CN106172509A - A kind of plants essential oil mosquito-dispelling tablet of band instruction function and preparation method thereof - Google Patents
A kind of plants essential oil mosquito-dispelling tablet of band instruction function and preparation method thereof Download PDFInfo
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract
Present invention relates particularly to plants essential oil mosquito-dispelling tablet of a kind of band instruction function and preparation method thereof, belong to domestic sanitary parasite killing articles for use field.The mosquito-dispelling tablet of the present invention uses the raw material of following percentage by weight to form: plants essential oil 1 ~ 10.0%, quintessence oil corrigent 1 ~ 10.0%, slow releasing agent 0.1 ~ 5.0%, forming agent 6 ~ 10.0%, preservative 0.02 ~ 0.5%, pigment 0.01 ~ 0.1%, deionized water 70.0 ~ 85.0%.The present invention uses plants essential oil to be repellant main component, safe and reliable, can the effective class mosquito of sucking blood such as repellent culex, Aedes albopictus, midge；The present invention adds quintessence oil corrigent, can improve the quintessence oil stimulation to people's sense organ；The present invention does not contains solubilizing agent, can reduce the quintessence oil residual at mosquito-dispelling tablet, promotes repelling effect；Present invention adds slow releasing agent, by the design time, the quintessence oil in mosquito-dispelling tablet can be volatilized；The present invention has the function of instruction Use Limitation, and during use, the volume of mosquito-dispelling tablet constantly reduces, and can dwindle into lump, show that mosquito-repellent essential oil exhausts, no longer have anophelifuge effect, facilitate user to change after reaching the design time.
Description
Technical field:
Present invention relates particularly to plants essential oil mosquito-dispelling tablet of a kind of band instruction function and preparation method thereof, belong to domestic sanitary parasite killing articles for use field.
Background technology:
At present, along with improving constantly of people's level of consumption, outdoor travel, body-building, the increasing of motion, increase the demand of outdoor mosquito repellent product.And open air anophelifuge typically uses the dropping mosquito expelling plaster of plants essential oil, anophelifuge watchband, also have containing dimethyl phthalate or the mosquito-driving liquid of diethyltoluamide, mosquito-repellent perfume.Although mosquito expelling plaster, anophelifuge watchband are also the modes of plants essential oil anophelifuge, but lack the function of instruction use time.The chemical compositions such as mosquito-driving liquid, mosquito-repellent perfume use diethyltoluamide, dimethyl phthalate or mosquitofugal oil, but skin surface to be applied directly to, can exert a certain influence to health, and be harmful to the silkworm of Fish, honeybee.
Plants essential oil mosquito repellent product is also evolving recent years, a kind of plants essential oil anophelifuge smeared disclosed in patent CN201210316045.0.But mosquito repellent product disclosed in above patent is for spreading upon on skin, the crowd of allergy easy for quintessence oil allergy or skin, the allergic phenomenas such as erythema easily occur.And the patented product cannot indicate the effective time of repelling effect.
A kind of plants essential oil anophelifuge gel disclosed in patent CN201310211166.3.But intensity is the poorest after mosquito repellent product molding disclosed in above patent, can only be filled in the container such as iron flask or plastic casing, use the most cumbersome as outdoor anophelifuge.Adding after solubilizing agent, plants essential oil remains in the ratio in gelinite and increases, and reduces quintessence oil rate of volatilization, when move out of doors, stroll etc. needs mobile in-convenience in use, and effect is not ideal.
Summary of the invention:
The plants essential oil mosquito-dispelling tablet of a kind of brand-new band instruction function that the invention aims to overcome presently commercially available mosquito repellent product disadvantages mentioned above and design, and the manufacture method of this mosquito-dispelling tablet is provided.
The present invention is achieved through the following technical solutions: the plants essential oil mosquito-dispelling tablet of a kind of band instruction function, the raw material comprising following percentage by weight forms: plants essential oil 1 ~ 10.0%, quintessence oil corrigent 1 ~ 10.0%, slow releasing agent 0.1 ~ 5.0%, forming agent 6 ~ 10.0%, preservative 0.02 ~ 0.5%, pigment 0.01 ~ 0.1%, deionized water 70.0 ~ 85.0%.
Described plants essential oil is two or more mixture mixed with arbitrary proportion of rose oil, Oleum Pelargonii Graveolentis, Semen Myristicae oil, Herba Schizonepetae oil, Oleum Anisi Stellati, Folium perillae acutae oil, Flos Jasmini Sambac oil, thyme oil, eucalyptus globolus oil.
