CN106174185A - A kind of production method of Armeniaca mume Sieb. extractive - Google Patents

A kind of production method of Armeniaca mume Sieb. extractive Download PDF

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Publication number
CN106174185A
CN106174185A CN201610548472.XA CN201610548472A CN106174185A CN 106174185 A CN106174185 A CN 106174185A CN 201610548472 A CN201610548472 A CN 201610548472A CN 106174185 A CN106174185 A CN 106174185A
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armeniaca mume
mume sieb
pulp
sieb
boiling
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CN201610548472.XA
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Chinese (zh)
Inventor
梁多
刘智钧
李淑红
李欣
姚莉
谢婧
黄敏
王凡
王一凡
杨承鸿
李殿鑫
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Guangdong Vocational College of Science and Trade
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Guangdong Vocational College of Science and Trade
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Priority to CN201610548472.XA priority Critical patent/CN106174185A/en
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Abstract

The invention discloses the production method of a kind of Armeniaca mume Sieb. extractive, it comprises the following steps: 1) cleaned up by Armeniaca mume Sieb., precook, enucleation, squeeze the juice, obtains Armeniaca mume Sieb. pulp;2) Armeniaca mume Sieb. pulp carrying out sterilization treatment, dress fills and seals, normal temperature storage 1~2 years;3) by step 2) in fill Armeniaca mume Sieb. pulp pour in heat preservation sandwich layer pot, be heated to boiling, boiling reflux 8~10h, stop heating, be incubated 8~10h;4) Armeniaca mume Sieb. pulp being heated to boiling again, normal pressure concentrates, is filtered to remove the pulp in Armeniaca mume Sieb. pulp, and filtrate is placed in insulation material insulation 8~10h;5) filtrate in step 4) being heated to boiling, normal pressure concentrates, obtains Armeniaca mume Sieb. extractive.In Armeniaca mume Sieb. extractive prepared by the present invention, syphilis content is high, and the weight/mass percentage composition of syphilis reaches more than 0.5%, and Armeniaca mume Sieb. extractive color and luster is limpid, and dissolubility is good, and without being charred taste, mouthfeel is pure, is of high nutritive value.The method of the present invention is easy and simple to handle, and production cost is low, it is easy to carry out large-scale industrial production.

