CN106282780A - A kind of 630MPa level high-strength hot-rolled steel bar steel and preparation method thereof - Google Patents
A kind of 630MPa level high-strength hot-rolled steel bar steel and preparation method thereof Download PDFInfo
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- CN106282780A CN106282780A CN201610867389.9A CN201610867389A CN106282780A CN 106282780 A CN106282780 A CN 106282780A CN 201610867389 A CN201610867389 A CN 201610867389A CN 106282780 A CN106282780 A CN 106282780A
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/06—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires
- C21D8/08—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires for concrete reinforcement
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/001—Ferrous alloys, e.g. steel alloys containing N
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/12—Ferrous alloys, e.g. steel alloys containing tungsten, tantalum, molybdenum, vanadium, or niobium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
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- Crystallography & Structural Chemistry (AREA)
- Heat Treatment Of Steel (AREA)
Abstract
The present invention relates to a kind of 630MPa level high-strength hot-rolled steel bar steel and preparation method thereof, it contains by weight percentage: 0.22~0.28%C, 0.40~0.80%Si, 1.40~1.60%Mn ,≤0.035%P ,≤0.035%S, 0.02~0.04%Nb, 0.05~0.07%V, 0.20~0.40%Cr, 0.008~0.012%N, remaining is Fe and inevitable impurity element.Processing method comprises the steps: to use said ratio and component, smelts in converter, electric arc furnace or other smelting furnace;The outer ladle argon-blown refine of stove;140 or 150 continuous small-billet castings;The rolling of thermal mechanical rolling technique is used on bar mill;Cooling.Under the conditions of existing technological equipment, using the microalloying mode of V, Nb combination, use cooling controlling and rolling controlling process, the 630MPa level reinforcement property of production is stable, and comprehensive mechanical property is preferable.
Description
Technical field
The present invention relates to Concrete-used Hot-rolling Ribbed Reinforcing Bar technology, be specifically related to a kind of 630MPa level high-strength hot-rolled steel bar and use
Steel and preparation method thereof.
Background technology
Compared with common hot-rolled reinforced bar, high-strength hot-rolled steel bar has that intensity is high, combination property (processing performance, welding performance,
Ductility, anti-seismic performance etc.) excellent, energy-conserving and environment-protective, length in service life, safety advantages of higher.Developed countries is eliminated already
The reinforcing bar of low intensity level, English, moral, Australia, Fa Deng state widely used 500MPa level reinforcing bar, 600MPa level reinforcing bar there has also been in a large number should
With.Compared with developed countries, China's reinforced steel bar strength is the most relatively low.Recently as national a series of high tensile reinforcement popularization and application political affairs
Plan is put into effect, and high tensile reinforcement usage percentage rises year by year, China's 400MPa level above high tensile reinforcement consumption in 2015 oneself reach to build
Build more than the 80% of steel axis force.
The research of engineering design shows, on the premise of not reducing xoncrete structure overall performance, can use little one-level
The 630MPa level reinforcing bar of specification replaces 400MPa level reinforcing bar, as φ 25mm HRB630 can be used to replace φ 28mm HRB400, from
And realize the purpose of construction(al)steel minimizing.Being computed, steel using amount can reduce more than 40%.It addition, 630MPa level high tensile reinforcement
Problems such as " fat beams and columns " can also be solved in building structure, increase building usable floor area, make structure design more reasonable, favorably
In scientific development and the adjustment of steel and iron industry product structure of promotion engineering construction, sustainable to eliminating the backward production facilities, implementing
Development strategy is significant.