Described quintessence oil corrigent is one or more mixture mixed with arbitrary proportion of MDJ, dihydromyrcenol, ethylene carbonate, ethyl acetate, Allyl carbonate.
Described slow releasing agent is one or more mixture mixed with arbitrary proportion of polyvinyl alcohol, polyvinyl acetate, polyglycolic acid.
Described forming agent is one or more mixture mixed with arbitrary proportion of sodium alginate, agar, diamantane (obsolete), microcrystalline Cellulose.
Described preservative is sodium D-isoascorbate and potassium sorbate, the one of sodium dehydroacetate.
Described pigment is water colo(u)r.
The plants essential oil mosquito-dispelling tablet of a kind of band instruction function, its manufacture method comprises the steps of
1) deionized water and slow releasing agent, forming agent, preservative, pigment are added in stirred tank, heating for dissolving；
2) various plants quintessence oil, quintessence oil corrigent are mixed into homogeneous phase solution；
3) stirred tank is cooled to 65 DEG C ± 5 DEG C, pours in stirred tank by plants essential oil mixed solution, and regulation mixing plant is to the most at a high speed；
4) after continuously stirred several minutes, by the strip mould of feed liquid fill extremely known sectional area, required form；
5) cooling is accelerated, temperature to material depanning when 30-40 DEG C, determine thickness according to the design use time, carry out cutting into slices, packing, plants essential oil mosquito-dispelling tablet i.e. molding.
By using technique scheme, advantages of the present invention and having the beneficial effect that:
The present invention uses plants essential oil to be repellant main component, safe and reliable, repelling effect is stable；With forming agent as carrier, intensity is high, plasticity is good, is beneficial to outdoor use；Present invention adds quintessence oil corrigent, can be effectively improved the quintessence oil stimulation to people's sense organ, abnormal smells from the patient gentleness is easily accepted by；The present invention, without solubilizing agent compositions such as surfactants, decreases the quintessence oil residual at mosquito-dispelling tablet, improves evaporation rate, so improve the effect of anophelifuge；Present invention adds slow releasing agent, it is possible to according to design mosquito repellent time, volatilized by the quintessence oil in mosquito-dispelling tablet stable, facilitate the use of user open air；The devices such as the present invention and supporting anophelifuge folder, Snap bracelet with the use of, it is not directly contacted with skin, safe to the human body harmless, it is clipped in the bottom of s trouser leg, shirt rim, belt or wears to wrist, ankle etc., plants essential oil be diffused in air just can light outdoor anophelifuge, and can the effective class mosquito of sucking blood such as repellent culex, Aedes albopictus, midge；The present invention has the function indicating its Use Limitation: owing to deionized water and quintessence oil can volatilize in atmosphere naturally, therefore the volume of mosquito-dispelling tablet will reduce therewith, after using a few hours, mosquito-dispelling tablet can dwindle into a lump, show that mosquito-repellent essential oil exhausts, no longer there is anophelifuge effect, facilitate the mosquito-dispelling tablet that user more renews.
Accompanying drawing explanation
Figure 1Structural representation for the present inventionFigure
Figure 2For mosquito-dispelling tablet and anophelifuge folder with the use of state referenceFigure。
Figure 2Shown in 1 be anophelifuge folder upper cover, 2 is plants essential oil mosquito-dispelling tablet, and 3 is anophelifuge grip box body.
Figure 3For mosquito-dispelling tablet and Snap bracelet with the use of state referenceFigure。
Figure 3Shown in 1 be Snap bracelet, 2 is mosquito expelling box base, and 3 is plants essential oil mosquito-dispelling tablet, and 4 is mosquito expelling box lid.
Figure 4For Y-shaped olfactometer referenceFigure。
Figure 4Middle A is sample arm pipe, and B is matched group arm pipe, and C is intermediate arm pipe, and D is discharge chamber, and E is that sample sets room, and F is control sample room, and G is for throwing insect population.
Detailed description of the invention
:
Below by combinationAccompanying drawingProvide embodiment technical scheme is further illustrated, technological means not specified in following example, all using conventional means well-known to those skilled in the art, in embodiment, the product of use, equipment are without special instruction, are commercially available prod, equipment.
