate phlegm,
Control effect of the spleen-stomach disease.
Lavandula angustifolia: can remove ant, except roach, acaricide, the when of being placed under wardrobe, medicated pillow, not only can replace camphor ball, moreover it is possible to stay
The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool contained in lavandula angustifolia is lavandula angustifolia
Antibacterial main component, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses
Long.
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature,
Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, dissipating blood stasis of subsiding a swelling, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria
Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Rhizoma Acori Graminei: its flower, stem aromatic flavor, has the effect had one's ideas straightened out, eliminate the phlegm, dissipate wind, and epidemic disease of can dispelling Fructus Alpiniae Oxyphyllae, building body can
Make spice or mosquito dispersing.
Herba Menthae: for the dry aerial parts of labiate Herba Menthae, dispelling wind and heat pathogens, the clear profit head, sore-throat relieving rash, soothing the liver row
Gas.
XIAONIE: evergreen shrubs, high 1-2 rice.Old branch is cylindrical, lead, and sprout is faint yellow, tool rib groove and wart point;Stem thorn
Three bifurcateds, slotless, long 1.5-2 centimetre, homochromy with branch.Cure mainly: remove steam in trusted subordinate, kill parasites, control metrorrhagia.Release name tiller, mountain
Punica granatum L..Abnormal smells from the patient: hardship, Great Cold, nontoxic.
Radix Salviae Miltiorrhizae: nature and flavor are bitter, are slightly cold.GUIXIN, Liver Channel." the southern regions of the Yunnan Province book on Chinese herbal medicine " is recorded: reinforcing the heart sedate, calming heart and tranquilizing mind.Control forgetful seized with terror
Punching, palpitation with fear is insomnia, and has stasis-dispelling and pain-killing, promoting blood circulation to restore menstrual flow, the effect of the relieving restlessness that clears away heart-fire, and for menoxenia, amenorrhea dysmenorrhea, lump in the abdomen amasss
Poly-, chest and abdomen twinge, pyretic arthralgia pain, skin infection.
Herba polygoni hydropiperis: all have inhibitory action, current clinical medicine research to show in test tube to various dysentery bacteriums, Herba polygoni hydropiperis has
There are the effects such as antibacterial, antiviral, antiinflammatory, antioxidation.
The Radix Stemonae: can driving away mosquito, resisting pathogenic microbes effect, to beta hemolytic streptococcus, meningococcus, golden yellow
The multiple pathomycetes such as staphylococcus, Staphylococcus albus, Bacillus typhi, pneumobacillus, bacillus pestis, anthrax bacillus have necessarily
Inhibitory action, its infusion all has killing action to mosquitos and flies larva, head louse, clothing louse and Cimex bedbug etc..
Fructus Schisandrae Chinensis: for Magnoliacea plant, have antibacterial action, to anthrax bacillus, staphylococcus aureus, white grapes ball
Bacterium, Bacillus typhi, vibrio cholera etc. all have inhibitory action.
Origanum majorana: can improve that mood is depressed and addictive disease, especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel,
Blood pressure lowering, alleviate and burden, help to eliminate cardiopalmus, have the nerve of excellence to pacify and calm function.
Herba Portulacae: Portulacaceae annual herb plant.Plump succulence, without hair, high 10-30cm, be born in roadside, field and
The area without shade such as ruins, flower garden.All there is distribution domestic various places.This kind is medicine food dual purpose plant.Herb hyoscine, has clearing away heat-damp and promoting diuresis, solution
Poison detumescence, antiinflammatory, quench the thirst, diuresis.
Herba Pogostemonis: acrid in the mouth, slightly warm in nature.Effect: removing dampness for regulating stomach, the effect of administration of inducing sweat, solve, cure mainly dampness taste, breast gastral cavity is vexed swollen,
Appetite is the most fragrant, Nausea and vomiting;Summer, heat-damp in summer was sleepy, uncomfortable in chest did not relaxed, and affection of exogenous wind-cold. the diseases such as aversion to cold is uncomfortable in chest, and have and have relatively
Strong Fungistasis and antibacterial action.
The Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae): the another name river Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae), continuous poison, Radix Stellerae, chervil, vexed fresh idea, Re Jiaba, Herba Senecionis Dianthui, Radix scopoliae sinensis, perfume,
Medicine sieve foretells, raw pull, flourishing bavin headdress flower, monkey root, Gelsemium elegans Benth., in Chinese medicine with its root eliminate the phlegm, pain relieving, removing food stagnancy, parasite killing.
Artemisia argyi Levl. et Van. var. argyi cv. Qiai: have another name called: containing 17 kinds of known compounds, has and relievings asthma, antitussive, eliminates the phlegm and clear scorching effect, reasonable QI and blood, by cold
The effects such as wet, regulating menstruation is antiabortive, warming the meridian for stopping bleeding, clearing and antitussive expectorant.Cure mainly cold type of pain in menoxenia, abdomen, vaginal bleeding during pregnancy hematochezia, fetal movement not
The diseases such as peace, infertility.
It should be noted that be proven, after carrying out the Radix Salviae Miltiorrhizae of certain part by weight, Herba polygoni hydropiperis and the Radix Stemonae compounding, no
Only it is remarkably improved degerming antibacterial ability, also can produce a kind of delicate fragrance taste having no side effect, refreshing, have certain
Effect of refreshing oneself;, it is proven, by the Aloe of certain part by weight, fly expelling plum, lavandula angustifolia, Rhizoma Acori Graminei and Herba Anemones Hupehensis meanwhile
After carrying out compounding, the mosquito dispersing ability of said composition is made to be significantly improved;It addition, Pericarpium Citri Reticulatae, Herba Menthae, XIAONIE, Fructus Schisandrae Chinensis and beg
After the components such as Chinese mugwort carry out compatibility, substantially increase the antibacterial degerming ability of compositions, through practice detection, the compositions pair after compounding
Staphylococcus aureus, anthrax bacillus, hemophilus influenza, micrococcus catarrhalis, streptococcus pneumoniae, escherichia coli, group B streptococcus, diphtheria bar
Bacterium, Bacillus typhi, green pus liver bacterium, dysentery bacteriums etc. more than 40 are planted pathogenic bacteria and have certain suppression and killing action.
The effect of the present invention:
The present invention uses Chinese medicine to compound with active mineral matter, makes the present invention not only have preferable radiating effect, it is also possible to drive
Mosquito, anion releasing, fresh air, simultaneously fragrant odour, character is gentle, has an anophelifuge, antibacterial and effect of health care, simultaneously
There is certain effect removing the finishing pollution things such as formaldehyde, toluene, TVOC.
Accompanying drawing explanation
Fig. 1 is radiator structure perspective exploded view of the present invention.
Fig. 2 is overall schematic of the present invention.
Fig. 3 is the schematic cross-section in Fig. 2 along a-a line.
Detailed description of the invention
Embodiment 1:
Referring to shown in Fig. 1 to Fig. 3, a kind of plug-in is except formaldehyde environmental protection LED, including lampshade 1, LED illumination assembly 2 and lamp
The metallic sheath 4 of cover 1 mutually socket and the heat carrier 3 between lampshade 1 and metallic sheath 4, described LED illumination assembly 2 device exists
By in the be coated with accommodation space formed of described heat carrier 3 and lampshade 1, the surface of described lampshade 1 is provided with multiple louvre 10, institute
Stating metallic sheath 4 and have some louvres 40, described heat carrier 3 has some louvres 31, and described heat carrier 3 is by silicon carbide material
It is prepared from.
Preferably, the louvre 40 of described metallic sheath 4 run through described metallic sheath 4 housing, described heat carrier 3
Louvre 31 also extend through the housing of described heat carrier 3, and the heat radiation of the louvre 40 of described metallic sheath 4 and described heat carrier 3
Hole 31 is corresponding, and extraneous air can be coated with formation by this corresponding louvre 31,40 with heat carrier 3 and lampshade 1
Air in accommodation space swaps.
