CN106278584A - The preparation method of a kind of compound fertilizer environment-friendly type anticaking agent and anticaking agent - Google Patents
The preparation method of a kind of compound fertilizer environment-friendly type anticaking agent and anticaking agent Download PDFInfo
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- CN106278584A CN106278584A CN201610643578.8A CN201610643578A CN106278584A CN 106278584 A CN106278584 A CN 106278584A CN 201610643578 A CN201610643578 A CN 201610643578A CN 106278584 A CN106278584 A CN 106278584A
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- anticaking agent
- preparation
- compound fertilizer
- environment
- friendly type
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/20—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for preventing the fertilisers being reduced to powder; Anti-dusting additives
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- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The present invention relates to preparation method and the anticaking agent of a kind of compound fertilizer environment-friendly type anticaking agent, the preparation method of compound fertilizer therein environment-friendly type anticaking agent includes: the surfactant of the paraffin of oils and fats, 10%～15%, 50%～60% and the fluffy powder of 5%～10% of 20%～30% are added in stirring pool by S1, by weight mark；S2, heating, stir；S3, agitation and filtration；S4, is transferred to cooling preservation in cooling tank.It has the fluffy powder of fluffing action by interpolation, in the actual operation of chemical fertilizer production, during the interpolation of this anticaking agent uses, it can be ensured that occur without dust, will not produce because dust sucks the harm healthy to staff, meet environmental requirement.
Description
Technical field
The present invention relates to fertilizer anti-caking agents preparing technical field, particularly relate to a kind of compound fertilizer environment-friendly type anticaking agent
Preparation method and anticaking agent.
Background technology
Compound fertilizer occupies increasingly consequence to integrate multiple nutritional components at fertilizer industry, but compound
Fertilizer is more easy to caking than single fertilizer during transport and storage, and its free mobility can be caused to fade away and make its quality become
Difference, for a long time, has a strong impact on the sale of producer and the use of user, and enterprise has to use various anticaking agent, to reach
The purpose of anti-caking.In order to prevent caking, the measure that can take has: use novel Granulation Equipments and drying process；Apply various
Anticaking agent, to reduce the water content of product, improves the intensity of product, uniformity, caking performance and laxity.
At present, the anticaking agent that market is developed, during adding use, easily produces a large amount of dust, to staff
Health cause certain harm, do not meet environmental requirement.
Summary of the invention
For the above-mentioned technical problem overcoming prior art to exist, the invention provides a kind of compound fertilizer environment-friendly type anticaking agent
Preparation method, it has the fluffy powder of fluffing action by interpolation, in the actual operation of chemical fertilizer production, this anti-caking
During the interpolation of agent uses, it can be ensured that occur without dust, will not produce because dust sucks the harm healthy to staff,
Meet environmental requirement.
The technical scheme is that the preparation side of a kind of compound fertilizer environment-friendly type anticaking agent
Method, it comprises the following steps:
S1, by weight mark by 20%～30% the surface activity of the paraffin of oils and fats, 10%～15%, 50%～60%
Agent and 5%～10% fluffy powder add in stirring pool；
S2, heating, stir；
S3, utilizes blender to stir and filters；
S4, is transferred to cooling preservation in cooling tank.
On the basis of technique scheme, the present invention can also do following improvement.
Further, the mixture after also including cooling after described step S4 condenses into the step of paste finished product.
Above-mentioned further scheme is used to provide the benefit that: the mixture after cooling to be condensed into paste finished product, it is simple to storage
Deposit and carry.
Further, described oils and fats includes the animal oil of 10 parts and the Vegetable oil lipoprotein of 16 parts.
Further, described surfactant includes the primary octadecylamine of 12 parts, the fatty acid of 20 parts, the stearic acid of 15 parts and 2
The magnesium stearate of part.
Further, the weight fraction of described fluffy powder is 8%.
Above-mentioned further scheme is used to provide the benefit that: to add the fluffy powder of 8%, it is ensured that the anticaking agent of preparation exists
Without dust during use, further avoid the impact on staff.
