CN106182278A - A kind of fire-resistant antistatic artware timber sofening treatment liquid and preparation method thereof - Google Patents
A kind of fire-resistant antistatic artware timber sofening treatment liquid and preparation method thereof Download PDFInfo
- Publication number
- CN106182278A CN106182278A CN201610715304.5A CN201610715304A CN106182278A CN 106182278 A CN106182278 A CN 106182278A CN 201610715304 A CN201610715304 A CN 201610715304A CN 106182278 A CN106182278 A CN 106182278A
- Authority
- CN
- China
- Prior art keywords
- fire
- treatment liquid
- sofening treatment
- timber
- resistant antistatic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/06—Softening or hardening of wood
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical And Physical Treatments For Wood And The Like (AREA)
Abstract
The invention discloses a kind of fire-resistant antistatic artware timber sofening treatment liquid, it is to be prepared by the raw material of following weight parts: Polyethylene Glycol 5 10, glacial acetic acid 46, Alumen 0.5 1, the hydrogen peroxide 24 of mass fraction 20 30%, polyvinyl alcohol 12, tallow amine polyoxyethylene ether 0.3 0.5, magnesium chloride 24, triethanolamine 35, tetramethylolmethane 12, chlorinated paraffin 52 0.1 0.15, ethyl hydroxybenzoate 0.01 0.015, water 50 60.The timber sofening treatment liquid of the present invention softens good processability, the intensity of timber, toughness are high, be difficult to bounce-back, do not affect subsequent treatment, and the finished size stability after drying and moulding is high, be difficult to craze and transfiguration, be not susceptible to mould corruption, and there is fire-retardant, effect of antistatic, applied widely, security performance is high, energy-conserving and environment-protective.
Description
Technical field
The present invention relates to chemical treatments technical field, particularly relate to a kind of fire-resistant antistatic artware timber sofening treatment
Liquid and preparation method thereof.
Background technology
In the course of processing of Wood craft, the timber as raw material is carried out softening is very important step.?
Under usual conditions, timber is a kind of material lacking plasticity, by timber is carried out sofening treatment, it can be made to show temporarily
Plasticity, now timber can be curved, compress, the plastic working such as embossment, then be dried under deformation, recover it
Original rigidity and intensity, it is achieved the permanent plastic deformation of timber, the artware intensity making making is high, and morphological appearance is ornamental
Can be good.Common softening method has decocting in water, high-temperature high-pressure steam to process and Chemical treatment.Process through these methods
Wood dimensional stability is poor, and processing characteristics and serviceability also can be adversely affected.Patent CN201510993437 is with ice vinegar
Acid, Polyethylene Glycol and anion surfactant are that main component prepares timber softening agent, make the timber after process have well
Strength and stiffness, although this softening agent improves processing characteristics and the stable molding of timber after sofening treatment to a certain extent
Property, but timber after softening processing is prone to craze and transfiguration, the most mould perishable defect is not significantly improved, it is therefore desirable to enter
One step is perfect.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of fire-resistant antistatic artware timber is soft
Change treatment fluid and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of fire-resistant antistatic artware timber sofening treatment liquid, it is to be prepared by the raw material of following weight parts:
The hydrogen peroxide 2-4 of Polyethylene Glycol 5-10, glacial acetic acid 4-6, Alumen 0.5-1, mass fraction 20-30%, polyvinyl alcohol 1-2, cattle
Fat amine polyoxyethylene ether 0.3-0.5, magnesium chloride 2-4, triethanolamine 3-5, tetramethylolmethane 1-2, chlorinated paraffin-52 0.1-0.15,
Ethyl hydroxybenzoate 0.01-0.015, water 50-60.
The preparation method of a kind of fire-resistant antistatic artware timber sofening treatment liquid, comprises the following steps:
(1) weigh raw material by weight, first polyvinyl alcohol is added to the water 80-90 DEG C and stirs until being completely dissolved, be subsequently adding cattle
Fat amine polyoxyethylene ether 600-1000r/min stirs 0.5-1h, is eventually adding hydrogen peroxide in 50-60 DEG C, 400-600r/min bar
Stir process 2-4h under part, is cooled to room temperature；
(2) tetramethylolmethane and ethyl hydroxybenzoate are added 60-80 DEG C of stirring 0.5-1h in the solution that step (1) obtains, after cooling
Add glacial acetic acid to stir, be eventually adding Alumen and magnesium chloride stirring at normal temperature 1-2h；
(3) remaining raw material is added stirring at normal temperature 1-2h in the solution that step (2) obtains, obtain fire-resistant antistatic artware timber
Sofening treatment liquid.
