CN106222880A - The waterproof processing method refusing dirty type silk needle-punched cotton mattress - Google Patents

The waterproof processing method refusing dirty type silk needle-punched cotton mattress Download PDF

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Publication number
CN106222880A
CN106222880A CN201610594087.9A CN201610594087A CN106222880A CN 106222880 A CN106222880 A CN 106222880A CN 201610594087 A CN201610594087 A CN 201610594087A CN 106222880 A CN106222880 A CN 106222880A
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Prior art keywords
raw material
silk
processing method
hydrophilic
silkworm silk
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CN201610594087.9A
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Chinese (zh)
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CN106222880B (en
Inventor
席敏皓
杨佩
左臣伟
张淑芬
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Sichuan Sima Silk Technology Co.,Ltd.
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席敏皓
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Classifications

    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4266Natural fibres not provided for in group D04H1/425
    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47GHOUSEHOLD OR TABLE EQUIPMENT
    • A47G9/00Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C3/00Treatment of animal material, e.g. chemical scouring of wool
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/44Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
    • D04H1/46Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47GHOUSEHOLD OR TABLE EQUIPMENT
    • A47G9/00Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
    • A47G2009/001Anti-allergen; Anti-mite

Abstract

The invention discloses a kind of waterproof processing method refusing dirty type silk needle-punched cotton mattress, comprise the steps: the solid glue of step (1), remove impurity, silkworm silk raw material is carried out screening and removing impurities, then silkworm silk raw material is carried out solid glue process, it is ensured that the content of fibroin and stability;Step (2), bleaching: Gu after surface moisture removed by the silkworm silk raw material after glue, put in liquid lime chloride and bleach, then clean, dry;Step (3), hydrophilic water repellent finish: the silkworm silk raw material after step (2) being dried puts in cationic hydrophilic agent solution and carries out hydrophilic treated, put into after surface moisture removed by the silkworm silk raw material of hydrophilic treated again and carry out water repellent process in water repellent solution;Step (4), short one-tenth short-fibre silk is beaten in the silkworm silk raw material combing through hydrophilic water repellent finish, then make product by needling process.Give the hydrophilic waterproofing function that silkworm silk is unique, while preventing the invasion of various spot, also assures that silk mattress original air-moisture-permeable ability.

