CN106191545A - A kind of LED substrate heat sink material and production method thereof - Google Patents

A kind of LED substrate heat sink material and production method thereof Download PDF

Info

Publication number
CN106191545A
CN106191545A CN201610662631.9A CN201610662631A CN106191545A CN 106191545 A CN106191545 A CN 106191545A CN 201610662631 A CN201610662631 A CN 201610662631A CN 106191545 A CN106191545 A CN 106191545A
Authority
CN
China
Prior art keywords
heat sink
sink material
auxiliary agent
led substrate
gained
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610662631.9A
Other languages
Chinese (zh)
Inventor
陈加根
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wave Island Anhui Recreation Facility Co Ltd
Original Assignee
Wave Island Anhui Recreation Facility Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wave Island Anhui Recreation Facility Co Ltd filed Critical Wave Island Anhui Recreation Facility Co Ltd
Priority to CN201610662631.9A priority Critical patent/CN106191545A/en
Publication of CN106191545A publication Critical patent/CN106191545A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/10Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/04Making non-ferrous alloys by powder metallurgy
    • C22C1/05Mixtures of metal powder with non-metallic powder
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C32/00Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ
    • C22C32/0005Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with at least one oxide and at least one of carbides, nitrides, borides or silicides as the main non-metallic constituents
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L33/00Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
    • H01L33/48Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof characterised by the semiconductor body packages
    • H01L33/64Heat extraction or cooling elements
    • H01L33/641Heat extraction or cooling elements characterized by the materials
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00Supplementary information concerning processes or compositions relating to powder metallurgy
    • B22F2998/10Processes characterised by the sequence of their steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00Aspects linked to processes or compositions used in powder metallurgy

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Power Engineering (AREA)
  • Cooling Or The Like Of Semiconductors Or Solid State Devices (AREA)
  • Led Device Packages (AREA)

Abstract

The present invention relates to light fixture heat sink material, being specifically related to a kind of LED substrate heat sink material and production method thereof, this heat sink material is made up of the raw material of following weight portion: aluminum 60 70, titanium dioxide 78, magnesium 8 10, nanometer silicon carbide 12 15, calcium fluoride 23, vermiculite power 68, styrene 13, auxiliary agent 45;The present invention combines the advantage of the compositions such as aluminum, magnesium, nanometer silicon carbide, has good heat conduction and insulating properties concurrently, and reduces production cost; perfluorinated calcium, phenylethene modified after vermiculite power; surface property is improved, and is more easy to compatible with other metal ingredient, and auxiliary agent can improve the sintering character of mixing material; shorten sintering time; the heat sink material compact structure that the present invention prepares, light weight insulate, and the capacity of heat transmission is strong; LED chip can be effectively protected, durable in use.