Inner surface all even spread at described heat carrier 3 surfaces externally and internally and described metallic sheath 4 have heat radiation coating 30,
Described heat radiation coating 30 is prepared from according to parts by weight by following component: hybrid resin 60 weight portion, sodium-based montmorillonite 4.5 weight
Amount part, carboxylic styrene butadiene latex 4 weight portion, silicones metlyl branching silicone oil 2 weight portion, Polyethylene Glycol 0.7 weight portion, pentane
1.8 weight portions, nano silicon 1 weight portion, polyacrylonitrile-based carbon fibre 9 weight portion, Graphene 5 weight portion, gas phase dioxy
SiClx 2 weight portion, fire retardant 5.5 weight portion, curing agent 6 weight portion, solvent 15 weight portion, ceria 0.1
Weight portion, active mineral matter powder 2 weight portion, essential oil of traditional Chinese medicine 1.5 weight portion;Wherein, described hybrid resin is phenolic resin and ring
The mass ratio of the mixture of epoxy resins, phenolic resin and epoxy resin is 3:1;Described polyacrylonitrile-based carbon fibre is a length of
0.01mm;Described fire retardant is the mixture of APP, tripolycyanamide and expanded graphites, described APP, trimerization
The mass ratio 2:1.5:1.3 of cyanamide and expanded graphites;Described solvent is the mixture of DAA and butyl ester, described two
The mass ratio of pyruvic alcohol and butyl ester is 3:1;Described active mineral matter powder be germanite, fluorite, tourmaline, gahnite by weight
The ratio mixture of 2.5:3:3.5:1.7, wherein tourmaline is dravite and the mixture of elbaite 4:3 by weight, institute
Stating particle diameter≤15 μm of active mineral matter powder, described heat radiation coating is made by the steps and forms:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight
Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put
In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender
Go out, i.e. prepare mixture A, standby;
S2, by material Aloe 70 weight portion, fly expelling plum 25 weight portion, Pericarpium Citri Reticulatae 15 weight portion, lavandula angustifolia 20 weight portion, Hubei anemone
Spend 3 weight portions, Rhizoma Acori Graminei 5 weight portion, Herba Menthae 1 weight portion, XIAONIE 3 weight portion, Radix Salviae Miltiorrhizae 3 weight portion, Herba polygoni hydropiperis 4 weight portion, the Radix Stemonae 5
Weight portion decontamination, is placed in the vacuum still 2 hours of-20 DEG C together, is placed in microwave dryer the most again and carries out pretreatment, Qi Zhonggan
The dry time is 30 minutes, and microwave power is 17kw;
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby
With;
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still
Crude oil is collected with triangular flask, standby;
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is
The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e.
Prepare volatile oil B, standby;
S6, by Fructus Schisandrae Chinensis 1 weight portion, Origanum majorana 2.5 weight portion, Herba Portulacae 3 weight portion, Herba Pogostemonis 4 weight portion, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3 weight
Part, Artemisia argyi Levl. et Van. var. argyi cv. Qiai 4 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, and then adding deionized water, to soak 5 little
Time, amount of water by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby;
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.13 weight portion and be dried process, i.e.
Prepare volatile oil C, standby;
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points
Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon
The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5;
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 70 DEG C, concentrates in blender and stirs
Mix mixing 15 minutes, obtain premix material, standby;
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change
Property aromatic amine curing agent, at 73 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity
Agent 3 weight portion, diethyltoluamide 0. 2 weight portion, butyl butyrate 9 weight portion, Eucalyptus oil 4 weight portion, isopropyl myristate 1 weight
Part, polyoxyethylenated alcohol sodium sulfate 15 weight portion and sodium benzoate 0.1 weight portion.
