CN106244003A - A kind of preparation method of ageing-resistant oil colour - Google Patents
A kind of preparation method of ageing-resistant oil colour Download PDFInfo
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- CN106244003A CN106244003A CN201610734975.6A CN201610734975A CN106244003A CN 106244003 A CN106244003 A CN 106244003A CN 201610734975 A CN201610734975 A CN 201610734975A CN 106244003 A CN106244003 A CN 106244003A
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F251/00—Macromolecular compounds obtained by polymerising monomers on to polysaccharides or derivatives thereof
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- C08F289/00—Macromolecular compounds obtained by polymerising monomers on to macromolecular compounds not provided for in groups C08F251/00 - C08F287/00
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C08L2205/00—Polymer mixtures characterised by other features
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Abstract
The invention discloses the preparation method of a kind of ageing-resistant oil colour, belong to oil colour preparing technical field.The present invention adds oil-soluble non-oxidizability after taking Camellia oil and Testa oryzae oil mixing and prepares pigment substrate oil, standby, take after Folium Ipomoea squeezes the juice again, obtain juice regulation pH post-heating, separate out precipitate, after drying and crushing, obtain Folium Ipomoea protein powder, and obtain reactant with after Sorghum vulgare Pers. powder mixing gelatinizing with acrylic acid cross-linking reaction, scrubbed, dried, mix with materials such as standby pigment substrate oil, pigment, and grind to obtain the method for ageing-resistant oil colour.Preparation process of the present invention is simple, products obtained therefrom rate of drying is fast, prepared pigment substrate is effectively increased its non-oxidizability and resistance to ag(e)ing, the mixture of Radix Ipomoeae egg albumen and Sorghum vulgare Pers. powder and acrylic acid react the reactant produced be added in oil colour, the resistance to water that can make oil colour strengthens, solve its light resistance poor, by illumination fugitive color, problem of aging.
Description
Technical field
The present invention relates to the preparation method of a kind of ageing-resistant oil colour, belong to oil colour preparing technical field.
Background technology
Oil colour is a kind of special drawing pigment of oil painting, pigment powder refuel and glue agitation grinding forms.Market is sold
It mostly is pipe dress, also can make by oneself.The basis of oil colour as other drawing pigment by colorant, extender pigment, vehicle
Constitute with the such as plastotype agent of some adjuvant, stabilizer, slow dry agent or drier etc..Pigment powder multi-source used by ancient times in soil property and
Mineral.Another part derives from plant or animal.Oil painting is quite expected as unguentum, has butter shape feature.Wet coating can be taken advantage of glibly
Smear, dry the most small with wet color difference.It is easily handled between oil colour, can tell on rapidly, and be readily available color
Fuse and mix.And can also draw a picture on what works in office and be covered, also can take advantage of and wet correct and revise.Oil painting face
The performance of painting skill can be had a huge impact by the quality of material quality, is also the prerequisite bar determining paint life-span length
One of part.In recent years, along with the development of drawing industry, people are more and more higher to the requirement of oil colour.Oil colour
Some direct shadows of performance such as color power, resistance to luminous power, covering power, transparency, oil absorption, toughness, aridity, plasticity and levelability
Ring the effect drawn a picture.Oil colour common problem is at present: rate of drying is slow, typically requires and dry in the air for a long time after using
Dry, and due to the electrostatic effect on picture, some dusts or tiny hair can be adsorbed, and infiltrated by the oiliness surface permanent of picture
Storage, the quality stability causing oil painting is poor；Light resistance is poor, by illumination fugitive color, aging.
