CN104195375B - A kind of LED aluminum-base composite heat sink material containing modified bamboo fiber - Google Patents

A kind of LED aluminum-base composite heat sink material containing modified bamboo fiber Download PDF

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CN104195375B
CN104195375B CN201410349525.6A CN201410349525A CN104195375B CN 104195375 B CN104195375 B CN 104195375B CN 201410349525 A CN201410349525 A CN 201410349525A CN 104195375 B CN104195375 B CN 104195375B
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heat sink
sodium
sink material
aluminum
containing modified
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CN104195375A (en
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陈金桃
谢士强
陶慧生
王春连
沈大进
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ANHUI GUANYU PHOTOELECTRIC TECHNOLOGY Co Ltd
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ANHUI GUANYU PHOTOELECTRIC TECHNOLOGY Co Ltd
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Abstract

The present invention relates to light fixture heat sink material, being specifically related to a kind of LED the aluminum-base composite heat sink material containing modified bamboo fiber and production method thereof, this heat sink material is made up of the raw material of following weight portion: aluminum 70 75, aluminium nitride 14 15, carborundum 68, bamboo fibre 15 18, disodium hydrogen phosphate 23, sodium tetraborate 13, sodium formate 0.3 0.4, sodium acetate 0.1 0.2, sodium lignin sulfonate 12, sodium sulfate 12, glyceryl monostearate 23, brown sugar 35, auxiliary agent 45;The advantage that the heat sink material of the present invention combines the compositions such as aluminum, aluminium nitride, carborundum; the mixing weak solution simultaneously utilizing the composition such as disodium hydrogen phosphate, sodium tetraborate carries out immersion treatment to bamboo fibre; improve the compatibility with other composition, reduce production cost, the heat sink material that the present invention prepares is prone to molding; compact structure after sintering; smooth surface, dielectric constant is big, durable in use; good heat-sinking capability can be effectively protected LED chip, extends the service life of light fixture.