Further, the weight fraction of described paraffin is 12%.
Further, the heating-up temperature in described step S2 is 90～120 DEG C.
Above-mentioned further scheme is used to provide the benefit that: temperature to be heated in the range of 90～120 DEG C, it is simple to stirring
Each component in pond is sufficiently mixed uniformly.
Further, the stir speed (S.S.) in described step S3 is 65～75r/min.
Above-mentioned further scheme is used to provide the benefit that: by controlling stir speed (S.S.), it is simple to by the material of mix homogeneously
Fully filter.
Further, the chilling temperature in described step S4 is 60～70 DEG C.
Present invention also offers a kind of anticaking agent, it is by the compound fertilizer's environment-friendly type anticaking agent described in any of the above-described item
Prepared by preparation method.
Beneficial effects of the present invention: this anticaking agent has the fluffy powder of fluffing action by interpolation, in chemical fertilizer production
In actual operation, during the interpolation of this anticaking agent uses, it can be ensured that occur without dust, will not produce because dust is inhaled
Enter the harm healthy to staff, meet environmental requirement；Meanwhile, add the chemical fertilizer after anticaking agent after usage, easily drop
Solve, environment will not be produced and pollute, and less amount can be used i.e. to can reach preferable preventing blocking effect, through experimental verification,
The present invention provide anticaking agent consumption is compound fertilizer 0.3～1.2%, and the consumption of traditional anticaking agent be 1.5～
2.5%.
Accompanying drawing explanation
The flow chart of the preparation method of compound fertilizer's environment-friendly type anticaking agent that Fig. 1 provides for the embodiment of the present invention one.
Detailed description of the invention
Being described principle and the feature of the present invention below in conjunction with accompanying drawing, example is served only for explaining the present invention, and
Non-for limiting the scope of the present invention.It should be noted that in the case of not conflicting, in embodiments herein and embodiment
Feature can be mutually combined.
Embodiment one
As it is shown in figure 1, the preparation method of compound fertilizer's environment-friendly type anticaking agent of the present embodiment offer, it includes following step
Rapid:
S1, by weight mark by 20%～30% the surface activity of the paraffin of oils and fats, 10%～15%, 50%～60%
Agent and 5%～10% fluffy powder add in stirring pool；
S2, heating, stir；
S3, agitation and filtration；
S4, is transferred to cooling preservation in cooling tank.
Fluffy powder therein is made water repellent agent by fatty acid, fatty amine makees efflorescence-resisting agent, possibly together with antiblocking agent, anti-blushing agent,
Lubricants etc. become to be grouped into, the quality proportioning of wherein each component be respectively as follows: 5～9 parts of water repellent agents, 35～50 parts of efflorescence-resisting agents,
15～25 parts of anti-blushing agents, 16～20 parts of lubricants, antiblocking agents of 6～10 parts.
The preparation method of compound fertilizer's environment-friendly type anticaking agent that the present embodiment provides, it has fluffing action by addition
Fluffy powder, in the actual operation of chemical fertilizer production, during the interpolation of this anticaking agent uses, it can be ensured that go out without dust
Existing, will not produce because dust sucks the harm healthy to staff, meet environmental requirement.
Embodiment two
The preparation method of compound fertilizer's environment-friendly type anticaking agent that the present embodiment provides, it comprises the following steps:
S1, by weight mark by 20%～30% the surface activity of the paraffin of oils and fats, 10%～15%, 50%～60%
Agent and 5%～10% fluffy powder add in stirring pool；
S2, heating, stir；
S3, agitation and filtration；
S4, is transferred to cooling preservation in cooling tank.
Fluffy powder therein is made water repellent agent by fatty acid, fatty amine makees efflorescence-resisting agent, possibly together with antiblocking agent, anti-blushing agent,
Lubricants etc. become to be grouped into, the quality proportioning of wherein each component be respectively as follows: 5～9 parts of water repellent agents, 35～50 parts of efflorescence-resisting agents,
15～25 parts of anti-blushing agents, 16～20 parts of lubricants, antiblocking agents of 6～10 parts.
