CN105602410B - A kind of antiquing paint and its manufacture craft - Google Patents
A kind of antiquing paint and its manufacture craft Download PDFInfo
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- CN105602410B CN105602410B CN201610182770.1A CN201610182770A CN105602410B CN 105602410 B CN105602410 B CN 105602410B CN 201610182770 A CN201610182770 A CN 201610182770A CN 105602410 B CN105602410 B CN 105602410B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/24—Homopolymers or copolymers of amides or imides
- C09D133/26—Homopolymers or copolymers of acrylamide or methacrylamide
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The present invention provides a kind of antiquing paint and its manufacture craft, is related to paint field, is composed of the following components in parts by weight：A kind of antiquing paint, it is characterised in that count, be made of following components in parts by weight：5 25 parts of epoxy resin, 26 parts of phthalic anhydride, 10 15 parts of polyacrylamide, 8 20 parts of isopropanol, 4 10 parts of titanium dioxide, 25 parts of nano phase ag_2 o, 0.1 0.4 parts of sodium soap, 58 parts of light calcium carbonate powder, 35 parts of kaolin, 0.7 2 parts of coupling agent, 0.5 6 parts of dispersant, 48 parts of defoamer, 3 10 parts of anti-settling agent, 38 parts of thickener, 13 parts of pigment, Tianna solution 5 25,5 15 parts of metal powder, 58 parts of alkyd resin, 55 75 parts of turpentine.Antiquing paint provided by the invention is not easy to crack after coating, glossiness is good, good decorating effect.
Description
Technical field
The invention belongs to paint field, concretely relates to a kind of antiquing paint and its manufacture craft.
Background technology
Paint is that one kind can firmly be covered in body surface, and the chemistry for playing protection, decoration, mark and other specific uses mixes
Compound coating.In present household and craftwork market, modelled after an antique is the direction that people pursue, and general household is coating paint modelled after an antique
Afterwards, it is not required to excessive do old technology with regard to pseudo-classic furniture can be obtained.Therefore antiquing paint is by widespread demand.China's ancient building ingeniously takes day by force
Work, it is exquisite beyond compare, but as time goes by, many ancient buildings are scarred, are badly in need of repairing.But the antiquing paint of in the market
Because of the specificity of execution conditions and environment, often there is easily the shortcomings that cracking, glossiness are low, and decorative effect is not strong.
The content of the invention
In view of this, the present invention provides a kind of antiquing paint and its manufacture craft, easily cracked with improving existing antiquing paint,
The problem of glossiness is low, and decorative effect is poor.
To reach above-mentioned purpose, the technical solution used in the present invention is：
A kind of antiquing paint, is counted in parts by weight, is made of following components：5-25 parts of epoxy resin, phthalic anhydride 2-6
Part, 10-15 parts of polyacrylamide, 8-20 parts of isopropanol, 4-10 parts of titanium dioxide, 2-5 parts of nano phase ag_2 o, sodium soap 0.1-
0.4 part, 5-8 parts of light calcium carbonate powder, 3-5 parts of kaolin, 0.7-2 parts of coupling agent, 0.5-6 parts of dispersant, defoamer 4-8
Part, 3-10 parts of anti-settling agent, 3-8 parts of thickener, 1-3 parts of pigment, Tianna solution 5-25,5-15 parts of metal powder, 5-8 parts of alkyd resin,
55-75 parts of turpentine.
Preferably, in the preferred embodiment, the pigment color is ultramarine or viridescent, the use of these colors
There is more preferable antique effect.
Preferably, in the preferred embodiment, the metal powder is Cu-Zn alloy powder and silver powder mixture, ratio 1-
2：2-5, metal dust is added in finishing coat can make the enhancing of finishing coat stereovision, there is more preferable decorative effect.
Present invention also offers a kind of manufacture craft of above-mentioned antiquing paint, comprise the following steps：
(1) epoxy resin, the phthalic anhydride, the polyacrylamide and the isopropanol is weighed according to quantity to fall
Enter in reaction kettle, it is 300-500r/min to adjust the reaction kettle rotating speed, and stirring 5-10min is rotated at 60-80 DEG C；
(2) continue to add the titanium dioxide, nano phase ag_2 o, the sodium soap, described in toward the reaction kettle
Light calcium carbonate powder, the kaolin, stir 3-8min；
(3) treat that the mixture that step (2) obtains is cooled to 45-60 DEG C, the coupling agent, institute are added into the mixture
Dispersant, the defoamer, the anti-settling agent, the thickener are stated, it is 350-450r/min to adjust the reaction kettle rotating speed, is stirred
1.5-2h is mixed, 20-35 DEG C is cooled to and can obtain semi-finished product；
(4) priming paint is modulated：The semi-finished product, the pigment, the Tianna solution are put into homogenizer 700- by proportioning
It is uniformly mixed under 900r/min；
(5) finishing coat is modulated：The alkyd resin, the metal powder, the turpentine are put into homogenizer by proportioning
It is uniformly mixed under 700-900r/min；
(6) coating process：Polished with 400 mesh sand paper wood product surface, to bottom described in the surface even application
Paint, carries out finishing polishing, finishing coat described in even application again after to be dried.