Description

A kind of LED substrate heat sink material and production method thereof
Technical field
The present invention relates to light fixture heat sink material, be specifically related to a kind of LED substrate heat sink material and production method thereof.
Background technology
LED is referred to as forth generation light source, has the advantages such as energy-saving and environmental protection, safety, low energy consumption, high brightness, at daily life In be widely used, the heat dispersion of LED lamp itself is most important, directly influence light fixture service life and illumination effect Really.Existing LED heat sink material is mainly made up of the metal material such as aluminum, copper, there is cost in actual use and limits, insulate The performance shortcoming such as not, the formula of the most necessary improvement material, make material reach the best radiating effect, improve lamp The serviceability of tool, increases the service life.
Summary of the invention
It is an object of the invention to, it is provided that a kind of LED substrate heat sink material, reduce production cost, improve material The purpose of heat dispersion, to achieve these goals, the technical solution used in the present invention is as follows:
A kind of LED substrate heat sink material, it is characterised in that material of the present invention is made up of the raw material of following weight portion: aluminum 60-70, titanium dioxide 7-8, magnesium 8-10, nanometer silicon carbide 12-15, calcium fluoride 2-3, vermiculite power 6-8, styrene 1-3, auxiliary agent 4-5.
Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 4-5, modified boccaro powder 15-18, zirconium acetate 4-5, phosphotungstic acid 1-2, iron powder 5-8, the preparation method of this auxiliary agent is: is first dissolved in appropriate water by phosphotungstic acid, is configured to concentration For the aqueous solution of 4-5%, and being put into by modification boccaro powder in solution, dispersed with stirring filters, in being washed to after uniformly soaking 8-10h Being dried after property, gained material mixes with other residual components, and is heated to 45-55 DEG C, is cooled to after constant temperature dispersed with stirring 2-3h Room temperature, then material is ground to form 450-500 mesh fine powder, to obtain final product;
Described LED substrate heat sink material, its production method is as follows:
(1) calcium fluoride is dissolved in the water of 15 times of its weight portions, subsequently vermiculite power is put in solution, soak 8- Filtering after 10h, filtrate is washed to cold drying after neutrality, adds styrene, standby after mixed grinding 2-3h;
(2) after step (1) gained material being mixed 2-3h with the stirring of other residual components, in input ball mill at ball milling Reason, makes 10000-hole sieve surplus≤0.05% of gained material;
(3) material of step (2) gained is sent in mould compressing, under nitrogen atmosphere with the temperature of 600-650 DEG C After degree sintering 5-6h, through naturally cooling to room temperature and get final product.
It is an advantage of the current invention that: relatively conventional aluminum heat exchanging material combines aluminum, magnesium, nanometer silicon carbide etc. on raw material and becomes Point advantage, have good heat conduction and insulating properties concurrently, and reduce production cost, perfluorinated calcium, phenylethene modified after trematodiasis Stone powder, surface property is improved, and is more easy to compatible with other metal ingredient, and auxiliary agent can improve the sintering character of mixing material, Shortening sintering time, the heat sink material compact structure that the present invention prepares, light weight insulate, and the capacity of heat transmission is strong, can effectively protect Protect LED chip, durable in use.
Detailed description of the invention
Embodiment 1:
The present embodiment LED heat sink material is made up of following raw material: aluminum 70, titanium dioxide 8, magnesium 10, nanometer silicon carbide 15, calcium fluoride 3, vermiculite power 8, styrene 3, auxiliary agent 5.
Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 5, modified boccaro powder 18, zirconium acetate 5, phosphorus Wolframic acid 2, iron powder 8, the preparation method of this auxiliary agent is: be first dissolved in appropriate water by phosphotungstic acid, be configured to concentration be 5% water-soluble Liquid, and modification boccaro powder is put in solution, dispersed with stirring filters after uniformly soaking 10h, is dried, gains after being washed to neutrality Material mixes with other residual components, and is heated to 45-55 DEG C, is cooled to room temperature, then is ground by material after constant temperature dispersed with stirring 3h Become 500 mesh fine powders, to obtain final product;
Described LED substrate heat sink material, its production method is as follows:
(1) calcium fluoride is dissolved in the water of 15 times of its weight portions, subsequently vermiculite power is put in solution, soak 10h Rear filtration, filtrate is washed to cold drying after neutrality, adds styrene, standby after mixed grinding 3h;
(2), after step (1) gained material being mixed 3h with the stirring of other residual components, ball-milling treatment in ball mill is put into, Make 10000-hole sieve surplus≤0.05% of gained material;
(3) material of step (2) gained is sent in mould compressing, under nitrogen atmosphere with the temperature of 600-650 DEG C After degree sintering 6h, through naturally cooling to room temperature and get final product.
The heat conduction system of the heat sink material more conventional LED heat sink material more conventional aluminum base heat sink material obtained by the present embodiment Number raising 23.5%, thermal diffusivity improves 26.8%, and heat balance time averagely shortens 165min, and light fixture improves service life 25.6%.
Embodiment 2:
The present embodiment LED heat sink material is made up of following raw material: aluminum 60, titanium dioxide 7, magnesium 8, nanometer silicon carbide 12, calcium fluoride 2, vermiculite power 6, styrene 1, auxiliary agent 4.
Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 4, modified boccaro powder 15, zirconium acetate 4, phosphorus Wolframic acid 1, iron powder 5, the preparation method of this auxiliary agent is: be first dissolved in appropriate water by phosphotungstic acid, be configured to concentration be 4% water-soluble Liquid, and modification boccaro powder is put in solution, dispersed with stirring filters after uniformly soaking 8h, is dried, gains after being washed to neutrality Material mixes with other residual components, and is heated to 45-55 DEG C, is cooled to room temperature, then is ground by material after constant temperature dispersed with stirring 2h Become 450 mesh fine powders, to obtain final product;
Described LED substrate heat sink material, its production method is as follows:
(1) calcium fluoride is dissolved in the water of 15 times of its weight portions, subsequently vermiculite power is put in solution, after soaking 8h Filtering, filtrate is washed to cold drying after neutrality, adds styrene, standby after mixed grinding 2h;
(2), after step (1) gained material being mixed 2h with the stirring of other residual components, ball-milling treatment in ball mill is put into, Make 10000-hole sieve surplus≤0.05% of gained material;
(3) material of step (2) gained is sent in mould compressing, under nitrogen atmosphere with the temperature of 600-650 DEG C After degree sintering 5h, through naturally cooling to room temperature and get final product.
The heat conduction system of the heat sink material more conventional LED heat sink material more conventional aluminum base heat sink material obtained by the present embodiment Number raising 23.6%, thermal diffusivity improves 26.8%, and heat balance time averagely shortens 163min, and light fixture improves service life 25.5%.

