CN106236611B - A kind of preparation method of tomato seed oil micro emulsion facial mask - Google Patents
A kind of preparation method of tomato seed oil micro emulsion facial mask Download PDFInfo
- Publication number
- CN106236611B CN106236611B CN201610675542.8A CN201610675542A CN106236611B CN 106236611 B CN106236611 B CN 106236611B CN 201610675542 A CN201610675542 A CN 201610675542A CN 106236611 B CN106236611 B CN 106236611B
- Authority
- CN
- China
- Prior art keywords
- tomato seed
- seed oil
- weight
- parts
- micro emulsion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Engineering & Computer Science (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation method of tomato seed oil micro emulsion facial mask, (1) first mixes xanthan gum and glycerol, and the mixture of the Tween 80, coconut oil, vaseline and the deionized water that have been pre-mixed is added in (2)；(3) dimethicone ethoxy urea is mixed simultaneously；(4) material stirring made from above-mentioned (2) and (3) two kinds is emulsified, is eventually adding tomato seed oil micro emulsion, stirs to get tomato seed oil micro emulsion facial mask.This product has character sense organ good, when application facial mask easy to form, the features such as without sticking soapy feeling, being comfortable on, cleaning is relatively easy to after application.
Description
Technical field
The present invention relates to a kind of preparation method of cosmetics, especially a kind of preparation method of tomato seed oil micro emulsion facial mask.
Background technique
Tomato also known as tomato tomato are Solanaceae annual herb plants.The total working ability of Xinjiang Tomatoes sauce in 2012
About 1,600,000 tons, generate about 200,000 tons of tomato skin seeds (dry weight meter) in process of production, wherein in Tomato Seed containing it is abundant fat,
Protein and cellulose etc., in the past lower to the comprehensive utilization degree of Tomato Seed, added value is lower, and existing research shows that kind
Eggplant seed cannot only be applied in the feed of livestock and poultry, can also be used to extract tomato seed oil, protein and cellulose etc..Many institute's weeks
Know, in tomato seed oil in addition to rich in unsaturated fatty acid (82%), also contains vitamin E, phytosterol carotenoid and tomato
The nutritional ingredients such as red pigment, and have and prevent and inhibit cancer, inhibit that mutagenesis, protection is cardiovascular, prevent cataract and adjusts body
The physiological functions such as immune are a kind of Special Plant greases full of nutrition.Therefore, how sufficiently effective development and utilization Tomato Seed
Oil is current urgent problem to be solved.
Tomato seed oil is drying oil, and wherein unsaturated fatty acid, tocopherol and other a variety of natural liposoluble vitamins can
Promote the cytothesis of body internal layer, repair subcutaneous damaged cell, enhance the self-renewing of skin, may also suppress ultraviolet light enliven because
Injury of the son to skin reinforces skin and supports anti-ultraviolet ability, adjust skin water and oil balance, inhibit under skin aging and elasticity
Drop.It is well known that tomato seed oil is deep by vast consumption due to the content of Ve (450-700mg/kg) and unsaturated fatty acid are higher
Person's favor, wherein vitamin E is a kind of excellent antioxidant and nutriment, is easy to be absorbed by the skin, be usually used in skin care item,
In facial cleanser, suncream.Vitamin E is added in skin care item to compete lipid peroxidation with the unsaturated fatty acid in formula,
Free radical chain reactions are blocked, lipid peroxidation is terminated, protects the oxidation of unsaturated fatty acid；Vitamin E is applied to skin simultaneously
The metabolism that can promote skin on skin, prevents pigementation, improves skin elasticity, with skin care, beauty, anti-aging function
Effect, therefore, it has become the favorites in cosmetic formulations, and therefore, tomato seed oil can serve as matrix oil in skin care item and provide fertility
The dual role of phenol, the advantage for having industry addition VE incomparable.
Therefore, develop a kind of adaptation market, there are preferable market prospects, when character sense organ good application face easy to form
Film is comfortable on without soapy feeling is sticked, and the tomato seed oil micro emulsion facial mask that cleaning is relatively easy to after application is imperative.