Preferably, in the preferred embodiment, the priming paint is coated woodwork, coating thickness 0.4-
0.5mm, is polished after coating with the sand paper of 2000 mesh.
Relative to the prior art, beneficial effects of the present invention：Paint pigment coating provided by the invention is strong, fast drying,
It is not easy to crack.Appropriately choose pigment, enhance the antique effect of antiquing paint.Added in finishing coat after coating finishing coat metal powder
Lacquer painting stereovision is enhanced, there is more preferable decorative effect.
Embodiment
Technical solution of the present invention is further described with reference to specific embodiment.
Embodiment 1：
The embodiment of the present invention 1 provides a kind of antiquing paint, counts in parts by weight, is made of following components：Epoxy resin 5
Part, 2 parts of phthalic anhydride, 10 parts of polyacrylamide, 8 parts of isopropanol, 4 parts of titanium dioxide, 2 parts of nano phase ag_2 o, sodium soap
0.1 part, 5 parts of light calcium carbonate powder, 3 parts of kaolin, 0.7 part of coupling agent, 0.5 part of dispersant, 4 parts of defoamer, anti-settling agent 3
Part, 3 parts of thickener, 1 part of pigment, Tianna solution 5,5 parts of metal powder, 5 parts of alkyd resin, 55 parts of turpentine.
Pigment color selected by antiquing paint is ultramarine or viridescent, and the use of these colors has more preferable antique effect.
Metal powder is Cu-Zn alloy powder and silver powder mixture in antiquing paint, ratio 1：2, addition metal dust can make in finishing coat
Finishing coat stereovision strengthens, and has more preferable decorative effect.
The present embodiment additionally provides a kind of preparation method of antiquing paint, comprises the following steps：
(1) epoxy resin, phthalic anhydride, polyacrylamide and isopropanol are weighed according to quantity to pour into reaction kettle, adjust
Reaction kettle rotating speed is 300r/min, and stirring 5min is rotated at 60 DEG C；
(2) continue to add titanium dioxide, nano phase ag_2 o, sodium soap, light calcium carbonate powder, kaolinite in toward reaction kettle
Soil, stirs 3min；
(3) treat that the mixture that step (2) obtains is cooled to 45 DEG C, coupling agent, dispersant, defoaming are added into mixture
Agent, anti-settling agent, thickener, adjustment reaction kettle rotating speed is 350r/min, stirs 1.5h, is cooled to 20 DEG C and can obtain semi-finished product；
(4) priming paint is modulated：Mixed by proportioning input semi-finished product, pigment, Tianna solution under homogenizer 700r/min
It is even；
(5) finishing coat is modulated：Mixed by proportioning input alkyd resin, metal powder, turpentine under homogenizer 700r/min
Close uniform；(6) coating process：Polished with 400 mesh sand paper wood product surface, it is to be dried to surface even application priming paint
Carry out finishing polishing, even application finishing coat again afterwards.
The priming paint of modulation is coated woodwork, and coating thickness 0.4mm, is beaten after coating with the sand paper of 2000 mesh
Mill.
Embodiment 2：
The embodiment of the present invention 2 provides a kind of antiquing paint, counts in parts by weight, is made of following components：Epoxy resin
25 parts, 6 parts of phthalic anhydride, 15 parts of polyacrylamide, 20 parts of isopropanol, 10 parts of titanium dioxide, 5 parts of nano phase ag_2 o, fat
Sour 0.4 part of sodium, 8 parts of light calcium carbonate powder, 5 parts of kaolin, 2 parts of coupling agent, 6 parts of dispersant, 8 parts of defoamer, anti-settling agent 10
Part, 8 parts of thickener, 3 parts of pigment, Tianna solution 25,15 parts of metal powder, 8 parts of alkyd resin, 75 parts of turpentine.
Pigment color selected by antiquing paint is ultramarine or viridescent.The use of these colors has more preferable antique effect.
Metal powder is Cu-Zn alloy powder and silver powder mixture in antiquing paint, ratio 2：5, addition metal dust can make in finishing coat
Finishing coat stereovision strengthens, and has more preferable decorative effect.