The patent documentation of Chinese Patent Application No. 201310444163.4 discloses " a kind of 630MPa level high-strength hot-rolled steel bar
And production technology ".This spiral comprises following component: 0.38~0.43%C, 0.8~1.1%Cr, 0.75~1.0%
Mn, 0.15~0.25%Mo, 0.15~0.3%Si ,≤0.035%S, P ,≤0.035%N, surplus is Fe.This spiral
Manufacture method " uses heating furnace to be heated to 1000-1200 DEG C, then reinforcing bar fast speed is cooled to through online first refrigerating work procedure
610-630 DEG C, then in quenching unit with water or quenching liquid carry out for time 12-14 second quenching, be then passed through tempering heating
Stove is heated to 550-660 DEG C of tempering, then is cooled to room temperature by the second cooling technique ".It has the disadvantage that (1) Cr content
More than more than 0.8%, it is unfavorable for extending index, easy brittle failure;(2) C, N content are too high, are unfavorable for welding performance;(3) domestic reinforcing bar
Production line does not has online back-fire arrangement mostly, and production technology is difficulty with.
The patent documentation of Chinese Patent Application No. 201410137203.5 discloses " a kind of 600MPa level carefully brilliant high-strength anti-shock
Method for producing steel bar ", reinforcing bar composition is: 0.24%~0.28%C, 0.62%~0.80%Si ,≤1.30%Mn ,≤
0.035%P, S, 0.10%~0.20%V, 0.20%~0.50%Cr, remaining is ferrum.The heating of heated stove and bar mill roll
System, then wear water management cooling after rolling.It has the disadvantage that (1) intensity rank is 600MPa, non-630MPa;(2) use
Cr improves intensity index, but is unfavorable for Ductility Index, and reinforcing bar easily occurs without yield phenomenon and brittle failure occurs;(3) thin crystalline substance is used
Invigoration effect improves intensity, but the welding performance of fine-grained steel muscle needs verification experimental verification.
The patent documentation of Chinese Patent Application No. 201210252106.1 discloses " a kind of 600MPa level antidetonation spiral
And manufacture method ".Reinforcing bar basis: 0.21~0.26%C, 0.61~0.80%Si, 1.30~1.60%Mn, 0.15~
0.21%V;Optional member: 0.001~0.050%Nb, 0.001~0.050%Ti, 0.10~0.50%Cr, 0.0001~
0.0050%B, any one or the two or more combination in 0.001~0.010%Mo;Remaining is Fe and the most miscellaneous
Matter.The manufacture method of this spiral uses " converter or electric furnace smelting+continuous small-billet casting tandem rolling+cold bed cooling " short route work
Skill.It has the disadvantage that (1) intensity rank is 600MPa, non-630MPa;(2) V content is more than more than 0.15%, and mainly
Being that the solution strengthening utilizing vanadium improves intensity, the precipitation strength not making full use of vanadium improves intensity, and vanadium improves the work of intensity
With being that precipitation strength is more than solution strengthening;(3) the alloying element price such as vanadium, molybdenum, chromium is higher, is unfavorable for that competitiveness improves in enterprise.
Summary of the invention
For above prior art problem, it is an object of the invention to provide a kind of 630MPa level high-strength hot-rolled steel bar steel
And preparation method thereof, make intensity rank reach 630MPa on the premise of not reducing Ductility Index, meet high-rise, large span and build
The needs of building structure.Concrete technical scheme is as follows:
A kind of 630MPa level high-strength hot-rolled steel bar steel, it contains by weight percentage: 0.22~0.28%C, 0.40~
0.80%Si, 1.40~1.60%Mn ,≤0.035%P ,≤0.035%S, 0.02~0.04%Nb, 0.05~0.07%V,
0.20~0.40%Cr, 0.008~0.012%N, remaining is Fe and inevitable impurity element.
The processing method of a kind of 630MPa level high-strength hot-rolled steel bar steel, comprises the steps:
(1) use said ratio and component, smelt in converter, electric arc furnace or other smelting furnace;
(2) the outer ladle argon-blown refine of stove;
(3) 140 or 150 continuous small-billet castings;
(4) rolling of thermal mechanical rolling technique is used on bar mill;
(5) cooling.