Summary of the invention
A kind of preparation method of tomato seed oil micro emulsion facial mask, it is characterised in that: the following steps are included:
The xanthan gum of (1) 1~3 parts by weight and the glycerol of 6~9 parts by weight, under magnetic agitation effect uniformly, whipping temp
It is 25~35 DEG C, 250~350r/min of speed of agitator；
(2) after (1) step sample is uniform, the Tween 80 for 1~3 parts by weight that addition has been pre-mixed, 1.5~3.5
The mixture and uniform stirring of the deionized water of the vaseline and 30~50 parts by weight of the coconut oil of parts by weight and 1~3 parts by weight,
Later in 60~85 DEG C of 20~30min of water bath with thermostatic control；
(3) by the ethoxy urea of the dimethicone of 1~3 parts by weight and 8~15 parts by weight, under magnetic agitation effect
Uniformly, whipping temp be 25~35 DEG C, 250~350r/min of speed of agitator, after mixing evenly 60~85 DEG C of waters bath with thermostatic control 20~
30min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp 60
~85 DEG C, 400~600r/min of speed of agitator, 5~8min of emulsification is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room in 400~600r/min of magnetic agitation rotating speed effect
Then the tomato seed oil micro emulsion of 25~35 parts by weight is added in temperature, continue to stir evenly under magnetic agitation effect, whipping temp is
60~85 DEG C, 400~600r/min of speed of agitator, tomato seed oil micro emulsion facial mask can be obtained.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 1.5~3 parts by weight tomato seed oils being mixed, the surface is living
Property agent include A and B, A be polysorbas20, polysorbate40, polysorbate60 perhaps in Tween 80 one in B be dehydrated alcohol, normal propyl alcohol or
One of isopropanol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 25 DEG C~30 DEG C, mixing time 5
~10 minutes；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 30~60r/min and persistently stirs, and
Be added 1.5~3.5 parts by weight deionized water, at 25 DEG C~30 DEG C of temperature according to 0.1~1 drop/sec speed dropwise addition go from
Sub- 6~8min of water later speeds rate of addition to 2~4 drops/sec, and 2~6min clarification is added dropwise, and stops adding water, gained after clarification
Supernatant liquid is tomato seed oil micro emulsion.
Surfactant A and B are mixed according to the ratio of 1~3:1.
A is Tween 80, and B is dehydrated alcohol.
Above-mentioned tomato seed oil is the tomato seed oil obtained using cold pressing process, the specific process is as follows: after taking cleaning impurity elimination
After Tomato Seed toasts 30-60min in 50-60 DEG C of environment, investment cold pressing expeller is squeezed, and holding cold pressing expeller extruder temperature is
It 50-55 DEG C, repeats to squeeze 2 times, collects expressed oil and removing solid residue is centrifuged, refined through low-temperature physics, i.e. object
Degumming: tomato seed oil: active carbon=20:1, pH4.5,48.2 DEG C is managed, 46min is adsorbed；Adsorption deacidification: tomato seed oil: cellulose
Sill=20:1, pH4.5,50-55 DEG C, under the mixing speed of 25-35r/min, adsorption deacidification 30min obtains cold press tomato
Seed oil.
The tomato seed oil micro emulsion facial mask character sense organ prepared by above-mentioned condition is good, when application facial mask easy to form, without glutinous
Soapy feeling is comfortable on, and is relatively easy to clean after application.
Specific embodiment
Embodiment 1: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 1 parts by weight and the glycerol of 6 parts by weight, under magnetic agitation effect uniformly, whipping temp 25
DEG C, speed of agitator 250r/min；
(2) after (1) step sample is uniform, the Tween 80s of 1 parts by weight, 1.5 parts by weight being pre-mixed is added
The mixture and uniform stirring of the deionized water of the vaseline and 30 parts by weight of coconut oil and 1 parts by weight, later in 60 DEG C of constant temperature
Water-bath 20min；
(3) the ethoxy urea of the dimethicone of 1 parts by weight and 8 parts by weight under magnetic agitation effect is uniformly stirred
Mixing temperature is 25 DEG C, speed of agitator 250r/min, after mixing evenly 60 DEG C of water bath with thermostatic control 20min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp 60
DEG C, speed of agitator 400r/min stands emulsification 5min after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 400r/min effect, so
The tomato seed oil micro emulsion of 25 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 60 DEG C, stirring
Tomato seed oil micro emulsion facial mask can be obtained in revolving speed 400r/min.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 1.5 parts by weight tomato seed oils being mixed, the surface-active
Agent is polysorbas20, dehydrated alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 25 DEG C, mixing time 5 minutes；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 30r/min and persistently stirs, and is added
Deionized water 6min is added dropwise according to 0.1 drop/sec of speed at 25 DEG C of temperature in the deionized water of 1.5 parts by weight, will be added dropwise later
Speed is speeded to 2 drops/sec, and 2min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are tomato seed oil micro emulsion.