The present embodiment additionally provides a kind of preparation method of antiquing paint, comprises the following steps：
(1) epoxy resin, phthalic anhydride, polyacrylamide and isopropanol are weighed according to quantity to pour into reaction kettle, adjust
Reaction kettle rotating speed is 500r/min, and stirring 10min is rotated at 80 DEG C；
(2) continue to add titanium dioxide, nano phase ag_2 o, sodium soap, light calcium carbonate powder, kaolinite in toward reaction kettle
Soil, stirs 8min；
(3) treat that the mixture that step (2) obtains is cooled to 60 DEG C, coupling agent, dispersant, defoaming are added into mixture
Agent, anti-settling agent, thickener, adjustment reaction kettle rotating speed is 450r/min, stirs 2h, is cooled to 35 DEG C and can obtain semi-finished product；
(4) priming paint is modulated：Mixed by proportioning input semi-finished product, pigment, Tianna solution under homogenizer 900r/min
It is even；
(5) finishing coat is modulated：Mixed by proportioning input alkyd resin, metal powder, turpentine under homogenizer 900r/min
Close uniform.
(6) coating process：Polished with 400 mesh sand paper wood product surface, it is to be dried to surface even application priming paint
Carry out finishing polishing, even application finishing coat again afterwards.
The priming paint of modulation is coated woodwork, and coating thickness 0.5mm, is beaten after coating with the sand paper of 2000 mesh
Mill.
Embodiment 3：
The embodiment of the present invention 3 provides a kind of antiquing paint, counts in parts by weight, is made of following components：Epoxy resin
15 parts, 4 parts of phthalic anhydride, 12 parts of polyacrylamide, 14 parts of isopropanol, 7 parts of titanium dioxide, 3 parts of nano phase ag_2 o, aliphatic acid
0.2 part of sodium, 6 parts of light calcium carbonate powder, 4 parts of kaolin, 1.3 parts of coupling agent, 3.3 parts of dispersant, 6 parts of defoamer, anti-settling agent 7
Part, 5 parts of thickener, 2 parts of pigment, Tianna solution 15,10 parts of metal powder, 7 parts of alkyd resin, 65 parts of turpentine.
Pigment color selected by antiquing paint is ultramarine or viridescent.The use of these colors has more preferable antique effect.
Metal powder is Cu-Zn alloy powder and silver powder mixture in antiquing paint, ratio 1.5：3.5, metal dust is added in finishing coat
It can strengthen finishing coat stereovision, there is more preferable decorative effect.
The present embodiment additionally provides a kind of preparation method of antiquing paint, comprises the following steps：
(1) epoxy resin, phthalic anhydride, polyacrylamide and isopropanol are weighed according to quantity to pour into reaction kettle, adjust
Reaction kettle rotating speed is 400r/min, and stirring 7min is rotated at 70 DEG C；
(2) continue to add titanium dioxide, nano phase ag_2 o, sodium soap, light calcium carbonate powder, kaolinite in toward reaction kettle
Soil, stirs 5min；
(3) treat that the mixture that step (2) obtains is cooled to 52 DEG C, coupling agent, dispersant, defoaming are added into mixture
Agent, anti-settling agent, thickener, adjustment reaction kettle rotating speed is 4000r/min, stirs 1.2h, is cooled to 27 DEG C and can obtain semi-finished product；
(4) priming paint is modulated：Mixed by proportioning input semi-finished product, pigment, Tianna solution under homogenizer 800r/min
It is even；
(5) finishing coat is modulated：Mixed by proportioning input alkyd resin, metal powder, turpentine under homogenizer 800r/min
Close uniform.
(6) coating process：Polished with 400 mesh sand paper wood product surface, it is to be dried to surface even application priming paint
Carry out finishing polishing, even application finishing coat again afterwards.
The priming paint of modulation is coated woodwork, coating thickness 0.45mm, is carried out after coating with the sand paper of 2000 mesh
Polishing.
Salt spray test when adhesive force and 24 to the finished product progress after the paint application obtained by embodiment 1-3 are small, salt fog
Effect is tested to be represented by defect area A (sample surfaces defect accounts for the percentage of the gross area).Found by contrasting, the institute of embodiment 3
The finished product strong adhesive force obtained, it is not easy to crack, there is more preferable glossiness.
