CN106237831A - A kind of manufacture method of natural plant essential oils taste removal plate - Google Patents

A kind of manufacture method of natural plant essential oils taste removal plate Download PDF

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Publication number
CN106237831A
CN106237831A CN201610713091.2A CN201610713091A CN106237831A CN 106237831 A CN106237831 A CN 106237831A CN 201610713091 A CN201610713091 A CN 201610713091A CN 106237831 A CN106237831 A CN 106237831A
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Prior art keywords
taste removal
manufacture method
essential oils
natural plant
removal plate
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CN201610713091.2A
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Chinese (zh)
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孙勤龙
孙明
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Individual
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/84Biological processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/46Removing components of defined structure
    • B01D53/72Organic compounds not provided for in groups B01D53/48 - B01D53/70, e.g. hydrocarbons
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/20Halogens or halogen compounds
    • B01D2257/206Organic halogen compounds
    • B01D2257/2064Chlorine
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/40Nitrogen compounds
    • B01D2257/404Nitrogen oxides other than dinitrogen oxide
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/50Carbon oxides
    • B01D2257/502Carbon monoxide
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2258/00Sources of waste gases
    • B01D2258/06Polluted air
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Biomedical Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to the manufacture method of a kind of natural plant essential oils taste removal plate, plant is placed on ice, add solvent, it is placed in mortar by liquid nitrogen grinding, adding after grinding in extracting solution and stand 3~4h on ice, low temperature, with centrifuge, centrifugal speed be 11100rpm/20min temperature be 4~10 DEG C, extract and obtain supernatant and obtain phytoprotein enzyme.Take protease and water preparation, take again 2ml be added drop-wise to 15mm × 20mm fiber scraps of paper suction float, constantly evaporate through 54 DEG C~56 DEG C controllable temperatures of heater, reach taste removal except special-effect, " eat " indoor 98% carbon monoxide, the formaldehyde of 99%, the hyponitric acid of 92%, absorb the benzene of 92%, the trichloro ethylene of 90%.