Surface active agent tween 20, dehydrated alcohol are mixed according to the ratio of 1:1.
Embodiment 2: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 1.2 parts by weight and the glycerol of 6.35 parts by weight, under magnetic agitation effect uniformly, whipping temp
It is 26 DEG C, speed of agitator 260r/min；
(2) after (1) step sample is uniform, Tween 80,2.5 parts by weight of 2.2 parts by weight being pre-mixed are added
Coconut oil and 2.2 parts by weight vaseline and 40 parts by weight deionized water mixture and uniform stirring, later at 74 DEG C
Water bath with thermostatic control 25min；
(3) by the ethoxy urea of the dimethicone of 1.8 parts by weight and 11.2 parts by weight, under magnetic agitation effect
Even, whipping temp is 29 DEG C, speed of agitator 300r/min, after mixing evenly 71 DEG C of water bath with thermostatic control 24min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp 63
DEG C, speed of agitator 420r/min stands emulsification 5.3min after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 420r/min effect, so
The tomato seed oil micro emulsion of 26 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 62.8 DEG C, is stirred
Revolving speed 420r/min is mixed, tomato seed oil micro emulsion facial mask can be obtained.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 1.98 parts by weight tomato seed oils being mixed, the surface-active
Agent includes polysorbate40, normal propyl alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 25.5 DEG C, and mixing time 5.5 is divided
Clock；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 41r/min and persistently stirs, and is added
Deionized water 6.66min is added dropwise according to 0.4 drop/sec of speed at 26.5 DEG C of temperature, later in the deionized water of 2.16 parts by weight
Rate of addition is speeded to 2.66 drops/sec, 3.4min clarification is added dropwise, stops after clarification plus water, gained supernatant liquid is Tomato Seed
Oil microemulsion.
Surface active agent tween 40, normal propyl alcohol are mixed according to the ratio of 1.2:1.
Embodiment 3: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 2.4 parts by weight and the glycerol of 8.1 parts by weight, under magnetic agitation effect uniformly, whipping temp is
31 DEG C, speed of agitator 330r/min；
(2) after (1) step sample is uniform, Tween 80,1.9 parts by weight of 1.4 parts by weight being pre-mixed are added
Coconut oil and 1.4 parts by weight vaseline and 34 parts by weight deionized water mixture and uniform stirring, later 65.6
DEG C water bath with thermostatic control 22min；
(3) by the ethoxy urea of the dimethicone of 1.4 parts by weight and 9.6 parts by weight, under magnetic agitation effect
Even, whipping temp is 27 DEG C, speed of agitator 280r/min, after mixing evenly 65.6 DEG C of water bath with thermostatic control 22min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is
71.1 DEG C, speed of agitator 490r/min, emulsification 6.2min is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 440r/min effect, so
The tomato seed oil micro emulsion of 27 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 65.6 DEG C, is stirred
Revolving speed 440r/min is mixed, tomato seed oil micro emulsion facial mask can be obtained.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 1.82 parts by weight tomato seed oils being mixed, the surface-active
Agent includes Tween 80, isopropanol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 27 DEG C, mixing time 7 minutes；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 57r/min and persistently stirs, and is added
Deionized water 7.8min is added dropwise according to 0.9 drop/sec of speed at 29 DEG C of temperature in the deionized water of 3.26 parts by weight, later will
Rate of addition is speeded to 3.8 drops/sec, and 5.6min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are that tomato seed oil is micro-
Cream.
Surface active agent tween 80, isopropanol are mixed according to the ratio of 1.4:1.