Embodiment 2:
A kind of plug-in is except formaldehyde environmental protection LED, the metallic sheath 4 being mutually socketed including lampshade 1, LED illumination assembly 1 and lampshade 1
And the heat carrier 3 between lampshade 1 and metallic sheath 4, the surface of described lampshade 1 is provided with multiple louvre 10, described metallic sheath 4
Having some louvres 40, described heat carrier 3 is prepared from by silicon carbide material, uniform at described heat carrier 3 surfaces externally and internally
Being coated with heat radiation coating 30, wherein, described heat radiation coating is prepared from according to parts by weight by following component: hybrid resin 75 weight
Amount part, sodium-based montmorillonite 3 weight portion, carboxylic styrene butadiene latex 6.5 weight portion, silicones metlyl branching silicone oil 1.5 weight portion, poly-second
Glycol 1.2 weight portion, pentane 0.7 weight portion, nano silicon 2.5 weight portion, polyacrylonitrile-based carbon fibre 8 weight portion,
Graphene 6 weight portion, aerosil 1.5 weight portion, fire retardant 6 weight portion, curing agent 5 weight portion, molten
Agent 17 weight portion, ceria 0.15 weight portion, active mineral matter powder 1.7 weight portion, essential oil of traditional Chinese medicine 2 weight portion;Wherein, described
Hybrid resin be the mass ratio of the mixture of phenolic resin and epoxy resin, phenolic resin and epoxy resin be 3:1;Described poly-third
Alkene itrile group carbon fiber length is 0.01mm;Described fire retardant is the mixture of APP, tripolycyanamide and expanded graphites,
The mass ratio 2:1.5:1.3 of described APP, tripolycyanamide and expanded graphites;Described solvent is DAA and fourth
The mixture of ester, the mass ratio of described DAA and butyl ester is 3:2;Described active mineral matter powder is germanite, fluorite, electrically
Stone, gahnite by weight the mixture of 2.5:3:3.5:1.7, wherein tourmaline be dravite and elbaite by weight
The ratio mixture of 4:3, particle diameter≤15 μm of described active mineral matter powder, described heat radiation coating is made by the steps and forms:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight
Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put
In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender
Go out, i.e. prepare mixture A, standby;
S2, by material Aloe 80 weight portion, fly expelling plum 20 weight portion, Pericarpium Citri Reticulatae 18 weight portion, lavandula angustifolia 15 weight portion, Hubei anemone
Spend 5 weight portions, Rhizoma Acori Graminei 3 weight portion, Herba Menthae 3 weight portion, XIAONIE 1 weight portion, Radix Salviae Miltiorrhizae 4 weight portion, Herba polygoni hydropiperis 3 weight portion, the Radix Stemonae 8
Weight portion decontamination, is placed in the vacuum still 3 hours of-20 DEG C together, is placed in microwave dryer the most again and carries out pretreatment, Qi Zhonggan
The dry time is 40 minutes, and microwave power is 17kw;
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby
With;
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still
Crude oil is collected with triangular flask, standby;
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is
The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e.
Prepare volatile oil B, standby;
S6, by Fructus Schisandrae Chinensis 3 weight portion, Origanum majorana 1.5 weight portion, Herba Portulacae 4 weight portion, Herba Pogostemonis 3 weight portion, the Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 4 weight
Part, Artemisia argyi Levl. et Van. var. argyi cv. Qiai 3 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, and then adding deionized water, to soak 5 little
Time, amount of water by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby;
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.18 weight portion and be dried process, i.e.
Prepare volatile oil C, standby;
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points
Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon
The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5;
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 75 DEG C, concentrates in blender and stirs
Mix mixing 15 minutes, obtain premix material, standby;
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change
Property aromatic amine curing agent, at 80 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
In a preferred embodiment, essential oil of traditional Chinese medicine in step s 8 also includes the component of following weight portion: surface activity
Agent 5 weight portion, diethyltoluamide 0.1 weight portion, butyl butyrate 15 weight portion, Eucalyptus oil 7 weight portion, isopropyl myristate 2 weight
Part, polyoxyethylenated alcohol sodium sulfate 10 weight portion and sodium benzoate 0.3 weight portion.
Remaining is with embodiment 1.