Mixture after the most also including cooling condenses into the step of paste finished product, by the mixing after cooling
Thing condenses into paste finished product, it is simple to stores and carries.Oils and fats therein includes the animal oil of 10 parts and the Vegetable oil lipoprotein of 16 parts,
Surfactant therein includes the primary octadecylamine of 12 parts, the fatty acid of 20 parts, the stearic acid of 15 parts and the magnesium stearate of 2 parts.
The weight fraction of fluffy powder therein is 8%, and the weight fraction of paraffin is 12%.
For ease of understanding the preparation method of compound fertilizer's environment-friendly type anticaking agent that the present embodiment provides, following specific descriptions its
Preparation process: first animal oil and Vegetable oil lipoprotein are imported in large-scale stirring pool, and add fluffy powder, paraffin, primary octadecylamine,
The auxiliary material such as fatty acid, stearic acid and magnesium stearate, and stirring of heating, heating-up temperature is 90～120 DEG C, to be mixed uniform after
Again by special equipment stirring and processing, filtrations such as pony mixers, stir speed (S.S.) therein can be 65～75r/min, to be filtered
By self priming pump, feed liquid being transferred to cooling preservation in cooling tank after completing, until being cooled to the temperature of 60～70 DEG C, then importing
Packing crates condenses into paste finished product, closes packaging, complete the preparation of compound fertilizer's environment-friendly type anticaking agent.
Embodiment three
Present embodiments providing a kind of anticaking agent, it is prevented by the compound fertilizer's environment-friendly type described in embodiment one or embodiment two
The preparation method of agglomeration agent is prepared.
The compound fertilizer's environment-friendly type anticaking agent prepared by said method with the addition of the fluffy powder with fluffing action, changing
In the fertile actual operation produced, during the interpolation of this anticaking agent uses, it can be ensured that occur without dust, will not produce
Because dust sucks the harm healthy to staff, meet environmental requirement；Meanwhile, the chemical fertilizer after anticaking agent is added in use
After, degradable, environment will not be produced and pollute, and less amount can be used i.e. to can reach preferable preventing blocking effect, Jing Guoshi
Checking, consumption is compound fertilizer the 0.3～1.2% of the anticaking agent that the present invention provides, and the consumption of traditional anticaking agent
It is 1.5～2.5%.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all spirit in the present invention and
Within principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (10)
1. the preparation method of compound fertilizer's environment-friendly type anticaking agent, it is characterised in that comprise the following steps:
S1, by weight mark by 20%～30% the paraffin of oils and fats, 10%～15%, 50%～60% surfactant and
The fluffy powder of 5%～10% adds in stirring pool；
S2, heating, stir；
S3, agitation and filtration；
S4, is transferred to cooling preservation in cooling tank.
The preparation method of compound fertilizer the most according to claim 2 environment-friendly type anticaking agent, it is characterised in that in described step
Mixture after also including cooling after S4 condenses into the step of paste finished product.
The preparation method of compound fertilizer the most according to claim 1 and 2 environment-friendly type anticaking agent, it is characterised in that described oil
Fat includes the animal oil of 10 parts and the Vegetable oil lipoprotein of 16 parts.
The preparation method of compound fertilizer the most according to claim 3 environment-friendly type anticaking agent, it is characterised in that live in described surface
Property agent includes the primary octadecylamine of 12 parts, the fatty acid of 20 parts, the stearic acid of 15 parts and the magnesium stearate of 2 parts.
The preparation method of compound fertilizer the most according to claim 1 and 2 environment-friendly type anticaking agent, it is characterised in that described pine
The weight fraction of powder is 8%.
The preparation method of compound fertilizer the most according to claim 5 environment-friendly type anticaking agent, it is characterised in that described paraffin
Weight fraction is 12%.
The preparation method of compound fertilizer the most according to claim 5 environment-friendly type anticaking agent, it is characterised in that described step S2
In heating-up temperature be 90～120 DEG C.