Embodiment 4: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 1.6 parts by weight and the glycerol of 7.05 parts by weight, under magnetic agitation effect uniformly, whipping temp
It is 28 DEG C, speed of agitator 290r/min；
(2) after (1) step sample is uniform, Tween 80,2.9 parts by weight of 2.6 parts by weight being pre-mixed are added
Coconut oil and 2.6 parts by weight vaseline and 44 parts by weight deionized water mixture and uniform stirring, later at 80 DEG C
Water bath with thermostatic control 27min；
(3) by the ethoxy urea of the dimethicone of 1.6 parts by weight and 10.4 parts by weight, under magnetic agitation effect
Even, whipping temp is 28 DEG C, speed of agitator 290r/min, after mixing evenly 68.4 DEG C of water bath with thermostatic control 23min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is
68.4 DEG C, speed of agitator 470r/min, emulsification 5.9min is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 470r/min effect, so
The tomato seed oil micro emulsion of 25~35 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp 68.4
DEG C, tomato seed oil micro emulsion facial mask can be obtained in speed of agitator 470r/min.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 1.66 parts by weight tomato seed oils being mixed, the surface-active
Agent includes polysorbas20, normal propyl alcohol
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 26.5 DEG C, and mixing time 6.5 is divided
Clock；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 34r/min and persistently stirs, and is added
Deionized water 6.2min is added dropwise according to 0.2 drop/sec of speed at 25.5 DEG C of temperature, later in the deionized water of 1.72 parts by weight
Rate of addition is speeded to 2.2 drops/sec, 2.4min clarification is added dropwise, stops after clarification plus water, gained supernatant liquid is tomato seed oil
Micro emulsion.
Surface active agent tween 20, normal propyl alcohol are mixed according to the ratio of 1.6:1.
Embodiment 5: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 1.8 parts by weight and the glycerol of 7.4 parts by weight, under magnetic agitation effect uniformly, whipping temp is
29 DEG C, speed of agitator 300r/min；
(2) after (1) step sample is uniform, Tween 80,2.3 parts by weight of 1.8 parts by weight being pre-mixed are added
Coconut oil and 1.8 parts by weight vaseline and 38 parts by weight deionized water mixture and uniform stirring, later 71.1
DEG C water bath with thermostatic control 24min；
(3) by the ethoxy urea of the dimethicone of 1.2 parts by weight and 8.8 parts by weight, under magnetic agitation effect
Even, whipping temp is 26 DEG C, speed of agitator 260r/min, after mixing evenly 63 DEG C of water bath with thermostatic control 21min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is
65.6 DEG C, speed of agitator 440r/min, emulsification 5.6min is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 550r/min effect, so
The tomato seed oil micro emulsion of 32 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 79.4 DEG C, is stirred
Revolving speed 550r/min is mixed, tomato seed oil micro emulsion facial mask can be obtained.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 2.14 parts by weight tomato seed oils being mixed, the surface-active
Agent includes polysorbate60, dehydrated alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 26 DEG C, mixing time 6 minutes；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 44r/min and persistently stirs, and is added
Deionized water 6.9min is added dropwise according to 0.5 drop/sec of speed at 27 DEG C of temperature in the deionized water of 2.38 parts by weight, later will
Rate of addition is speeded to 3.0 drops/sec, and 3.8min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are that tomato seed oil is micro-
Cream.
Surface active agent tween 60, dehydrated alcohol are mixed according to the ratio of 1.8:1.
Embodiment 6: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 2.8 parts by weight and the glycerol of 8.8 parts by weight, under magnetic agitation effect uniformly, whipping temp is
33 DEG C, speed of agitator 330r/min；
(2) after (1) step sample is uniform, Tween 80,1.7 parts by weight of 1.2 parts by weight being pre-mixed are added
Coconut oil and 1.2 parts by weight vaseline and 32 parts by weight deionized water mixture and uniform stirring, later 62.8
DEG C water bath with thermostatic control 21min；
(3) by the ethoxy urea of the dimethicone of 2.2 parts by weight and 12 parts by weight, under magnetic agitation effect
Even, whipping temp is 30 DEG C, speed of agitator 315r/min, after mixing evenly 74 DEG C of water bath with thermostatic control 25min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is
73.9 DEG C, speed of agitator 510r/min, emulsification 6.5min is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 510r/min effect, so
The tomato seed oil micro emulsion of 30 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 73.9 DEG C, is stirred
Revolving speed 510r/min is mixed, tomato seed oil micro emulsion facial mask can be obtained.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 2.3 parts by weight tomato seed oils being mixed, the surface-active
Agent includes Tween 80, normal propyl alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 27.5 DEG C, and mixing time 7.5 is divided
Clock；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 52r/min and persistently stirs, and is added
Deionized water 7.3min is added dropwise according to 0.7 drop/sec of speed at 28 DEG C of temperature in the deionized water of 2.82 parts by weight, later will
Rate of addition is speeded to 3.3 drops/sec, and 4.7min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are that tomato seed oil is micro-
Cream.
Surface active agent tween 80, normal propyl alcohol are mixed according to the ratio of 2.2:1.