Description

A kind of production method of Armeniaca mume Sieb. extractive
Technical field
The present invention relates to the production method of a kind of Armeniaca mume Sieb. extractive, belong to food processing field.
Background technology
Armeniaca mume Sieb., is also called dark plum or fruit prunus mume (sieb.) sieb.et zucc., is the Rosaceae Fructus Pruni fruit that belongs to arbor, be mainly distributed on China Yangtze river basin and South China, southwest, more with the yield that Guangdong, Guangxi, Yunnan, Fujian, Zhejiang, Jiangsu, Sichuan, Guizhou etc. save.Armeniaca mume Sieb. Economic worth is high, and 3~5 annual bearing after plantation reaches the phase of abounding with in 12~20 years, and fruit is in clear and bright after ripening.
Armeniaca mume Sieb. is the medicine-food two-purpose fruit that China is traditional, has the health care of uniqueness.It is known that most fruit are with sweet Well-known, and Armeniaca mume Sieb. is famous, rich in citric acid, malic acid, tannic acid and tartaric acid etc., the organic acid kind altogether contained with acid only Class is more than 16 kinds.Owing to the acid content of Armeniaca mume Sieb. is high, sugar content is low, there is astringent taste, eats local flavor raw not good enough, and few people directly eat Use Armeniaca mume Sieb. fresh fruit, eat again after being substantially processing.Armeniaca mume Sieb. has the highest medical value, has allaying tiredness, antitumor, clear Except blood rubbish, improve the effects such as gastrointestinal function, the liver protecting, antibacterial, anthelmintic, antiallergic, slow down aging, beauty treatment.In tradition In food processing industry, Armeniaca mume Sieb. be mainly used in process the product such as preserved fruit, preserve, fabricated product mainly have prune in brine, prunus mume (sieb.) sieb.et zucc. base, dried plum, Flos Jasmini Nudiflori etc..Armeniaca mume Sieb. or the lowest fruit of a kind of energy content, the heat of every 100 grams of sarcocarp is only 29 kilocalories.
Armeniaca mume Sieb. extractive is a kind of food being in fashion in Japan, Taiwan, it is common that with Armeniaca mume Sieb. fresh fruit as raw material, cleaned, making beating, Use ceramic vessel long-time heating to concentrate again to form, be known as the king of basic food.(mumefrual, Taiwan translated name is prunus mume (sieb.) sieb.et zucc. to syphilis China) it is one of the main functional component of Armeniaca mume Sieb. extractive, there is the sanguimotor effect of improvement, its molecular structural formula is as follows:
Syphilis mainly obtains with sugar, aminoacid etc. for substrate reactions, and reaction temperature is the highest, and generating rate is the fastest.Tradition Armeniaca mume Sieb. extractive generally use terrine heating concentrate, require heat to about 105 DEG C, concentration time is at more than 48h, although can promote Syphilis generates, but easily burns generation carcinogen.Meanwhile, in Armeniaca mume Sieb., pulp is more, the green grass or young crops being directly concentrated to give by plum pulp Prunus mume (sieb.) sieb.et zucc. essence outward appearance is rough, if but filter plum pulp in early days, the most easily block filter membrane, sad filter.
The invention discloses the production method of a kind of Armeniaca mume Sieb. extractive, filling storage by Armeniaca mume Sieb. pulp being carried out long-time room temperature dress Deposit, add the content of syphilis, the polysaccharide thing such as pectin by Armeniaca mume Sieb. pulp being carried out boiling reflux, in hydrolysis Armeniaca mume Sieb. pulp Matter, makes the pulp in Armeniaca mume Sieb. pulp to be filtered smoothly.
Summary of the invention
It is an object of the invention to provide the production method of a kind of Armeniaca mume Sieb. extractive.
The production method of a kind of Armeniaca mume Sieb. extractive comprises the following steps:
1) Armeniaca mume Sieb. cleaned up, precook, enucleation, squeeze the juice, obtain Armeniaca mume Sieb. pulp;
2) Armeniaca mume Sieb. pulp carrying out sterilization treatment, dress fills and seals, normal temperature storage 1~2 years;
3) by step 2) in fill Armeniaca mume Sieb. pulp pour in heat preservation sandwich layer pot, be heated to boiling, boiling reflux 8~10h, stop Heating, is incubated 8~10h;
4) Armeniaca mume Sieb. pulp being heated to boiling again, normal pressure concentrates, is filtered to remove the pulp in Armeniaca mume Sieb. pulp, and filtrate is placed in Insulation material is incubated 8~10h;
5) filtrate in step 4) being heated to boiling, normal pressure concentrates, obtains Armeniaca mume Sieb. extractive.
The temperature precooked described in step 1) is 95~100 DEG C, and the time of precooking is 10~15min.
Step 2) described sterilization treatment is instantaneous ultrahigh-temperature sterilization.
