CN106153163A - A kind of sample Weighing method in automatic industrial analytical tool - Google Patents
A kind of sample Weighing method in automatic industrial analytical tool Download PDFInfo
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- CN106153163A CN106153163A CN201510183944.1A CN201510183944A CN106153163A CN 106153163 A CN106153163 A CN 106153163A CN 201510183944 A CN201510183944 A CN 201510183944A CN 106153163 A CN106153163 A CN 106153163A
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Abstract
The invention discloses a kind of sample Weighing method in automatic industrial analytical tool, the steps include: S1: place all of dress sample container;S2: sample dish declines, and sample balance will be claimed to reset;S3: add sample in dress sample container, utilizes and claims sample balance directly to weigh, obtain example weight, is denoted as sample weight M1, sample dish rises;S4: taken out from title sample balance by dress sample container, now claims the absolute value of the weight negative value obtained on sample balance to be dress sample container weight, is denoted as M0;S5: the M obtained by weighing0And M1, participate in the calculating of index.The present invention has can simplify step, reduce the advantage such as activity duration, raising whole efficiency.
Description
Technical field
Present invention relates generally to automatic industrial analytical equipment, refer in particular to one and be applicable to sample Weighing method in automatic industrial analytical tool.
Background technology
Automatic industrial analytical equipment is progressively applied to numerous industry and field, be used for sample is carried out automatically, the analysis of pipeline system or measurement operation.In the middle of various automatic industrial analytical equipments, in order to improve the efficiency of Instrumental Analysis test, often multiple sample on-position or the sample dish equipped with multiple samples are set on instrument, test sample is changed by conversion sample on-position or rotation sample dish, repeatedly load and unload the problem changing sample when avoiding multiple sample test task, thus multiple sample sequentially determining one by one can be made.
For by the analytical tool of weight difference before and after mensuration example reaction, it is both needed to dress sample container (such as crucible, beaker etc.) and sample are weighed respectively before example reaction, i.e. needs to carry out twice weighing stage.
Routine weighing flow process is: first weigh dress sample container (such as crucible, beaker etc.);In dress sample container, add sample again, weigh sample and the weight of dress sample container (such as crucible, beaker etc.);Finally by being calculated example weight.That is:
As it is shown in figure 1, coal sample is carried out moisture and the application process of ash analysis detection for existing weighting manner in automatic industrial analytical tool.Idiographic flow is:
S1: place all crucibles;
S2: balance of weighing resets;
S3: sample dish declines, and weighs the weight of current crucible, is denoted as M0, sample dish rises;Rotate to next bushing position, operate successively, until all crucibles are weighed;
S4: rotate at first sample position, sample dish declines, and to weighing, balance resets, and places sample, and the weight weighing sample is M1, sample dish rises;Rotate to next bushing position, operate successively, until all crucibles are weighed;
S5: the M obtained by weighing0And M1, participate in the calculating of index.
Have in the instrument of multiple sample test at the same time, use conventional flow process of weighing, after each shuttle (such as crucible, beaker etc.) need to being weighed respectively, then add sample one by one;The most respectively the container after adding sample is weighed, be finally calculated the actual weight of each sample.
In existing instrument and equipment, weigh dress sample container (such as crucible, beaker etc.) and sample, can be by weighing manually and instrument automatic Weighing realizes.As used the artificial manual mode weighed, this is accomplished by weighing each dress sample container (such as crucible, beaker etc.) and sample respectively, the most also needs to carry out the operation of twice weighing stage, and when sample size is more, manual steps is more, and the operating time is long.As used the mode of instrument automatic Weighing, test sample need to be changed by conversion sample on-position or rotation sample dish.But, in existing instrument and equipment, generally using motor drives sample dish to realize the conversion of sample position, it is required to start a driving means every time after weighing and is transformed into next sample position, it is longer that this conveying transformation process expends the time, especially when sample number is more time, the conveying conversion time is long, eventually has influence on Instrumental Analysis testing efficiency.It addition, the most general automatic Metage Eguipment is all to support sample dish by a sample weighting rod to complete to weigh operation, in the transformation process repeatedly weighed, it is easy to the problem producing off-centring of weighing, weighing precision impacts.Specifically, have the disadvantage that
1, during twice weighing, owing to industrial analysis instrument weighing room environment is unstable, the possible gap of other factors such as the ambient temperature of twice weighing, humidity is relatively big, and the accuracy of weighing has certain uncertain impact.
