CN106189480A - Water-base ink cleaning agent of printed substrate and preparation method thereof - Google Patents
Water-base ink cleaning agent of printed substrate and preparation method thereof Download PDFInfo
- Publication number
- CN106189480A CN106189480A CN201610855027.8A CN201610855027A CN106189480A CN 106189480 A CN106189480 A CN 106189480A CN 201610855027 A CN201610855027 A CN 201610855027A CN 106189480 A CN106189480 A CN 106189480A
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- Prior art keywords
- sodium
- water
- cleaning agent
- base ink
- ink cleaning
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D9/00—Chemical paint or ink removers
- C09D9/04—Chemical paint or ink removers with surface-active agents
Abstract
The present invention proposes water-base ink cleaning agent of a kind of printed substrate and preparation method thereof, calculate according to mass percent, its component is: butylphosphoric acid ester 4～10%, triolein 2～4%, alkali inorganic substance 1～5%, surfactant 3～6%, sodium metasilicate 0.2～0.6%, Disodium oxalate. 0.2～0.6% surplus are deionized water.Preparation method: at normal temperatures, is first added to the water surfactant, alkali inorganic substance, is sufficiently stirred for, after making each component be completely dissolved, adding butylphosphoric acid ester, triolein, sodium metasilicate and Disodium oxalate., stirring to transparent clarification, the uniform liquid obtained is water-base ink cleaning agent.The not only environmental protection of this abluent, and cleaning efficiency is high, system stability is good strong with anti-corrosion capability.
Description
Technical field
The invention belongs to detergent for ink technical field, be specifically related to a kind of printed substrate water-base ink cleaning agent and
Its preparation method.
Background technology
The development of China printing industry is swift and violent, in Pearl River Delta, the Yangtze River Delta, the developed region such as Bohai Economic Rim define product
Industrial belt, and just in accelerated development, the regional economy just having due to China's press increases bright spot and receives much concern.And in printing
While producing high speed development, also will increasingly as the demand of requisite auxiliary material ink abluent in printing
Greatly.Printing enterprise of China there are about 170,000 at present, and every printing equipment of Mei Jia enterprise the most at least consumes 100 liters of abluents,
From this, the whole nation is every year to the printing ink washing agent at least demand of 6.12 hundred million liters, the Yangtze River Delta, area, Pearl River Delta are then
Occupying the ratio of about 70%, therefore, printing ink washing agent has huge market capacity.
Printed circuit board (PCB) is indispensable critical electronic interconnect in each electronic product.Send out at a high speed with electronic industry
Exhibition, a large amount of household electrical appliance start upgrading, and the quantity of waste and old circuit board is increasing, in order to build economy environmental friendliness
Type society, the recycling to be carried out of a large amount of waste and old circuit boards.Printed circuit board surface has one layer of photosensitive development through heat cure
Ink protection metal, should clean up the ink on its surface before recycling.Cleaning forme in current printing industry,
The ink at ink position waited by printing machinery, printing manuscript, is used mostly organic washing agent and alkaline cleaner, organic washing agent poison
Property big, big to human body and environmental hazard, be therefore badly in need of that exploitation cleaning performance is good, the abluent of environmental protection.
Summary of the invention
The present invention proposes the water-base ink cleaning agent of a kind of printed substrate, the not only environmental protection of this abluent, and cleans effect
Rate is high, system stability is good strong with anti-corrosion capability.
The technical scheme is that and be achieved in that:
The water-base ink cleaning agent of a kind of printed substrate, calculates according to mass percent, and its component is:
Butylphosphoric acid ester 4～10%, triolein 2～4%, alkali inorganic substance 1～5%, surfactant 3～6%,
Sodium metasilicate 0.2～0.6%, Disodium oxalate. 0.2～0.6%, surplus is deionized water.
Further, during described alkali inorganic substance is sodium carbonate, sodium hydroxide, tertiary sodium phosphate, sodium silicate and sodium tripolyphosphate
One or both combination.
Further, described surfactant is fatty alcohol-polyoxyethylene ether, polyoxyethylene lauryl ether sodium sulfate, dodecane
The mixing of one or more in base benzene sulfonic acid sodium salt or aliphatic alcohol polyoxyvinethene phosphate salt.
It is a further object to provide the preparation method of the water-base ink cleaning agent of a kind of printed substrate, including
Following steps: weigh each component in above ratio, at normal temperatures, first surfactant, alkali inorganic substance are added to the water, fully
Stirring, after making each component be completely dissolved, adds butylphosphoric acid ester, triolein, sodium metasilicate and Disodium oxalate., and stirring is extremely
Transparent clarification, the uniform liquid obtained is water-base ink cleaning agent.
Further, during described alkali inorganic substance is sodium carbonate, sodium hydroxide, tertiary sodium phosphate, sodium silicate and sodium tripolyphosphate
One or both combination.
Further, described surfactant is fatty alcohol-polyoxyethylene ether (AEO-9), polyoxyethylene lauryl ether sulphuric acid
One in sodium, dodecylbenzene sodium sulfonate (LAS) or aliphatic alcohol polyoxyvinethene phosphate salt (such as AES-Na or MOA-3p)
Or several mixing.