Further, step (5) including: (5-1) cold bed natural cooling;(5-2) stacking natural cooling.
Further, step (4) including: (4-1) heating and temperature control is at 1000~1200 DEG C;Soaking temperature controls
1050~1150 DEG C;(4-2) start rolling temperature controls at 950~1100 DEG C;(4-3) enter finishing mill temperature to control 850~950
℃;(4-4) upper cold bed red temperature controls at 780~900 DEG C.
Further, in step (4-4), rolling specs is the biggest, it is desirable to upper cold bed red temperature the lowest.
Further, step (1) uses 60 tons of converter smeltings.
Further, strong argon blowing time >=4min, soft argon blowing time >=4min. in step (2)
Further, 150 billet continuous castings in step (3), step (4) rolls on continuous rod mill.
Compared with currently available technology, the present invention is designed by the composition of resource-conserving, and combines thermal mechanical rolling technique
(TMCP) high-strength, the 630MPa level hot rolled ribbed bars of high-ductility is produced, its yield strength >=630MPa, tensile strength >=
790MPa, elongation after fracture >=14%, percentage of total elongation >=9% under maximum, force, strong flexor ratio >=1.25, bend ratio≤1.30.Wanted
The key technology solved is to provide alloy component range and the thermal mechanical rolling technique of a kind of 630MPa level high tensile reinforcement, to meet city
The field demand to 630MPa level high-strength hot-rolled steel bar.Specifically: under the conditions of existing technological equipment, the micro-of V, Nb combination is used
Alloying mode, uses cooling controlling and rolling controlling process, and the 630MPa level reinforcement property of production is stable, and comprehensive mechanical property is preferable, and it is bent
Take intensity >=630MPa, tensile strength >=790MPa, elongation after fracture >=14%, percentage of total elongation >=9% under maximum, force, strong flexor ratio
>=1.25, bend ratio≤1.30.Microalloy element consumption is suitable with HRB500 reinforcing bar, can reduce than using pair rolling technique
The microalloy element consumption of more than 50%, remarkable benefit.
Accompanying drawing explanation
Fig. 1 is 630MPa level reinforcing bar tissue (lot number K15-63 × 100)
Fig. 2 is 630MPa level reinforcing bar tissue (lot number K15-64 × 100)
Detailed description of the invention
Describing the present invention below according to accompanying drawing, it is that the one in numerous embodiments of the present invention is the most real
Execute example.
In a preferred embodiment, the chemical composition proportioning (by weight hundred of 630MPa level high tensile reinforcement steel of the present invention
Proportion by subtraction) be: 0.22~0.28%C, 0.40~0.80%Si, 1.40~1.60%Mn ,≤0.035%P ,≤0.035%S,
0.02~0.04Nb, 0.05~0.07%V, 0.20~0.40%Cr, 0.008~0.012%N, remaining is that Fe is with inevitable
Impurity element.
The present invention need to be smelted in converter, electric arc furnace or other smelting furnace by mentioned component requirement, stove outer ladle argon-blown essence
Refining, 140 or 150 continuous small-billet castings, bar mill uses the rolling of thermal mechanical rolling technique, cold bed natural cooling, stacking is the coldest
But.
TMCP thermal mechanical rolling technology controlling and process point is as follows:
(1) heating and temperature control is at 1000~1200 DEG C;Soaking temperature;Control at 1050~1150 DEG C;
(2) start rolling temperature controls at 950~1100 DEG C;
(3) enter finishing mill temperature to control at 850~950 DEG C;
(4) upper cold bed red temperature controls at 780~900 DEG C, and rolling specs is the biggest, it is desirable to upper cold bed red temperature
The lowest.