Summary of the invention
The technical problem to be solved: slow for current oil colour rate of drying, light resistance is poor, easy by illumination
Fade, aging drawback, it is provided that one take Camellia oil and Testa oryzae oil mixing after add oil-soluble non-oxidizability prepare pigment base
Body oils, standby, then take after Folium Ipomoea squeezes the juice, obtain juice regulation pH post-heating, separate out precipitate, after drying and crushing Folium Ipomoea egg
White lead end, and obtain reactant with after Sorghum vulgare Pers. powder mixing gelatinizing with acrylic acid cross-linking reaction, scrubbed, dried, with standby pigment
The mixing of the material such as matrix oil, pigment, and grind to obtain the method for ageing-resistant oil colour.Preparation process of the present invention is simple, and gained produces
Product rate of drying is fast, and prepared pigment substrate is effectively increased its non-oxidizability and resistance to ag(e)ing, by Radix Ipomoeae egg albumen and Sorghum vulgare Pers. powder
Mixture and acrylic acid react the reactant produced and are added in oil colour, and the resistance to water of oil colour can be made to strengthen, and solve
Its light resistance of having determined is poor, by illumination fugitive color, problem of aging.
For solving above-mentioned technical problem, the present invention uses the technical scheme as described below to be:
(1) weigh 100～200g Camellia oil and 150～300g Testa oryzae oil respectively, obtain miscella after stirring mixing, be added thereto to
Miscella quality 2～5% tea polyphenols and miscella quality 1～3% Butylated hydroxyanisole, after stirring mixing 40～50min, obtain face
Material matrix oil, standby；
(2) choose 200～300g fresh Folium Ipomoea, after cleaning leaf surface, put into and juice extractor squeezes the juice 15～20min, obtain red
Potato leaf juice, is 8.0～9.0 with mass fraction 20% sodium hydroxide regulation Folium Ipomoea juice pH value, is heated to by Folium Ipomoea juice after regulation
80～90 DEG C, insulation stands after 20～30min, and centrifugation while hot obtains precipitate, put into by precipitate in baking oven, 55～
Being dried 5～6h at a temperature of 65 DEG C, crushed after being dried, 100～120 mesh sieves, obtain Folium Ipomoea protein powder excessively；
(3) 1:3 in mass ratio, mixes above-mentioned Folium Ipomoea protein powder and 100～120 mesh Sorghum vulgare Pers. powder, after stirring, puts into
In four-hole boiling flask, and add 200～300mL deionized waters, put in water-bath, be heated to 85 DEG C, stirring gelatinizing 30～
40min, is cooled to 55～60 DEG C after gelatinizing, be subsequently added 100～120g acrylic acid, and molten with mass fraction 30% sodium hydroxide
After liquid regulation pH value is 7.0, then it is separately added into 15～20mL mass fraction 5% ammonium persulfate solutions and 0.1～0.3gN, N-methylene
Base bisacrylamide, after insulated and stirred reaction 1～2h, is cooled to room temperature and obtains reactant, by reactant with absolute ethanol washing 2～
After 4 times, put in baking oven, at a temperature of 50～60 DEG C, be dried 5～6h, cross 200～220 mesh sieves, obtain reactant powders；
(4) count by weight, choose 40～45 parts of standby pigment substrate oil of step (1), 20～25 parts of above-mentioned reactions respectively
Thing powder, 25～30 parts of pigment, 3～5 parts of nano titanium oxides, 2～4 part 200～220 mesh Pearls and 0.2～0.5 part hard
Fat acid aluminum, be added sequentially in three-roll grinder grind, through three-roll grinder be ground to slurry fineness in 3～8 μm after, discharging,
I.e. can get ageing-resistant oil colour.
The application process of the present invention: take the ageing-resistant oil colour that the 25～28g present invention prepare and be put on palette, through face
After material allotment mixing, dipping pigment with paintbrush and carry out painting, after testing, this oil colour rate of drying is fast, draws a picture dry
Time is 2～3 days, oil painting by illumination 40～60 years, without fading, obscission occur, light fastness is good, and resistance to ag(e)ing is than common
Oil colour exceeds 4～6 times, is worthy to be popularized and uses.
