CN106272797A - A kind of high-strength abrasion-proof artware timber sofening treatment liquid and preparation method thereof - Google Patents
A kind of high-strength abrasion-proof artware timber sofening treatment liquid and preparation method thereof Download PDFInfo
- Publication number
- CN106272797A CN106272797A CN201610712815.1A CN201610712815A CN106272797A CN 106272797 A CN106272797 A CN 106272797A CN 201610712815 A CN201610712815 A CN 201610712815A CN 106272797 A CN106272797 A CN 106272797A
- Authority
- CN
- China
- Prior art keywords
- treatment liquid
- proof
- sofening treatment
- timber
- strength abrasion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/06—Softening or hardening of wood
Abstract
The invention discloses a kind of high-strength abrasion-proof artware timber sofening treatment liquid, it is to be prepared by the raw material of following weight parts: Disulfatozirconic acid. 12, hexagonal boron nitride 0.1 0.15, Polyethylene Glycol 5 10, glacial acetic acid 46, Alumen 0.5 1, the hydrogen peroxide 24 of mass fraction 20 30%, polyvinyl alcohol 12, polyoxylethylene abietate 0.3 0.5, ptfe emulsion 0.5 1, hydroxyethyl cellulose 0.3 0.5, ethyl hydroxybenzoate 0.01 0.015, water 50 60.The timber sofening treatment liquid of the present invention softens good processability, the intensity of timber, toughness are high, anti-wear performance is strong, it is difficult to bounce-back, do not affect subsequent treatment, and the finished appearance quality after drying and moulding is good, dimensional stability is high, be difficult to craze and transfiguration, be not susceptible to mould corruption, and applied widely, energy-conserving and environment-protective.
Description
Technical field
The present invention relates to chemical treatments technical field, particularly relate to a kind of high-strength abrasion-proof artware timber sofening treatment
Liquid and preparation method thereof.
Background technology
In the course of processing of Wood craft, the timber as raw material is carried out softening is very important step.?
Under usual conditions, timber is a kind of material lacking plasticity, by timber is carried out sofening treatment, it can be made to show temporarily
Plasticity, now timber can be curved, compress, the plastic working such as embossment, then be dried under deformation, recover it
Original rigidity and intensity, it is achieved the permanent plastic deformation of timber, the artware intensity making making is high, and morphological appearance is ornamental
Can be good.Common softening method has decocting in water, high-temperature high-pressure steam to process and Chemical treatment.Process through these methods
Wood dimensional stability is poor, and processing characteristics and serviceability also can be adversely affected.Patent CN201510993437 is with ice vinegar
Acid, Polyethylene Glycol and anion surfactant are that main component prepares timber softening agent, make the timber after process have well
Strength and stiffness, although this softening agent improves processing characteristics and the stable molding of timber after sofening treatment to a certain extent
Property, but timber after softening processing is prone to craze and transfiguration, the most mould perishable defect is not significantly improved, it is therefore desirable to enter
One step is perfect.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of high-strength abrasion-proof artware timber is soft
Change treatment fluid and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of high-strength abrasion-proof artware timber sofening treatment liquid, it is to be prepared by the raw material of following weight parts:
Disulfatozirconic acid. 1-2, hexagonal boron nitride 0.1-0.15, Polyethylene Glycol 5-10, glacial acetic acid 4-6, Alumen 0.5-1, mass fraction 20-
The hydrogen peroxide 2-4 of 30%, polyvinyl alcohol 1-2, polyoxylethylene abietate 0.3-0.5, ptfe emulsion 0.5-1, ethoxy
Cellulose 0.3-0.5, ethyl hydroxybenzoate 0.01-0.015, water 50-60.
The preparation method of a kind of high-strength abrasion-proof artware timber sofening treatment liquid, comprises the following steps:
(1) weigh raw material by weight, first polyvinyl alcohol is added to the water 80-90 DEG C and stirs until being completely dissolved, be subsequently adding pine
Fragrant acid polyoxyethylene ester and hexagonal boron nitride 600-1000r/min stir 0.5-1h, be eventually adding hydrogen peroxide in 50-60 DEG C,
Stir process 2-4h under the conditions of 400-600r/min, is cooled to room temperature；
(2) hydroxyethyl cellulose and ethyl hydroxybenzoate are added 60-80 DEG C of stirring 0.5-1h in the solution that step (1) obtains, cold
Add glacial acetic acid the most afterwards to stir, be eventually adding Disulfatozirconic acid. and Alumen stirring at normal temperature 1-2h；
(3) remaining raw material is added stirring at normal temperature 1-2h in the solution that step (2) obtains, obtain high-strength abrasion-proof artware timber
Sofening treatment liquid.