Beneficial effects of the present invention:
1, the present invention selects butylphosphoric acid ester and triolein as the host of ink, and it has good in alkaline environment
Decontamination well, emulsifying, wettability, stronger degreasing power, and printed wire board device is also had good corrosion inhibition.
2, add sodium metasilicate, not only strong detergency, and there is antiseptic and rustproof effect；Disodium oxalate. can effectively prevent ink
Other components corrosion to board metal surface in abluent, and effectively metal ingredient can be deposited in circuit board surface
Above.
3, the water-base ink cleaning agent of the printed substrate of the present invention to plain edition printed substrate dipping clean 2～
3min, baking property printed substrate dipping cleans 15～20min, and ink clearance is up to 100%；Performance test results such as following table
1:
The performance test results of the water-base ink cleaning agent of the printed substrate of table 1 present invention
| Detection project | Technical specification | Testing result |
| Outward appearance | Uniformly, not stratified, without precipitation | Conformance with standard specifies |
| PH value | 6-12 | 6～10 |
| Washing power | 90% | 98 |
| Foaming properties | (5min height)≤20 | 5 |
| Stability | Uniformly, not stratified | Conformance with standard specifies |
| No. 45 steel corrosions | 0 grade ,≤2mg | 0 grade, 0.2mg |
| LY12 duralumin corrosivity | 0 grade ,≤2mg | 0 grade, 0.1mg |
Detailed description of the invention
Embodiment 1
The water-base ink cleaning agent of a kind of printed substrate, calculates according to mass percent, and its component is:
Butylphosphoric acid ester 4%, triolein 2%, sodium hydroxide 1%, tertiary sodium phosphate 0.5%, aliphatic alcohol polyethenoxy
Ether 1%, polyoxyethylene lauryl ether sodium sulfate 1%, sodium metasilicate 0.2%, Disodium oxalate. 0.2%, surplus is deionized water.
Preparation method:
Each component is weighed, at normal temperatures, first by fatty alcohol-polyoxyethylene ether, polyoxyethylene lauryl ether sulfur in above ratio
Acid sodium, sodium hydroxide, tertiary sodium phosphate are added to the water, and are sufficiently stirred for, and after making each component be completely dissolved, add butylphosphoric acid ester, sweet
Oil trioleate, sodium metasilicate and Disodium oxalate., stirring to transparent clarification, the uniform liquid obtained is water-based inks and cleans
Agent.
Embodiment 2
The water-base ink cleaning agent of a kind of printed substrate, calculates according to mass percent, and its component is:
Butylphosphoric acid ester 6%, triolein 2%, tertiary sodium phosphate 0.5%, sodium silicate 0.5%, DBSA
Sodium 3%, sodium metasilicate 0.3%, Disodium oxalate. 0.3%, surplus is deionized water.
Preparation method:
Weigh each component in above ratio, at normal temperatures, first dodecylbenzene sodium sulfonate, sodium silicate, tertiary sodium phosphate are added
Enter in water, be sufficiently stirred for, after making each component be completely dissolved, add butylphosphoric acid ester, triolein, sodium metasilicate and grass
Acid sodium, stirring to transparent clarification, the uniform liquid obtained is water-base ink cleaning agent.
Embodiment 3
The water-base ink cleaning agent of a kind of printed substrate, calculates according to mass percent, and its component is:
Butylphosphoric acid ester 4～10%, triolein 2～4%, sodium silicate 2%, sodium tripolyphosphate 1%, MOA-3p
3%, polyoxyethylene lauryl ether sodium sulfate 1%, sodium metasilicate 0.3%, Disodium oxalate. 0.4%, surplus is deionized water.
Preparation method:
Each component is weighed, at normal temperatures, first by MOA-3p, polyoxyethylene lauryl ether sodium sulfate, trimerization in above ratio
Sodium phosphate, sodium silicate are added to the water, and are sufficiently stirred for, and after making each component be completely dissolved, add butylphosphoric acid ester, glycerol three oleic acid
Ester, sodium metasilicate and Disodium oxalate., stirring to transparent clarification, the uniform liquid obtained is water-base ink cleaning agent.
Embodiment 4
The water-base ink cleaning agent of a kind of printed substrate, calculates according to mass percent, and its component is:
Butylphosphoric acid ester 10%, triolein 4%, sodium carbonate 2%, sodium hydroxide 3%, polyoxyethylene lauryl ether sulfur
Acid sodium 3%, dodecylbenzene sodium sulfonate 3%, sodium metasilicate 0.6%, Disodium oxalate. 0.6%, surplus is deionized water.
Preparation method:
Each component is weighed, at normal temperatures, first by dodecylbenzene sodium sulfonate, polyoxyethylene lauryl ether sulfur in above ratio
Acid sodium, sodium carbonate, sodium hydroxide are added to the water, and are sufficiently stirred for, after making each component be completely dissolved, add butylphosphoric acid ester, glycerol
Trioleate, sodium metasilicate and Disodium oxalate., stirring to transparent clarification, the uniform liquid obtained is water-base ink cleaning agent.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Within god and principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (6)
1. the water-base ink cleaning agent of a printed substrate, it is characterised in that calculating according to mass percent, its component is:
Butylphosphoric acid ester 4～10%, triolein 2～4%, alkali inorganic substance 1～5%, surfactant 3～6%, inclined silicon
Acid sodium 0.2～0.6%, Disodium oxalate. 0.2～0.6%, surplus is deionized water.