Claims (1)

1. a LED substrate heat sink material, it is characterised in that this material is made up of the raw material of following weight portion: aluminum 60-70, Titanium dioxide 7-8, magnesium 8-10, nanometer silicon carbide 12-15, calcium fluoride 2-3, vermiculite power 6-8, styrene 1-3, auxiliary agent 4-5;
Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 4-5, modified boccaro powder 15-18, zirconium acetate 4-5, Phosphotungstic acid 1-2, iron powder 5-8, the preparation method of this auxiliary agent is: be first dissolved in appropriate water by phosphotungstic acid, and being configured to concentration is 4- The aqueous solution of 5%, and modification boccaro powder is put in solution, dispersed with stirring filters, after being washed to neutrality after uniformly soaking 8-10h Being dried, gained material mixes with other residual components, and is heated to 45-55 DEG C, is cooled to room temperature after constant temperature dispersed with stirring 2-3h, Material is ground to form 450-500 mesh fine powder again, to obtain final product;
Described LED substrate heat sink material, its production method is as follows:
(1) calcium fluoride is dissolved in the water of 15 times of its weight portions, subsequently vermiculite power is put in solution, after soaking 8-10h Filtering, filtrate is washed to cold drying after neutrality, adds styrene, standby after mixed grinding 2-3h;
(2), after step (1) gained material being mixed 2-3h with the stirring of other residual components, put into ball-milling treatment in ball mill, make 10000-hole sieve surplus≤0.05% of gained material;
(3) material of step (2) gained is sent in mould compressing, burn with the temperature of 600-650 DEG C under nitrogen atmosphere After knot 5-6h, through naturally cooling to room temperature and get final product.
CN201610662631.9A 2016-08-11 2016-08-11 A kind of LED substrate heat sink material and production method thereof Pending CN106191545A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610662631.9A CN106191545A (en) 2016-08-11 2016-08-11 A kind of LED substrate heat sink material and production method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610662631.9A CN106191545A (en) 2016-08-11 2016-08-11 A kind of LED substrate heat sink material and production method thereof

Publications (1)

Publication Number Publication Date
CN106191545A true CN106191545A (en) 2016-12-07

Family

ID=57515155

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610662631.9A Pending CN106191545A (en) 2016-08-11 2016-08-11 A kind of LED substrate heat sink material and production method thereof

Country Status (1)

Country Link
CN (1) CN106191545A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104087796A (en) * 2014-07-08 2014-10-08 安徽艳阳电气集团有限公司 Antirust and high-strength aluminum-based composite heat radiating material for LED
CN104087792A (en) * 2014-07-08 2014-10-08 安徽艳阳电气集团有限公司 Insulating temperature-resisting aluminum-based composite heat dispersing material for light emitting diode (LED)
CN104141067A (en) * 2014-07-07 2014-11-12 马鞍山市万鑫铸造有限公司 Aluminum-based composite heat radiating material containing mesoporous molecular sieves for LED (Light Emitting Diode)
CN104141069A (en) * 2014-07-07 2014-11-12 马鞍山市万鑫铸造有限公司 Aluminum-based composite heat radiating material with low heat resistance for LED (Light Emitting Diode)
CN104164594A (en) * 2014-07-07 2014-11-26 马鞍山市万鑫铸造有限公司 A temperature-resistant anti-imbibition aluminum-based composite heat dissipation material used for LED lamps
CN104532073A (en) * 2014-12-26 2015-04-22 合肥瑞华电子科技有限责任公司 Aluminum-based composite radiating material for high strength LED