The present invention is compared with additive method, and Advantageous Effects is:
(1) ageing-resistant oil colour prepared by the present invention is effectively increased its non-oxidizability and resistance to ag(e)ing；
(2) present invention mixture of Radix Ipomoeae egg albumen and Sorghum vulgare Pers. powder and acrylic acid are reacted produce reactant be added on oil colour
In, the resistance to water of oil colour can be made to strengthen, solve its light resistance poor, by illumination fugitive color, problem of aging；
(3) the oil colour rate of drying that the present invention prepares is fast, uses rear oil painting quality stability good；
(4) oil colour that the present invention prepares, has good acid and alkali resistance performance and heat stability, and ageing-resistant performance is good.
Detailed description of the invention
Weigh 100～200g Camellia oil and 150～300g Testa oryzae oil the most respectively, after stirring mixing, obtain miscella, Xiang Qi
Middle addition miscella quality 2～5% tea polyphenols and miscella quality 1～3% Butylated hydroxyanisole, stirring mixing 40～50min
After, obtain pigment substrate oil, standby；Then choose 200～300g fresh Folium Ipomoea, after cleaning leaf surface, put in juice extractor
Squeeze the juice 15～20min, obtain Folium Ipomoea juice, be 8.0～9.0 with mass fraction 20% sodium hydroxide regulation Folium Ipomoea juice pH value, will adjust
After joint, Folium Ipomoea juice is heated to 80～90 DEG C, after insulation stands 20～30min, and centrifugation while hot, obtain precipitate, by precipitate
Putting in baking oven, be dried 5～6h at a temperature of 55～65 DEG C, crushed after being dried, 100～120 mesh sieves, obtain Folium Ipomoea egg albumen powder excessively
End；1:3 the most in mass ratio, mixes above-mentioned Folium Ipomoea protein powder and 100～120 mesh Sorghum vulgare Pers. powder, after stirring, puts into four
In mouth flask, and add 200～300mL deionized waters, put in water-bath, be heated to 85 DEG C, stir gelatinizing 30～40min,
It is cooled to 55～60 DEG C after gelatinizing, is subsequently added 100～120g acrylic acid, and regulates with mass fraction 30% sodium hydroxide solution
After pH value is 7.0, then it is separately added into 15～20mL mass fraction 5% ammonium persulfate solutions and 0.1～0.3gN, N-di-2-ethylhexylphosphine oxide third
Acrylamide, after insulated and stirred reaction 1～2h, is cooled to room temperature and obtains reactant, by reactant with after absolute ethanol washing 2～4 times,
Put in baking oven, at a temperature of 50～60 DEG C, be dried 5～6h, cross 200～220 mesh sieves, obtain reactant powders；The most by weight
Number meter, choose respectively 40～45 parts of standby pigment substrate oil, 20～25 parts of above-mentioned reactant powders, 25～30 parts of pigment, 3～
5 parts of nano titanium oxides, 2～4 part 200～220 mesh Pearls and 0.2～0.5 part of aluminium stearate, be added sequentially to three rollers and grind
In grinding machine grind, through three-roll grinder be ground to slurry fineness in 3～8 μm after, discharging, i.e. can get ageing-resistant oil colour.