Description

The waterproof processing method refusing dirty type silk needle-punched cotton mattress
Technical field
The present invention relates to a kind of waterproof processing method refusing dirty type silk needle-punched cotton mattress, belong to silkworm silk process technology neck Territory.
Background technology
Silkworm silk is a kind of natural protein fibre.Mainly being made up of fibroin albumen and sericin, wherein sericin accounts for 10%~40%.18 kinds of aminoacid contained in fibroin have health care, Nutrition to human body.It practice, silkworm silk Albumen is very much like with human body skin keratin, often contacts with fibroin and can obviously improve skin, therefore silkworm silk Often it is made into non-woven fabrics for cosmetics and various bedding etc..
Silkworm silk has its unrivaled advantage as mattress: moisture absorption is ventilative, antibiosis anti-acarien, but has one among these and ask It is difficult to clean up after topic, i.e. mattress contamination dirt.The cleaning procedure of mattress is troublesome, needs to place and is exposed to the sun in the sun, in addition it is also necessary to The abluent of specialty removes mildew, colored drink, sweat stain, urine stain etc., has a lot of family that the drycleaner's of specialty also can be asked to process, This brings a lot of inconvenience to our life.
Summary of the invention
Based on the deficiencies in the prior art, the technical problem to be solved in the present invention is to provide a kind of waterproof refuses dirty type silk needle-punched The processing method of cotton mattress, gives the hydrophilic waterproofing function that silkworm silk is unique, also ensures while preventing the invasion of various spot Silk mattress original air-moisture-permeable ability.
To achieve these goals, the technical scheme is that and a kind of waterproof refuse adding of dirty type silk needle-punched cotton mattress Work method, it is characterised in that: comprise the steps:
Step (1), the solid glue of remove impurity, carry out silkworm silk raw material screening and removing impurities, then silkworm silk raw material carry out solid glue process, protect The content of card fibroin and stability;
Step (2), bleaching: Gu after surface moisture removed by the silkworm silk raw material after glue, put in liquid lime chloride and bleach, so Rear cleaning, drying;
Step (3), hydrophilic water repellent finish: it is molten that the silkworm silk raw material after step (2) being dried puts into cationic hydrophilic agent Liquid carries out hydrophilic treated, after surface moisture removed by the silkworm silk raw material of hydrophilic treated, puts into water repellent solution used for textiles again In carry out water repellent process;
Step (4), short one-tenth short-fibre silk is beaten in the silkworm silk raw material combing through hydrophilic-water repellent finish, then pass through acupuncture Technique makes product.
Such scheme, the present invention is processed by the solid glue of solid colloid, it is ensured that the content of fibroin and stability, thus ensures The health and beauty of made mattress.Silkworm silk first carries out hydrophilic finiss, and hydrophilizing agent gives silkworm silk sucting wet air permeability, then enters Row water repellent finish, the cored structure of hydrophilic outer water repellent in being formed, thus reach hydrone and can not pass through, and air can freely lead to The purpose crossed, also assures that silk mattress original air-moisture-permeable ability while preventing the invasion of various spot.Especially silkworm silk Fiber through cationic hydrophilic agent process after, can allow and there is between fiber certain repulsion, outward manifestation be fluffy, be difficult to collapse Fall into.
Preferred: silkworm silk raw material carries out in step (1) solid glue processing the solid colloid used is tetra methylol phosphonium salt or first Aldehyde or modified glutaraldehyde, will be 20-50 in temperature in solid colloid solution that silkworm silk raw material input mass concentration is 0.1%-5% DEG C, carry out solid glue process under pH6-7.Gu during glue processes, use alkali compounds sodium carbonate or sodium bicarbonate regulation pH.Described four Methylol microcosmic salt is THPC or tetrakis hydroxymetyl phosphonium sulfuric.It is preferred: Gu the time that glue processes is 1-24h.
In such scheme, in step (3), liquid lime chloride be mass concentration be the hydrogen peroxide solution of 0.1%-5%, pH control System is at 8-12, bleaching time 0.5-24h.
In such scheme: in step (3), cationic hydrophilic agent is glycidyl dimethyl dodecyl ammonium chloride.Should Fatty amine long-chain (dodecyl) in surfactant gives the softness that fiber is excellent, and it is hydrophilic that glycidyl gives fiber Property, hygroscopicity.Azelon is processed so that it is more soft, smooth with it, and less to application on human skin zest, will not be to people Body and environmental pollution.Soluble in water, when processing protein fibre without adding organic solvent, penetrating agent and diffusant, Simple to operate, energy consumption is relatively low, is greatly saved production cost.
Preferred: in step (3), the mass concentration of cationic hydrophilic agent solution is 0.5%-1.5%.
In such scheme, in step (3), described waterproofing agent is ZJ-FCB1428 type waterproofing agent or Organic fluoride family macromolecule Polymer waterproofing agent.ZJ-FCB1428 type waterproofing agent is produced by Guangzhou Zhuan Jie Chemical Co., Ltd..Water-proofing treatment is effective.
In such scheme, the mass concentration of water repellent solution is 0.3-1%.
In such scheme: step (4), the silkworm silk combing through hydrophilic-water repellent finish is beaten short one-tenth average length be 2~ The short-fibre silk of 8 centimetres, then according to traditional needling process becomes cotton sheet through comb and parallel cotton fibers prior to spinning, lapping, acupuncture, dries at 40-100 DEG C Dry obtain product.