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104141067A (en) * 2014-07-07 2014-11-12 马鞍山市万鑫铸造有限公司 Aluminum-based composite heat radiating material containing mesoporous molecular sieves for LED (Light Emitting Diode)
CN104141069A (en) * 2014-07-07 2014-11-12 马鞍山市万鑫铸造有限公司 Aluminum-based composite heat radiating material with low heat resistance for LED (Light Emitting Diode)
CN104164594A (en) * 2014-07-07 2014-11-26 马鞍山市万鑫铸造有限公司 A temperature-resistant anti-imbibition aluminum-based composite heat dissipation material used for LED lamps
CN104087796A (en) * 2014-07-08 2014-10-08 安徽艳阳电气集团有限公司 Antirust and high-strength aluminum-based composite heat radiating material for LED
CN104087792A (en) * 2014-07-08 2014-10-08 安徽艳阳电气集团有限公司 Insulating temperature-resisting aluminum-based composite heat dispersing material for light emitting diode (LED)
CN104532073A (en) * 2014-12-26 2015-04-22 合肥瑞华电子科技有限责任公司 Aluminum-based composite radiating material for high strength LED

Similar Documents

Publication Publication Date Title
CN104178664A (en) Aluminum-based composite heat dissipating material of copper-contained anode mud for LED
CN104195378A (en) LED aluminum-base composite heat dissipation material with high thermal conductivity and high thermal stability
CN104195375B (en) A kind of LED aluminum-base composite heat sink material containing modified bamboo fiber
CN104152751B (en) A kind of LED aluminum-base composite heat sink material containing modified potassium titanate crystal whisker
CN104532073A (en) Aluminum-based composite radiating material for high strength LED
CN104164596A (en) LED aluminum-based composite heat-dissipating material containing modified fly ash
CN106048326A (en) LED substrate lightweight heat radiation material and production method thereof
CN106191546A (en) A kind of durable type LED-baseplate composite heat dissipation material and production method thereof
CN104195376A (en) LED aluminum-base composite heat dissipation material containing modified powdered pumice
CN104141069B (en) A kind of LED low thermal resistance aluminum-base composite heat sink material
CN106191545A (en) A kind of LED substrate heat sink material and production method thereof
CN104073695B (en) The aluminum-base composite heat sink material of a kind of LED doping neodymium oxide
CN104073692A (en) Thermally conductive and insulating aluminum base compound radiating material for LED
CN104087792B (en) A kind of LED insulation heatproof aluminum-base composite heat sink material
CN104087793B (en) A kind of LED high heat transfer aluminum-base composite heat sink material
CN106180679A (en) A kind of LED-baseplate composite heat dissipation material and production method thereof
CN106048327A (en) LED substrate composite heat radiation material and production method thereof
CN104711466A (en) Silver powder-containing aluminum-based composite heat dissipating material for high-thermal-conductivity LED
CN104152756A (en) Aluminum-based composite heat radiating material containing modified bentonite for LED (Light-emitting Diode)
CN104073694A (en) High-heat conductivity temperature-resistant aluminum-based composite radiating material for LED (Light-Emitting Diode)
CN104164595A (en) An aluminum-based composite heat dissipation material with good optical properties for LEDs
CN104178708A (en) Aluminum-based composite heat dissipating material containing modified alkali-free glass fibers for LED
CN104164631B (en) A kind of LED aluminum-base composite heat sink material containing modified alumina silicate fibre
CN104152752B (en) A kind of efficient aluminium base composite heat dissipation material of low bulk for LED
CN104152754B (en) Aluminum-based composite heat radiation material containing modified aluminum nitride for LED (light-emitting diode)

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20161207

WD01 Invention patent application deemed withdrawn after publication