Embodiment one:
A kind of band instruction function plants essential oil mosquito-dispelling tablet prepare example, the 6 hours use time of design, each component is weighed by following part by weight: agar 6%, polyglycolic acid 2%, Semen Myristicae oil 2%, Oleum Pelargonii Graveolentis 4%, Flos Jasmini Sambac oil 2%, MDJ 2%, ethylene carbonate 3%, sodium D-isoascorbate 0.05%, water colo(u)r 0.01%, deionized water 78.94%.
Deionized water, agar, polyglycolic acid, sodium D-isoascorbate and the water colo(u)r weighed by above-mentioned weight adds in stirred tank, heating for dissolving；Semen Myristicae oil, Oleum Pelargonii Graveolentis, Flos Jasmini Sambac oil and MDJ, ethylene carbonate are mixed into homogeneous phase solution；Stirred tank is cooled to 65 DEG C ± 5 DEG C, pours in stirred tank by plants essential oil mixed solution, and regulation mixing plant is to the most at a high speed；After continuously stirred several minutes, it is 6cm by feed liquid fill to sectional area2, in circular strip mould；Accelerate cooling, material depanning during temperature to 30 DEG C, according to 0.25cm thickness, carry out cutting into slices, packing, embodiment one i.e. molding.
Embodiment two:
A kind of band instruction function plants essential oil mosquito-dispelling tablet prepare example, the 10 hours use time of design, each component is weighed by following part by weight: agar 8%, polyvinyl acetate 3%, Herba Schizonepetae oil 5%, Oleum Anisi Stellati 3%, dihydromyrcenol 2%, ethyl acetate 2%, potassium sorbate 0.3%, water colo(u)r 0.05%, deionized water 76.65%.
Deionized water, agar, polyvinyl acetate, potassium sorbate and the water colo(u)r weighed by above-mentioned weight adds in stirred tank, heating for dissolving；Herba Schizonepetae oil, Oleum Anisi Stellati and dihydromyrcenol, ethyl acetate are mixed into homogeneous phase solution；Stirred tank is cooled to 65 DEG C ± 5 DEG C, pours in stirred tank by plants essential oil mixed solution, and regulation mixing plant is to the most at a high speed；After continuously stirred several minutes, it is 7cm by feed liquid fill to sectional area2, in circular strip mould；Accelerate cooling, material depanning during temperature to 40 DEG C, according to 0.3cm thickness, carry out cutting into slices, packing, embodiment two i.e. molding.
Embodiment three:
A kind of band instruction function plants essential oil mosquito-dispelling tablet prepare example, the 16 hours use time of design, each component is weighed by following part by weight: sodium alginate 7%, polyvinyl alcohol 5%, eucalyptus globolus oil 4%, Folium perillae acutae oil 2%, Herba Schizonepetae oil 4%, Allyl carbonate 5%, sodium dehydroacetate 0.2%, water colo(u)r 0.05%, deionized water 72.75%.
Deionized water, sodium alginate, polyvinyl alcohol, sodium dehydroacetate and the water colo(u)r weighed by above-mentioned weight adds in stirred tank, heating for dissolving；Folium perillae acutae oil, eucalyptus globolus oil, Herba Schizonepetae oil and Allyl carbonate are mixed into homogeneous phase solution；Stirred tank is cooled to 65 DEG C ± 5 DEG C, pours in stirred tank by plants essential oil mixed solution, and regulation mixing plant is to the most at a high speed；After continuously stirred several minutes, it is 8cm by feed liquid fill to sectional area2, in circular strip mould；Accelerate cooling, material depanning during temperature to 37 DEG C, according to 0.4cm thickness, carry out cutting into slices, packing, embodiment three i.e. molding.
Volatilization time experimental example
The present invention volatilize the time test method summary:
Testing equipment: climatic chamber；
Test method: the temperature arranging climatic chamber is 30 DEG C, relative humidity 65%, by embodiment assembles mosquito-dispelling tablet anophelifuge press from both sides, Snap bracelet claim its initial weight, put into climatic chamber afterwards.Each hour takes out and claims its current weight, calculates rate of volatilization percentage ratio, and a current secondary data and this data difference less than 1%, then stop experiment, the time (h) of record test last time.Retest three times, test result is averaged.The volatilization time according to the plants essential oil mosquito-dispelling tablet that above example formula is preparedSuch as table 1。
The volatilization time test of table 1 different formulations embodimentTable 1
| Embodiment | Design volatilization time (h) | Averagely volatilize the time (h) |
| Embodiment one | 6 | 6.5 |
| Embodiment two | 10 | 10.3 |
| Embodiment three | 16 | 16.7 |
ByTable 1Result understands, and 3 kinds of embodiments of the present invention all can reach to design the volatilization time, andSuch as figure 1Shown in, become a lump, reach the function indicating quintessence oil volatilization complete.