In a preferred embodiment, described lampshade 1 is prepared from according to parts by weight by following component:
Resin 50 weight portion;Glass fibre 13 weight portion;Fire retardant 6 weight portion;Graphene 3 weight portion;Modified aromatic amine solidifies
Agent 3 weight portion;Fluorescent material 0.2 weight portion, good solid 754 light trigger 3 weight portions of vapour Ba Yan;Polyetheramine catalyst 0.6 weight portion;
Active mineral matter powder 2 weight portion;Essential oil of traditional Chinese medicine 2.5 weight portion;Wherein, described resin is epoxy soybean oil acrylate and bis-phenol
The mixture of A type E51 epoxy resin, the mass ratio of described epoxy soybean oil acrylate and bisphenol A-type E51 epoxy resin is 2:
1, described fire retardant is the mixture of APP, tripolycyanamide and expanded graphites, described APP, tripolycyanamide with
And the mass ratio 2:1.5:1.3 of expanded graphites, described fluorescent material is Ce and YAG fluorescent powder mixture, described fluorescent material
Particle diameter≤15 μm, described active mineral matter powder is that germanite, fluorite, tourmaline, gahnite are by weight 2.5:3:3.7:2
Mixture, wherein tourmaline is dravite and the mixture of elbaite 5:3 by weight, the grain of described active mineral matter powder
Footpath≤15 μm, described lampshade shell is made by the steps and forms:
S1, the resin by required parts by weight, fire retardant, Graphene, fluorescent material, vapour Ba Yan are good to be consolidated 754 light triggers and gathers
Ether amines catalyst is placed in blender, mixes well in the stirring of 75 DEG C of next part high speeds, and mixing time is 15-30 minute, to be mixed all
Take out from blender after even, i.e. prepare resin compound, standby;
S2, by Pu, material mountain race 60 weight portion, Bulbus Lycoridis Radiatae stem 10 weight portion, floral leaf 15 weight portion of walking to and for, shaven head grass roots leaf 6 weight
Amount part, Firmiana platanifolia (Linn. f.) Marsili bark 5 weight portion, sheep Cortex Jujubae 3.5 weight portion, Flos lupuli (Flos Humuli Lupuli) 3 weight portion, Herba Violae dissectae 2 weight portion, Radix et Rhizoma Dysosmatis 2.5
Weight portion, Fructus Hordei Germinatus 2 weight portion, the Radix Angelicae Dahuricae 1 weight portion, Herba Lysimachiae foenum-graeci 1.5 weight portion and Flos Caryophylli 1.5 weight portion, decontamination, together
Being placed in the vacuum still 2.5 hours of-20 DEG C, be placed in microwave dryer the most again and carry out pretreatment, wherein drying time is 35 minutes,
Microwave power is 17kw;
S3, step S2 is processed after material put into together in super micron mill and be crushed to 80 mesh, prepare crude drug powder, standby
With;
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 31MPa, extraction temperature 40 DEG C, carbon dioxide flow is 1100L/h, and dynamic extraction 2.5 hours directly goes out at separating still
Mouth triangular flask collects crude oil, then prepared crude oil is placed in 5 DEG C of environment freezing 65 minutes, then the crude oil after freezing is put
It is centrifuged 30 minutes in the High speed refrigerated centrifuge that rotating speed is 18000r/min, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation
3.5 hours, i.e. prepare essential oil of traditional Chinese medicine, standby;
The resin compound that S5, essential oil of traditional Chinese medicine step S4 prepared and step S1 prepare, at 75 DEG C, concentrates in blender
Stirring mixing 35 minutes, obtains compound, then this compound is put into ball mill, adds active mineral matter powder, modified aromatic
Amine hardener and glass fibre, carry out concentrating at 85 DEG C and grind 3 hours, filter decontamination, i.e. prepare premix material;
S6, the premix material of step S5 is put into twin-screw extrusion equipment, wherein, the rotating speed of twin-screw extrusion equipment is 200 turns/
Point, extrusion temperature is 200 ° of C, extrusion, cooling, and pelletizing i.e. obtains composite;
S7, the composite that step S6 is prepared through injection machine heating, extruding, molding, cool down, repair, obtain lampshade 1.