Embodiment 7: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 1.4 parts by weight and the glycerol of 6.7 parts by weight, under magnetic agitation effect uniformly, whipping temp is
27 DEG C, speed of agitator 280r/min；
(2) after (1) step sample is uniform, Tween 80,3.2 parts by weight of 2.8 parts by weight being pre-mixed are added
Coconut oil and 2.8 parts by weight vaseline and 46 parts by weight deionized water mixture and uniform stirring, later at 83 DEG C
Water bath with thermostatic control 28min；
(3) by the ethoxy urea of the dimethicone of 2.4 parts by weight and 12.8 parts by weight, under magnetic agitation effect
Even, whipping temp is 31 DEG C, speed of agitator 330r/min, after mixing evenly 76.6 DEG C of water bath with thermostatic control 26min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is
76.6 DEG C, speed of agitator 530r/min, emulsification 6.8min is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 530r/min effect, so
The tomato seed oil micro emulsion of 31 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 76.6 DEG C, is stirred
Revolving speed 530r/min is mixed, tomato seed oil micro emulsion facial mask can be obtained.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 2.46 parts by weight tomato seed oils being mixed, the surface-active
Agent includes polysorbate40, dehydrated alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 28 DEG C, mixing time 8 minutes；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 48r/min and persistently stirs, and is added
Deionized water 7.1min is added dropwise according to 0.6 drop/sec of speed at 27.5 DEG C of temperature in the deionized water of 2.6 parts by weight, later will
Rate of addition is speeded to 3.1 drops/sec, and 4.3min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are that tomato seed oil is micro-
Cream.
Surface active agent tween 40, dehydrated alcohol are mixed according to the ratio of 2.4:1.
Embodiment 8: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 2.6 parts by weight and the glycerol of 8.45 parts by weight, under magnetic agitation effect uniformly, whipping temp
It is 32 DEG C, speed of agitator 340r/min；
(2) after (1) step sample is uniform, Tween 80,2.1 parts by weight of 1.6 parts by weight being pre-mixed are added
Coconut oil and 1.6 parts by weight vaseline and 36 parts by weight deionized water mixture and uniform stirring, later 68.4
DEG C water bath with thermostatic control 23min；
(3) by the ethoxy urea of the dimethicone of 2.4 parts by weight and 13.6 parts by weight, under magnetic agitation effect
Even, whipping temp is 32 DEG C, speed of agitator 340r/min, after mixing evenly 80 DEG C of water bath with thermostatic control 27min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is
79.4 DEG C, speed of agitator 550r/min, emulsification 7.1min is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 490r/min effect, so
The tomato seed oil micro emulsion of 29 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 71.1 DEG C, is stirred
Revolving speed 490r/min is mixed, tomato seed oil micro emulsion facial mask can be obtained.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 2.62 parts by weight tomato seed oils being mixed, the surface-active
Agent includes Tween 80, normal propyl alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 28.5 DEG C, and mixing time 8.5 is divided
Clock；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 54r/min and persistently stirs, and is added 3
Deionized water 7.54min is added dropwise according to 0.8 drop/sec of speed at 28.5 DEG C of temperature in the deionized water of parts by weight, later will drop
Acceleration is speeded to 3.6 drops/sec, and 5.2min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are that tomato seed oil is micro-
Cream.
Surface active agent tween 80, normal propyl alcohol are mixed according to the ratio of 2.6:1.
Embodiment 9: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 2.2 parts by weight and the glycerol of 7.75 parts by weight, under magnetic agitation effect uniformly, whipping temp
It is 30 DEG C, speed of agitator 320r/min；
(2) after (1) step sample is uniform, Tween 80,2.7 parts by weight of 2.4 parts by weight being pre-mixed are added
Coconut oil and 2.4 parts by weight vaseline and 42 parts by weight deionized water mixture and uniform stirring, later 76.6
DEG C water bath with thermostatic control 26min；
(3) by the ethoxy urea of the dimethicone of 2.6 parts by weight and 14.4 parts by weight, under magnetic agitation effect
Even, whipping temp is 33 DEG C, speed of agitator 330r/min, after mixing evenly 83 DEG C of water bath with thermostatic control 28min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is
82.8 DEG C, speed of agitator 580r/min, emulsification 7.4min is stood after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 580r/min effect, so
The tomato seed oil micro emulsion of 33 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 83 DEG C, stirring
Tomato seed oil micro emulsion facial mask can be obtained in revolving speed 580r/min.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 2.78 parts by weight tomato seed oils being mixed, the surface-active
Agent includes polysorbate40, isopropanol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 29 DEG C, mixing time 9 minutes；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 37r/min and persistently stirs, and is added
Deionized water 6.44min is added dropwise according to 0.3 drop/sec of speed at 26 DEG C of temperature in the deionized water of 1.94 parts by weight, later will
Rate of addition is speeded to 2.5 drops/sec, and 2.9min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are that tomato seed oil is micro-
Cream.