Repelling effect experimental example
The laboratory test methods summary of plants essential oil repelling effect of the present invention:
Test examination worm: Aedes albopictus Aedes albopictus introduces a fine variety from disease prevention and control center of Sichuan Province, in indoor [T:26 ± 2 DEG C of Chengdu Rainbow Electrical Appliances's biological culture, RH:65 ± 5%, 12L:12D] to raise, test chooses the female insect sprouted wings latter 3 days～do not suck blood for 5 days for examination.
Test apparatus and reagent: (self-control, is shown in for electronic analytical balance, Y-shaped olfactometerFigure 4), vacuum air pump, LZB-3WB type glass rotameter, Meng Shi wash bottle, 10 μ l microsyringes, mosquito cage (40cm × 30cm × 30cm), pipettor, tasteless silica gel tube, culture dish, tweezers, drying tower, filter paper etc..5%NaOH solution, granular active carbon, distilled water etc..
Test specimen: three kinds of embodiments.
Test method: use Y-shaped olfactometer to measure the plants essential oil repellent activity to Aedes albopictus female adult worm.Its method is with reference to F.Erler et al. (B.2006.Repellent activity
Of five essential oils against Culex pipiens.Fitoterapia, 77 (7-8): 491-494), more than wait quietly people (2008. culex pipiens pallens are to the feeler physiology of some compounds and behavior reaction. parasite and medical insect journal, 15 (3): 155), Lin Jie et al. (2011.Y type olfactometer flea class to host selectable study in application. Chinese media biology and control magazine, 22 (2): 103-106.127), and made some amendment.Mensuration system is made up of Y-shaped olfactometer, vacuum air pump, drying tower, Meng Shi wash bottle, sample room, LZB-3WB type glass rotameter, tasteless silica gel tube.Wherein: the long 100mm of supervisor of Y-shaped pipe, two-arm pipe range 150mm, 70 degree of two test arm pipe clamp angle, a diameter of 5cm.Assay method: under the conditions of room temperature (26 ± 1) DEG C relative humidity (65 ± 10) %, intensity of illumination 140Lux, install device as requested, after outside air purifies via drying tower, after entrance water tower is moistening, divide two-way to be connected by silica gel tube respectively and enter sample determination room, then connected the arm pipe entrance supervisor of Y-shaped pipe by silica gel tube, main tube gas's flow velocity is 20ml/min, eventually passes silica gel tube and discharges.When measuring every time, first put into 20 female mosquito from throwing insect population, clog throwing insect population with rubber stopper, and clog three mouths of pipe of Y-piece with the ground glass stopper being cased with gauze.The mosquito-dispelling tablet of 10mg embodiment is weighed with electronic analytical balance, put into sample room, side, opposite side sample room is placed the identical filter paper bar being marked with 10 μ l distilled water of size and is compared, open vacuum air pump, start timing, observe mosquito distribution of (A, B, C) in each arm, record 1 respectively, 5,10,15,20,25, the mosquito number of 30min two-arm pipe.Every kind of every 2h of embodiment carries out a test, till the design time, to observe the anophelifuge lasting effectiveness of embodiment.Every kind of embodiment is done 3 times and is repeated test, with the repeatability of viewing test.Process of the test arranges another identical device simultaneously and puts into 20 female mosquito of same batch, as blank group.
Scattering ratio PR(%) computing formula: PR=((Nc-Nt)/(Nc+Nt)) 100%
Wherein Nc: represent the mosquito number in matched group arm pipe；Nt: represent the mosquito number in processing arm pipe.
Table 2The different formulations embodiment average anophelifuge rate under the different designs volatilization time
ByTable 2Result understands, the repelling effect of the present invention is outstanding, and 3 kinds of described embodiments all anophelifuge rate PR can keep more than 87% within the design repellent time, and tests the PR when 10～15min every time and can reach more than 90%, illustrating that the evaporation rate of quintessence oil is stablized controlled, repelling effect is good.
The above, it it is only the preferred embodiment as technological innovation of the present invention, not the present invention is done any pro forma restriction, therefore it is every without departing from technical solution of the present invention content, any simple modification, modification or the equivalent variations done embodiment according to the technology contents essence of the present invention, all still falls within the range of technical solution of the present invention.