The invention have the advantage that
The present invention utilizes hydrogen peroxide to make polyvinyl alcohol partial hydrolysis, reduces viscosity, improves dissolubility, has lumber fibre
Good lubrication permeability and binding ability, also advantageously improve the toughness of lumber fibre；Add Alumen, Disulfatozirconic acid. introduce aluminum,
Zirconium ion, by the combination of metal ion Yu wood fibre, is conducive to improving the rigidity of timber, intensity and anti-wear performance, simultaneously
Improve the dimensional stability of lumber fibre；By the composite synergistic effect of above-mentioned raw materials, then with glacial acetic acid, surfactant, poly-
Ethylene glycol conventional wood emollient ingredients and remaining raw material compound, and the timber sofening treatment liquid obtained softens processing characteristics
Good, the intensity of timber, toughness are high, anti-wear performance is strong, are difficult to bounce-back, do not affect the finished product after subsequent treatment, and drying and moulding
Intensity, dimensional stability are high, are difficult to craze and transfiguration, are not susceptible to mould corruption, and applied widely, energy-conserving and environment-protective.
Detailed description of the invention
A kind of high-strength abrasion-proof artware timber sofening treatment liquid, is prepared from by the component raw material of following weight (kg):
Disulfatozirconic acid. 1, hexagonal boron nitride 0.1, Polyethylene Glycol 5, glacial acetic acid 4, Alumen 0.5, the hydrogen peroxide 2 of mass fraction 20%, poly-second
Enol 1, polyoxylethylene abietate 0.3, ptfe emulsion 0.5, hydroxyethyl cellulose 0.3, ethyl hydroxybenzoate 0.01, water
50。
The preparation method of a kind of high-strength abrasion-proof artware timber sofening treatment liquid, comprises the following steps:
(1) weigh raw material by weight, first polyvinyl alcohol is added to the water 80 DEG C and stirs until being completely dissolved, be subsequently adding rosin acid
Polyoxyethylene ester and hexagonal boron nitride 600r/min stir 0.5h, be eventually adding hydrogen peroxide in 50 DEG C, stir under the conditions of 400r/min
Mix process 2h, be cooled to room temperature；
Hydroxyethyl cellulose and ethyl hydroxybenzoate are added 60 DEG C of stirring 0.5h in the solution that step (1) obtains, adds after cooling
Glacial acetic acid stirs, and is eventually adding Disulfatozirconic acid. and Alumen stirring at normal temperature 1h；
(3) remaining raw material is added stirring at normal temperature 1h in the solution that step (2) obtains, obtain high-strength abrasion-proof artware timber soft
Change treatment fluid.
Timber pickling being softened in sofening treatment liquid obtained above, soft condition is 50 DEG C, 12h, at softening
Preparing handicraft article after reason, then tests to its effect.
Through inspection, the timber after above-mentioned sofening treatment liquid processes is easily worked, and shape after being processed into Wood craft
Dimensionally stable, uses 3 years nothing crackings, metabolies, and mould corruption does not occur.
Claims (2)
1. a high-strength abrasion-proof artware timber sofening treatment liquid, it is characterised in that it is by the raw material system of following weight parts
:
Disulfatozirconic acid. 1-2, hexagonal boron nitride 0.1-0.15, Polyethylene Glycol 5-10, glacial acetic acid 4-6, Alumen 0.5-1, mass fraction 20-
The hydrogen peroxide 2-4 of 30%, polyvinyl alcohol 1-2, polyoxylethylene abietate 0.3-0.5, ptfe emulsion 0.5-1, ethoxy
Cellulose 0.3-0.5, ethyl hydroxybenzoate 0.01-0.015, water 50-60.