Example 1
Weigh 100g Camellia oil and 150g Testa oryzae oil the most respectively, after stirring mixing, obtain miscella, be added thereto to mixing oil
Measure 2% tea polyphenols and miscella quality 1% Butylated hydroxyanisole, after stirring mixing 40min, obtain pigment substrate oil, standby；Then
Choose the fresh Folium Ipomoea of 200g, after cleaning leaf surface, put into the 15min that squeezes the juice in juice extractor, obtain Folium Ipomoea juice, use mass fraction
20% sodium hydroxide regulation Folium Ipomoea juice pH value is 8.0, and Folium Ipomoea juice after regulation is heated to 80 DEG C, after insulation stands 20min,
Centrifugation while hot, obtains precipitate, is put into by precipitate in baking oven, is dried 5h, crushed after being dried, crosses 100 at a temperature of 55 DEG C
Mesh sieve, obtains Folium Ipomoea protein powder；1:3 the most in mass ratio, mixes above-mentioned Folium Ipomoea protein powder and 100 mesh Sorghum vulgare Pers. powder, stirs
After mixing uniformly, put in four-hole boiling flask, and add 200mL deionized water, put in water-bath, be heated to 85 DEG C, stir gelatinizing
30min, is cooled to 55 DEG C after gelatinizing, be subsequently added 100g acrylic acid, and regulate pH value with mass fraction 30% sodium hydroxide solution
After being 7.0, then being separately added into 15mL mass fraction 5% ammonium persulfate solution and 0.1gN, N-methylene-bisacrylamide, insulation is stirred
After mixing reaction 1h, it is cooled to room temperature and obtains reactant, by reactant with after absolute ethanol washing 2 times, put in baking oven, 50 DEG C of temperature
Degree is lower is dried 5h, crosses 200 mesh sieves, obtains reactant powders；Finally count by weight, choose 40 parts of standby pigment substrate respectively
Oil, 20 parts of above-mentioned reactant powders, 25 parts of pigment, 3 parts of nano titanium oxides, 2 part of 200 mesh Pearl and 0.2 part of stearic acid
Aluminum, be added sequentially in three-roll grinder grind, through three-roll grinder be ground to slurry fineness in 3 μm after, discharging, the most available
Ageing-resistant oil colour.
Take the ageing-resistant oil colour that the 25g present invention prepares to be put on palette, after pigment allotment mixing, dip in paintbrush
Taking pigment to carry out painting, after testing, this oil colour rate of drying is fast, and drying time of drawing a picture is 20h, and oil painting is by illumination 40
Year, nothing is faded, obscission occurs, and light fastness is good, and resistance to ag(e)ing exceeds 4 times than conventional oil paint, is worthy to be popularized and makes
With.
Example 2
Weigh 150g Camellia oil and 225g Testa oryzae oil the most respectively, after stirring mixing, obtain miscella, be added thereto to mixing oil
Measure 3% tea polyphenols and miscella quality 2% Butylated hydroxyanisole, after stirring mixing 45min, obtain pigment substrate oil, standby；Then
Choose the fresh Folium Ipomoea of 250g, after cleaning leaf surface, put into the 18min that squeezes the juice in juice extractor, obtain Folium Ipomoea juice, use mass fraction
20% sodium hydroxide regulation Folium Ipomoea juice pH value is 8.5, and Folium Ipomoea juice after regulation is heated to 85 DEG C, after insulation stands 25min,
Centrifugation while hot, obtains precipitate, is put into by precipitate in baking oven, is dried 6h, crushed after being dried, crosses 110 at a temperature of 60 DEG C
Mesh sieve, obtains Folium Ipomoea protein powder；1:3 the most in mass ratio, mixes above-mentioned Folium Ipomoea protein powder and 110 mesh Sorghum vulgare Pers. powder, stirs
After mixing uniformly, put in four-hole boiling flask, and add 250mL deionized water, put in water-bath, be heated to 85 DEG C, stir gelatinizing
35min, is cooled to 58 DEG C after gelatinizing, be subsequently added 110g acrylic acid, and regulate pH value with mass fraction 30% sodium hydroxide solution
After being 7.0, then being separately added into 18mL mass fraction 5% ammonium persulfate solution and 0.2gN, N-methylene-bisacrylamide, insulation is stirred
After mixing reaction 2h, it is cooled to room temperature and obtains reactant, by reactant with after absolute ethanol washing 3 times, put in baking oven, 55 DEG C of temperature
Degree is lower is dried 6h, crosses 210 mesh sieves, obtains reactant powders；Finally count by weight, choose 43 parts of standby pigment substrate respectively
Oil, 22 parts of above-mentioned reactant powders, 28 parts of pigment, 4 parts of nano titanium oxides, 3 part of 210 mesh Pearl and 0.4 part of stearic acid
Aluminum, be added sequentially in three-roll grinder grind, through three-roll grinder be ground to slurry fineness in 5 μm after, discharging, the most available
Ageing-resistant oil colour.