Description

A kind of manufacture method of natural plant essential oils taste removal plate
Technical field
The present invention relates to field of deodorization, particularly relate to the manufacture method of a kind of natural plant essential oils taste removal plate.
Background technology
In recent decades, along with expanding economy and the raising of human living standard, curb environmental pollution the most more to come More become a global difficult problem.During curbing environmental pollution, people have employed various method, achieves A large amount of successfully experiences.And in the practice process processing debirs, biological method the most gradually gets the nod, and becomes main flow Processing method.
The most commonly used chemistry management for using chemical drugs and harmful gas to show effect chemical change, as photocatalyst, Formaldehyde remover, gram benzene spirit, eliminating smell agent etc. aoxidize the gas being contaminated;And biological management absorbs in air for selection plant Harmful gas, or carry out biological oxidation, decomposition with microorganism, enzyme.
Current the Main Developed Countries such as U.S., Japan etc., had more ripe scientific achievement in this respect.And it is big by meaning Headed by sharp famous biology teaches the western doctor of Beaune, the research group being made up of France, Italy, Switzerland biology expert, 10 " enzyme can the nation " preparation (MAKERPAN) developed on the Research foundation in remaining year is then handsome person therein.Up to now, it has been It is widely used in the various fields such as industry all over the world, civilian, animal husbandry and agricultural, and in all many environmental issues On serve the effect of brilliance, the technical barrier in terms of successfully utilizing biotechnology to solve many environmental protection." enzyme can nation " be raw The dozens of formula of produce product, not only helps people to solve formaldehyde odor and sanitary sewage, municipal refuse, zootechnical waste, Also solve the difficult problem of environmental protections such as river, city body pollution, sewage ditch, petrifaction sewage for us and provide an effective way.
Its advantage is many: avirulence, non-corrosiveness, the danger of non-secondary pollution;To organic degraded more Add quickly;Its full spectrum microorganism can play a role, even in the condition having various polluter under aerobic and anaerobic state Under can also degradation of organic substances;There is no any special requirement in using or avoid by scope, easy to operate, simple.
Universal along with environmental protection knowledge, the noun such as air detection, formaldehyde improvement is come into huge numbers of families, is increasingly paid close attention to indoor Environmental health problems.Activated carbon has formaldehyde adsorption, people easy to use accept, and is situated between according to the staff of certain activated carbon producer Continue, the activated carbon of high-quality be utilize Linesless charcoal, bamboo charcoal, various shell and rare ore deposit soil etc. as raw material, at high temperature at a temperature of dry Dry, by its organic organization's carbonization.The most physically or chemically form completes activation process, is formed and has pore structure prosperity, huge Specific surface area, the feature such as high iodine number, harmful substance in adsorbable air.
Photocatalyst is except the principle of formaldehyde.It is the construction technology by specialty, and the spray of titanium dioxide aqueous solution is implanted in pollution The surface in source.Then under the irradiation of light, surface excitation goes out electronics, and electronics reacts with the water in air, generates hydrogen and oxygen Free radical.It easily and contains hydrogen or the reaction of decomposing of oxygen in chemical formula, generate and carbon dioxide and water.Such that it is able to Effectively decompose the harmful gass such as the formaldehyde in air, benzene, TVOC.Enzyme is except the principle of formaldehyde.Enzyme is from plant The protein of middle extraction, and the harmful gass such as formaldehyde are dissolved in protein, so enzyme can reduce to a certain extent Indoor formaldehyde equal size.But enzyme the most just occurs, from the principle, formaldehyde can be removed, but be necessarily required to Long-term spraying, just can have certain effect, if only sprayed once, is the pollutant that at all cannot remove indoor, and And a lot of companies all say that the product of oneself is enzyme on the market, but real enzyme is few, and a lot of companies hang Caput Caprae seu ovis and sell Canis familiaris L. Meat, consumer must remove the scales from eyes.There is Urine scent ability.
And use natural plants to carry out pollution control, not only environmental protection but also safety.Aspidlsiraelatior, Monstera deliciosa can root out having in air Pest matter, tiger bracketplant, the absorbable formaldehyde of indoor more than 80% of bracketplant, moreover it is possible to the carbon monoxide of " eating " indoor 96%, the mistake of 86% Nitrogen oxide;Aloe then can absorb 1 cubic metres of air always contained 90% formaldehyde.Milan, Chimonanthus praecox (L.) Link. etc. can be rooted out in air effectively Sulfur dioxide, the nuisance such as carbon monoxide.The cilium of the plants such as Cymbidium ensifolium (L.) Sw., Flos Osmanthi Fragrantis, Chimonanthus praecox (L.) Link. can retain and absorb and retain wafing in air Floating microgranule and flue dust.Hedera nepalensis var.sinensis, Cycas revoluta can in effective absorption chamber 85% benzene and 60% trichloro ethylene.Rhizoma Arisaematis also can absorb The benzene of 80%, the trichloro ethylene of 50%.Therefore, solve the problems referred to above to be just particularly important.
Summary of the invention