The temperature of described instantaneous ultrahigh-temperature sterilization is 100~110 DEG C, and sterilization time is 20~40s.
The aperture filtering selected filter cloth described in step 4) is 50~100 μm.
In step 4), Armeniaca mume Sieb. pulp solid content after normal pressure concentrates is 30~40 ° of Brix.
In step 5), filtrate solid content after normal pressure concentrates is 74~78 ° of Brix.
The invention has the beneficial effects as follows:
1) by Armeniaca mume Sieb. pulp being carried out long-time room temperature tankage, it is added significantly to the content of syphilis, the Armeniaca mume Sieb. extractive of preparation The weight/mass percentage composition of middle syphilis reaches more than 0.5%;
2) by Armeniaca mume Sieb. pulp is carried out boiling reflux, the polysaccharose substances such as the pectin in Armeniaca mume Sieb. pulp are made to be fully hydrolyzed, and blue or green In prunus mume (sieb.) sieb.et zucc. pulp, remaining pulp can also be easy to be filtered to remove;
3) the Armeniaca mume Sieb. extractive color and luster that prepared by the present invention is limpid, and dissolubility is good, is of high nutritive value, and endures owing to being provided without traditional high temperature Technique processed, without being charred taste, without carcinogen, mouthfeel is pure;
4) method of the present invention is easy and simple to handle, and production cost is low, it is easy to carry out large-scale industrial production.
Detailed description of the invention
The production method of a kind of Armeniaca mume Sieb. extractive comprises the following steps:
1) Armeniaca mume Sieb. cleaned up, precook, enucleation, squeeze the juice, obtain Armeniaca mume Sieb. pulp;
2) Armeniaca mume Sieb. pulp carrying out sterilization treatment, dress fills and seals, normal temperature storage 1~2 years;
3) by step 2) in fill Armeniaca mume Sieb. pulp pour in heat preservation sandwich layer pot, be heated to boiling, boiling reflux 8~10h, stop Heating, is incubated 8~10h;
4) Armeniaca mume Sieb. pulp being heated to boiling again, normal pressure concentrates, is filtered to remove the pulp in Armeniaca mume Sieb. pulp, and filtrate is placed in Insulation material is incubated 8~10h;
5) filtrate in step 4) being heated to boiling, normal pressure concentrates, obtains Armeniaca mume Sieb. extractive.
Preferably, the temperature precooked described in step 1) is 95~100 DEG C, and the time of precooking is 10~15min.
Preferably, step 2) described sterilization treatment is instantaneous ultrahigh-temperature sterilization.
Preferably, the temperature of described instantaneous ultrahigh-temperature sterilization is 100~110 DEG C, and sterilization time is 20~40s.
Preferably, the aperture filtering selected filter cloth described in step 4) is 50~100 μm.
Preferably, in step 4), Armeniaca mume Sieb. pulp solid content after normal pressure concentrates is 30~40 ° of Brix.
Preferably, in step 5), filtrate solid content after normal pressure concentrates is 74~78 ° of Brix.
Below in conjunction with specific embodiment, the present invention is made further explanation and description.
Embodiment 1:
1) taking 2 tons of Armeniaca mume Sieb.s, clean up, join in spiral precooker, 95 DEG C are boiled 15min, enucleation, use spiral juice extractor to squeeze Juice, obtains Armeniaca mume Sieb. pulp 1.2 tons;
2) Armeniaca mume Sieb. pulp is after 105 DEG C of instantaneous ultrahigh-temperature sterilization 30s, carries out sterile filling, obtains 6 barrels of 200L dress aseptic cannings blue or green Prunus mume (sieb.) sieb.et zucc. pulp, room temperature storage 1 year;
3) take 200kg fill Armeniaca mume Sieb. pulp, pour 300L into and be incubated in jacketed pan with cover, be heated to boiling, turn heating power down, make Its micro-boiling, adds Stainless steel pot cover, micro-boiling backflow 8h, stops heating, 10h is placed in insulation;
4) Armeniaca mume Sieb. pulp being again heated to boiling, it is 35 ° of Brix that normal pressure is concentrated into solid content, uses 200 mesh filter cloth mistakes Filter, filtrate is incubated placement 9h in insulation material;
5) filtrate of step 4) being put in the electrical heating jacketed pan of 100L band stirring, agitating heating 3h, solid content reaches 74 ° of Brix, obtain Armeniaca mume Sieb. extractive 18kg.
After measured, in Armeniaca mume Sieb. extractive, the weight/mass percentage composition of syphilis is 0.51%.
Embodiment 2:
1) taking 2 tons of Armeniaca mume Sieb.s, clean up, join in spiral precooker, 100 DEG C are boiled 10min, enucleation, use spiral juice extractor Squeeze the juice, obtain Armeniaca mume Sieb. pulp 1.2 tons;
2) Armeniaca mume Sieb. pulp is after 100 DEG C of instantaneous ultrahigh-temperature sterilization 40s, carries out sterile filling, obtains 6 barrels of 200L dress aseptic cannings blue or green Prunus mume (sieb.) sieb.et zucc. pulp, room temperature storage 2 years;