The water-base ink cleaning agent of printed substrate the most according to claim 1, it is characterised in that described alkali inorganic substance
For one or both the combination in sodium carbonate, sodium hydroxide, tertiary sodium phosphate, sodium silicate and sodium tripolyphosphate.
The water-base ink cleaning agent of printed substrate the most according to claim 1, it is characterised in that described surfactant
For fatty alcohol-polyoxyethylene ether, polyoxyethylene lauryl ether sodium sulfate, dodecylbenzene sodium sulfonate or fatty alcohol-polyoxyethylene ether
The mixing of one or more in phosphate ester salt.
4. the preparation method of the water-base ink cleaning agent of a printed substrate as claimed in claim 1, it is characterised in that bag
Include following steps: weigh each component in above ratio, at normal temperatures, first surfactant, alkali inorganic substance are added to the water, fill
Divide stirring, after making each component be completely dissolved, add butylphosphoric acid ester, triolein, sodium metasilicate and Disodium oxalate., stirring
To transparent clarification, the uniform liquid obtained is water-base ink cleaning agent.
The preparation method of the water-base ink cleaning agent of printed substrate the most according to claim 4, it is characterised in that described
Alkali inorganic substance is one or both the combination in sodium carbonate, sodium hydroxide, tertiary sodium phosphate, sodium silicate and sodium tripolyphosphate.
The preparation method of the water-base ink cleaning agent of printed substrate the most according to claim 4, it is characterised in that described
Surfactant is fatty alcohol-polyoxyethylene ether, polyoxyethylene lauryl ether sodium sulfate, dodecylbenzene sodium sulfonate or fatty alcohol
The mixing of one or more in polyoxyethylene ether phosphate salt.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610855027.8A CN106189480A (en) | 2016-09-27 | 2016-09-27 | Water-base ink cleaning agent of printed substrate and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610855027.8A CN106189480A (en) | 2016-09-27 | 2016-09-27 | Water-base ink cleaning agent of printed substrate and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106189480A true CN106189480A (en) | 2016-12-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610855027.8A Pending CN106189480A (en) | 2016-09-27 | 2016-09-27 | Water-base ink cleaning agent of printed substrate and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107603326A (en) * | 2017-09-04 | 2018-01-19 | 惠州威尔高电子有限公司 | A kind of remover of printed circuit board (PCB) solder mask and preparation method thereof |
| CN113214914A (en) * | 2021-02-08 | 2021-08-06 | 深圳市松柏实业发展有限公司 | Silicone oil cleaning fluid |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102888140A (en) * | 2011-07-20 | 2013-01-23 | 深圳市裕同印刷股份有限公司 | Formula and preparation process of environment-friendly printing ink cleaning agent |
| CN103469228A (en) * | 2013-09-25 | 2013-12-25 | 太仓市微贯机电有限公司 | Environmentally-friendly water-based metal cleaner |
| CN104232328A (en) * | 2014-09-29 | 2014-12-24 | 江苏中容铜业有限公司 | Household copper appliance detergent |
| CN104845432A (en) * | 2015-04-30 | 2015-08-19 | 青岛德翕拓创高新技术有限公司 | Low foam ink cleaning agent |
-
2016
- 2016-09-27 CN CN201610855027.8A patent/CN106189480A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102888140A (en) * | 2011-07-20 | 2013-01-23 | 深圳市裕同印刷股份有限公司 | Formula and preparation process of environment-friendly printing ink cleaning agent |
| CN103469228A (en) * | 2013-09-25 | 2013-12-25 | 太仓市微贯机电有限公司 | Environmentally-friendly water-based metal cleaner |
| CN104232328A (en) * | 2014-09-29 | 2014-12-24 | 江苏中容铜业有限公司 | Household copper appliance detergent |
| CN104845432A (en) * | 2015-04-30 | 2015-08-19 | 青岛德翕拓创高新技术有限公司 | Low foam ink cleaning agent |
Non-Patent Citations (2)
| Title |
|---|
| 司春波: "《实用涂装工手册》", 31 May 2007, 广东科技出版社 * |
| 路甬祥: "《文物修复和辨伪》", 30 September 2007, 大象出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107603326A (en) * | 2017-09-04 | 2018-01-19 | 惠州威尔高电子有限公司 | A kind of remover of printed circuit board (PCB) solder mask and preparation method thereof |
| CN107603326B (en) * | 2017-09-04 | 2020-06-02 | 惠州威尔高电子有限公司 | Stripping agent for solder mask layer of printed circuit board and preparation method thereof |
| CN113214914A (en) * | 2021-02-08 | 2021-08-06 | 深圳市松柏实业发展有限公司 | Silicone oil cleaning fluid |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161207 |