CN106221331B - A kind of inner wall mold-proof paint and preparation method thereof - Google Patents
A kind of inner wall mold-proof paint and preparation method thereof Download PDFInfo
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- CN106221331B CN106221331B CN201610776707.0A CN201610776707A CN106221331B CN 106221331 B CN106221331 B CN 106221331B CN 201610776707 A CN201610776707 A CN 201610776707A CN 106221331 B CN106221331 B CN 106221331B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
- C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D201/00—Coating compositions based on unspecified macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/14—Applications used for foams
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of inner wall mold-proof paint and preparation method thereof, inner wall mold-proof paint is prepared from the following raw materials in parts by weight:20 30 parts of butyl acrylate, 15 25 parts of dibutyl phthalate, 20 30 parts of elastic emulsion, 10 20 parts of NPE, 20 30 parts of titanium dioxide, 10 20 parts of thickener, 10 30 parts of foaming agent, 20 30 parts of mould inhibitor, 10 20 parts of water-soluble silicon oil, 20 30 parts of deionized water.After coating of the present invention is applied, the coated film of formation has the advantages that tensile strength and fracture elongation are high, coated film flat smooth, exquisite in texture, with silk gloss, high covering power, strong adhesive force, splendid antibacterial and fungicidal properties, excellent water-alkali resistance performance, film can be scrubbed, and printing resistance is strong, and gloss is lasting, the present invention is applied to indoor interior wall, play waterproof, prevent blending mould proof effect, and with high durable, stain resistance, manufacturing cost is relatively low, toxic is relatively low, is adapted to promote the use of.
Description
Technical field
The present invention relates to a kind of inner wall mold-proof paint and preparation method thereof, belong to building coating field.
Background technology
The generation of mould not only declines the coating surface dicoration weathered, but also can cause paint film cracking or stripping
Fall.The moist place of darkness of improper ventilation, material or production environment especially rich in microbial nutrition source, such as beer, beans system
The industries such as product, plastic products, the breeding and growth of all very suitable mould of temperature and humidity and bacterium.If applied using general decor
Material, will occur the erosion of mould in various degree, can gradually be faded, stain so that coming off by the later coating of mold corrosion.Have
Machine antimildew disinfectant antimycotic antiseptic efficiency high, but there is long-term effect, heat resistance, the disadvantage of security difference, inorganic antimildew disinfectant
It is mould proof to kill just on the contrary, its antimycotic antiseptic long-term effect, heat-resist and germicidal efficiency is lower slightly.
The content of the invention
The technical problem to be solved in the present invention is to overcome existing defect there is provided a kind of inner wall mold-proof paint and its preparation
Method, the inner wall mold-proof paint can be coated in the building surface of humidity, and will not go mouldy.
In order to solve the above-mentioned technical problem, the invention provides following technical scheme:
A kind of inner wall mold-proof paint, is prepared from the following raw materials in parts by weight:20-30 parts of butyl acrylate, O-phthalic
15-25 parts of dibutyl phthalate, 20-30 parts of elastic emulsion, 10-20 parts of NPE, 20-30 parts of titanium dioxide, thickener
10-20 parts, 10-30 parts of foaming agent, 20-30 parts of mould inhibitor, 10-20 parts of water-soluble silicon oil, 20-30 parts of deionized water.
In such scheme preferably, the thickener be polyacrylate, hydroxyethyl cellulose, methylcellulose,
One or more in gelatin and guar gum.
In any of the above-described scheme preferably, the mould inhibitor is BIT, 2- (4- thiazoles
Base) benzimidazole, double thiocarbamates, chloro- 2-N- octyl groups -3 (the 2H)-isothiazolones of 4,5- bis- and 2- octyl groups -3 (2H) -
One or more in isothiazolone.
In any of the above-described scheme preferably, the foaming agent is N, N dinitrosopentamethlyene tetramines, benzene sulfonyl hydrazide
With the one or more in azodicarbonamide.
The preparation method of inner wall mold-proof paint of the present invention, including following steps:
(1) in Scattered Kettle, butyl acrylate, dibutyl phthalate, elastic emulsion and polyoxyethylene nonyl phenyl second are added
5-10min is stirred under alkene ether, 1500-2000r/min rotating speeds, mixture A is obtained;
(2) in Scattered Kettle, titanium dioxide, thickener, foaming agent, mould inhibitor, water-soluble silicon oil and deionized water are added,
10-20min is stirred under 3000-4000r/min rotating speeds, mixture B is obtained;
(3) the mixture A and mixture B mixing, obtains the inner wall mold-proof paint.