The present invention uses the method that V, Nb combine, and utilizes V Yu C, N disperse educt invigoration effect in steel, utilizes Nb to show
Write and postpone austenite recrystallization, the effect of crystal grain thinning, and the compound invigoration effect ratio of V, Nb to be used alone one of which more aobvious
Write.The strict content limiting N element, controls between 4~6 by V/N ratio, plays the precipitation strength effect of V to greatest extent, and not
The defects such as strand rimhole can be too much caused because of N element.N content scope the most of the present invention requires model at GB 1499.2-2007
In enclosing, also it is easily able in big commercial production.Steel adds Cr, the quenching degree of steel, refinement pearlitic structrure, secondary can be improved
Induration is obvious, can further improve reinforced steel bar strength, also improves the anti-corrosion capability of reinforcing bar simultaneously.
The present invention uses 140 or 150 small billet, is used by current most domestic steel mill, is not required to little to 140 or 150
Square billet is transformed into the square billet of more than 165.
Thermal mechanical rolling technique of the present invention, heating and temperature control is at 1000~1200 DEG C;Soaking temperature control 1050~
1150 DEG C, start rolling temperature controls at 950~1100 DEG C, enters finishing mill temperature and controls at 850~950 DEG C.
Arranging rapid water device for cooling after finishing mill, by stopping cooling after being as cold as phase change zone after rolling soon, rebar surface obtains
The thinnest ferrite+pearlitic structrure.Compared with rolling rear Water cooling production technology, thermal mechanical rolling is also adopted by wearing water
Cooling technique.The purpose rolling rear Water cooling mainly realizes transformation of austenite to martensite at low temperatures, forms martensite
Top layer, then obtain tempered structure by the heart portion self tempering to surface;And thermal mechanical rolling is to make rolled piece fast by rapid cooling after finish rolling
Speed, by austenite phase field, keeps rolled piece austenite hardening state, terminates to the dynamic phase trasnsition point of ferrite transformation at austenite
Cooling, growing up of suppression ferrite crystal grain, top layer is fine grain ferrite+pearlitic structrure, and grain size reaches 9 grades.
The present invention uses composition design and the PMCP thermal mechanical rolling technique of resource-conserving, comprehensively utilizes microalloy element
The multiple strengthening means such as solid solution, precipitation strength and refined crystalline strengthening, it is achieved on the premise of keeping material plasticity, produce comprehensive
The 630MPa level reinforcing bar of function admirable.
In a further advantageous embodiment, the melting chemical composition of the present invention is shown in Table 1, uses 60 tons of converter smeltings, ladles
Ar blowing refining, strong argon blowing time >=4min, soft argon blowing time >=4min, 150 billet continuous castings, roll on continuous rod mill
System, its TMCP thermal mechanical rolling technological parameter is shown in Table 2, and mechanical property is shown in Table 3.
The melting chemical composition of table 1 embodiment of the present invention
The TMCP technological parameter of table 2 embodiment of the present invention
The mechanical property of table 3 embodiment of the present invention
Wherein: ReL is yield strength;Rm is tensile strength;Strong flexor ratio (Rmo/ReLo), RmoFor surveying tensile strength,
ReLoFor actual measurement yield strength;Bend than (ReLo/ 630), 630 is HRB630 reinforcement yielding strength characteristics value, units MPa;A is
Elongation after fracture;Agt is elongation percentage under maximum, force.
Above in conjunction with accompanying drawing, the present invention is exemplarily described, it is clear that the present invention implements not by aforesaid way
Restriction, as long as have employed method design and the various improvement that carry out of technical scheme of the present invention, or the most improved direct application
In other occasion, all within protection scope of the present invention.
Claims (8)
1. a 630MPa level high-strength hot-rolled steel bar steel, it is characterised in that it contains by weight percentage: 0.22~0.28%
C, 0.40~0.80%Si, 1.40~1.60%Mn ,≤0.035%P ,≤0.035%S, 0.02~0.04%Nb, 0.05~
0.07%V, 0.20~0.40%Cr, 0.008~0.012%N, remaining is Fe and inevitable impurity element.