Surface active agent tween 40, isopropanol are mixed according to the ratio of 2.8:1.
Embodiment 10: a kind of preparation method of tomato seed oil micro emulsion facial mask,
The xanthan gum of (1) 3.0 parts by weight and the glycerol of 9 parts by weight, under magnetic agitation effect uniformly, whipping temp 35
DEG C, speed of agitator 350r/min；
(2) after (1) step sample is uniform, Tween 80,3.5 parts by weight of 3.0 parts by weight being pre-mixed are added
Coconut oil and 3 parts by weight vaseline and 50 parts by weight deionized water mixture and uniform stirring, later in 85 DEG C of perseverances
Tepidarium 30min；
(3) by the ethoxy urea of the dimethicone of 3 parts by weight and 15 parts by weight, under magnetic agitation effect uniformly,
Whipping temp is 35 DEG C, speed of agitator 350r/min, after mixing evenly 85 DEG C of water bath with thermostatic control 30min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp 85
DEG C, speed of agitator 600r/min stands emulsification 8min after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in magnetic agitation rotating speed 600r/min effect, so
The tomato seed oil micro emulsion of 35 parts by weight is added afterwards, continues to stir evenly under magnetic agitation effect, whipping temp is 85 DEG C, stirring
Tomato seed oil micro emulsion facial mask can be obtained in revolving speed 600r/min.
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 3 parts by weight tomato seed oils being mixed, the surfactant
Include Tween 80, dehydrated alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 30 DEG C, mixing time 10 minutes；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 60r/min and persistently stirs, and is added
Deionized water 8min is added dropwise according to 1 drop/sec of speed at 30 DEG C of temperature in the deionized water of 3.5 parts by weight, and speed will be added dropwise later
Degree is speeded to 4 drops/sec, and 6min clarification is added dropwise, and stops after clarification plus water, gained supernatant liquid are tomato seed oil micro emulsion.
Surface active agent tween 80, dehydrated alcohol are mixed according to the ratio of 3:1.
Embodiment 11: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 50 DEG C of environment
After 30min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 50 DEG C, is repeated to squeeze 2 times, is collected expressed oil simultaneously
Removing solid residue is centrifuged, is refined through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,50 DEG C, 25r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 12: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 54 DEG C of environment
After 44min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 52 DEG C, is repeated to squeeze 2 times, is collected expressed oil simultaneously
Removing solid residue is centrifuged, is refined through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,52 DEG C, 29r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 13: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 58 DEG C of environment
After 57min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 54 DEG C, is repeated to squeeze 2 times, is collected expressed oil simultaneously
Removing solid residue is centrifuged, is refined through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,54 DEG C, 33r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 14: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 56 DEG C of environment
After 51min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 53 DEG C, is repeated to squeeze 2 times, is collected expressed oil simultaneously
Removing solid residue is centrifuged, is refined through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,53 DEG C, 31r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 15: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 51 DEG C of environment
After 33.5min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 50.5 DEG C, is repeated to squeeze 2 times, is collected squeezing
Simultaneously removing solid residue is centrifuged in oil, refines through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,50.5 DEG C, 26r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 16: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 55 DEG C of environment
After 47.5min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 52.5 DEG C, is repeated to squeeze 2 times, is collected squeezing
Simultaneously removing solid residue is centrifuged in oil, refines through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,52.5 DEG C, 30r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 17: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 53 DEG C of environment
After 40.5min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 51.5 DEG C, is repeated to squeeze 2 times, is collected squeezing
Simultaneously removing solid residue is centrifuged in oil, refines through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,51.5 DEG C, 28r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 18: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 57 DEG C of environment
After 54.5min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 53.5 DEG C, is repeated to squeeze 2 times, is collected squeezing
Simultaneously removing solid residue is centrifuged in oil, refines through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,53.5 DEG C, 32r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 19: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 52 DEG C of environment
After 37min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 51 DEG C, is repeated to squeeze 2 times, is collected expressed oil simultaneously
Removing solid residue is centrifuged, is refined through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,51 DEG C, 27r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Embodiment 20: compared with embodiment 1-10 any embodiment, the present embodiment the difference is that: tomato seed oil is
The tomato seed oil obtained using cold pressing process, the specific process is as follows: the Tomato Seed after cleaning impurity elimination is taken to toast in 60 DEG C of environment
After 60min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 55 DEG C, is repeated to squeeze 2 times, is collected expressed oil simultaneously
Removing solid residue is centrifuged, is refined through low-temperature physics, i.e. physics degumming: tomato seed oil: active carbon=20:1,
PH4.5, adsorbs 46min by 48.2 DEG C；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,55 DEG C, 35r/
Under the mixing speed of min, adsorption deacidification 30min obtains cold press tomato seed oil.