The problem existed for above-mentioned prior art, it is an object of the invention to provide a kind of natural plant essential oils taste removal plate Manufacture method, by processing natural plants, enables natural plants to clear up indoor air, solves chemistry Process and the problem of biological treatment existence.
The present invention provides the manufacture method of a kind of natural plant essential oils taste removal plate, and described manufacturing step is as follows:
Step one: be put on ice for by plant, after adding solution, is placed in mortar and uses liquid nitrogen grinding;
Step 2: add after grinding in extracting solution and stand 3~4h on ice;
Step 3: be centrifuged standing liquid with centrifuge, extraction obtains supernatant and obtains phytoprotein enzyme;
Step 4: taking protease and water preparation is dissolved, then take 2ml solution, the suction dripping to 15mm × 20mm fiber scraps of paper is floated;
Step 5: constantly evaporate through heater, reaches indoor and outdoor taste removal special-effect.
Further improvement is that: the plant in described step one is Aspidlsiraelatior, Monstera deliciosa, tiger bracketplant, bracketplant, Milan, cured One or more combinations therein of prunus mume (sieb.) sieb.et zucc., Hedera nepalensis var.sinensis, Cycas revoluta and Rhizoma Arisaematis.
Further improvement is that: the solvent in described step one be ethanol, ethyl acetate, acetone, petroleum ether, methanol and DMF one or more combinations therein.
Further improvement is that: in described step 3, the running parameter of centrifuge is 8000rpm/40min or 11100rpm/ 20min/, the operating temperature of centrifuge is-4~10 DEG C.
Further improvement is that: in described step 5, the temperature of heater is 40 DEG C~100 DEG C.
The invention has the beneficial effects as follows: by above-mentioned process, solving phytoprotein enzyme, not reach temperature unvaporized Problem;Solve and solved taste removal degasification taste by spraying at that time, it is impossible to the problem of long-acting taste removal;The method natural plant product, nothing Poison is tasteless, and continuous action is safe and reliable, is 500 times of effects of activated carbon.
Detailed description of the invention
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, this embodiment It is only used for explaining the present invention, is not intended that limiting the scope of the present invention.
Embodiment one:
By plant (Aspidlsiraelatior, Monstera deliciosa, tiger bracketplant, bracketplant) 100Kg, it is placed on ice, puts into 500L and grind in still, add Acetone 350Kg, is placed in mortar by liquid nitrogen grinding, adds and stand 3h in extracting solution on ice after grinding, temperature at-6 DEG C, with from Scheming is centrifuged, and centrifugal speed is 11100rpm/20min, and temperature is 4 DEG C, and extraction obtains supernatant and obtains phytoprotein enzyme 520g, content 99.9%.Taking protease is 0.05g, is dissolved in 100ml water, takes 2ml and is added drop-wise to 15mm × 20mm fibrous paper The suction of sheet is floated, and constantly evaporates through 54 DEG C~56 DEG C controllable temperatures of heater, reaches taste removal except special-effect, " eating " indoor The carbon monoxide of 95%, the formaldehyde of 99%, the hyponitric acid of 95%, absorb the benzene of 90%, the trichloro ethylene of 92%.
Embodiment two:
By plant (Milan, Chimonanthus praecox (L.) Link.) 100Kg, it is placed on ice, puts into 500L and grind in still, add acetone 350Kg, be placed on mortar Middle liquid nitrogen grinding, adds in extracting solution after grinding and stands 3h on ice, and temperature is at-6 DEG C, by centrifuge, centrifugal speed For 11100rpm/20min, temperature is 4 DEG C, and extraction obtains supernatant and obtains phytoprotein enzyme 480g, content 99.9%.Take egg White matter enzyme is 0.05g, is dissolved in 100ml water, take 2ml be added drop-wise to 15mm × 20mm fiber scraps of paper suction float, through heater 54 DEG C~56 DEG C of controllable temperatures constantly evaporate, and reach taste removal except special-effect, the carbon monoxide of " eating " indoor 97%, the first of 99% Aldehyde, the hyponitric acid of 92%, absorb the benzene of 94%, the trichloro ethylene of 93%.
Embodiment three:
By plant (Hedera nepalensis var.sinensis, Cycas revoluta) 100Kg, it is placed on ice, puts into 500L and grind in still, add acetone 350Kg, be placed on and grind By liquid nitrogen grinding in alms bowl, adding in extracting solution and stand 3h on ice after grinding, temperature is at-6 DEG C, by centrifuge, centrifugal speed Degree is 11100rpm/20min, and temperature is 4 DEG C, and extraction obtains supernatant and obtains phytoprotein enzyme 580g, content 99.9%.Take Protease is 0.05g, is dissolved in 100ml water, take 2ml be added drop-wise to 15mm × 20mm fiber scraps of paper suction float, through heating 54 DEG C~56 DEG C controllable temperatures of device constantly evaporate, reach taste removal except special-effect, the carbon monoxide of " eating " indoor 98%, 99% Formaldehyde, the hyponitric acid of 92%, absorb the benzene of 94%, the trichloro ethylene of 92%.
Embodiment four:
By plant (Rhizoma Arisaematis) 100Kg, it is placed on ice, puts into 500L and grind in still, add acetone 350Kg, be placed in mortar By liquid nitrogen grinding, adding in extracting solution and stand 3h on ice after grinding, temperature is at-6 DEG C, and with centrifuge, centrifugal speed is 11100rpm/20min, temperature is 4 DEG C, and extraction obtains supernatant and obtains phytoprotein enzyme 460g, content 99.9%.Take albumen Matter enzyme is 0.05g, is dissolved in 100ml water, take 2ml be added drop-wise to 15mm × 20mm fiber scraps of paper suction float, through heater 54 DEG C~56 DEG C of controllable temperatures constantly evaporate, reach taste removal except special-effect, the carbon monoxide of " eating " indoor 98%, the first of 99% Aldehyde, the hyponitric acid of 92%, absorb the benzene of 92%, the trichloro ethylene of 90%.

