CN106179224A - A kind of nanometer ore deposit crystalline substance containing Graphene purifies granule and preparation method thereof - Google Patents
A kind of nanometer ore deposit crystalline substance containing Graphene purifies granule and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of nanometer ore deposit crystalline substance containing Graphene and purify granule, the component including following weight portion is made: meerschaum 50 70 parts, Graphene 0.1 0.5 parts, attapulgite 5 10 parts, activated carbon powder 10 20 parts, 5 10 parts of kieselguhr, bentonite 10 15 parts, anion powder 35 parts.Preparation method, comprises the following steps: each component is crossed 200 mesh sieves by (1) respectively；(2) it is uniformly mixed, obtains mixed powder；(3) add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；(4) carrying out primary being dried 12 hours in cold drying stove, baking temperature is 180 260 DEG C；(5) put in high-temperature activation stove and activate, activation temperature 600 780 DEG C, constant temperature 1 hour.The nanometer ore deposit crystalline substance of the present invention purifies granule and is possible not only to the harmful gass such as formaldehyde adsorption, benzene, TVOC, and can play and decompose the effect removed with anion releasing, it is ensured that the pure natural property of product, the preparation method of the present invention, and step is simple, technical maturity.
Description
Technical field
The present invention relates to environment-friendly materials technical field, a kind of nanometer ore deposit crystalline substance containing Graphene purify granule and
Preparation method.
Background technology
The purification product of pure natural is based on activated carbon, bamboo charcoal in the market, but this two series products only has simply
Physical absorption function, can not play remove the harmful substance such as formaldehyde, benzene effect, be adsorbed onto a certain amount of in the case of there will be
Adsorb saturated, the most under given conditions it is also possible to again discharge.Although also occurring in that photocatalyst activity charcoal on market, but system
Standby complex process is easily saturated during using.
Summary of the invention
It is an object of the invention to provide a kind of absorbability higher, can play simultaneously decompose remove formaldehyde containing stone
The nanometer ore deposit crystalline substance of ink alkene purifies granule and preparation method thereof, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of nanometer ore deposit crystalline substance containing Graphene purifies granule, and the component including following weight portion is made: meerschaum 50-70 part,
Graphene 0.1-0.5 part, attapulgite 5-10 part, activated carbon powder 10-20 part, kieselguhr 5-10 part, bentonite 10-15 part, negative
Ion powder 3-5 part.
As the further scheme of the present invention: include that the component of following weight portion is made: meerschaum 55-65 part, Graphene
0.2-0.4 part, attapulgite 6.5-8.5 part, activated carbon powder 12.5-17.5 part, kieselguhr 6.5-8.5 part, bentonite 11-14
Part, anion powder 3-5 part.
As the present invention further scheme: include that the component of following weight portion is made: meerschaum 60 parts, Graphene
0.3 part, attapulgite 7.5 parts, activated carbon powder 15 parts, 7.5 parts of kieselguhr, bentonite 12.5 parts, anion powder 4 parts.
As the present invention further scheme: described meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr,
The grain graininess of bentonite and anion powder is respectively less than 200 mesh.
As the present invention further scheme: described meerschaum active substance purity ＞ 90%.
As the present invention further scheme: the described nanometer ore deposit crystalline substance containing Graphene purifies the preparation side of granule
Method, comprises the following steps:
(1) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder are crossed respectively 200 mesh
Sieve, standby；
(2) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and the anion powder after sieving is by weight
Amount part proportioning is stirred mix homogeneously, obtains mixed powder；
(3) in described mixed powder, add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；
(4) pellet being put into cold drying stove and carries out primary being dried 1-2 hour, baking temperature is 180-260 DEG C；
(5) again ball material is put in high-temperature activation stove and activate, activation temperature 600-780 DEG C, constant temperature 1 hour.
As the present invention further scheme: described meerschaum active substance purity ＞ 90%.
Compared with prior art, the invention has the beneficial effects as follows: it is main former material that the present invention adds Graphene with meerschaum
The nanometer ore deposit crystalline substance purification granule of material is advantageously harmful in formaldehyde, benzene etc. by the fine pore size that enrichment boring technique is formed and divides
The attachment of son and suction, meanwhile, it is polar substances that the nanometer ore deposit crystalline substance of the present invention purifies granule, compares nonpolar activity
Charcoal, PARA FORMALDEHYDE PRILLS(91,95) isopolarity molecule has higher adsorption.
It addition, make the activity of product and heat conductivity increase after interpolation Graphene, the time that granule is dried is greatly shortened, and saves
Cost, adds Graphene and makes nanometer ore deposit crystalline substance have more stable molecular structure, and meerschaum, kieselguhr, bentonite etc. is natural former
Material is organically combined with anion powder, is possible not only to the harmful gass such as formaldehyde adsorption, benzene, TVOC, and can play decomposition and go
Except the effect with anion releasing.The present invention utilizes the mineral material such as meerschaum and attapulgite to bond, it is ensured that produce
The pure natural property of product, the preparation method of the present invention, step is simple, technical maturity.