Claims (8)
1. the plants essential oil mosquito-dispelling tablet of a band instruction function, it is characterized in that the raw material comprising following percentage by weight forms: plants essential oil 1 ~ 10.0%, quintessence oil corrigent 1 ~ 10.0%, slow releasing agent 0.1 ~ 5.0%, forming agent 6 ~ 10.0%, preservative 0.02 ~ 0.5%, pigment 0.01 ~ 0.1%, deionized water 70.0 ~ 85.0%.
The plants essential oil mosquito-dispelling tablet of a kind of band the most according to claim 1 instruction function, it is characterised in that described plants essential oil is two or more mixture mixed with arbitrary proportion of rose oil, Oleum Pelargonii Graveolentis, Semen Myristicae oil, Herba Schizonepetae oil, Oleum Anisi Stellati, Folium perillae acutae oil, Flos Jasmini Sambac oil, thyme oil, eucalyptus globolus oil.
The plants essential oil mosquito-dispelling tablet of a kind of band the most according to claim 1 instruction function, it is characterised in that described quintessence oil corrigent is one or more mixture mixed with arbitrary proportion of MDJ, dihydromyrcenol, ethylene carbonate, ethyl acetate, Allyl carbonate.
The plants essential oil mosquito-dispelling tablet of a kind of band the most according to claim 1 instruction function, it is characterised in that described slow releasing agent is one or more mixture mixed with arbitrary proportion of polyvinyl alcohol, polyvinyl acetate, polyglycolic acid.
The plants essential oil mosquito-dispelling tablet of a kind of band the most according to claim 1 instruction function, it is characterised in that described forming agent is one or more mixture mixed with arbitrary proportion of sodium alginate, agar, diamantane (obsolete), microcrystalline Cellulose.
The plants essential oil mosquito-dispelling tablet of a kind of band the most according to claim 1 instruction function, it is characterised in that described preservative is sodium D-isoascorbate and potassium sorbate, the one of sodium dehydroacetate.
The plants essential oil mosquito-dispelling tablet of a kind of band the most according to claim 1 instruction function, it is characterised in that described pigment is water colo(u)r.
The manufacture method of the plants essential oil mosquito-dispelling tablet of a kind of band the most according to claim 1 instruction function, it is characterised in that comprise the steps of
1) deionized water and slow releasing agent, forming agent, preservative, pigment are added in stirred tank, heating for dissolving；
2) various plants quintessence oil, quintessence oil corrigent are mixed into homogeneous phase solution；
3) stirred tank is cooled to 65 DEG C ± 5 DEG C, pours in stirred tank by plants essential oil mixed solution, and regulation mixing plant is to the most at a high speed；
4) after continuously stirred several minutes, by the strip mould of feed liquid fill extremely known sectional area, required form；
5) cooling is accelerated, temperature to material depanning when 30-40 DEG C, determine thickness according to the design use time, carry out cutting into slices, packing, plants essential oil mosquito-dispelling tablet i.e. molding.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108077328A (en) * | 2017-11-21 | 2018-05-29 | 浙江森马服饰股份有限公司 | A kind of sustained release mosquito-dispelling tablet |
| CN110800730A (en) * | 2019-10-16 | 2020-02-18 | 吉林石油集团有限责任公司 | Vertical rod type camera device, spider netting prevention device, medicament and preparation method |
| CN113854285A (en) * | 2021-10-25 | 2021-12-31 | 成都彩虹电器（集团）股份有限公司 | Mosquito-repelling volatile core and preparation method thereof |
| CN115669649A (en) * | 2022-11-02 | 2023-02-03 | 中山榄菊日化实业有限公司 | Mosquito-repellent incense tablet and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108077328A (en) * | 2017-11-21 | 2018-05-29 | 浙江森马服饰股份有限公司 | A kind of sustained release mosquito-dispelling tablet |
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| CN113854285A (en) * | 2021-10-25 | 2021-12-31 | 成都彩虹电器（集团）股份有限公司 | Mosquito-repelling volatile core and preparation method thereof |
| CN115669649A (en) * | 2022-11-02 | 2023-02-03 | 中山榄菊日化实业有限公司 | Mosquito-repellent incense tablet and preparation method thereof |
| CN115669649B (en) * | 2022-11-02 | 2024-06-11 | 中山榄菊日化实业有限公司 | Mosquito-repellent incense tablet and preparation method thereof |
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