2. the processing method of a 630MPa level high-strength hot-rolled steel bar steel, it is characterised in that comprise the steps:
(1) use proportioning and component described in claim 1, smelt in converter, electric arc furnace or other smelting furnace;
(2) the outer ladle argon-blown refine of stove;
(3) 140 or 150 continuous small-billet castings;
(4) rolling of thermal mechanical rolling technique is used on bar mill;
(5) cooling.
3. the processing method of 630MPa level high-strength hot-rolled steel bar steel as claimed in claim 2, it is characterised in that step (5)
Including:
(5-1) cold bed natural cooling;
(5-2) stacking natural cooling.
4. the processing method of the 630MPa level high-strength hot-rolled steel bar steel as described in claim 2 and 3, it is characterised in that step
(4) including:
(4-1) heating and temperature control is at 1000~1200 DEG C;Soaking temperature controls at 1050~1150 DEG C;
(4-2) start rolling temperature controls at 950~1100 DEG C;
(4-3) enter finishing mill temperature to control at 850~950 DEG C;
(4-4) upper cold bed red temperature controls at 780~900 DEG C.
5. the processing method of 630MPa level high-strength hot-rolled steel bar steel as claimed in claim 4, it is characterised in that step (4-
4), in, rolling specs is the biggest, it is desirable to upper cold bed red temperature the lowest.
6. the processing method of the 630MPa level high-strength hot-rolled steel bar steel as described in claim 2-5, it is characterised in that step
(1) 60 tons of converter smeltings are used in.
7. the processing method of the 630MPa level high-strength hot-rolled steel bar steel as described in claim 2-6, it is characterised in that step
(2) strong argon blowing time >=4min, soft argon blowing time >=4min in.
8. the processing method of 630MPa level high-strength hot-rolled steel bar steel as claimed in claim 2-7, it is characterised in that step
(3) 150 billet continuous casting in, rolls in step (4) on continuous rod mill.
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Cited By (18)
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CN106756566A (en) * | 2017-01-17 | 2017-05-31 | 浙江富钢金属制品有限公司 | A kind of Aldecor transmission rod and its manufacture method |
CN107245649A (en) * | 2017-06-13 | 2017-10-13 | 马鞍山钢铁股份有限公司 | A kind of High-strength high-plasticity heavy duty goods train wheel-use steel material and its production method |
CN107723603A (en) * | 2017-11-29 | 2018-02-23 | 安徽工业大学 | Yield strength 500MPa levels corrosion-resistant steel bar and manufacture method |
CN107747048A (en) * | 2017-11-30 | 2018-03-02 | 攀钢集团攀枝花钢铁研究院有限公司 | Steel wire rod and its production method are built containing V, Nb, Ti, Cr microalloy |
CN107747045A (en) * | 2017-11-29 | 2018-03-02 | 安徽工业大学 | A kind of 400MPa levels environmental corrosion of resistance to Cl reinforcing bar and its manufacture method |
CN107747061A (en) * | 2017-09-14 | 2018-03-02 | 河钢股份有限公司 | A kind of 630MPa levels high-strength tenacity hot rolled ribbed bars and its production method |
CN109023123A (en) * | 2018-10-12 | 2018-12-18 | 石横特钢集团有限公司 | A kind of production method of 840MPa grades of hot rolling anchor pole reinforcing bar |
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CN110343962A (en) * | 2019-07-26 | 2019-10-18 | 马鞍山钢铁股份有限公司 | A kind of 700Mpa grades or more hot-rolled ribbed high tensile reinforcement steel and its production method |
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CN107723603A (en) * | 2017-11-29 | 2018-02-23 | 安徽工业大学 | Yield strength 500MPa levels corrosion-resistant steel bar and manufacture method |
CN107747045A (en) * | 2017-11-29 | 2018-03-02 | 安徽工业大学 | A kind of 400MPa levels environmental corrosion of resistance to Cl reinforcing bar and its manufacture method |
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