Claims (4)
1. a kind of preparation method of tomato seed oil micro emulsion facial mask, it is characterised in that: the following steps are included:
The xanthan gum of (1) 1~3 parts by weight and the glycerol of 6~9 parts by weight, under magnetic agitation effect uniformly, whipping temp 25
~35 DEG C, 250~350r/min of speed of agitator；
(2) after (1) step sample is uniform, Tween 80,1.5~3.5 weight of 1~3 parts by weight being pre-mixed are added
The mixture and uniform stirring of the deionized water of the vaseline and 30~50 parts by weight of the coconut oil and 1~3 parts by weight of part, later
In 60~85 DEG C of 20~30min of water bath with thermostatic control；
(3) by the ethoxy urea of the dimethicone of 1~3 parts by weight and 8~15 parts by weight, under magnetic agitation effect
It is even, whipping temp be 25~35 DEG C, 250~350r/min of speed of agitator, after mixing evenly 60~85 DEG C of waters bath with thermostatic control 20~
30min；
(4) material made from above-mentioned steps (2) and (3) is mixed, under magnetic agitation effect uniformly, whipping temp is 60~85
DEG C, 400~600r/min of speed of agitator stands 5~8min of emulsification after mixing evenly；
(5) the resulting sample emulsification system of step (4) is dropped into room temperature in 400~600r/min of magnetic agitation rotating speed effect,
Then the tomato seed oil micro emulsion of 25~35 parts by weight is added, continues to stir evenly under magnetic agitation effect, whipping temp 60
~85 DEG C, 400~600r/min of speed of agitator, tomato seed oil micro emulsion facial mask can be obtained,
Tomato seed oil micro emulsion used in step (5) is prepared by the following method:
A, raw material mixes: the surfactant of 1 parts by weight and 1.5~3 parts by weight tomato seed oils being mixed, the surfactant
Comprising A and B, A be polysorbas20, polysorbate40, polysorbate60 perhaps in Tween 80 one in B be dehydrated alcohol, normal propyl alcohol or isopropyl
One of alcohol；
B, it stirring and emulsifies: being placed on magnetic stirring apparatus and stir evenly, whipping temp is 25 DEG C~30 DEG C, mixing time 5~10
Minute；
C, Jia Shui: the mixture that b step is obtained is placed under the blender that revolving speed is 30~60r/min and persistently stirs, and is added
Deionized water 6 is added dropwise according to 0.1~1 drop/sec of speed at 25 DEG C~30 DEG C of temperature in the deionized water of 1.5~3.5 parts by weight
~8min later speeds rate of addition to 2~4 drops/sec, and 2~6min clarification is added dropwise, and stops after clarification plus water, gained are clarified
Liquid is tomato seed oil micro emulsion.
2. the preparation method of tomato seed oil micro emulsion facial mask according to claim 1, it is characterised in that: surfactant A and B
It is mixed according to the ratio of 1~3:1.
3. the preparation method of tomato seed oil micro emulsion facial mask according to claim 1 or 2, it is characterised in that: A is Tween 80, B
For dehydrated alcohol.