Beneficial effects of the present invention:After coating of the present invention is applied, the coated film of formation has tensile strength and extension
The high advantage of rate, coated film flat smooth, exquisite in texture, with silk gloss, high covering power, strong adhesive force, splendid antibacterial and
Fungicidal properties, excellent water-alkali resistance performance, film can be scrubbed, and printing resistance is strong, and persistently, the present invention is applied in indoor gloss
Wall, plays waterproof, prevents blending mould proof effect, and with high durable, stain resistance, manufacturing cost is relatively low, and toxic is relatively low,
It is adapted to promote the use of.
Embodiment
The preferred embodiments of the present invention are illustrated below, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1:
A kind of inner wall mold-proof paint, is prepared from the following raw materials in parts by weight:26 parts of butyl acrylate, phthalic acid two
20 parts of butyl ester, 24 parts of elastic emulsion, 17 parts of NPE, 23 parts of titanium dioxide, 14 parts of guar gum, azodicarbonamide
26 parts, 22 parts of 1,2- benzisothiazole-3-ketones, 14 parts of water-soluble silicon oil, 24 parts of deionized water.
The preparation method of the inner wall mold-proof paint, it is characterised in that:Including following steps:
(1) in Scattered Kettle, butyl acrylate, dibutyl phthalate, elastic emulsion and polyoxyethylene nonyl phenyl second are added
8min is stirred under alkene ether, 1800r/min rotating speeds, mixture A is obtained;
(2) in Scattered Kettle, titanium dioxide, guar gum, azodicarbonamide, BIT, water are added
Dissolubility silicone oil and deionized water, 15min is stirred under 3500r/min rotating speeds, obtains mixture B;
(3) the mixture A and mixture B mixing, obtains the inner wall mold-proof paint.
Embodiment 2:
A kind of inner wall mold-proof paint, is prepared from the following raw materials in parts by weight:20 parts of butyl acrylate, phthalic acid two
15 parts of butyl ester, 20 parts of elastic emulsion, 10 parts of NPE, 20 parts of titanium dioxide, 10 parts of guar gum, azodicarbonamide
10 parts, 20 parts of 1,2- benzisothiazole-3-ketones, 10 parts of water-soluble silicon oil, 20 parts of deionized water.
The preparation method of the inner wall mold-proof paint, it is characterised in that:Including following steps:
(1) in Scattered Kettle, butyl acrylate, dibutyl phthalate, elastic emulsion and polyoxyethylene nonyl phenyl second are added
8min is stirred under alkene ether, 1800r/min rotating speeds, mixture A is obtained;
(2) in Scattered Kettle, titanium dioxide, guar gum, azodicarbonamide, BIT, water are added
Dissolubility silicone oil and deionized water, 15min is stirred under 3500r/min rotating speeds, obtains mixture B;
(3) the mixture A and mixture B mixing, obtains the inner wall mold-proof paint.
Embodiment 3:
A kind of inner wall mold-proof paint, is prepared from the following raw materials in parts by weight:30 parts of butyl acrylate, phthalic acid two
25 parts of butyl ester, 30 parts of elastic emulsion, 20 parts of NPE, 30 parts of titanium dioxide, 20 parts of guar gum, azodicarbonamide
30 parts, 30 parts of 1,2- benzisothiazole-3-ketones, 20 parts of water-soluble silicon oil, 30 parts of deionized water.
The preparation method of the inner wall mold-proof paint, it is characterised in that:Including following steps:
(1) in Scattered Kettle, butyl acrylate, dibutyl phthalate, elastic emulsion and polyoxyethylene nonyl phenyl second are added
8min is stirred under alkene ether, 1800r/min rotating speeds, mixture A is obtained;
(2) in Scattered Kettle, titanium dioxide, guar gum, azodicarbonamide, BIT, water are added
Dissolubility silicone oil and deionized water, 15min is stirred under 3500r/min rotating speeds, obtains mixture B;
(3) the mixture A and mixture B mixing, obtains the inner wall mold-proof paint.
Embodiment 4:
A kind of inner wall mold-proof paint, is prepared from the following raw materials in parts by weight:30 parts of butyl acrylate, phthalic acid two
25 parts of butyl ester, 30 parts of elastic emulsion, 20 parts of NPE, 30 parts of titanium dioxide, 20 parts of methylcellulose, N, N bis- are sub-
30 parts of five methine tetramine of nitro, 30 parts of 2- (4- thiazolyls) benzimidazole, 20 parts of water-soluble silicon oil, 30 parts of deionized water.