Description

A kind of LED aluminum-base composite heat sink material containing modified bamboo fiber
Technical field
The present invention relates to light fixture heat sink material, be specifically related to a kind of LED the aluminum-base composite heat sink material containing modified bamboo fiber and production method thereof.
Background technology
LED is referred to as forth generation light source, has the advantages such as energy-saving and environmental protection, safety, low energy consumption, high brightness, is widely used in daily life, and the heat dispersion of LED lamp itself is most important, directly influences service life and the illuminating effect of light fixture.Existing LED heat sink material is mainly made up of the metal material such as aluminum, copper, exist in actual use cost limit, the insulating properties shortcoming such as not, the formula of the most necessary improvement material, make material reach the best radiating effect, improve the serviceability of light fixture, increase the service life.
Summary of the invention
It is an object of the invention to, it is provided that a kind of LED aluminum-base composite heat sink material containing modified bamboo fiber, to improve the heat dispersion of material, reduce production cost, to achieve these goals, the technical solution used in the present invention is as follows:
A kind of LED aluminum-base composite heat sink material containing modified bamboo fiber, it is characterized in that, material of the present invention is made up of the raw material of following weight portion: aluminum 70-75, aluminium nitride 14-15, carborundum 6-8, bamboo fibre 15-18, disodium hydrogen phosphate 2-3, sodium tetraborate 1-3, sodium formate 0.3-0.4, sodium acetate 0.1-0.2, sodium lignin sulfonate 1-2, sodium sulfate 1-2, glyceryl monostearate 2-3, brown sugar 3-5, auxiliary agent 4-5.
Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 4-5, fluorite fine powder 15-18, zirconium acetate 4-5, glycolic 1-2, iron powder 5-8, potassium fluoroaluminate 6-8, preparation method is: be first dissolved in by glycolic in appropriate water, it is configured to the aqueous solution that concentration is 4-5%, and fluorite fine powder is put in solution, dispersed with stirring filters after uniformly soaking 10-12h, it is dried after being washed to neutrality, gained material mixes with other residual components, and it is heated to 40-50 DEG C, it is cooled to room temperature after constant temperature dispersed with stirring 2-3h, material is ground to form 400-500 mesh fine powder again, obtain.
The described a kind of LED aluminum-base composite heat sink material containing modified bamboo fiber, its production method comprises the steps of
(1) first disodium hydrogen phosphate, sodium tetraborate, sodium formate, sodium acetate, sodium lignin sulfonate being dissolved in the water of 10 times of its weight portions total, and bamboo fibre puts into cold drying after immersion 10-12h in solution, gained material is standby;
(2), after step (1) gained material being mixed 2-3h with the stirring of other residual components, put into ball-milling treatment in ball mill, make 10000-hole sieve surplus≤0.05% of gained material;
(3) material of step (2) gained is sent in mould compressing, after sintering 4-6h with the temperature of 650-700 DEG C under nitrogen atmosphere, through naturally cooling to room temperature and get final product.
It is an advantage of the current invention that: relatively conventional aluminum heat exchanging material combines aluminum on raw material, aluminium nitride, the advantage of the compositions such as carborundum, possess good heat conduction and heat-sinking capability, simultaneously in order to improve the serviceability of bamboo fibre, utilize disodium hydrogen phosphate, sodium tetraborate, sodium formate, sodium acetate, the mixing weak solution of sodium lignin sulfonate carries out immersion treatment to it, improve the compatibility of it and other composition, reduce production cost, auxiliary agent can improve the sintering character of mixing material, shorten sintering time, the heat sink material that the present invention prepares is prone to molding, compact structure after sintering, smooth surface, dielectric constant is big, durable in use, good heat-sinking capability can be effectively protected LED chip, extend the service life of light fixture.
Detailed description of the invention
Embodiment
The present embodiment LED heat sink material is made up of following raw material: aluminum 75, aluminium nitride 15, carborundum 8, bamboo fibre 18, disodium hydrogen phosphate 2, sodium tetraborate 3, sodium formate 0.3, sodium acetate 0.2, sodium lignin sulfonate 2, sodium sulfate 2, glyceryl monostearate 2, brown sugar 5, auxiliary agent 5.
Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 5, fluorite fine powder 18, zirconium acetate 5, glycolic 2, iron powder 8, potassium fluoroaluminate 6, preparation method is: be first dissolved in by glycolic in appropriate water, it is configured to the aqueous solution that concentration is 5%, and fluorite fine powder is put in solution, dispersed with stirring filters after uniformly soaking 12h, it is dried after being washed to neutrality, gained material mixes with other residual components, and it is heated to 40-50 DEG C, it is cooled to room temperature after constant temperature dispersed with stirring 3h, material is ground to form 500 mesh fine powders again, to obtain final product.
The described a kind of LED aluminum-base composite heat sink material containing modified bamboo fiber, its production method comprises the steps of
(1) first disodium hydrogen phosphate, sodium tetraborate, sodium formate, sodium acetate, sodium lignin sulfonate being dissolved in the water of 10 times of its weight portions total, and bamboo fibre puts into cold drying after immersion 12h in solution, gained material is standby;
(2), after step (1) gained material being mixed 3h with the stirring of other residual components, put into ball-milling treatment in ball mill, make 10000-hole sieve surplus≤0.05% of gained material;
(3) material of step (2) gained is sent in mould compressing, after sintering 6h with the temperature of 650-700 DEG C under nitrogen atmosphere, through naturally cooling to room temperature and get final product.
The heat conductivity of the heat sink material more conventional LED heat sink material more conventional aluminum base heat sink material obtained by the present embodiment improves 26.2%, and thermal diffusivity improves 27.3%, and heat balance time averagely shortens 150min, and light fixture improves 28.3% service life.

Claims (1)

1. a LED aluminum-base composite heat sink material containing modified bamboo fiber, it is characterized in that, this heat sink material is made up of the raw material of following weight portion: aluminum 70-75, aluminium nitride 14-15, carborundum 6-8, bamboo fibre 15-18, disodium hydrogen phosphate 2-3, sodium tetraborate 1-3, sodium formate 0.3-0.4, sodium acetate 0.1-0.2, sodium lignin sulfonate 1-2, sodium sulfate 1-2, glyceryl monostearate 2-3, brown sugar 3-5, auxiliary agent 4-5;
Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 4-5, fluorite fine powder 15-18, zirconium acetate 4-5, glycolic 1-2, iron powder 5-8, potassium fluoroaluminate 6-8, preparation method is: be first dissolved in by glycolic in appropriate water, it is configured to the aqueous solution that concentration is 4-5%, and fluorite fine powder is put in solution, dispersed with stirring filters after uniformly soaking 10-12h, it is dried after being washed to neutrality, gained material mixes with other residual components, and it is heated to 40-50 DEG C, it is cooled to room temperature after constant temperature dispersed with stirring 2-3h, material is ground to form 400-500 mesh fine powder again, obtain;
Described LED is as follows by the production method of the aluminum-base composite heat sink material containing modified bamboo fiber:
(1) first disodium hydrogen phosphate, sodium tetraborate, sodium formate, sodium acetate, sodium lignin sulfonate being dissolved in the water of 10 times of its weight portions total, and bamboo fibre puts into cold drying after immersion 10-12h in solution, gained material is standby;
(2), after step (1) gained material being mixed 2-3h with the stirring of other residual components, put into ball-milling treatment in ball mill, make 10000-hole sieve surplus≤0.05% of gained material;
(3) material of step (2) gained is sent in mould compressing, after sintering 4-6h with the temperature of 650-700 DEG C under nitrogen atmosphere, through naturally cooling to room temperature and get final product.
CN201410349525.6A 2014-07-22 2014-07-22 A kind of LED aluminum-base composite heat sink material containing modified bamboo fiber Active CN104195375B (en)

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CN105585788B (en) * 2015-11-24 2018-01-12 杭州杭复新材料科技有限公司 A kind of reticulated thermoplastic's heat-conduction electric insulation composite material radiator structure
CN105524423B (en) * 2015-11-24 2017-11-07 合复新材料科技(无锡)有限公司 A kind of cellular thermosetting heat-conduction electric insulation composite material radiator structure
CN105924888A (en) * 2016-04-19 2016-09-07 安徽路明光电科技有限公司 Mainboard for LED lamp and production process thereof
CN107761017B (en) * 2017-10-09 2019-12-20 青海大学 Lightweight aluminum bamboo/carbon composite material and preparation method and application thereof
CN111961994A (en) * 2020-09-03 2020-11-20 王思记 Explosion suppression aluminum-titanium pipe and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4134759A (en) * 1976-09-01 1979-01-16 The Research Institute For Iron, Steel And Other Metals Of The Tohoku University Light metal matrix composite materials reinforced with silicon carbide fibers
JP2002128044A (en) * 2000-10-30 2002-05-09 Taiheiyo Cement Corp Electronic component housing tray
CN101864532A (en) * 2010-05-17 2010-10-20 盐城市赛瑞特半导体照明有限公司 Superconductive aluminum-based alloy for LED heat dissipation device
CN103014396A (en) * 2012-12-05 2013-04-03 安徽徽铝铝业有限公司 Preparation method of refining agent used for smelting aluminium alloy sections

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4134759A (en) * 1976-09-01 1979-01-16 The Research Institute For Iron, Steel And Other Metals Of The Tohoku University Light metal matrix composite materials reinforced with silicon carbide fibers
JP2002128044A (en) * 2000-10-30 2002-05-09 Taiheiyo Cement Corp Electronic component housing tray
CN101864532A (en) * 2010-05-17 2010-10-20 盐城市赛瑞特半导体照明有限公司 Superconductive aluminum-based alloy for LED heat dissipation device
CN103014396A (en) * 2012-12-05 2013-04-03 安徽徽铝铝业有限公司 Preparation method of refining agent used for smelting aluminium alloy sections

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