Claims (5)

1. the manufacture method of a natural plant essential oils taste removal plate, it is characterised in that: described manufacturing step is as follows:
Step one: be put on ice for by plant, after adding solution, is placed in mortar and uses liquid nitrogen grinding;
Step 2: add after grinding in extracting solution and stand 3~4h on ice;
Step 3: be centrifuged standing liquid with centrifuge, extraction obtains supernatant and obtains phytoprotein enzyme;
Step 4: taking protease and water preparation is dissolved, then take 2ml solution, the suction dripping to 15mm × 20mm fiber scraps of paper is floated;
Step 5: constantly evaporate through heater, reaches indoor and outdoor taste removal special-effect.
The manufacture method of a kind of natural plant essential oils taste removal plate the most as claimed in claim 1, it is characterised in that: described step one In plant be Aspidlsiraelatior, Monstera deliciosa, tiger bracketplant, bracketplant, Milan, Chimonanthus praecox (L.) Link., Hedera nepalensis var.sinensis, Cycas revoluta and Rhizoma Arisaematis one therein or Multiple combination.
The manufacture method of a kind of natural plant essential oils taste removal plate the most as claimed in claim 1, it is characterised in that: described step one In solvent be ethanol, ethyl acetate, acetone, petroleum ether, methanol and DMF therein one or more combination.
The manufacture method of a kind of natural plant essential oils taste removal plate the most as claimed in claim 1, it is characterised in that: described step 3 The running parameter of middle centrifuge is 8000rpm/40min or 11100rpm/20min/, and the operating temperature of centrifuge is-4~10 ℃。
The manufacture method of a kind of natural plant essential oils taste removal plate the most as claimed in claim 1, it is characterised in that: described step 5 The temperature of middle heater is 40 DEG C~100 DEG C.
CN201610713091.2A 2016-08-24 2016-08-24 A kind of manufacture method of natural plant essential oils taste removal plate Pending CN106237831A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108940223A (en) * 2018-08-04 2018-12-07 安徽科浦环保科技有限公司 A kind of preparation method of the compound scavenger of indoor formaldehyde
CN109432979A (en) * 2018-10-12 2019-03-08 福建省居乐康环保科技有限公司 A kind of scavenger with efficient formaldehyde purification function

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102698305A (en) * 2012-05-25 2012-10-03 上海复振科技有限公司 Botanical compound odor-removal antibacterial solution and preparation method and application thereof
CN105013319A (en) * 2015-08-06 2015-11-04 常州思宇环保材料科技有限公司 Biological agent for removing low-content formaldehyde
CN105126602A (en) * 2015-08-17 2015-12-09 王平 Manufacturing method of controlled natural biological odor-removal formaldehyde-removal product

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102698305A (en) * 2012-05-25 2012-10-03 上海复振科技有限公司 Botanical compound odor-removal antibacterial solution and preparation method and application thereof
CN105013319A (en) * 2015-08-06 2015-11-04 常州思宇环保材料科技有限公司 Biological agent for removing low-content formaldehyde
CN105126602A (en) * 2015-08-17 2015-12-09 王平 Manufacturing method of controlled natural biological odor-removal formaldehyde-removal product

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108940223A (en) * 2018-08-04 2018-12-07 安徽科浦环保科技有限公司 A kind of preparation method of the compound scavenger of indoor formaldehyde
CN109432979A (en) * 2018-10-12 2019-03-08 福建省居乐康环保科技有限公司 A kind of scavenger with efficient formaldehyde purification function

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