The preparation method of the inner wall mold-proof paint, it is characterised in that:Including following steps:
(1) in Scattered Kettle, butyl acrylate, dibutyl phthalate, elastic emulsion and polyoxyethylene nonyl phenyl second are added
5min is stirred under alkene ether, 1500r/min rotating speeds, mixture A is obtained;
(2) in Scattered Kettle, titanium dioxide, guar gum, azodicarbonamide, BIT, water are added
Dissolubility silicone oil and deionized water, 10min is stirred under 3000r/min rotating speeds, obtains mixture B;
(3) the mixture A and mixture B mixing, obtains the inner wall mold-proof paint.
Embodiment 5:
A kind of inner wall mold-proof paint, is prepared from the following raw materials in parts by weight:30 parts of butyl acrylate, phthalic acid two
25 parts of butyl ester, 30 parts of elastic emulsion, 20 parts of NPE, 30 parts of titanium dioxide, 20 parts of polyacrylate, benzene sulfonyl hydrazide
30 parts, 30 parts of double thiocarbamates, 20 parts of water-soluble silicon oil, 30 parts of deionized water.
The preparation method of the inner wall mold-proof paint, it is characterised in that:Including following steps:
(1) in Scattered Kettle, butyl acrylate, dibutyl phthalate, elastic emulsion and polyoxyethylene nonyl phenyl second are added
10min is stirred under alkene ether, 2000r/min rotating speeds, mixture A is obtained;
(2) in Scattered Kettle, titanium dioxide, guar gum, azodicarbonamide, BIT, water are added
Dissolubility silicone oil and deionized water, 20min is stirred under 4000r/min rotating speeds, obtains mixture B;
(3) the mixture A and mixture B mixing, obtains the inner wall mold-proof paint.
Embodiment 1-5 product passes through performance measurement, the results are shown in Table 1.
Table 1, performance measurement
The test of sterilizing rate is as follows:Bacterium solution (Escherichia coli, black-koji mould) is spread evenly across to the load for scribbling above-mentioned coating
On glass side, it is placed in through 0, after 4,12,24,48,100 hours in physiological saline with picking bacterium solution, takes 0.5ml in culture dish, plus
Enter culture medium, cultivated 48 hours in incubator, take out number clump count, sterilizing rate is calculated according to formula:Sterilizing rate=(initial bacterium
Fall clump count after number-sterilization)/initial clump count × 100%, it the results are shown in Table 2.
The bactericidal property of table 2 is tested
Finally it should be noted that:The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention,
Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic.
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., should be included in the present invention's
Within protection domain.
Claims (2)
1. a kind of inner wall mold-proof paint, it is characterised in that:It is prepared from the following raw materials in parts by weight:26 parts of butyl acrylate, neighbour
20 parts of dibatyl phithalate, 24 parts of elastic emulsion, 17 parts of NPE, 23 parts of titanium dioxide, 14 parts of guar gum, idol
26 parts of nitrogen diformamide, 22 parts of 1,2- benzisothiazole-3-ketones, 14 parts of water-soluble silicon oil, 24 parts of deionized water.
2. the preparation method of inner wall mold-proof paint according to claim 1, it is characterised in that:Including following steps:
(1)In Scattered Kettle, butyl acrylate, dibutyl phthalate, elastic emulsion and NPE are added,
5-10min is stirred under 1500-2000r/min rotating speeds, mixture A is obtained;
(2)In Scattered Kettle, titanium dioxide, guar gum, azodicarbonamide, BIT, water solubility are added
Silicone oil and deionized water, stir 10-20min under 3000-4000 r/min rotating speeds, obtain mixture B;
(3)The mixture A and mixture B mixing, obtains the inner wall mold-proof paint.
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CN201610776707.0A CN106221331B (en) | 2016-08-31 | 2016-08-31 | A kind of inner wall mold-proof paint and preparation method thereof |
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CN201610776707.0A CN106221331B (en) | 2016-08-31 | 2016-08-31 | A kind of inner wall mold-proof paint and preparation method thereof |
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CN106221331B true CN106221331B (en) | 2017-08-29 |
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CN109880413A (en) * | 2019-01-15 | 2019-06-14 | 河北晨阳工贸集团有限公司 | A kind of disinsection mold-proof interior wall coating and preparation method thereof |
CN112430403A (en) * | 2020-10-19 | 2021-03-02 | 江苏汉卫环境安全科技有限公司 | Antibacterial coating for mobile laboratory |
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