Take the ageing-resistant oil colour that the 26g present invention prepares to be put on palette, after pigment allotment mixing, dip in paintbrush
Taking pigment to carry out painting, after testing, this oil colour rate of drying is fast, and drying time of drawing a picture is 22h, and oil painting is by illumination 50
Year, nothing is faded, obscission occurs, and light fastness is good, and resistance to ag(e)ing exceeds 5 times than conventional oil paint, is worthy to be popularized and makes
With.
Example 3
Weigh 200g Camellia oil and 300g Testa oryzae oil the most respectively, after stirring mixing, obtain miscella, be added thereto to mixing oil
Measure 5% tea polyphenols and miscella quality 3% Butylated hydroxyanisole, after stirring mixing 50min, obtain pigment substrate oil, standby；Then
Choose the fresh Folium Ipomoea of 300g, after cleaning leaf surface, put into the 20min that squeezes the juice in juice extractor, obtain Folium Ipomoea juice, use mass fraction
20% sodium hydroxide regulation Folium Ipomoea juice pH value is 9.0, and Folium Ipomoea juice after regulation is heated to 90 DEG C, after insulation stands 30min,
Centrifugation while hot, obtains precipitate, is put into by precipitate in baking oven, is dried 6h, crushed after being dried, crosses 120 at a temperature of 65 DEG C
Mesh sieve, obtains Folium Ipomoea protein powder；1:3 the most in mass ratio, mixes above-mentioned Folium Ipomoea protein powder and 120 mesh Sorghum vulgare Pers. powder, stirs
After mixing uniformly, put in four-hole boiling flask, and add 300mL deionized water, put in water-bath, be heated to 85 DEG C, stir gelatinizing
40min, is cooled to 60 DEG C after gelatinizing, be subsequently added 120g acrylic acid, and regulate pH value with mass fraction 30% sodium hydroxide solution
After being 7.0, then being separately added into 20mL mass fraction 5% ammonium persulfate solution and 0.3gN, N-methylene-bisacrylamide, insulation is stirred
After mixing reaction 2h, it is cooled to room temperature and obtains reactant, by reactant with after absolute ethanol washing 4 times, put in baking oven, 60 DEG C of temperature
Degree is lower is dried 6h, crosses 220 mesh sieves, obtains reactant powders；Finally count by weight, choose 45 parts of standby pigment substrate respectively
Oil, 25 parts of above-mentioned reactant powders, 30 parts of pigment, 5 parts of nano titanium oxides, 4 part of 220 mesh Pearl and 0.5 part of stearic acid
Aluminum, be added sequentially in three-roll grinder grind, through three-roll grinder be ground to slurry fineness in 8 μm after, discharging, the most available
Ageing-resistant oil colour.
Take the ageing-resistant oil colour that the 28g present invention prepares to be put on palette, after pigment allotment mixing, dip in paintbrush
Taking pigment to carry out painting, after testing, this oil colour rate of drying is fast, and drying time of drawing a picture is 24h, and oil painting is by illumination 60
Year, nothing is faded, obscission occurs, and light fastness is good, and resistance to ag(e)ing exceeds 6 times than conventional oil paint, is worthy to be popularized and makes
With.
