CN106260501A - A kind of microcapsule-type soybean phospholipid and preparation method - Google Patents
A kind of microcapsule-type soybean phospholipid and preparation method Download PDFInfo
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- CN106260501A CN106260501A CN201610641270.XA CN201610641270A CN106260501A CN 106260501 A CN106260501 A CN 106260501A CN 201610641270 A CN201610641270 A CN 201610641270A CN 106260501 A CN106260501 A CN 106260501A
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- soybean phospholipid
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- oil phase
- microcapsule
- aqueous phase
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- 239000008347 soybean phospholipid Substances 0.000 title claims abstract description 59
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000012071 phase Substances 0.000 claims abstract description 35
- 239000008346 aqueous phase Substances 0.000 claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 102000011632 Caseins Human genes 0.000 claims abstract description 14
- 108010076119 Caseins Proteins 0.000 claims abstract description 14
- 108010010803 Gelatin Proteins 0.000 claims abstract description 14
- 229920000159 gelatin Polymers 0.000 claims abstract description 14
- 239000008273 gelatin Substances 0.000 claims abstract description 14
- 235000019322 gelatine Nutrition 0.000 claims abstract description 14
- 235000011852 gelatine desserts Nutrition 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 229940080237 sodium caseinate Drugs 0.000 claims abstract description 14
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 12
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 11
- 239000006174 pH buffer Substances 0.000 claims abstract description 11
- -1 sucrose fatty acid ester Chemical class 0.000 claims abstract description 11
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229930006000 Sucrose Natural products 0.000 claims abstract description 9
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 9
- 229930195729 fatty acid Natural products 0.000 claims abstract description 9
- 239000000194 fatty acid Substances 0.000 claims abstract description 9
- 239000005720 sucrose Substances 0.000 claims abstract description 9
- 229940014259 gelatin Drugs 0.000 claims abstract description 3
- 239000003921 oil Substances 0.000 claims description 21
- 238000003756 stirring Methods 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- 238000004945 emulsification Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 5
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 5
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 5
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000000265 homogenisation Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 230000001804 emulsifying effect Effects 0.000 claims description 2
- 235000010956 sodium stearoyl-2-lactylate Nutrition 0.000 claims description 2
- KNYAZNABVSEZDS-UHFFFAOYSA-M sodium;2-octadecanoyloxypropanoate Chemical group [Na+].CCCCCCCCCCCCCCCCCC(=O)OC(C)C([O-])=O KNYAZNABVSEZDS-UHFFFAOYSA-M 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 210000000481 breast Anatomy 0.000 claims 1
- WTJKGGKOPKCXLL-RRHRGVEJSA-N phosphatidylcholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCCC=CCCCCCCCC WTJKGGKOPKCXLL-RRHRGVEJSA-N 0.000 abstract description 11
- 238000010521 absorption reaction Methods 0.000 abstract description 5
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 3
- 230000036541 health Effects 0.000 abstract description 3
- 239000011574 phosphorus Substances 0.000 abstract description 3
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 description 6
- 150000003904 phospholipids Chemical class 0.000 description 6
- 239000000839 emulsion Substances 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000003094 microcapsule Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 150000002333 glycines Chemical class 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- SBJKKFFYIZUCET-JLAZNSOCSA-N Dehydro-L-ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(=O)C1=O SBJKKFFYIZUCET-JLAZNSOCSA-N 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 229960005069 calcium Drugs 0.000 description 1
- 235000001465 calcium Nutrition 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 230000010261 cell growth Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 229960001231 choline Drugs 0.000 description 1
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000019152 folic acid Nutrition 0.000 description 1
- 229960000304 folic acid Drugs 0.000 description 1
- 239000011724 folic acid Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000002519 immonomodulatory effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000037356 lipid metabolism Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 125000001095 phosphatidyl group Chemical group 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 235000016804 zinc Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J7/00—Phosphatide compositions for foodstuffs, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of microcapsule-type soybean phospholipid and preparation method, relate to field of health care products.The microcapsule-type soybean phospholipid of the present invention, prepare raw material and comprise aqueous phase and oil phase, wherein, described aqueous phase comprises maltodextrin, Sodium Caseinate, gelatin, pH buffer agent, water, and described oil phase comprises soybean phospholipid, 95% ethanol, sucrose fatty acid ester, monoglyceride, embedding medium, VE；By preparing raw material in regulation microcapsule-type soybean phospholipid, making the microcapsule-type phosphorus level in soya lecithin phosphatidylcholine content for preparing high, good stability, mouthfeel is good；Further, each component addition in raw material aqueous phase and oil phase is prepared by regulation, improve the maximum embedding concentration of soybean phospholipid, thus improve the content of phosphatidylcholine in product, improve the mobility of microcapsule-type soybean phospholipid, moisture absorption, dispersibility, mouthfeel, enhance it to light, the stability of empty air and heat.