Accompanying drawing explanation
Fig. 1 is the flow chart that the nanometer ore deposit crystalline substance containing Graphene purifies the preparation method of granule.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Describe, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments wholely.Based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under not making creative work premise
Embodiment, broadly falls into the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of nanometer ore deposit crystalline substance containing Graphene purifies granule, and the component including following weight portion is made:
Meerschaum 50 parts, Graphene 0.1 part, attapulgite 5 parts, activated carbon powder 10 parts, 5 parts of kieselguhr, bentonite 10 parts, anion powder
3 parts.
The grain graininess of described meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder
It is 250 mesh.
Described meerschaum active substance purity ＞ 90%.
Referring to Fig. 1, in the embodiment of the present invention, the described nanometer ore deposit crystalline substance containing Graphene purifies the preparation side of granule
Method, comprises the following steps:
(1) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder are crossed respectively 250 mesh
Sieve, standby, described meerschaum active substance purity ＞ 90%；
(2) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and the anion powder after sieving is by weight
Amount part proportioning is stirred mix homogeneously, obtains mixed powder；
(3) in described mixed powder, add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；
(4) pellet being put into cold drying stove and carries out primary being dried 1 hour, baking temperature is 180-DEG C；
(5) again ball material is put in high-temperature activation stove and activate, activation temperature 600 DEG C, constant temperature 1 hour.
Embodiment 2
In the embodiment of the present invention, a kind of nanometer ore deposit crystalline substance containing Graphene purifies granule, and the component including following weight portion is made:
Meerschaum 55 parts, Graphene 0.2 part, attapulgite 6.5 parts, activated carbon powder 12.5 parts, 6.5 parts of kieselguhr, bentonite 11 parts, negative
3 parts of ion powder.
The grain graininess of described meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder
It is 300 mesh.
Described meerschaum active substance purity ＞ 90%.
Referring to Fig. 1, in the embodiment of the present invention, the described nanometer ore deposit crystalline substance containing Graphene purifies the preparation side of granule
Method, comprises the following steps:
(1) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder are crossed respectively 300 mesh
Sieve, standby, described meerschaum active substance purity ＞ 90%；
(2) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and the anion powder after sieving is by weight
Amount part proportioning is stirred mix homogeneously, obtains mixed powder；
(3) in described mixed powder, add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；
(4) pellet being put into cold drying stove and carries out primary being dried 1 hour, baking temperature is 200 DEG C；
(5) again ball material is put in high-temperature activation stove and activate, activation temperature 630 DEG C, constant temperature 1 hour.
Embodiment 3
In the embodiment of the present invention, a kind of nanometer ore deposit crystalline substance containing Graphene purifies granule, and the component including following weight portion is made:
Meerschaum 60 parts, Graphene 0.3 part, attapulgite 7.5 parts, activated carbon powder 15 parts, 7.5 parts of kieselguhr, bentonite 12.5 parts, negative
4 parts of ion powder.
The grain graininess of described meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder
It is 350 mesh.
As the present invention further scheme: described meerschaum active substance purity ＞ 90%.
Referring to Fig. 1, in the embodiment of the present invention, the described nanometer ore deposit crystalline substance containing Graphene purifies the preparation side of granule
Method, comprises the following steps:
(1) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder are crossed respectively 350 mesh
Sieve, standby, described meerschaum active substance purity ＞ 90%；
(2) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and the anion powder after sieving is by weight
Amount part proportioning is stirred mix homogeneously, obtains mixed powder；
(3) in described mixed powder, add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；
(4) pellet being put into cold drying stove and carries out primary being dried 1.5 hours, baking temperature is 220 DEG C；
(5) again ball material is put in high-temperature activation stove and activate, activation temperature 690 DEG C, constant temperature 1 hour.
Embodiment 4
In the embodiment of the present invention, a kind of nanometer ore deposit crystalline substance containing Graphene purifies granule, and the component including following weight portion is made:
Meerschaum 65 parts, Graphene 0.4 part, attapulgite 8.5 parts, activated carbon powder 17.5 parts, 8.5 parts of kieselguhr, bentonite 14 parts, negative
5 parts of ion powder.
The grain graininess of described meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder
It is 400 mesh.
Described meerschaum active substance purity ＞ 90%.
Referring to Fig. 1, in the embodiment of the present invention, the described nanometer ore deposit crystalline substance containing Graphene purifies the preparation side of granule
Method, comprises the following steps:
(1) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder are crossed respectively 400 mesh
Sieve, standby, described meerschaum active substance purity ＞ 90%；
(2) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and the anion powder after sieving is by weight
Amount part proportioning is stirred mix homogeneously, obtains mixed powder；
(3) in described mixed powder, add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；
(4) pellet being put into cold drying stove and carries out primary being dried 1.5 hours, baking temperature is 240 DEG C；
(5) again ball material is put in high-temperature activation stove and activate, activation temperature 730 DEG C, constant temperature 1 hour.