Claims (1)
1. the preparation method of an ageing-resistant oil colour, it is characterised in that concrete preparation process is:
(1) weigh 100～200g Camellia oil and 150～300g Testa oryzae oil respectively, obtain miscella after stirring mixing, be added thereto to
Miscella quality 2～5% tea polyphenols and miscella quality 1～3% Butylated hydroxyanisole, after stirring mixing 40～50min, obtain face
Material matrix oil, standby；
(2) choose 200～300g fresh Folium Ipomoea, after cleaning leaf surface, put into and juice extractor squeezes the juice 15～20min, obtain red
Potato leaf juice, is 8.0～9.0 with mass fraction 20% sodium hydroxide regulation Folium Ipomoea juice pH value, is heated to by Folium Ipomoea juice after regulation
80～90 DEG C, insulation stands after 20～30min, and centrifugation while hot obtains precipitate, put into by precipitate in baking oven, 55～
Being dried 5～6h at a temperature of 65 DEG C, crushed after being dried, 100～120 mesh sieves, obtain Folium Ipomoea protein powder excessively；
(3) 1:3 in mass ratio, mixes above-mentioned Folium Ipomoea protein powder and 100～120 mesh Sorghum vulgare Pers. powder, after stirring, puts into
In four-hole boiling flask, and add 200～300mL deionized waters, put in water-bath, be heated to 85 DEG C, stirring gelatinizing 30～
40min, is cooled to 55～60 DEG C after gelatinizing, be subsequently added 100～120g acrylic acid, and molten with mass fraction 30% sodium hydroxide
After liquid regulation pH value is 7.0, then it is separately added into 15～20mL mass fraction 5% ammonium persulfate solutions and 0.1～0.3gN, N-methylene
Base bisacrylamide, after insulated and stirred reaction 1～2h, is cooled to room temperature and obtains reactant, by reactant with absolute ethanol washing 2～
After 4 times, put in baking oven, at a temperature of 50～60 DEG C, be dried 5～6h, cross 200～220 mesh sieves, obtain reactant powders；
(4) count by weight, choose 40～45 parts of standby pigment substrate oil of step (1), 20～25 parts of above-mentioned reactions respectively
Thing powder, 25～30 parts of pigment, 3～5 parts of nano titanium oxides, 2～4 part 200～220 mesh Pearls and 0.2～0.5 part hard
Fat acid aluminum, be added sequentially in three-roll grinder grind, through three-roll grinder be ground to slurry fineness in 3～8 μm after, discharging,
I.e. can get ageing-resistant oil colour.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107418276A (en) * | 2017-09-27 | 2017-12-01 | 河北科技师范学院 | A kind of odorlessness type ring protects oil colour |
| CN108359300A (en) * | 2018-02-10 | 2018-08-03 | 谢新昇 | A kind of preparation method of the anti-dust suction oil colour of quick-dry type |
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| CN104017436A (en) * | 2014-05-28 | 2014-09-03 | 南昌大学 | Children pigment composed of edible composition |
| CN104650639A (en) * | 2013-11-19 | 2015-05-27 | 青岛古宇石墨有限公司 | Manufacturing formula of waterproof oil paint |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5320670A (en) * | 1992-12-22 | 1994-06-14 | Foster Avis A | Soybean oil paint base |
| CN101225253A (en) * | 2007-12-26 | 2008-07-23 | 宋健 | Art oil paint containing nano-pigment and method for manufacturing same |
| CN104650639A (en) * | 2013-11-19 | 2015-05-27 | 青岛古宇石墨有限公司 | Manufacturing formula of waterproof oil paint |
| CN104017436A (en) * | 2014-05-28 | 2014-09-03 | 南昌大学 | Children pigment composed of edible composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107418276A (en) * | 2017-09-27 | 2017-12-01 | 河北科技师范学院 | A kind of odorlessness type ring protects oil colour |
| CN108359300A (en) * | 2018-02-10 | 2018-08-03 | 谢新昇 | A kind of preparation method of the anti-dust suction oil colour of quick-dry type |
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Address after: 213164 Changzhou Province, north of the New District, Jiangsu Biguiyuan, unit B, room 1601, room 32 Applicant after: Ding Yuqin Address before: 213164 Changzhou Province, north of the new North Industrial Park Road, one hundred environmental protection (Fan Qun drying equipment Co., Ltd.) Applicant before: Ding Yuqin |
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