The preparation method of a kind of high-strength abrasion-proof artware timber sofening treatment liquid the most according to claim 1, its feature
It is, comprises the following steps:
(1) weigh raw material by weight, first polyvinyl alcohol is added to the water 80-90 DEG C and stirs until being completely dissolved, be subsequently adding pine
Fragrant acid polyoxyethylene ester and hexagonal boron nitride 600-1000r/min stir 0.5-1h, be eventually adding hydrogen peroxide in 50-60 DEG C,
Stir process 2-4h under the conditions of 400-600r/min, is cooled to room temperature；
(2) hydroxyethyl cellulose and ethyl hydroxybenzoate are added 60-80 DEG C of stirring 0.5-1h in the solution that step (1) obtains, cold
Add glacial acetic acid the most afterwards to stir, be eventually adding Disulfatozirconic acid. and Alumen stirring at normal temperature 1-2h；
(3) remaining raw material is added stirring at normal temperature 1-2h in the solution that step (2) obtains, obtain high-strength abrasion-proof artware timber
Sofening treatment liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610712815.1A CN106272797A (en) | 2016-08-24 | 2016-08-24 | A kind of high-strength abrasion-proof artware timber sofening treatment liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610712815.1A CN106272797A (en) | 2016-08-24 | 2016-08-24 | A kind of high-strength abrasion-proof artware timber sofening treatment liquid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106272797A true CN106272797A (en) | 2017-01-04 |
Family
ID=57615760
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610712815.1A Pending CN106272797A (en) | 2016-08-24 | 2016-08-24 | A kind of high-strength abrasion-proof artware timber sofening treatment liquid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106272797A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015168456A1 (en) * | 2014-05-02 | 2015-11-05 | Arch Wood Protection, Inc. | Wood preservative composition |
| CN105599088A (en) * | 2015-12-28 | 2016-05-25 | 常熟市石林木材有限责任公司 | Timber softener |
-
2016
- 2016-08-24 CN CN201610712815.1A patent/CN106272797A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015168456A1 (en) * | 2014-05-02 | 2015-11-05 | Arch Wood Protection, Inc. | Wood preservative composition |
| CN105599088A (en) * | 2015-12-28 | 2016-05-25 | 常熟市石林木材有限责任公司 | Timber softener |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106313243A (en) | Wood softening processing fluid for mould-proof and insect-proof crafts and preparation method of wood softening processing fluid | |
| CN106313245A (en) | Wood softening treatment fluid for polyglutamic acid-aloe vera gel artworks and preparation method of wood softening treatment fluid | |
| CN105291221A (en) | Bactericidal mildew-proof wicker treatment agent and preparation method thereof | |
| CN103351546B (en) | A kind of imitation leather goods additive and preparation method | |
| CN104692761A (en) | Environment-friendly composite decoration board containing agave sisalana dregs and production method thereof | |
| CN105368240A (en) | Insect-proofing and moth-proofing wicker treating agent and preparation method thereof | |
| CN106272807A (en) | A kind of high-strength ageing artware timber sofening treatment liquid and preparation method thereof | |
| CN107793675A (en) | A kind of preparation method of wood plastic composite | |
| CN106272797A (en) | A kind of high-strength abrasion-proof artware timber sofening treatment liquid and preparation method thereof | |
| CN106272809A (en) | A kind of chitosan hydroxyl apatite artware timber sofening treatment liquid and preparation method thereof | |
| CN104070574B (en) | Strengthening modification agent for a kind of timber floor timber | |
| CN102911385A (en) | Preparation method of high-strength degradable composite film | |
| CN104085005B (en) | A kind of timber floor fungus-proof antisepsis inorganic agent used for wood modification | |
| CN106078986A (en) | A kind of pulullan polysaccharide artware timber sofening treatment liquid and preparation method thereof | |
| CN105482481B (en) | A kind of bamboo fiber-based biomass composite and preparation method thereof | |
| CN106182278A (en) | A kind of fire-resistant antistatic artware timber sofening treatment liquid and preparation method thereof | |
| CN106272808A (en) | A kind of myrica extract soyasaponins artware timber sofening treatment liquid and preparation method thereof | |
| CN106313244A (en) | Wood softening processing fluid for cationic guar gum crafts and preparation method of wood softening processing fluid | |
| CN103509360B (en) | A kind of nanometer glass modified synergic strengthens the preparation method that plate moulded by wood | |
| CN106078987A (en) | A kind of artware timber sofening treatment liquid containing Fructus Luffae extracting solution and preparation method thereof | |
| CN106147269A (en) | A kind of modified bamboo fiber-reinforced composite fire-retardant cabinet slab of high-density polyethylene resin base and preparation method thereof | |
| CN106757063A (en) | A kind of cyclodextrin wood powder graft copolymer absorption decontaminates enhanced water-based metal cleaning agent | |
| CN106078978A (en) | A kind of processing method improving Lignum seu Ramulus Cunninghamiae Lanceolatae wood chip toughness | |
| CN104529298A (en) | Catalpa tea table and production method thereof | |
| CN105504356A (en) | Chitosan and cellulose compound plastic material and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170104 |