| Embodiment | Adhesive force (come off degree) | Defect area A (%) |
| Embodiment 1 | 6% | 0.11 |
| Embodiment 2 | 7% | 0.12 |
| Embodiment 3 | 5% | 0.09 |
Claims (2)
1. a kind of antiquing paint, it is characterised in that count, be made of following components in parts by weight：5-25 parts of epoxy resin, adjacent benzene two
2-6 parts of formic anhydride, 10-15 parts of polyacrylamide, 8-20 parts of isopropanol, 4-10 parts of titanium dioxide, 2-5 parts of nano phase ag_2 o, fat
Sour sodium 0.1-0.4 parts, 5-8 parts of light calcium carbonate powder, 3-5 parts of kaolin, 0.7-2 parts of coupling agent, 0.5-6 parts of dispersant, disappear
4-8 parts of infusion, 3-10 parts of anti-settling agent, 3-8 parts of thickener, 1-3 parts of pigment, 5-25 parts of Tianna solution, 5-15 parts of metal powder, alkyd tree
5-8 parts of fat, 55-75 parts of turpentine；
Pigment color described above is ultramarine or viridescent；
Metal powder described above is Cu-Zn alloy powder and silver powder mixture, mass ratio 1-2：2-5；
The manufacture craft of antiquing paint described above, comprises the following steps：
(1) epoxy resin, the phthalic anhydride, the polyacrylamide and the isopropanol is weighed according to quantity to pour into instead
Answer in kettle, it is 300-500r/min to adjust the reaction kettle rotating speed, and stirring 5-10min is rotated at 60-80 DEG C；
(2) continue to add the titanium dioxide, the nano phase ag_2 o, the sodium soap, the lightweight in toward the reaction kettle
Calcium carbonate powder, the kaolin, stir 3-8min；
(3) treat that the mixture that step (2) obtains is cooled to 45-60 DEG C, added into the mixture coupling agent, described point
Powder, the defoamer, the anti-settling agent, the thickener, it is 350-450r/min to adjust the reaction kettle rotating speed, stirring
1.5-2h, is cooled to 20-35 DEG C and can obtain semi-finished product；
(4) priming paint is modulated：The semi-finished product, the pigment, the Tianna solution are put into homogenizer 700-900r/ by proportioning
It is uniformly mixed under min；
(5) finishing coat is modulated：The alkyd resin, the metal powder, the turpentine are put into homogenizer 700- by proportioning
It is uniformly mixed under 900r/min；
(6) coating process：Polished wood product surface with 400 mesh sand paper, to priming paint described in the surface even application, treated
Finishing polishing, finishing coat described in even application are carried out after drying again.
2. antiquing paint as claimed in claim 1, the priming paint is coated woodwork, coating thickness 0.4-0.5mm, applies
Polished after covering with the sand paper of 2000 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610182770.1A CN105602410B (en) | 2016-03-28 | 2016-03-28 | A kind of antiquing paint and its manufacture craft |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610182770.1A CN105602410B (en) | 2016-03-28 | 2016-03-28 | A kind of antiquing paint and its manufacture craft |
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| Publication Number | Publication Date |
|---|---|
| CN105602410A CN105602410A (en) | 2016-05-25 |
| CN105602410B true CN105602410B (en) | 2018-05-11 |
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| CN201610182770.1A Active CN105602410B (en) | 2016-03-28 | 2016-03-28 | A kind of antiquing paint and its manufacture craft |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106380913A (en) * | 2016-09-26 | 2017-02-08 | 笪亚臣 | Wardrobe surface environment-friendly paint and preparation method thereof |
| CN106675269B (en) * | 2017-01-05 | 2018-08-31 | 广东绿色大地化工有限公司 | A kind of aqueous antique artistic paint and preparation method thereof |
| CN106752731A (en) * | 2017-02-24 | 2017-05-31 | 东莞市榴花艺术有限公司 | A kind of imitative wood paint |
| CN110484092A (en) * | 2019-08-09 | 2019-11-22 | 湖州南浔鑫荣木业有限公司 | A kind of fire-retardant paint for wood furniture |
| CN110564298A (en) * | 2019-08-09 | 2019-12-13 | 湖州南浔鑫荣木业有限公司 | antique paint with repairing function |
| CN111361342A (en) * | 2020-04-16 | 2020-07-03 | 邢台市洛宸牌匾碑刻艺术有限公司 | Method for engraving convex book body |
| CN115260898A (en) * | 2022-07-29 | 2022-11-01 | 武汉雅美佳联合新材料有限公司 | High-temperature-resistant water-based multi-layer antique paint and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103305096B (en) * | 2013-07-09 | 2016-02-17 | 湖南太子化工涂料有限公司 | A kind of Multifunctional undercoat and preparation method thereof |
| CN104449272B (en) * | 2014-10-09 | 2016-08-31 | 安徽省孟府家工艺品有限公司 | A kind of paint modelled after an antique |
| CN104384088B (en) * | 2014-11-13 | 2016-11-09 | 厦门建霖工业有限公司 | A kind of electroless plating metal surface treating method modelled after an antique |
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2016
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