Embodiment 5
In the embodiment of the present invention, a kind of nanometer ore deposit crystalline substance containing Graphene purifies granule, and the component including following weight portion is made:
Meerschaum 70 parts, Graphene 0.5 part, attapulgite 10 parts, activated carbon powder 20 parts, 10 parts of kieselguhr, bentonite 15 parts, anion
5 parts of powder.
The grain graininess of described meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder
It is 450 mesh.
Described meerschaum active substance purity ＞ 90%.
Referring to Fig. 1, in the embodiment of the present invention, the described nanometer ore deposit crystalline substance containing Graphene purifies the preparation side of granule
Method, comprises the following steps:
(1) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder are crossed respectively 450 mesh
Sieve, standby, described meerschaum active substance purity ＞ 90%；
(2) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and the anion powder after sieving is by weight
Amount part proportioning is stirred mix homogeneously, obtains mixed powder；
(3) in described mixed powder, add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；
(4) pellet being put into cold drying stove and carries out primary being dried 2 hours, baking temperature is 260 DEG C；
(5) again ball material is put in high-temperature activation stove and activate, activation temperature 780 DEG C, constant temperature 1 hour.
The present invention adds the Graphene nanometer ore deposit crystalline substance with meerschaum as main raw material(s) and purifies granule by enrichment pore-creating skill
The fine pore size that art is formed is advantageously in attachment and the suction of the deleterious molecular such as formaldehyde, benzene, and meanwhile, the present invention receives
It is polar substances that rice ore deposit crystalline substance purifies granule, compares nonpolar activated carbon, and PARA FORMALDEHYDE PRILLS(91,95) isopolarity molecule has higher absorption and makees
With.
It addition, make the activity of product and heat conductivity increase after interpolation Graphene, the time that granule is dried is greatly shortened, and saves
Cost, adds Graphene and makes nanometer ore deposit crystalline substance have more stable molecular structure, and meerschaum, kieselguhr, bentonite etc. is natural former
Material is organically combined with anion powder, is possible not only to the harmful gass such as formaldehyde adsorption, benzene, TVOC, and can play decomposition and go
Except the effect with anion releasing.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.Should not be considered as limiting involved claim by any reference in claim.
Although moreover, it will be appreciated that this specification is been described by according to embodiment, but the most each embodiment only wraps
Containing an independent technical scheme, this narrating mode of description is only that for clarity sake those skilled in the art should
Description can also be formed those skilled in the art through appropriately combined as an entirety, the technical scheme in each embodiment
May be appreciated other embodiments.
Claims (7)
1. the nanometer ore deposit crystalline substance containing Graphene purifies granule, it is characterised in that include that the component of following weight portion is made: sea
Afrodite 50-70 part, Graphene 0.1-0.5 part, attapulgite 5-10 part, activated carbon powder 10-20 part, kieselguhr 5-10 part, swelling
Soil 10-15 part, anion powder 3-5 part.
Nanometer ore deposit crystalline substance containing Graphene the most according to claim 1 purifies granule, it is characterised in that include following weight
The component of part is made: meerschaum 55-65 part, Graphene 0.2-0.4 part, attapulgite 6.5-8.5 part, activated carbon powder 12.5-
17.5 parts, kieselguhr 6.5-8.5 part, bentonite 11-14 part, anion powder 3-5 part.
Nanometer ore deposit crystalline substance containing Graphene the most according to claim 1 purifies granule, it is characterised in that include following weight
Part component make: meerschaum 60 parts, Graphene 0.3 part, attapulgite 7.5 parts, activated carbon powder 15 parts, 7.5 parts of kieselguhr, swollen
Profit soil 12.5 parts, anion powder 4 parts.
Nanometer ore deposit crystalline substance containing Graphene the most according to claim 1 purifies granule, it is characterised in that described meerschaum,
The grain graininess of Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder is respectively less than 200 mesh.
Nanometer ore deposit crystalline substance containing Graphene the most according to claim 1 purifies granule, it is characterised in that described meerschaum has
Effective substance purity ＞ 90%.
6. the nanometer ore deposit crystalline substance containing Graphene as described in claim 1-5 is arbitrary purifies a preparation method for granule, and it is special
Levy and be, comprise the following steps:
(1) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and anion powder are crossed respectively 200 mesh
Sieve, standby；
(2) meerschaum, Graphene, attapulgite, activated carbon powder, kieselguhr, bentonite and the anion powder after sieving is by weight
Amount part proportioning is stirred mix homogeneously, obtains mixed powder；
(3) in described mixed powder, add moderate amount of sulfuric acid aluminum water to stir, then carry out pelletize balling-up；
(4) pellet being put into cold drying stove and carries out primary being dried 1-2 hour, baking temperature is 180-260 DEG C；
(5) again ball material is put in high-temperature activation stove and activate, activation temperature 600-780 DEG C, constant temperature 1 hour.
Nanometer ore deposit crystalline substance containing Graphene the most according to claim 6 purifies the preparation method of granule, it is characterised in that institute
State meerschaum active substance purity ＞ 90%.
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