2, in the Industrial Analysis instrument of automatic Weighing, commonly used balance connects push rod and weighs weight, the method being dropped to realize on push rod weighing reading by rotating disk or manipulator control crucible during weighing.In such Weighing system, owing to selecting disc spins or mechanical hand running accuracy error when repeatedly weighing, rising or falling speed and the diversity in direction, may cause the center of gravity of placed crucible to be varied from every time, and impact weighs the moment of balance thus produces weighing error.
3, owing to, in Weighing system, weighing and being required for carrying out last result the revision of the convention every time, unnecessary weighing number of times will increase the cumulative error that the revision of the convention brings, and has influence on weighing precision.
Summary of the invention
The technical problem to be solved in the present invention is that the technical problem existed for prior art, and the present invention provides a kind of can simplify step, minimizing activity duration, the sample Weighing method in automatic industrial analytical tool of raising whole efficiency.
For solve above-mentioned technical problem, the present invention by the following technical solutions:
A kind of sample Weighing method in automatic industrial analytical tool, the steps include:
S1: place all of dress sample container;
S2: sample dish declines, and sample balance will be claimed to reset;
S3: add sample in dress sample container, utilizes and claims sample balance directly to weigh, obtain example weight, is denoted as sample weight M1, sample dish rises;
S4: taken out from title sample balance by dress sample container, now claims the absolute value of the weight negative value obtained on sample balance to be dress sample container weight, is denoted as M0;
S5: the M obtained by weighing0And M1, participate in the calculating of index.
As a further improvement on the present invention: described dress sample container is crucible or beaker.
Compared with prior art, it is an advantage of the current invention that: the Weighing method of the present invention, for the efficient Weighing method of one, i.e. clearing after dress sample container is placed on balance, add sample, directly weighing example weight, then taken out from balance by dress sample container, the absolute value reading the negative value that now balance shows is crucible weight.Two quality are used draw with the most once weighing, it is to avoid the generation of this error.Use this Weighing method, decrease dress sample container weighing stage, saved the weighing time, decrease operator simultaneously and participate in and the waiting time.
Accompanying drawing explanation
Fig. 1 is the schematic flow sheet that prior art is weighed.
Fig. 2 is the schematic flow sheet that the present invention weighs in concrete application example.
Detailed description of the invention
Below with reference to Figure of description and specific embodiment, the present invention is described in further details.
The sample Weighing method in automatic industrial analytical tool of the present invention, step is:
S1: place all of dress sample container;
S2: sample dish declines, and sample balance will be claimed to reset;
S3: add sample in dress sample container, utilizes and claims sample balance directly to weigh, obtain example weight, is denoted as sample weight M1, sample dish rises;
S4: taken out from title sample balance by dress sample container, now claims the absolute value of the weight negative value obtained on sample balance to be dress sample container weight, is denoted as M0;
S5: the M obtained by weighing0And M1, participate in the calculating of index.
Thus can disposably obtain the weight of sample, it is not necessary to carry out the calculating of complexity, it is to avoid inevitably compensate error in the middle of calculating, improve the precision weighed.
As in figure 2 it is shown, be present invention schematic flow sheet in a concrete application example.This example is so that coal sample to carry out moisture and the process of ash analysis detection in automatic industrial analytical tool.Idiographic flow is:
S1: place all of crucible;
S2: sample dish declines, and sample balance will be claimed to reset;
S3: add sample in crucible, utilizes and claims sample balance directly to weigh, obtain example weight, is denoted as sample weight M1, sample dish rises;
S4: by crucible from claiming taking-up sample balance, now claim the absolute value of the weight negative value obtained on sample balance to be crucible weight, be denoted as M0;
S5: the M obtained by weighing0And M1, participate in the calculating of index.