The preparation method of compound fertilizer the most according to claim 5 environment-friendly type anticaking agent, it is characterised in that described step S3
In stir speed (S.S.) be 65～75r/min.
The preparation method of compound fertilizer the most according to claim 5 environment-friendly type anticaking agent, it is characterised in that described step S4
In chilling temperature be 60～70 DEG C.
10. an anticaking agent, it is characterised in that described anticaking agent is by the compound fertilizer's environmental protection described in the claims 1 to 9
Prepared by the preparation method of type anticaking agent.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610643578.8A CN106278584A (en) | 2016-08-08 | 2016-08-08 | The preparation method of a kind of compound fertilizer environment-friendly type anticaking agent and anticaking agent |
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| CN201610643578.8A CN106278584A (en) | 2016-08-08 | 2016-08-08 | The preparation method of a kind of compound fertilizer environment-friendly type anticaking agent and anticaking agent |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107353134A (en) * | 2017-08-28 | 2017-11-17 | 北京尧之龙科技发展有限公司 | A kind of special anticaking agent of UHA |
| CN108794206A (en) * | 2018-08-22 | 2018-11-13 | 苏州丰倍生物科技有限公司 | A kind of micro-emulsion type Water soluble fertilizer anticaking agent and preparation method thereof |
| CN109111277A (en) * | 2017-06-23 | 2019-01-01 | 深圳市芭田生态工程股份有限公司 | Anti-compaction oil, preparation method and anti-compaction fertilizer |
| CN110903127A (en) * | 2019-11-19 | 2020-03-24 | 山东聊城鲁西硝基复肥有限公司 | Anti-caking agent, preparation method thereof, anti-caking compound fertilizer and preparation method thereof |
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| CN1342628A (en) * | 2001-10-26 | 2002-04-03 | 蔡剑斌 | Anti-blocking loosening agent for preparing loose composite fertilizer with long storage period |
| CN102050679A (en) * | 2011-01-14 | 2011-05-11 | 福建工程学院 | Straw powder-based anti-blocking agent of compound fertilizer |
| CN104119000A (en) * | 2014-08-15 | 2014-10-29 | 苏州丰倍生物科技有限公司 | Anti-caking agent for fertilizer, as well as production method and applications thereof |
| CN104211521A (en) * | 2014-09-12 | 2014-12-17 | 北京富瑞雪科技发展有限公司 | Black fertilizer multifunctional additive and preparation method and application thereof |
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2016
- 2016-08-08 CN CN201610643578.8A patent/CN106278584A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1342628A (en) * | 2001-10-26 | 2002-04-03 | 蔡剑斌 | Anti-blocking loosening agent for preparing loose composite fertilizer with long storage period |
| CN102050679A (en) * | 2011-01-14 | 2011-05-11 | 福建工程学院 | Straw powder-based anti-blocking agent of compound fertilizer |
| CN104119000A (en) * | 2014-08-15 | 2014-10-29 | 苏州丰倍生物科技有限公司 | Anti-caking agent for fertilizer, as well as production method and applications thereof |
| CN104211521A (en) * | 2014-09-12 | 2014-12-17 | 北京富瑞雪科技发展有限公司 | Black fertilizer multifunctional additive and preparation method and application thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109111277A (en) * | 2017-06-23 | 2019-01-01 | 深圳市芭田生态工程股份有限公司 | Anti-compaction oil, preparation method and anti-compaction fertilizer |
| CN107353134A (en) * | 2017-08-28 | 2017-11-17 | 北京尧之龙科技发展有限公司 | A kind of special anticaking agent of UHA |
| CN108794206A (en) * | 2018-08-22 | 2018-11-13 | 苏州丰倍生物科技有限公司 | A kind of micro-emulsion type Water soluble fertilizer anticaking agent and preparation method thereof |
| CN110903127A (en) * | 2019-11-19 | 2020-03-24 | 山东聊城鲁西硝基复肥有限公司 | Anti-caking agent, preparation method thereof, anti-caking compound fertilizer and preparation method thereof |
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Application publication date: 20170104 |