The test index of Example 1 and Example 2 of the present invention is as follows:
(1) abnormal smells from the patient inspection: sense organ, nonirritant abnormal flavour.
(2) repelling effect test.
Contrast test is carried out according to the repelling effect of ordinary lamp and lantern of the prior art with above-described embodiment 1 and embodiment 2,
Test data ask for an interview table 1.
Conclusion: Example 1 and Example 2 of the present invention all can play preferable mosquito-repelling function, with ordinary lamp and lantern on market
Comparing, the present invention has certain repelling effect.
(3) anionic textiles.
Use anion test instrument, be primarily directed to timber, Ore, ceramic material, negative ion powder are made to relevant
The anion quantity that commodity (such as anion medicated clothing, necklace, woollen blanket) etc. are discharged makes measurement.
Test result is shown in Table 2.
Conclusion: the embodiment of the present invention 1, embodiment 2 can be with sustained release negative aeroions, with ordinary lamps of the prior art
Tool compares, and the present invention has obviously advantage.
Claims (1)
1. a plug-in is except formaldehyde environmental protection LED, it is characterised in that: include lampshade (1), LED illumination assembly (2) and lampshade
(1) metallic sheath (4) being mutually socketed and the heat carrier (3) between lampshade (1) and metallic sheath (4), described LED illumination assembly
(2) device is being coated with in the accommodation space formed by described heat carrier (3) and lampshade (1), and the surface of described lampshade (1) is provided with
Multiple louvres (10), described metallic sheath (4) has some louvres (40), and described heat carrier (3) has some louvres
(31), described heat carrier (3) is prepared from by silicon carbide material, wherein, at described heat carrier (3) surfaces externally and internally and described
Inner surface all even spread of metallic sheath (4) have heat radiation coating (30), described heat radiation coating by following component according to weight portion
Number is prepared from: hybrid resin 60-75 weight portion, sodium-based montmorillonite 3-4.5 weight portion, carboxylic styrene butadiene latex 4-6.5 weight portion,
Silicones metlyl branching silicone oil 1.5-2 weight portion, Polyethylene Glycol 0.7-1.2 weight portion, pentane 0.7-1.8 weight portion, nanometer
Silica 1-2.5 weight portion, polyacrylonitrile-based carbon fibre 7-9 weight portion, Graphene 5-6.5 weight portion, aerosil
1-2 weight portion, fire retardant 5.5-7 weight portion, curing agent 4-6 weight portion, solvent 15-20 weight portion, titanium dioxide
Cerium 0.1-0.15 weight portion, active mineral matter powder 1.5-2 weight portion, essential oil of traditional Chinese medicine 1.5-2.5 weight portion;Wherein, described mixing
Resin be the mass ratio of the mixture of phenolic resin and epoxy resin, phenolic resin and epoxy resin be 2:1-3:1;Described poly-third
Alkene itrile group carbon fiber length is 0.01mm;Described fire retardant is the mixture of APP, tripolycyanamide and expanded graphites,
The mass ratio 2:1.5:1.3 of described APP, tripolycyanamide and expanded graphites;Described solvent is DAA and fourth
The mixture of ester, the mass ratio of described DAA and butyl ester is 3:1-3:2;Described active mineral matter powder be germanite, fluorite,
Tourmaline, gahnite by weight the mixture of 2.5:3:3.5:1.7, wherein tourmaline be dravite and elbaite by
The mixture of weight ratio 4:3, particle diameter≤15 μm of described active mineral matter powder, described heat radiation coating be made by the steps and
Become:
S1, weigh hybrid resin, sodium-based montmorillonite, carboxylic styrene butadiene latex, silicones metlyl branching silicone oil, poly-second two by weight
Alcohol, pentane, nano silicon, polyacrylonitrile-based carbon fibre, Graphene, aerosil, fire retardant and solvent are put
In blender, mixing well in the stirring of 80 DEG C of next part high speeds, mixing time is 40 minutes, to be mixed uniformly after take from blender