The invention have the advantage that
The present invention utilizes hydrogen peroxide to make polyvinyl alcohol partial hydrolysis, reduces viscosity, improves dissolubility, has lumber fibre
Good lubrication permeability and binding ability, also advantageously improve the toughness of lumber fibre；Add Alumen and introduce aluminium ion, pass through
Metal ion and the combination of wood fibre, be conducive to improving rigidity and the intensity of timber, and the size simultaneously improving lumber fibre is steady
Qualitative；By the composite synergistic effect of above-mentioned raw materials, then with glacial acetic acid, surfactant, Polyethylene Glycol conventional wood softening agent
Composition and remaining raw material compound, the timber sofening treatment liquid softening good processability obtained, the intensity of timber, toughness height,
It is difficult to bounce-back, does not affect that the finished size stability after subsequent treatment, and drying and moulding is high, be difficult to craze and transfiguration, be difficult to send out
Mildewing corruption, and have fire-retardant, effect of antistatic, applied widely, security performance is high, energy-conserving and environment-protective.
Detailed description of the invention
A kind of fire-resistant antistatic artware timber sofening treatment liquid, is prepared from by the component raw material of following weight (kg):
Polyethylene Glycol 5, glacial acetic acid 4, Alumen 0.5, the hydrogen peroxide 2 of mass fraction 20%, polyvinyl alcohol 1, tallow amine polyoxyethylene ether
0.3, magnesium chloride 2, triethanolamine 3, tetramethylolmethane 1, chlorinated paraffin-52 0.1, ethyl hydroxybenzoate 0.01, water 50.
The preparation method of a kind of fire-resistant antistatic artware timber sofening treatment liquid, comprises the following steps:
(1) weigh raw material by weight, first polyvinyl alcohol is added to the water 80 DEG C and stirs until being completely dissolved, be subsequently adding tallow amine
Polyoxyethylene ether 600r/min stirs 0.5h, is eventually adding hydrogen peroxide in 50 DEG C, stir process 2h, cooling under the conditions of 400r/min
To room temperature；
(2) tetramethylolmethane and ethyl hydroxybenzoate are added 60 DEG C of stirring 0.5h in the solution that step (1) obtains, after cooling, add ice
Acetic acid stirs, and is eventually adding Alumen and magnesium chloride stirring at normal temperature 1h；
(3) remaining raw material is added stirring at normal temperature 1h in the solution that step (2) obtains, obtain fire-resistant antistatic artware timber soft
Change treatment fluid.
Timber pickling being softened in sofening treatment liquid obtained above, soft condition is 50 DEG C, 12h, at softening
Preparing handicraft article after reason, then tests to its effect.
Through inspection, the timber after above-mentioned sofening treatment liquid processes is easily worked, and shape after being processed into Wood craft
Dimensionally stable, uses 3 years nothing crackings, metabolies, and mould corruption does not occur.
Claims (2)
1. a fire-resistant antistatic artware timber sofening treatment liquid, it is characterised in that it is by the raw material system of following weight parts
:
The hydrogen peroxide 2-4 of Polyethylene Glycol 5-10, glacial acetic acid 4-6, Alumen 0.5-1, mass fraction 20-30%, polyvinyl alcohol 1-2, cattle
Fat amine polyoxyethylene ether 0.3-0.5, magnesium chloride 2-4, triethanolamine 3-5, tetramethylolmethane 1-2, chlorinated paraffin-52 0.1-0.15,
Ethyl hydroxybenzoate 0.01-0.015, water 50-60.
The preparation method of a kind of fire-resistant antistatic artware timber sofening treatment liquid the most according to claim 1, its feature
It is, comprises the following steps:
(1) weigh raw material by weight, first polyvinyl alcohol is added to the water 80-90 DEG C and stirs until being completely dissolved, be subsequently adding cattle
Fat amine polyoxyethylene ether 600-1000r/min stirs 0.5-1h, is eventually adding hydrogen peroxide in 50-60 DEG C, 400-600r/min bar
Stir process 2-4h under part, is cooled to room temperature；
(2) tetramethylolmethane and ethyl hydroxybenzoate are added 60-80 DEG C of stirring 0.5-1h in the solution that step (1) obtains, after cooling
Add glacial acetic acid to stir, be eventually adding Alumen and magnesium chloride stirring at normal temperature 1-2h；
(3) remaining raw material is added stirring at normal temperature 1-2h in the solution that step (2) obtains, obtain fire-resistant antistatic artware timber
Sofening treatment liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610715304.5A CN106182278A (en) | 2016-08-25 | 2016-08-25 | A kind of fire-resistant antistatic artware timber sofening treatment liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610715304.5A CN106182278A (en) | 2016-08-25 | 2016-08-25 | A kind of fire-resistant antistatic artware timber sofening treatment liquid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106182278A true CN106182278A (en) | 2016-12-07 |
Family
ID=57525173
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610715304.5A Pending CN106182278A (en) | 2016-08-25 | 2016-08-25 | A kind of fire-resistant antistatic artware timber sofening treatment liquid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106182278A (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105599088A (en) * | 2015-12-28 | 2016-05-25 | 常熟市石林木材有限责任公司 | Timber softener |
-
2016
- 2016-08-25 CN CN201610715304.5A patent/CN106182278A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105599088A (en) * | 2015-12-28 | 2016-05-25 | 常熟市石林木材有限责任公司 | Timber softener |
Non-Patent Citations (1)
| Title |
|---|
| 毛敏: ""白泥纤维的增强软化改性及其对纸张性能影响的研究"", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106313243A (en) | Wood softening processing fluid for mould-proof and insect-proof crafts and preparation method of wood softening processing fluid | |
| CN106313245A (en) | Wood softening treatment fluid for polyglutamic acid-aloe vera gel artworks and preparation method of wood softening treatment fluid | |
| CN101269508A (en) | Manufacturing technique for moisture-proof middle, high-density pressed-fibre board | |
| CN103696224B (en) | A kind of method improving eider down degreasing efficiency | |
| CN104047156A (en) | Low-temperature cashmere bleaching agent and bleaching method thereof | |
| CN102690403A (en) | Modified phenol formaldehyde resin and preparation method thereof | |
| CN107116644A (en) | A kind of production technology of the wooden door and window of antiseptic fire-retardation | |
| CN106272807A (en) | A kind of high-strength ageing artware timber sofening treatment liquid and preparation method thereof | |
| CN107449224B (en) | A kind of drying of wood processing method | |
| CN106182278A (en) | A kind of fire-resistant antistatic artware timber sofening treatment liquid and preparation method thereof | |
| CN104070574B (en) | Strengthening modification agent for a kind of timber floor timber | |
| CN106272809A (en) | A kind of chitosan hydroxyl apatite artware timber sofening treatment liquid and preparation method thereof | |
| CN106272797A (en) | A kind of high-strength abrasion-proof artware timber sofening treatment liquid and preparation method thereof | |
| CN106078986A (en) | A kind of pulullan polysaccharide artware timber sofening treatment liquid and preparation method thereof | |
| CN106313244A (en) | Wood softening processing fluid for cationic guar gum crafts and preparation method of wood softening processing fluid | |
| CN106272808A (en) | A kind of myrica extract soyasaponins artware timber sofening treatment liquid and preparation method thereof | |
| CN106042118A (en) | Wicker sol-gel surface treating agent for reinforcing and toughening wickerwork and preparation method thereof | |
| CN106078987A (en) | A kind of artware timber sofening treatment liquid containing Fructus Luffae extracting solution and preparation method thereof | |
| CN104858977A (en) | Well erosion resistant wood treatment agent | |
| CN103726329B (en) | A kind of fabric decolorizer | |
| CN106188886A (en) | A kind of aging resistance corrosion resistant wood plastic composite board and preparation method thereof | |
| CN106757063A (en) | A kind of cyclodextrin wood powder graft copolymer absorption decontaminates enhanced water-based metal cleaning agent | |
| CN107488537A (en) | Clothes final finishing detergent | |
| CN106186800B (en) | A kind of cement fibrolite plate additive | |
| CN109354892A (en) | A kind of de- content rubber wood-flour/high-density polyethylene composite material and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161207 |