The invention has the beneficial effects as follows: silkworm silk is used for making mattress by the present invention there is natural environmental-protective, flexible, breathable, resist The effects such as the anti-demodicid mite of bacterium, the silkworm silk after processing with solid glue does silk mattress, it is ensured that the content of albumen and stability on mattress, Ensure the beauty treatment health care efficacy of silk mattress.The present invention gives the hydrophilic waterproofing function that silk mattress is unique, prevents various Silk mattress original air-moisture-permeable ability is also assures that while spot invasion.The operational maintenance cleaning making silk mattress becomes Must be easier to.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described:
Embodiment 1
The waterproof processing method refusing dirty type silk needle-punched cotton mattress, is completed by following steps:
1. remove impurity: husks is carried out screening and removing impurities.
2. solid glue: husks is soaked in concentration is 0.3% THPC and 0.1% sodium bicarbonate solution 6 little Time, regulation PH is 6, deviates from surface moisture after immersion, and dehydration can use dewaterer to deviate from, it is also possible to naturally dries or wrings out.
3. bleaching: the husks after dehydration is put into and soaks 12 hours in the solution that PH=10, hydrogen peroxide content are 3%, clearly Wash, dry.
The most hydrophilic water repellent finish: by husks in the glycidyl dimethyl dodecyl ammonium chloride solution of 0.5% Soak 1h, then remove surface moisture, then be placed in 0.3% waterproofing agent ZJ-FCB1428 (production of Guangzhou Zhuan Jie Chemical Co., Ltd.) In solution, at 25 DEG C, soak 30min, then bake at 100 DEG C.
5. combing: it is the short-fibre silk of 2cm that husks combing is beaten short one-tenth average length;
6. nonwoven technical process: use needled conventionally Processes and apparatus, becomes continuous lamellar, drying to obtain through comb and parallel cotton fibers prior to spinning, lapping, acupuncture Product;Drying temperature is 60 DEG C.
Embodiment 2
The waterproof processing method refusing dirty type silk needle-punched cotton mattress, is completed by following steps:
1. remove impurity: silkworm silk machine cotton is carried out screening and removing impurities.
2. solid glue: soak 12 in concentration is 0.5% tetrakis hydroxymetyl phosphonium sulfuric and 0.6% sodium carbonate liquor by cotton for silkworm silk machine Hour.Regulation PH=7, deviates from surface moisture after immersion.
3. bleaching: the silkworm silk machine cotton after dehydration is put in the solution that PH=9, hydrogen peroxide content are 2% and soaks 8 hours, Clean, dry;
The most hydrophilic water repellent finish: by husks in the glycidyl dimethyl dodecyl ammonium chloride solution of 1.5% Soak 0.5h, take out and be placed in again in 0.5% waterproofing agent ZJ-FCB1428 solution after removing surface moisture, soak at 25 DEG C 20min, then bakes at 100 DEG C.
5. combing: silkworm silk machine cotton combing is beaten short one-tenth average length is the short-fibre silk of 3cm;
6. nonwoven technical process: use needled conventionally Processes and apparatus, becomes continuous lamellar, drying to obtain through comb and parallel cotton fibers prior to spinning, lapping, acupuncture Product;Drying temperature is 80 DEG C.
Embodiment 3
The waterproof processing method refusing dirty type silk needle-punched cotton mattress, is completed by following steps:
1. remove impurity: husks is carried out screening and removing impurities.
2. solid glue: husks is soaked 0.5 hour in concentration is 5% formaldehyde and 0.1% sodium bicarbonate solution, during tune Joint PH is 6, deviates from surface moisture after immersion, and dehydration can use dewaterer to deviate from, it is also possible to naturally dries or wrings out.
3. bleaching: the husks after dehydration is put into and soaks 0.5 hour in the solution that PH=12, hydrogen peroxide content are 5%, clearly Wash, dry.
The most hydrophilic water repellent finish: by husks in the glycidyl dimethyl dodecyl ammonium chloride solution of 1.5% Soak 1h, then remove surface moisture, then be placed in 1% Organic fluoride family macromolecule polymer (fluorine-containing water repellent FUNCTEX (Fick This) F-659) in water repellent solution, at 25 DEG C, soak 30min, then bake at 100 DEG C.
5. combing: it is the short-fibre silk of 5cm that husks combing is beaten short one-tenth average length;
6. nonwoven technical process: use needled conventionally Processes and apparatus, becomes continuous lamellar, drying to obtain through comb and parallel cotton fibers prior to spinning, lapping, acupuncture Product;Drying temperature is 60 DEG C.
Embodiment 4
The waterproof processing method refusing dirty type silk needle-punched cotton mattress, is completed by following steps:
1. remove impurity: silkworm silk machine cotton is carried out screening and removing impurities.
2. solid glue: silkworm silk machine cotton is soaked 0.5 in concentration is 0.1% modified glutaraldehyde and 0.5% sodium carbonate liquor little Time.Regulation PH=7, deviates from surface moisture after immersion.
3. bleaching: the silkworm silk machine cotton after dehydration is put into that to soak 24 in the solution that PH=8, hydrogen peroxide content are 0.1% little Time, clean, dry;
The most hydrophilic water repellent finish: by husks in the glycidyl dimethyl dodecyl ammonium chloride solution of 1.0% Soak 0.5h, take out and be placed in again in 0.5% waterproofing agent ZJ-FCB1428 solution after removing surface moisture, soak at 25 DEG C 20min, then bakes at 100 DEG C.
5. combing: silkworm silk machine cotton combing is beaten short one-tenth average length is the short-fibre silk of 8cm;
6. nonwoven technical process: use needled conventionally Processes and apparatus, becomes continuous lamellar, drying to obtain through comb and parallel cotton fibers prior to spinning, lapping, acupuncture Product;Drying temperature is 80 DEG C.
The present invention is not limited to above-described embodiment, it will be appreciated that those of ordinary skill in the art is without creative work Just can make many modifications and variations according to the design of the present invention.All technical staff in the art are under this invention's idea On the basis of existing technology by the available technical scheme of logical analysis, reasoning, or a limited experiment, all should by In protection domain determined by claims.