Go out, i.e. prepare mixture A, standby;
S2, by material Aloe 70-80 weight portion, fly expelling plum 20-25 weight portion, Pericarpium Citri Reticulatae 15-18 weight portion, lavandula angustifolia 15-20 weight
Amount part, Herba Anemones Hupehensis 3-5 weight portion, Rhizoma Acori Graminei 3-5 weight portion, Herba Menthae 1-3 weight portion, XIAONIE 1-3 weight portion, Radix Salviae Miltiorrhizae 3-4 weight
Amount part, Herba polygoni hydropiperis 3-4 weight portion, Radix Stemonae 5-8 weight portion decontamination, it is placed in vacuum still 2-3 hour of-20 DEG C together, the most again
Being placed in microwave dryer and carry out pretreatment, wherein drying time is 30-40 minute, and microwave power is 17kw;
S3, step S2 is processed after material put into together in super micron mill and be crushed to 60 mesh, prepare crude drug powder, standby
With;
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 28MPa, extraction temperature 45 DEG C, carbon dioxide flow is 1100L/h, dynamic extraction 2 hours, directly exports at separating still
Crude oil is collected with triangular flask, standby;
S5, the crude oil prepared in step S4 is placed in 5 DEG C of environment freezing 70 minutes, then the crude oil after freezing is placed in rotating speed is
The High speed refrigerated centrifuge of 17000r/min is centrifuged 25 minutes, goes the removal of impurity to be placed on 85 DEG C of vacuum tank evacuation 3 hours, i.e.
Prepare volatile oil B, standby;
S6, by Fructus Schisandrae Chinensis 1-3 weight portion, Origanum majorana 1.5-2.5 weight portion, Herba Portulacae 3-4 weight portion, Herba Pogostemonis 3-4 weight portion,
Radix Euphorbiae Fischerianae (Radix Euphorbiae Ebracteolatae) 3-4 weight portion, Artemisia argyi Levl. et Van. var. argyi cv. Qiai 3-4 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 30 mesh, then add from
Sub-water soaking 5 hours, amount of water by 7 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby;
S7, Traditional Chinese drug mixture step S6 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2.5:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate 0.13-0.2 weight portion and be dried place
Reason, i.e. prepares volatile oil C, standby;
S8, made to step S5 and S7 volatile oil B and volatile oil C are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, Fructus Citri Limoniae quintessence oil and grapefruit essential oil, be sufficiently stirred for 45 minutes, stands 30 points
Clock, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Tritici aestivi quintessence oil, Geranium Essential, Herba Saussureae Involueratae quintessence oil, lemon
The mass ratio of lemon quintessence oil and grapefruit essential oil is 2:0.5:0.5:0.6:0.4:0.5;Wherein, described essential oil of traditional Chinese medicine also includes following
The component of weight portion: surfactant 3-5 weight portion, diethyltoluamide 0.1-0.2 weight portion, butyl butyrate 9-15 weight portion, Eucalyptus
Oil 4-7 weight portion, isopropyl myristate 1-2 weight portion, polyoxyethylenated alcohol sodium sulfate 10-15 weight portion and benzoic acid
Sodium 0.1-0.3 weight portion;
The mixture A that S9, essential oil of traditional Chinese medicine step S8 prepared prepare with step S1, at 70-80 DEG C, concentrates in blender
Stirring mixing 15 minutes, obtains premix material, standby;
S10, premix material step S9 prepared put into ball mill, then add ceria, active mineral matter powder and change
Property aromatic amine curing agent, at 70-80 DEG C, concentrate grind 4.5 hours, filter decontamination, i.e. obtain heat radiation coating.
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CN201610574133.9A Pending CN106189652A (en) | 2016-05-23 | 2016-07-20 | A kind of plug-in is except formaldehyde environmental protection LED |
CN201710130354.1A Pending CN107420765A (en) | 2016-05-23 | 2017-03-07 | A kind of plug-in LED |
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Application publication date: 20170104 |