4. the preparation method of tomato seed oil micro emulsion facial mask according to claim 1 or 2, it is characterised in that: above-mentioned Tomato Seed
Oil is the tomato seed oil obtained using cold pressing process, the specific process is as follows: taking the Tomato Seed after cleaning impurity elimination in 50-60 DEG C of environment
After middle baking 30-60min, investment cold pressing expeller is squeezed, and keeping cold pressing expeller extruder temperature is 50-55 DEG C, repeats to squeeze 2 times,
It collects expressed oil and removing solid residue is centrifuged, refined through low-temperature physics, i.e. physics degumming: tomato seed oil: activity
Charcoal=20:1, pH4.5,48.2 DEG C adsorbs 46min；Adsorption deacidification: tomato seed oil: cellulosic-based material=20:1, pH4.5,
50-55 DEG C, under the mixing speed of 25-35r/min, adsorption deacidification 30min obtains cold press tomato seed oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610675542.8A CN106236611B (en) | 2016-08-16 | 2016-08-16 | A kind of preparation method of tomato seed oil micro emulsion facial mask |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610675542.8A CN106236611B (en) | 2016-08-16 | 2016-08-16 | A kind of preparation method of tomato seed oil micro emulsion facial mask |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106236611A CN106236611A (en) | 2016-12-21 |
| CN106236611B true CN106236611B (en) | 2019-02-26 |
Family
ID=57593418
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610675542.8A Active CN106236611B (en) | 2016-08-16 | 2016-08-16 | A kind of preparation method of tomato seed oil micro emulsion facial mask |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106236611B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107684529A (en) * | 2017-08-21 | 2018-02-13 | 上海相宜本草化妆品股份有限公司 | A kind of microemulsified facial mask liquid and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105053256A (en) * | 2015-07-29 | 2015-11-18 | 广州金酮医疗科技有限公司 | Flavored nutrition balanced blend oil |
-
2016
- 2016-08-16 CN CN201610675542.8A patent/CN106236611B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105053256A (en) * | 2015-07-29 | 2015-11-18 | 广州金酮医疗科技有限公司 | Flavored nutrition balanced blend oil |
Non-Patent Citations (4)
| Title |
|---|
| Dermalogica德美乐嘉草本保湿面膜;专业测评;《http://fashion.qq.com/a/20150718/005305_all.htm#page1》;20150718;第1-6页 |
| 几种特色油脂的营养功能特性及冷榨工艺研究;陈钊等;《食品工业科技》;20101231(第3期);第274-277页 |
| 番茄籽的综合利用;赵文正等;《食品科学》;19900531;第34-36页 |
| 驼乳面膜的研制;陈宸;《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》;20131215(第S1期);第10页 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106236611A (en) | 2016-12-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103194334A (en) | Cold process soap added with fresh fig protoplasm | |
| CN105534770B (en) | A kind of passion fruit facial mask and preparation method thereof | |
| CN108670882A (en) | A kind of edible lipstick and preparation method thereof | |
| CN105362150A (en) | Hair conditioner | |
| CN107858202A (en) | Selenium-rich tea oil and its processing technology | |
| CN106433970A (en) | Production method for high-quality cosmetic oil | |
| CN106236611B (en) | A kind of preparation method of tomato seed oil micro emulsion facial mask | |
| CN107286068B (en) | A method of preparing lutein crystal oil suspending agent | |
| CN105886165A (en) | Handmade soap capable of clearing away heat and toxic materials and making method thereof | |
| CN101104015B (en) | Olive soft capsule raw material formulation and its preparation technology | |
| CN109381388A (en) | A kind of passion fruit skin cream and preparation method thereof | |
| CN108553339A (en) | Unreal change lipstick of light sensation and preparation method thereof | |
| CN107308029A (en) | Edible natural lipstick of haematococcus pluvialis and preparation method thereof | |
| CN109770312A (en) | A kind of production method of Semen sesami nigrum honey food | |
| CN108785205A (en) | A kind of shaddock skims the cream off milk liquid and preparation method thereof | |
| CN107898682A (en) | A kind of safflower compounded thing and preparation method and a kind of lipstick and preparation method | |
| CN108403485A (en) | Natural herb sunscreen | |
| CN107569443A (en) | A kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution | |
| CN107156372A (en) | A kind of rose hip oil inulin beauty treatment weight reducing milk tea | |
| CN107519120A (en) | A kind of formula of the skin care oil of pregnant woman | |
| CN106929229A (en) | A kind of sheep tail fat perfumed soap and preparation method thereof | |
| KR100511222B1 (en) | Cosmetic products containing the Dong-A extracts for inhibiting acne and a method for preparing thereof | |
| CN107760491A (en) | It is a kind of can toxin expelling detumescence whitening matrimony vine peach gum adlay soap of Chinese medicine preparation method | |
| CN110384135A (en) | A kind of oleic acid, linoleic acid and ready-mixed oil of alpha-linolenic acid balanced proportion and preparation method thereof | |
| CN108904411A (en) | One kind is for anti-wrinkle health-care skin-protecting products of whitening and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |