CN106189935A - Adhesive and preparation method thereof used by bamboo pole bamboo cane of growing up - Google Patents

Adhesive and preparation method thereof used by bamboo pole bamboo cane of growing up Download PDF

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Publication number
CN106189935A
CN106189935A CN201610533407.XA CN201610533407A CN106189935A CN 106189935 A CN106189935 A CN 106189935A CN 201610533407 A CN201610533407 A CN 201610533407A CN 106189935 A CN106189935 A CN 106189935A
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China
Prior art keywords
water
parts
add
adhesive
take
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CN201610533407.XA
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Chinese (zh)
Inventor
王静
肖可可
李勇
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Funan Mingyu Wicker-Wood Crafts Co Ltd
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Funan Mingyu Wicker-Wood Crafts Co Ltd
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Priority to CN201610533407.XA priority Critical patent/CN106189935A/en
Publication of CN106189935A publication Critical patent/CN106189935A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J123/00Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers
    • C09J123/26Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers modified by chemical after-treatment
    • C09J123/32Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers modified by chemical after-treatment by reaction with compounds containing phosphorus or sulfur
    • C09J123/34Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers modified by chemical after-treatment by reaction with compounds containing phosphorus or sulfur by chlorosulfonation
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/04Non-macromolecular additives inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/06Non-macromolecular additives organic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

Grow up adhesive used by bamboo pole bamboo cane and preparation method thereof, by an agitator tank, two reactors separately work, prepare base material, then base material is mixed with obtains adhesive.The adhesive prepared by this law, adhesive is half thick, can convenient construction, instill adhesive simultaneously, adhesive adhesive force is strong, without flowing, free from extraneous odour, also rapid solidification, the gluing effect time is longer, overall corrosion-free, it is prevented effectively from bamboo weaving viscose and adheres to over a long time and cause bamboo weaving junction to be ruptured, it is simple to promote and use.

Description

Adhesive and preparation method thereof used by bamboo pole bamboo cane of growing up
Technical field:
The present invention relates to relate to a kind of adhesive, be specifically related to grow up adhesive and preparation method thereof used by bamboo pole bamboo cane.
Background technology:
Chemical industry is to develop the most rapid mainstay of the national economy industry modern times, and fine chemistry industry tail gas important set Becoming part, obtained the development advanced by leaps and bounds in 20th century, the clothing, food, lodging and transportion--basic necessities of life of the unresolved mankind and the energy, resource and environment are asked Topic makes significant contribution.
Adhesive is development of modern industry and human living standard improves requisite important materials, adhesive and bonding Technology, with the incomparable special warfare of other connected modes, plays great in modern economy, modern national defense, modern science and technology Effect.
Summary of the invention:
The technical problem to be solved is to overcome the defect of prior art, it is provided that a kind of bamboo pole bamboo cane institute that grows up With adhesive and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions.
Adhesive used by bamboo pole bamboo cane of growing up, it is characterised in that: mainly include that following mass parts component is prepared from:
1) chlorosulfonated polyethylene 100-110 part, 30-40 part ethyl acetate, 20-25 part n-octyl alcohol, 25-30 part isoamyl alcohol, 20-25 part isobutanol, 8-10 part castor oil polyoxyethylene ether, 6-8 part dodecylbenzene sodium sulfonate, Herba Moslae 0.5-1 part, Rhizoma Pinelliae 0.5-1 part, Poria 0.5-1 part, Fructus Aurantii Immaturus 0.2-0.5 part, Caulis Bambusae In Taenia 1-2 part and Folium Isatidis 1-2 part;
Take Herba Moslae 0.5-1 part, Rhizoma Pinelliae 0.5-1 part, Poria 0.5-1 part, Fructus Aurantii Immaturus 0.2-0.5 part, Caulis Bambusae In Taenia 1-2 part and Folium Isatidis Leaf 1-2 part, grinds to form powdery, adds in the water of 10 parts, and steaming and decocting treats that raw material is dissolved completely in water, and entirety is in the pasty state;
By chloromethyloxirane, ethyl acetate, n-octyl alcohol, isoamyl alcohol, isobutanol, castor oil polyoxyethylene ether, 12 Sodium alkyl benzene sulfonate, being placed in agitator tank, mixing speed is 2500r/mim, and whipping temp is 80-90 DEG C, 5 minutes time;
Pasty mixture is filtered, adds and agitator tank continues stirring;
2) water repellent agent: 50-60 part, starch: 12-15 part, Borax: 0.3-0.4 part, soluble polyurethane: 0.2-0.3 part, Acidic oxidation agent: 0.2-0.3 part, organic acid: 0.1-0.2 part, water: 40-50 part, Herba Ephedrae 10-15 part, Concha Margaritifera 10-15 part, process Radix Polygalae 7-12 part, Rhizoma Acori Graminei 5-10 part;
Take and add after Herba Ephedrae 10-15 part, Concha Margaritifera 10-15 part, Cortex et Radix Polygalae (processed) 7-12 part and Rhizoma Acori Graminei 5-10 part are pulverized Soaking in the water of 50%, soaking temperature is 40 DEG C, soaks and is often 30 parts, takes out liquid;
Water repellent agent and 70% liquid mixing are added in reactor, within 4 hours, makes water repellent agent be completely dissolved with 90 DEG C of stirrings, fall Temperature is to 75 DEG C, by soluble polyurethane, acidic oxidation agent and 10% liquid mixing, dropping Borax and soluble polyurethane, acidity Oxidant and water mixed solution, drip off for about 1-2 hour, insulation reaction 1 hour, is subsequently adding starch, continues heated and stirred 1 little Time, add organic acid stirring, drop to less than 50 DEG C to temperature;
3) chlorosulfonated polyethylene 100-110 part, gas-phase silica 2-3 part, titanium dioxide 3-5 part, disproportionated rosin 5-10 part, TOTD2-3 part, ethylene thiourea 2-3 part, epoxy resin 15-20 part, four sulfuration tetramethyl thiuram 2-5 part, Oryza glutinosa 10-70 part, purples Rice 10-70 part, fructus zizaniae caduciflorae 10-70 part, SEMEN COICIS 5-10 part, Semen arachidis hypogaeae 5-10 part, kidney bean 1-5 part, Bulbus Lilii 5-10 part, Semen Phaseoli 1-5 part, Semen phaseoli radiati 1-5 part, water 80-90 part;
Raw material is preheated, loads in tank, select chlorosulfonated polyethylene, gas-phase silica, titanium dioxide, add reactor, It is simultaneously introduced fructus zizaniae caduciflorae, SEMEN COICIS, Semen arachidis hypogaeae water grinds, adds 50% water mixing, make mixture one,
Select disproportionated rosin, TOTD, epoxy resin, four sulfuration tetramethyl thiuram, ethylene thioureas, be simultaneously introduced Oryza glutinosa, purple rice, Kidney bean, Bulbus Lilii, Semen Phaseoli, Semen phaseoli radiati mixing, add 50% water mixing, make mixture two, takes 50% mixture one and 85% mix Compound two, adds in reactor and heats, and heating-up temperature 160 DEG C, is cooled to 100 DEG C at 1 hour time, 1 hour time, then is down to 50 DEG C, impurity screening, obtain hot glue;
4) take 50% mixture one and add step 1) agitator tank in, add 20% hot glue;Take the mixture two of 15 to add Enter step 2) in reactor in, add 30% hot glue, then by both mix, obtain semi-finished product adhesive;Take the heat of 50% Glue, distillation, take distilled water, add in semi-finished product adhesive, obtain finished product.
The present invention has the beneficial effects that: the adhesive prepared by this law, and adhesive is half thick, can convenient construction, Instilling adhesive, adhesive adhesive force is strong simultaneously, and without flowing, free from extraneous odour, also rapid solidification, the gluing effect time is longer, overall Corrosion-free, it is prevented effectively from bamboo weaving viscose and adheres to over a long time and cause bamboo weaving junction to be ruptured, it is simple to promote and use.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below knot Close specific embodiment, the present invention is expanded on further.
Embodiment 1: adhesive used by bamboo pole bamboo cane of growing up, mainly includes that following mass parts component is prepared from:
1) 100 parts, 30 parts ethyl acetate of chlorosulfonated polyethylene, 20 parts of n-octyl alcohols, 25 parts of isoamyl alcohol, 20 parts of isobutanol, 8 parts Castor oil polyoxyethylene ether, 6 parts of dodecylbenzene sodium sulfonate, Herba Moslae 0.5 part, Rhizoma Pinelliae 0.5 part, 0.5 part of Poria, Fructus Aurantii Immaturuss 0.2 Part, Caulis Bambusae In Taenia 1 part and Folium Isatidis 1 part;
Take Herba Moslae 0.5 part, Rhizoma Pinelliae 0.5 part, 0.5 part of Poria, Fructus Aurantii Immaturus 0.2 part, Caulis Bambusae In Taenia 1 part and Folium Isatidis 1 part, grind to form Powdery, adds in the water of 10 parts, and steaming and decocting treats that raw material is dissolved completely in water, and entirety is in the pasty state;
By chloromethyloxirane, ethyl acetate, n-octyl alcohol, isoamyl alcohol, isobutanol, castor oil polyoxyethylene ether, 12 Sodium alkyl benzene sulfonate, being placed in agitator tank, mixing speed is 2500r/mim, and whipping temp is 80-90 DEG C, 5 minutes time;
Pasty mixture is filtered, adds and agitator tank continues stirring;
2) water repellent agent: 50 parts, starch: 12 parts, Borax: 0.3 part, soluble polyurethane: 0.2 part, acidic oxidation agent: 0.2 Part, organic acid: 0.1 part, water: 40 parts, 10 parts of Herba Ephedrae, Concha Margaritifera 10 parts, Cortex et Radix Polygalae (processed) 7 parts, Rhizoma Acori Graminei 5 parts;
Take in the water joining 50% after 10 parts of Herba Ephedrae, Concha Margaritifera 10 parts, Cortex et Radix Polygalae (processed) 7 parts and Rhizoma Acori Graminei 5 parts are pulverized Soaking, soaking temperature is 40 DEG C, soaks and is often 30 parts, takes out liquid;
Water repellent agent and 70% liquid mixing are added in reactor, within 4 hours, makes water repellent agent be completely dissolved with 90 DEG C of stirrings, fall Temperature is to 75 DEG C, by soluble polyurethane, acidic oxidation agent and 10% liquid mixing, dropping Borax and soluble polyurethane, acidity Oxidant and water mixed solution, drip off for about 1-2 hour, insulation reaction 1 hour, is subsequently adding starch, continues heated and stirred 1 little Time, add organic acid stirring, drop to less than 50 DEG C to temperature;
3) chlorosulfonated polyethylene 100 parts, gas-phase silica 2 parts, titanium dioxide 3 parts, disproportionated rosin 5 parts, TOTD2 part, second Alkene thiourea 2 parts, epoxy resin 15 parts, four sulfuration tetramethyl thiuram 2 parts, 10 parts of Oryza glutinosa, purple rice 10 parts, fructus zizaniae caduciflorae 10 parts, SEMEN COICIS 5 Part, Semen arachidis hypogaeae 5 parts, kidney bean 1 part, Bulbus Lilii 5 parts, 1 part of Semen Phaseoli, 1 part of Semen phaseoli radiati, 80 parts of water;
Raw material is preheated, loads in tank, select chlorosulfonated polyethylene, gas-phase silica, titanium dioxide, add reactor, It is simultaneously introduced fructus zizaniae caduciflorae, SEMEN COICIS, Semen arachidis hypogaeae water grinds, adds 50% water mixing, make mixture one,
Select disproportionated rosin, TOTD, epoxy resin, four sulfuration tetramethyl thiuram, ethylene thioureas, be simultaneously introduced Oryza glutinosa, purple rice, Kidney bean, Bulbus Lilii, Semen Phaseoli, Semen phaseoli radiati mixing, add 50% water mixing, make mixture two, takes 50% mixture one and 85% mix Compound two, adds in reactor and heats, and heating-up temperature 160 DEG C, is cooled to 100 DEG C at 1 hour time, 1 hour time, then is down to 50 DEG C, impurity screening, obtain hot glue;
4) take 50% mixture one and add step 1) agitator tank in, add 20% hot glue;Take the mixture two of 15 to add Enter step 2) in reactor in, add 30% hot glue, then by both mix, obtain semi-finished product adhesive;Take the heat of 50% Glue, distillation, take distilled water, add in semi-finished product adhesive, obtain finished product.
Embodiment 2: adhesive used by bamboo pole bamboo cane of growing up, mainly includes that following mass parts component is prepared from:
1) 110 parts, 40 parts ethyl acetate of chlorosulfonated polyethylene, 25 parts of n-octyl alcohols, 30 parts of isoamyl alcohol, 25 parts of isobutanol, 10 Part castor oil polyoxyethylene ether, 8 parts of dodecylbenzene sodium sulfonate, Herba Moslae 1 part, Rhizoma Pinelliae 1 part, 1 part of Poria, Fructus Aurantii Immaturuss 0.5 part, bamboo Eat 2 parts and Folium Isatidis 2 parts;
Take Herba Moslae 1 part, Rhizoma Pinelliae 1 part, 1 part of Poria, Fructus Aurantii Immaturus 0.5 part, Caulis Bambusae In Taenia 2 parts and Folium Isatidis 2 parts, grind to form powdery, Add in the water of 10 parts, steaming and decocting, treat that raw material is dissolved completely in water, entirety is in the pasty state;
By chloromethyloxirane, ethyl acetate, n-octyl alcohol, isoamyl alcohol, isobutanol, castor oil polyoxyethylene ether, 12 Sodium alkyl benzene sulfonate, being placed in agitator tank, mixing speed is 2500r/mim, and whipping temp is 80-90 DEG C, 5 minutes time;
Pasty mixture is filtered, adds and agitator tank continues stirring;
2) water repellent agent: 60 parts, starch: 15 parts, Borax: 0.4 part, soluble polyurethane: 0.3 part, acidic oxidation agent: 0.3 Part, organic acid: 0.2 part, water: 50 parts, 15 parts of Herba Ephedrae, Concha Margaritifera 15 parts, Cortex et Radix Polygalae (processed) 12 parts, Rhizoma Acori Graminei 10 parts;
Take the water joining 50% after 15 parts of Herba Ephedrae, Concha Margaritifera 15 parts, Cortex et Radix Polygalae (processed) 12 parts and Rhizoma Acori Graminei 10 parts are pulverized Middle immersion, soaking temperature is 40 DEG C, soaks and is often 30 parts, takes out liquid;
Water repellent agent and 70% liquid mixing are added in reactor, within 4 hours, makes water repellent agent be completely dissolved with 90 DEG C of stirrings, fall Temperature is to 75 DEG C, by soluble polyurethane, acidic oxidation agent and 10% liquid mixing, dropping Borax and soluble polyurethane, acidity Oxidant and water mixed solution, drip off for about 1-2 hour, insulation reaction 1 hour, is subsequently adding starch, continues heated and stirred 1 little Time, add organic acid stirring, drop to less than 50 DEG C to temperature;
3) chlorosulfonated polyethylene 110 parts, gas-phase silica 3 parts, titanium dioxide 5 parts, disproportionated rosin 10 parts, TOTD3 part, second Alkene thiourea 3 parts, epoxy resin 20 parts, four sulfuration tetramethyl thiuram 5 parts, 70 parts of Oryza glutinosa, purple rice 70 parts, fructus zizaniae caduciflorae 70 parts, SEMEN COICIS 10 parts, Semen arachidis hypogaeae 10 parts, kidney bean 5 parts, Bulbus Lilii 10 parts, 5 parts of Semen Phaseoli, 5 parts of Semen phaseoli radiati, 90 parts of water;
Raw material is preheated, loads in tank, select chlorosulfonated polyethylene, gas-phase silica, titanium dioxide, add reactor, It is simultaneously introduced fructus zizaniae caduciflorae, SEMEN COICIS, Semen arachidis hypogaeae water grinds, adds 50% water mixing, make mixture one,
Select disproportionated rosin, TOTD, epoxy resin, four sulfuration tetramethyl thiuram, ethylene thioureas, be simultaneously introduced Oryza glutinosa, purple rice, Kidney bean, Bulbus Lilii, Semen Phaseoli, Semen phaseoli radiati mixing, add 50% water mixing, make mixture two, takes 50% mixture one and 85% mix Compound two, adds in reactor and heats, and heating-up temperature 160 DEG C, is cooled to 100 DEG C at 1 hour time, 1 hour time, then is down to 50 DEG C, impurity screening, obtain hot glue;
4) take 50% mixture one and add step 1) agitator tank in, add 20% hot glue;Take the mixture two of 15 to add Enter step 2) in reactor in, add 30% hot glue, then by both mix, obtain semi-finished product adhesive;Take the heat of 50% Glue, distillation, take distilled water, add in semi-finished product adhesive, obtain finished product.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these become Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and Equivalent defines.

Claims (1)

1. grow up adhesive used by bamboo pole bamboo cane, it is characterised in that: mainly include that following mass parts component is prepared from:
1) chlorosulfonated polyethylene 100-110 part, 30-40 part ethyl acetate, 20-25 part n-octyl alcohol, 25-30 part isoamyl alcohol, 20-25 Part isobutanol, 8-10 part castor oil polyoxyethylene ether, 6-8 part dodecylbenzene sodium sulfonate, Herba Moslae 0.5-1 part, Rhizoma Pinelliae 0.5-1 Part, Poria 0.5-1 part, Fructus Aurantii Immaturus 0.2-0.5 part, Caulis Bambusae In Taenia 1-2 part and Folium Isatidis 1-2 part;
Take Herba Moslae 0.5-1 part, Rhizoma Pinelliae 0.5-1 part, Poria 0.5-1 part, Fructus Aurantii Immaturus 0.2-0.5 part, Caulis Bambusae In Taenia 1-2 part and Folium Isatidis 1- 2 parts, grind to form powdery, add in the water of 10 parts, steaming and decocting, treat that raw material is dissolved completely in water, entirety is in the pasty state;
By chloromethyloxirane, ethyl acetate, n-octyl alcohol, isoamyl alcohol, isobutanol, castor oil polyoxyethylene ether, dodecyl Benzene sulfonic acid sodium salt, being placed in agitator tank, mixing speed is 2500r/mim, and whipping temp is 80-90 DEG C, 5 minutes time;
Pasty mixture is filtered, adds and agitator tank continues stirring;
2) water repellent agent: 50-60 part, starch: 12-15 part, Borax: 0.3-0.4 part, soluble polyurethane: 0.2-0.3 part, acid Oxidant: 0.2-0.3 part, organic acid: 0.1-0.2 part, water: 40-50 part, Herba Ephedrae 10-15 part, Concha Margaritifera 10-15 part, Cortex et Radix Polygalae (processed) 7-12 part, Rhizoma Acori Graminei 5-10 part;
Take after Herba Ephedrae 10-15 part, Concha Margaritifera 10-15 part, Cortex et Radix Polygalae (processed) 7-12 part and Rhizoma Acori Graminei 5-10 part are pulverized and join Soaking in the water of 50%, soaking temperature is 40 DEG C, soaks and is often 30 parts, takes out liquid;
Water repellent agent and 70% liquid mixing are added in reactor, within 4 hours, makes water repellent agent be completely dissolved with 90 DEG C of stirrings, be cooled to 75 DEG C, by soluble polyurethane, acidic oxidation agent and 10% liquid mixing, dropping Borax and soluble polyurethane, acidic oxidation Agent and water mixed solution, drip off for about 1-2 hour, insulation reaction 1 hour, is subsequently adding starch, continues heated and stirred 1 hour, adds Enter organic acid stirring, drop to less than 50 DEG C to temperature;
3) chlorosulfonated polyethylene 100-110 part, gas-phase silica 2-3 part, titanium dioxide 3-5 part, disproportionated rosin 5-10 part, TOTD2-3 part, ethylene thiourea 2-3 part, epoxy resin 15-20 part, four sulfuration tetramethyl thiuram 2-5 part, Oryza glutinosa 10-70 part, purples Rice 10-70 part, fructus zizaniae caduciflorae 10-70 part, SEMEN COICIS 5-10 part, Semen arachidis hypogaeae 5-10 part, kidney bean 1-5 part, Bulbus Lilii 5-10 part, Semen Phaseoli 1-5 part, Semen phaseoli radiati 1-5 part, water 80-90 part;
Raw material is preheated, loads in tank, select chlorosulfonated polyethylene, gas-phase silica, titanium dioxide, add reactor, simultaneously Add fructus zizaniae caduciflorae, SEMEN COICIS, Semen arachidis hypogaeae water grinds, add 50% water mixing, make mixture one,
Select disproportionated rosin, TOTD, epoxy resin, four sulfuration tetramethyl thiuram, ethylene thioureas, be simultaneously introduced Oryza glutinosa, purple rice, cloud Bean, Bulbus Lilii, Semen Phaseoli, Semen phaseoli radiati mixing, add 50% water mixing, make mixture two, take 50% mixture one and the mixing of 85% Thing two, adds in reactor and heats, and heating-up temperature 160 DEG C, is cooled to 100 DEG C at 1 hour time, 1 hour time, then is down to 50 DEG C, impurity screening, obtain hot glue;
4) take 50% mixture one and add step 1) agitator tank in, add 20% hot glue;The mixture two taking 15 adds step Rapid 2), in the reactor in, add the hot glue of 30%, then both are mixed, obtain semi-finished product adhesive;Take the hot glue of 50%, steam Evaporate, take distilled water, add in semi-finished product adhesive, obtain finished product.
CN201610533407.XA 2016-07-07 2016-07-07 Adhesive and preparation method thereof used by bamboo pole bamboo cane of growing up Pending CN106189935A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105001809A (en) * 2015-06-26 2015-10-28 蚌埠市鸿安精密机械有限公司 Bio-adhesive timber glue
CN105017975A (en) * 2015-06-26 2015-11-04 蚌埠市鸿安精密机械有限公司 Micro-foamed wood adhesive

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105001809A (en) * 2015-06-26 2015-10-28 蚌埠市鸿安精密机械有限公司 Bio-adhesive timber glue
CN105017975A (en) * 2015-06-26 2015-11-04 蚌埠市鸿安精密机械有限公司 Micro-foamed wood adhesive

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