From said process, the efficient Weighing method of the present embodiment applies sample water/ash weighing process in automatic industrial analytical tool, main advantage resides in reduced a circle and weighs the action of whole crucibles, place after crucible without waiting for, be the most directly initially added into sample and claim sample operation.So, additionally it is possible to greatly reduce the participation time of switch gate action frequency and operator.As a example by the volatile matter of coal sample detects, without weighing crucible weight on every single project weighs, it will reduce by about 5min(10 sample weighing on the whole), substantially increase the efficiency of entirety.
Below being only the preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-described embodiment, and all technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that, for those skilled in the art, some improvements and modifications without departing from the principles of the present invention, should be regarded as protection scope of the present invention.
Claims (2)
1. a sample Weighing method in automatic industrial analytical tool, it is characterised in that step is:
S1: place all dress sample containers;
S2: sample dish declines, and sample balance will be claimed to reset;
S3: add sample in dress sample container, utilizes and claims sample balance directly to weigh, obtain example weight, is denoted as sample weight M1, sample dish rises;
S4: taken out from title sample balance by dress sample container, now claims the absolute value of the weight negative value obtained on sample balance to be dress sample container weight, is denoted as M0;
S5: the M obtained by weighing0And M1, participate in the calculating of index.
Sample Weighing method in automatic industrial analytical tool the most according to claim 1, it is characterised in that described dress sample container is crucible or beaker.
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CN201510183944.1A CN106153163A (en) | 2015-04-17 | 2015-04-17 | A kind of sample Weighing method in automatic industrial analytical tool |
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CN201510183944.1A CN106153163A (en) | 2015-04-17 | 2015-04-17 | A kind of sample Weighing method in automatic industrial analytical tool |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110333120A (en) * | 2019-07-24 | 2019-10-15 | 合肥工业大学 | A kind of machine components cleannes rapid detection method and device |
CN113533117A (en) * | 2021-07-16 | 2021-10-22 | 深圳诺普信农化股份有限公司 | Method for measuring retention of impregnation liquid medicine on surface of plant leaf |
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CN88211093U (en) * | 1988-02-11 | 1988-12-07 | 杨继和 | Spring balance |
EP1632760A1 (en) * | 2004-09-02 | 2006-03-08 | Metrohm Ag | Sample exchanger with integrated weighing device |
CN102313591A (en) * | 2010-07-07 | 2012-01-11 | 航天信息股份有限公司 | Weighing processing method and system |
CN102778290A (en) * | 2012-08-03 | 2012-11-14 | 昆山旭虹精密零组件有限公司 | Anti-overweight electronic balance |
CN103292886A (en) * | 2012-03-02 | 2013-09-11 | 梅特勒-托莱多有限责任公司 | System and method for differential weighing of items and reusable container for use therewith |
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2015
- 2015-04-17 CN CN201510183944.1A patent/CN106153163A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN88211093U (en) * | 1988-02-11 | 1988-12-07 | 杨继和 | Spring balance |
EP1632760A1 (en) * | 2004-09-02 | 2006-03-08 | Metrohm Ag | Sample exchanger with integrated weighing device |
CN102313591A (en) * | 2010-07-07 | 2012-01-11 | 航天信息股份有限公司 | Weighing processing method and system |
CN103292886A (en) * | 2012-03-02 | 2013-09-11 | 梅特勒-托莱多有限责任公司 | System and method for differential weighing of items and reusable container for use therewith |
CN102778290A (en) * | 2012-08-03 | 2012-11-14 | 昆山旭虹精密零组件有限公司 | Anti-overweight electronic balance |
Non-Patent Citations (1)
Title |
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竺江峰 等: "《大学物理实验教程》", 30 September 2011 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110333120A (en) * | 2019-07-24 | 2019-10-15 | 合肥工业大学 | A kind of machine components cleannes rapid detection method and device |
CN110333120B (en) * | 2019-07-24 | 2022-01-25 | 合肥工业大学 | Method and device for rapidly detecting cleanliness of mechanical part |
CN113533117A (en) * | 2021-07-16 | 2021-10-22 | 深圳诺普信农化股份有限公司 | Method for measuring retention of impregnation liquid medicine on surface of plant leaf |
CN113533117B (en) * | 2021-07-16 | 2024-03-19 | 深圳诺普信农化股份有限公司 | Method for measuring retention of impregnating liquid on plant leaf surface |
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