Claims (10)

1. the waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: comprise the steps:
Step (1), the solid glue of remove impurity, carry out silkworm silk raw material screening and removing impurities, then silkworm silk raw material carry out solid glue process, it is ensured that silkworm The content of fibroin and stability;
Step (2), bleaching: Gu after surface moisture removed by the silkworm silk raw material after glue, put in liquid lime chloride and bleach, the most clearly Wash, dry;
Step (3), hydrophilic water repellent finish: the silkworm silk raw material after step (2) being dried puts in cationic hydrophilic agent solution Carry out hydrophilic treated, put into again in water repellent solution used for textiles after surface moisture removed by the silkworm silk raw material of hydrophilic treated Row water repellent processes;
Step (4), short one-tenth short-fibre silk is beaten in the silkworm silk raw material combing through hydrophilic-water repellent finish, then pass through needling process Make product.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: step (1) In silkworm silk raw material carries out solid glue to process the solid colloid used be tetra methylol phosphonium salt or formaldehyde or modified glutaraldehyde, silkworm silk is former Material puts in the solid colloid solution that mass concentration is 0.1%-5% and is 20-50 DEG C in temperature, carries out solid glue process under pH6-7.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: Gu glue processes In, using alkali compounds sodium carbonate or sodium bicarbonate regulation pH, described tetra methylol phosphonium salt is THPC or four Methylol sulphuric acid phosphorus.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: Gu glue processes Time be 1-24h.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: step (3) In, liquid lime chloride be mass concentration be the hydrogen peroxide solution of 0.1%-5%, pH controls at 8-12, bleaching time 0.5-24h.
6. according to the processing method refusing dirty type silk needle-punched cotton mattress waterproof described in any one of claim 1-5, it is characterised in that: In step (3), cationic hydrophilic agent is glycidyl dimethyl dodecyl ammonium chloride.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: step (3) In, the mass concentration of cationic hydrophilic agent solution is 0.5%-1.5%.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: step (3) In, described waterproofing agent is ZJ-FCB1428 type waterproofing agent or Organic fluoride family macromolecule polymer waterproofing agent.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: step (3) In, the mass concentration of water repellent solution is 0.3-1%.
The most waterproof processing method refusing dirty type silk needle-punched cotton mattress, it is characterised in that: step (4) short-fibre silk that short one-tenth average length is 2~8 centimetres, by the silkworm silk raw material combing through hydrophilic-water repellent finish is beaten, then Become cotton sheet according to traditional needling process through comb and parallel cotton fibers prior to spinning, lapping, acupuncture, dry at 40-100 DEG C and obtain product.
CN201610594087.9A 2016-07-26 2016-07-26 The processing method that waterproof refuses dirty type silk needle-punched cotton mattress Active CN106222880B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111335028A (en) * 2020-03-27 2020-06-26 席敏皓 Glue-fixing production method for steam filature
CN111411518A (en) * 2020-03-27 2020-07-14 席敏皓 Antibacterial and anti-virus silk fiber filtering base cloth and application thereof
CN113604889A (en) * 2021-07-06 2021-11-05 邹雪梅 Intelligent weaving-based water-proof and dirt-resistant silk mattress processing equipment

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1410623A (en) * 2001-09-27 2003-04-16 中国科学院化学研究所 Treatment method of fabric possessing ultra biphilic/ultra biphobic composite functions at same time
CN2845585Y (en) * 2005-10-08 2006-12-13 曾令福 Mattress made from silkworm velvet
CN101130898A (en) * 2007-07-25 2008-02-27 席星航 Cocoon glue producing method
CN102162195A (en) * 2011-01-28 2011-08-24 达利(中国)有限公司 Dyeing and finishing process of washable organza fabric
CN202653669U (en) * 2012-05-04 2013-01-09 曾令福 Multi-functional washable health-care silk mattress
CN203802087U (en) * 2013-10-21 2014-09-03 重庆玮兰床垫家具有限公司 Mattress

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1410623A (en) * 2001-09-27 2003-04-16 中国科学院化学研究所 Treatment method of fabric possessing ultra biphilic/ultra biphobic composite functions at same time
CN2845585Y (en) * 2005-10-08 2006-12-13 曾令福 Mattress made from silkworm velvet
CN101130898A (en) * 2007-07-25 2008-02-27 席星航 Cocoon glue producing method
CN102162195A (en) * 2011-01-28 2011-08-24 达利(中国)有限公司 Dyeing and finishing process of washable organza fabric
CN202653669U (en) * 2012-05-04 2013-01-09 曾令福 Multi-functional washable health-care silk mattress
CN203802087U (en) * 2013-10-21 2014-09-03 重庆玮兰床垫家具有限公司 Mattress

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111335028A (en) * 2020-03-27 2020-06-26 席敏皓 Glue-fixing production method for steam filature
CN111411518A (en) * 2020-03-27 2020-07-14 席敏皓 Antibacterial and anti-virus silk fiber filtering base cloth and application thereof
CN111411518B (en) * 2020-03-27 2022-09-09 席敏皓 Antibacterial and anti-virus silk fiber filtering base cloth and application thereof
CN111335028B (en) * 2020-03-27 2022-09-27 席敏皓 Glue-fixing production method for steam filature
CN113604889A (en) * 2021-07-06 2021-11-05 邹雪梅 Intelligent weaving-based water-proof and dirt-resistant silk mattress processing equipment

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