Description
Technical field
The present invention relates to health product technology field, particularly relate to a kind of microcapsule-type soybean phospholipid and preparation method.
Background technology
Soybean phospholipid have promotion cell growth, strengthen nervous tissue, nourishing the brain and improving intelligence, promotion lipid metabolism, regulation blood fat,
Reducing the special physiological functions such as cholesterol in human body, immunomodulating and antitumor, people can be by oral doses
Soybean phospholipid product prevents and treats some disease.
At present, soybean phospholipid product on the market mainly has capsule-type and granular pattern two kinds, wherein, capsule-type soybean phospholipid
Product, containing Oleum Glycines and glycerol, has deleterious effect to people with hyperlipidemia, and content of phospholipid and phosphatidylcholine content are relatively simultaneously
Low；By the capsule-type soybean phospholipid product after compositional refinements, although replace Oleum Glycines with the oils and fats with health care, and improve
Phosphatidylcholine content, but its phosphatidylcholine content is the highest, less than 15%.And commercially available granular pattern soybean phospholipid
Product, content of phospholipid is higher, reaches 98%, and phosphatidylcholine content reaches 24%, and comparing capsule-type soybean phospholipid product has and change the most greatly
Entering, but it is more sensitive to light, empty air and heat, and the easy moisture absorption, quality stability are poor, mouthfeel is poor.
Summary of the invention
For the deficiencies in the prior art, an object of the present invention is to provide a kind of microcapsule-type soybean phospholipid, phospholipid
Phatidylcholine content is high, and good stability, mouthfeel is good.
For reaching this purpose, the present invention by the following technical solutions:
A kind of microcapsule-type soybean phospholipid, prepares raw material and comprises aqueous phase and oil phase, and wherein, described aqueous phase comprises Fructus Hordei Germinatus and sticks with paste
Essence, Sodium Caseinate, gelatin, pH buffer agent, water, described oil phase comprises soybean phospholipid, 95% ethanol, sucrose fatty acid ester, single the sweetest
Ester, embedding medium, VE.
Microencapsulation technology is the new and high technology that a development is very fast, and it is by solid, liquid, gas material by any special measures
Being included in the process in a capsule small, that close, utricule size is general in microns, is shaped like spheroid.By micro-glue
Encapsulated can protect wrapped material, is allowed to should not be isolated by environment with the external world, reaches to keep original color to greatest extent
Fragrance, performance and biological activity, prevent destruction and the loss of nutrient substance.Additionally, some material can be covered certainly after encapsulated
The abnormal flavour of body, or by being originally difficult to the gas of processing storage, liquid changes into more stable solid form, thus greatly prevents
Or delayed the generation of product deterioration.The mouthfeel of simple soybean phospholipid is bad, and very poor to the stability of light, empty air and heat,
In the present invention, soybean phospholipid is got up by microcapsule technology embedding, and by the group of each component in regulation aqueous phase and oil phase
Become and proportioning, improve the embedding degree of soybean phospholipid so that the microcapsule-type soybean phospholipid product of preparation in good taste, phosphatidyl
Content of choline is high, strong to the stability of light, empty air and heat.
Wherein, by weight, described aqueous phase comprises the maltodextrin of 30～60 parts, the Sodium Caseinate of 1～5 part, 1～
The gelatin of 5 parts, the pH buffer agent of 1～5 part, the water of 40～70 parts；Such as, the weight portion of maltodextrin be 30 parts, 35 parts, 40
Part, 45 parts, 50 parts, 55 parts, 60 parts；The weight portion of Sodium Caseinate is 1 part, 2 parts, 3 parts, 4 parts, 5 parts；The weight portion of gelatin is 1
Part, 2 parts, 3 parts, 4 parts, 5 parts；The weight portion of pH buffer agent is 1 part, 2 parts, 3 parts, 4 parts, 5 parts；The weight portion of water is 40 parts, 45
Part, 50 parts, 55 parts, 60 parts, 65 parts, 70 parts.
Preferably, described pH buffer agent is the mixture of disodium hydrogen phosphate and sodium dihydrogen phosphate, in order to regulate mixture
PH, described disodium hydrogen phosphate is 1:1 with the mass ratio of described sodium dihydrogen phosphate.
Wherein, by weight, described oil phase comprises the soybean phospholipid of 50～70 parts, 95% ethanol of 20～40 parts, 1
～the sucrose fatty acid ester of 3 parts, the monoglyceride of 1～3 part, the embedding medium of 0.5～2 part, the VE of 0.5～2 part；Such as, Semen sojae atricolor phosphorus
The weight portion of fat is 50 parts, 55 parts, 60 parts, 65 parts, 70 parts；The weight portion of 95% ethanol is 20 parts, 25 parts, 30 parts, 35 parts, 40
Part；The weight portion of sucrose fatty acid ester is 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts；The weight portion of monoglyceride is 1 part, 1.5 parts, 2
Part, 2.5 parts, 3 parts；The weight portion of embedding medium is 0.5 part, 1 part, 1.5 parts, 2 parts；The weight portion of VE is 0.5 part, 1 part, 1.5 parts,
2 parts.
Preferably, described embedding medium is sodium stearoyl lactate.
The two of the purpose of the present invention are to provide the preparation method of a kind of microcapsule-type soybean phospholipid, and preparation technology is simple,
The microcapsule-type phosphorus level in soya lecithin phosphatidylcholine content for preparing is high, improve microcapsule-type soybean phospholipid mobility,
Moisture absorption, dispersibility, mouthfeel, enhance it to light, the stability of empty air and heat；Prepare including aqueous phase, prepared by oil phase, aqueous phase and
Oil phase mixing, pre-emulsification, homogenizing, dry step.
Wherein, the process that prepared by described aqueous phase is:
1) by weight, weigh the maltodextrin of 30～60 parts in the Plastic Drum of 20L, add 85 DEG C of 30～60 parts
Water in stirring and dissolving；
2) by weight, weigh the Sodium Caseinate of 1～5 part in the beaker of 1000mL, add 85 DEG C of 2～5 parts
In water, 85 DEG C of heating in water bath stirring and dissolving；
3) by weight, the gelatin of 1～5 part is weighed in the beaker of 1000mL, in the water of add 2～5 parts 85 DEG C,
85 DEG C of heating in water bath stirring and dissolving；
4) by step 2), step 3) Sodium Caseinate that dissolved, gelatin pour step 1 into) in the maltodextrin that dissolved, stir
Mix mixing；
5) by weight, to step 4) solution that mixes adds the pH buffer agent of 1～5 part, after stirring and dissolving
To aqueous phase.
Wherein, the process that prepared by described oil phase is:
6) by weight, weigh in 95% ethanol that the soybean phospholipid of 50～70 parts joins 20～40 parts, 60 DEG C of water
Bath is heated to soybean phospholipid and is completely dissolved；
7) by weight, to step 6) dissolve after soybean phospholipid in add sucrose fatty acid ester, 1～3 of 1～3 part
The monoglyceride of part, the embedding medium of 0.5～2 part, the VE of 0.5～2 part, obtain oil phase after stirring and dissolving.
Wherein, the process of described aqueous phase and oil phase mixing is: by step 5) aqueous phase for preparing and step 7) it is prepared into
To oil phase be heated to 50 DEG C respectively after mix homogeneously.
Pre-emulsified effect is to make the distribution of aqueous phase and oil phase in mixed liquor more uniform.Wherein, described pre-emulsified mistake
Cheng Wei, adds water to solid content reach 30% by aqueous phase and the oil phase of mix homogeneously, inserts in cutter and shears, makes aqueous phase and oil phase pre-
Emulsifying.
Homogenizing also referred to as homogenate, is to make dispersion micronized in suspension (or emulsion) system, the process of homogenization
Journey, this process plays simultaneously and reduces dispersion yardstick and improve the effect of dispersion distributing homogeneity.Wherein, the mistake of described homogenizing
Cheng Wei: the emulsion after pre-emulsification is placed in homogenizing in homogenizer, control homogenization pressure is 40MPa.
Wherein, described dry process is: the emulsion after homogenizing is sent into spray dryer and is dried, and controls spraying machine and does
Dry inlet temperature is 200 DEG C, and leaving air temp is 82 DEG C, and feed pressure is 16MPa.
Compared with prior art, the invention have the benefit that the microcapsule-type soybean phospholipid of the present invention, prepare raw material bag
Aqueous phase and oil phase, wherein, described aqueous phase comprises maltodextrin, Sodium Caseinate, gelatin, pH buffer agent, water, and described oil phase comprises
Soybean phospholipid, 95% ethanol, sucrose fatty acid ester, monoglyceride, embedding medium, VE；By in regulation microcapsule-type soybean phospholipid
Preparing raw material, make phosphatidylcholine content in the microcapsule-type soybean phospholipid product prepared high, good stability, mouthfeel is good；
Further, prepare each component addition in raw material aqueous phase and oil phase by regulation, improve the maximum embedding concentration of soybean phospholipid,
Thus improve the content of phosphatidylcholine in microcapsule-type soybean phospholipid product, improve the flowing of microcapsule-type soybean phospholipid
Property, moisture absorption, dispersibility, mouthfeel, enhance it to light, the stability of empty air and heat.
Detailed description of the invention
Technical scheme is further illustrated below by detailed description of the invention.
As no specific instructions, the various raw materials of the present invention are the most commercially available to be buied, or prepares according to the conventional method of this area
Obtain.
The concrete preparation process of the microcapsule-type soybean phospholipid of the present invention is as follows:
1) accurately weighing maltodextrin 6Kg in the Plastic Drum of 20L, add the pure water 6Kg of 85 DEG C, period constantly stirs
Mix so that maltodextrin fully dissolves.
2) accurately weighing Sodium Caseinate 150g in 1000mL beaker, add the pure water 500g of 85 DEG C, period constantly stirs
Mix, and heat with water-bath (bath temperature controls at about 85 DEG C), be completely dissolved to Sodium Caseinate.
3) accurately weighing gelatin 150g in 1000mL beaker, add the pure water 500g of 85 DEG C, period is stirred continuously, and
Heat with water-bath (bath temperature controls at about 85 DEG C), be completely dissolved to gelatin.
4) by step 2) Sodium Caseinate that dissolved and step 3) gelatin that dissolved pours step 1 into) Fructus Hordei Germinatus that dissolved
In dextrin, stirring, allow it be sufficiently mixed uniformly.
5) to step 4) mix solution in, add disodium hydrogen phosphate and each 75g of sodium dihydrogen phosphate, stirring, phosphoric acid
After salt fully dissolves, aqueous phase prepares completely, standby.
6) accurately weighing soybean phospholipid 9kg, and add the ethanol 6L of 95%, water-bath (60 DEG C) is heated, until soybean phospholipid
It is completely dissolved, 5 hours used times.
7) until step 6) in soybean phospholipid be completely dissolved mutually after, be added thereto to sucrose fatty acid ester, monoglyceride, tristearin
Acyl lactylate and VE are respectively 150g, 150g, 75g, 75g, stirring, fully dissolve, and oil phase prepares completely, standby.
8) by step 5) aqueous phase and step 7) oil phase, stirring be warmed up to 50 DEG C
9) by step 8) in the aqueous phase of 50 DEG C and oil phase mixing, and to add pure water to gross weight be 50kg, and solid content contains
Amount reaches 30%, is sheared by cutter, makes biphase pre-emulsification.
10) by pre-emulsified emulsion homogenizing, homogenization pressure controls at 40MPa, homogenizing one time.
11) product that homogenizing is good is sent into spray dryer and is dried, and controlling to be spray-dried inlet temperature is 200 DEG C, goes out
Air temperature is 82 DEG C, and feed pressure is 16MPa, and the used time is 52 minutes, finally gives microcapsule-type soybean phospholipid product population and is
13.2kg。
By the addition of each component, raw material powdery soybean in aqueous phase, oil phase in regulation microcapsule-type soybean phospholipid formula
Phospholipid (PC25, i.e. phosphatidylcholine content are the soybean phospholipid of 25%), (PC50, i.e. phosphatidylcholine content are soybean phospholipid
The soybean phospholipid of 50%) after micro encapsulation, mobility, moisture absorption, dispersibility respectively obtain and are obviously improved, the de-luxe compartment of phospholipid
Burying concentration and be able to reach 90% and 75%, PC content all can bring up to 20% even more than 35%.
Furthermore it is also possible to according to all ages and classes level crowd different demands to nutrition, design different microcapsule soys
Phospholipid prod formula, meets the demand of Market Consumer significantly, such as, for infant crowd, and can be at microcapsule
Preparing of type soybean phospholipid additionally adds DHA to meet the Growing Demand of infant in raw material；For population of adolescent, can be micro-
Preparing of capsule-type soybean phospholipid additionally adds calcium, ferrum, zinc, DHA to meet the teenager demand to nutrition in raw material；For pregnant
At microcapsule-type soybean phospholipid, puerpera crowd, can prepare that additionally to add ferrum, zinc, calcium, folic acid, vitamin in raw material pregnant to meet
Puerpera's demand to nutrition.
Above example is only used for illustrating the method detailed of the present invention, the invention is not limited in above-mentioned method detailed, i.e.
Do not mean that the present invention has to rely on above-mentioned method detailed and could implement.Person of ordinary skill in the field is it will be clearly understood that right
Any improvement of the present invention, the equivalence of raw material each to product of the present invention is replaced and the interpolation of auxiliary element, concrete way choice
Deng, within the scope of all falling within protection scope of the present invention and disclosure.
Claims (10)
1. a microcapsule-type soybean phospholipid, it is characterised in that prepare raw material and comprise aqueous phase and oil phase, wherein, described aqueous phase bag
Containing maltodextrin, Sodium Caseinate, gelatin, pH buffer agent, water, described oil phase comprises soybean phospholipid, 95% ethanol, sucrose-fatty
Ester, monoglyceride, embedding medium, VE.
Microcapsule-type soybean phospholipid the most according to claim 1, it is characterised in that by weight, wraps in described aqueous phase
Containing the maltodextrins of 30～60 parts, the Sodium Caseinate of 1～5 part, the gelatin of 1～5 part, the pH buffer agent of 1～5 part, 40～70 parts
Water；
Preferably, described pH buffer agent is the mixture of disodium hydrogen phosphate and sodium dihydrogen phosphate, and described disodium hydrogen phosphate is with described
The mass ratio of sodium dihydrogen phosphate is 1:1.
Microcapsule-type soybean phospholipid the most according to claim 1, it is characterised in that by weight, wraps in described oil phase
Containing the soybean phospholipids of 50～70 parts, 95% ethanol of 20～40 parts, the sucrose fatty acid ester of 1～3 part, the monoglyceride of 1～3 part,
The embedding medium of 0.5～2 part, the VE of 0.5～2 part；
Preferably, described embedding medium is sodium stearoyl lactate.
4. the preparation method of a microcapsule-type soybean phospholipid as claimed in claim 1, it is characterised in that include aqueous phase system
Prepared by standby, oil phase, aqueous phase and oil phase mixing, pre-emulsification, homogenizing, dry step.
Preparation method the most according to claim 4, it is characterised in that process prepared by described aqueous phase is:
1) by weight, weigh the maltodextrin of 30～60 parts in the Plastic Drum of 20L, add the water of 85 DEG C of 30～60 parts
Middle stirring and dissolving；
2) by weight, the Sodium Caseinate of 1～5 part is weighed in the beaker of 1000mL, in the water of add 2～5 parts 85 DEG C,
85 DEG C of heating in water bath stirring and dissolving；
3) by weight, the gelatin of 1～5 part is weighed in the beaker of 1000mL, in the water of add 2～5 parts 85 DEG C, 85 DEG C
Heating in water bath stirring and dissolving；
4) by step 2), step 3) Sodium Caseinate that dissolved, gelatin pour step 1 into) in the maltodextrin that dissolved, stirring is mixed
Close；
5) by weight, to step 4) solution that mixes adds the pH buffer agent of 1～5 part, obtain water after stirring and dissolving
Phase.
Preparation method the most according to claim 5, it is characterised in that process prepared by described oil phase is:
6) by weight, weighing in 95% ethanol that the soybean phospholipid of 50～70 parts joins 20～40 parts, 60 DEG C of water-baths add
Heat to soybean phospholipid is completely dissolved；
7) by weight, to step 6) dissolve after soybean phospholipid in add 1～3 part sucrose fatty acid ester, 1～3 part
Monoglyceride, the embedding medium of 0.5～2 part, the VE of 0.5～2 part, obtain oil phase after stirring and dissolving.
Preparation method the most according to claim 6, it is characterised in that the process of described aqueous phase and oil phase mixing is: will step
Rapid 5) aqueous phase prepared and step 7) oil phase for preparing be heated to 50 DEG C respectively after mix homogeneously.
Preparation method the most according to claim 7, it is characterised in that described pre-emulsified process is, by mix homogeneously
Aqueous phase and oil phase add water to solid content and reach 30%, insert in cutter and shear, make aqueous phase and oil phase pre-emulsification.
Preparation method the most according to claim 8, it is characterised in that the process of described homogenizing is: by the breast after pre-emulsification
Changing liquid and be placed in homogenizing in homogenizer, control homogenization pressure is 40MPa.
Preparation method the most according to claim 9, it is characterised in that described dry process is: by the emulsifying after homogenizing
Liquid is sent into spray dryer and is dried, and the inlet temperature that control spraying machine is dried is 200 DEG C, and leaving air temp is 82 DEG C, feed pressure
For 16MPa.
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| CN112674344A (en) * | 2021-01-21 | 2021-04-20 | 江苏曼氏生物科技股份有限公司 | Phospholipid granule and preparation method thereof |
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