3) take 200kg fill Armeniaca mume Sieb. pulp, pour 300L into and be incubated in jacketed pan with cover, be heated to boiling, turn heating power down, make Its micro-boiling, adds Stainless steel pot cover, micro-boiling backflow 10h, stops heating, 9h is placed in insulation;
4) Armeniaca mume Sieb. pulp being again heated to boiling, it is 40 ° of Brix that normal pressure is concentrated into solid content, uses 200 mesh filter cloth mistakes Filter, filtrate is incubated placement 8h in insulation material;
5) filtrate of step 4) being added in the electrical heating jacketed pan of 100L band stirring, agitating heating 3h, solid content reaches 75 ° of Brix, obtain Armeniaca mume Sieb. extractive 18kg.
After measured, in Armeniaca mume Sieb. extractive, the weight/mass percentage composition of syphilis is 0.55%.
Embodiment 3:
1) taking 2 tons of Armeniaca mume Sieb.s, clean up, join in spiral precooker, 95 DEG C are boiled 10min, enucleation, use spiral juice extractor to squeeze Juice, obtains Armeniaca mume Sieb. pulp 1.2 tons;
2) Armeniaca mume Sieb. pulp is after 110 DEG C of instantaneous ultrahigh-temperature sterilization 20s, carries out sterile filling, obtains 6 barrels of 200L dress aseptic cannings blue or green Prunus mume (sieb.) sieb.et zucc. pulp, room temperature storage 1 year;
3) take 200kg fill Armeniaca mume Sieb. pulp, pour 300L into and be incubated in jacketed pan with cover, be heated to boiling, turn heating power down, make Its micro-boiling, adds Stainless steel pot cover, micro-boiling backflow 9h, stops heating, 8h is placed in insulation;
4) Armeniaca mume Sieb. pulp being again heated to boiling, it is 30 ° of Brix that normal pressure is concentrated into solid content, uses 200 mesh filter cloth mistakes Filter, filtrate is incubated placement 10h in insulation material;
5) filtrate of step 4) being added in the electrical heating jacketed pan of 100L band stirring, agitating heating 3h, solid content reaches 78 ° of Brix, obtain Armeniaca mume Sieb. extractive 18kg.
After measured, in Armeniaca mume Sieb. extractive, the weight/mass percentage composition of syphilis is 0.54%.
Comparative example 1:
1) taking 2 tons of Armeniaca mume Sieb.s, clean up, join in spiral precooker, 95 DEG C are boiled 15min, enucleation, use spiral juice extractor to squeeze Juice, obtains Armeniaca mume Sieb. pulp 1.2 tons;
2) take 200kg Armeniaca mume Sieb. pulp, pour 300L into and be incubated in jacketed pan with cover, be heated to boiling, turn heating power down so that it is micro- Boiling, adds Stainless steel pot cover, micro-boiling backflow 8h, stops heating, 10h is placed in insulation.
3) Armeniaca mume Sieb. pulp being again heated to boiling, it is 30 ° of Brix that normal pressure is concentrated into solid content, uses 200 mesh filters Cloth filters, and filtrate is incubated placement 9h in insulation material;
4) filtrate of step 3) being added in the electrical heating jacketed pan of 100L band stirring, agitating heating 3h, solid content reaches 75 ° of Brix, obtain Armeniaca mume Sieb. extractive 18kg.
After measured, in Armeniaca mume Sieb. extractive, the weight/mass percentage composition of syphilis is 0.24%.
Comparative example 2:
1) taking 2 tons of Armeniaca mume Sieb.s, clean up, join in spiral precooker, 100 DEG C are boiled 10min, enucleation, use spiral juice extractor Squeeze the juice, obtain Armeniaca mume Sieb. pulp 1.2 tons;
2) Armeniaca mume Sieb. pulp is after 105 DEG C of instantaneous ultrahigh-temperature sterilization 30s, carries out sterile filling, obtains 6 barrels of 200L dress aseptic cannings blue or green Prunus mume (sieb.) sieb.et zucc. pulp, room temperature storage 6 months;
3) take 200kg fill Armeniaca mume Sieb. pulp, pour 300L into and be incubated in jacketed pan with cover, be heated to boiling, turn heating power down, make Its micro-boiling, adds Stainless steel pot cover, micro-boiling backflow 10h, stops heating, 8h is placed in insulation;
4) Armeniaca mume Sieb. pulp being again heated to boiling, it is 30 ° of Brix that normal pressure is concentrated into solid content, uses 200 mesh filter cloth mistakes Filter, filtrate is incubated placement 8h in insulation material;
5) filtrate of step 4) being added in the electrical heating jacketed pan of 100L band stirring, agitating heating 3h, solid content reaches 75 ° of Brix, obtain Armeniaca mume Sieb. extractive 18kg.
After measured, in Armeniaca mume Sieb. extractive, the weight/mass percentage composition of syphilis is 0.33%.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention are not by above-described embodiment Limit, the change made under other any spirit without departing from the present invention and principle, modify, substitute, combine, simplify, All should be the substitute mode of equivalence, within being included in protection scope of the present invention.

Claims (7)

1. the production method of an Armeniaca mume Sieb. extractive, it is characterised in that: comprise the following steps:
1) Armeniaca mume Sieb. cleaned up, precook, enucleation, squeeze the juice, obtain Armeniaca mume Sieb. pulp;
2) Armeniaca mume Sieb. pulp carrying out sterilization treatment, dress fills and seals, normal temperature storage 1~2 years;
3) by step 2) in fill Armeniaca mume Sieb. pulp pour in heat preservation sandwich layer pot, be heated to boiling, boiling reflux 8~10h, stop Heating, is incubated 8~10h;
4) Armeniaca mume Sieb. pulp being heated to boiling again, normal pressure concentrates, is filtered to remove the pulp in Armeniaca mume Sieb. pulp, and filtrate is placed in Insulation material is incubated 8~10h;
5) filtrate in step 4) being heated to boiling, normal pressure concentrates, obtains Armeniaca mume Sieb. extractive.
Production method the most according to claim 1, it is characterised in that: the temperature precooked described in step 1) is 95~100 DEG C, The time of precooking is 10~15min.
Production method the most according to claim 1, it is characterised in that: step 2) to be that superhigh temperature is instantaneous go out described sterilization treatment Bacterium.
Production method the most according to claim 3, it is characterised in that: the temperature of described instantaneous ultrahigh-temperature sterilization be 100~ 110 DEG C, sterilization time is 20~40s.
Production method the most according to claim 1, it is characterised in that: filter the aperture of selected filter cloth described in step 4) It is 50~100 μm.
Production method the most according to claim 1, it is characterised in that: in step 4), Armeniaca mume Sieb. pulp is after normal pressure concentrates Solid content is 30~40 ° of Brix.
Production method the most according to claim 1, it is characterised in that: filtrate solid after normal pressure concentrates in step 5) Thing content is 74~78 ° of Brix.
CN201610548472.XA 2016-07-13 2016-07-13 A kind of production method of Armeniaca mume Sieb. extractive Pending CN106174185A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108936658A (en) * 2018-07-06 2018-12-07 广西壮族自治区亚热带作物研究所 A kind of preparation method of green plum essence
CN109601915A (en) * 2018-12-27 2019-04-12 南京林业大学 A kind of preparation method of green plum essence
CN112493484A (en) * 2020-11-09 2021-03-16 广东省农业科学院蚕业与农产品加工研究所 Preparation method of mume fructus essence rich in mume fructus extract and high-purity mume fructus extract
CN115777930A (en) * 2022-11-30 2023-03-14 浙江中医药大学 Green plum extract and preparation method and application thereof
CN116711856A (en) * 2023-08-08 2023-09-08 南京农业大学三亚研究院 Green plum essence rich in myricetin and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101889709A (en) * 2010-08-17 2010-11-24 济南康森生物科技有限公司 Wild jujube juice beverage for tranquilization and health care and production method thereof
JP2012201637A (en) * 2011-03-25 2012-10-22 Kose Corp Efficacious drug having prunus mume extract as active ingredient
CN104172379A (en) * 2014-08-06 2014-12-03 浙江百惠生物科技有限公司 Preparation method of mumefural

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101889709A (en) * 2010-08-17 2010-11-24 济南康森生物科技有限公司 Wild jujube juice beverage for tranquilization and health care and production method thereof
JP2012201637A (en) * 2011-03-25 2012-10-22 Kose Corp Efficacious drug having prunus mume extract as active ingredient
CN104172379A (en) * 2014-08-06 2014-12-03 浙江百惠生物科技有限公司 Preparation method of mumefural

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108936658A (en) * 2018-07-06 2018-12-07 广西壮族自治区亚热带作物研究所 A kind of preparation method of green plum essence
CN109601915A (en) * 2018-12-27 2019-04-12 南京林业大学 A kind of preparation method of green plum essence
CN112493484A (en) * 2020-11-09 2021-03-16 广东省农业科学院蚕业与农产品加工研究所 Preparation method of mume fructus essence rich in mume fructus extract and high-purity mume fructus extract
CN115777930A (en) * 2022-11-30 2023-03-14 浙江中医药大学 Green plum extract and preparation method and application thereof
CN116711856A (en) * 2023-08-08 2023-09-08 南京农业大学三亚研究院 Green plum essence rich in myricetin and preparation method thereof

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Application publication date: 20161207