CN106148008A - A kind of preparation method of Herba Lysimachiae foenum-graeci quintessence oil - Google Patents
A kind of preparation method of Herba Lysimachiae foenum-graeci quintessence oil Download PDFInfo
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- CN106148008A CN106148008A CN201510143664.8A CN201510143664A CN106148008A CN 106148008 A CN106148008 A CN 106148008A CN 201510143664 A CN201510143664 A CN 201510143664A CN 106148008 A CN106148008 A CN 106148008A
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- herba lysimachiae
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Abstract
The present invention provides the preparation method of a kind of Herba Lysimachiae foenum-graeci quintessence oil, and this preparation method is with lavandula angustifolia dry flower piece as raw material, through series of steps such as vapor distillation, separation, column chromatographies, prepares Herba Lysimachiae foenum-graeci quintessence oil；The lavandula angustifolia preparation method that the present invention provides uses modernization separating and purifying technology, new technology, is suitable for industrialized production, has the strongest practicality.
Description
Technical field
The present invention relates to the preparation method of a kind of Herba Lysimachiae foenum-graeci quintessence oil, belong to technical field of plant extraction.
Background technology
Lavandula angustifolia (lavandula pedunculata) is that Labiatae lavandula angustifolia belongs to perennial undershrub, divides from purposes and can be divided into quintessence oil
Class and view and admire the big class of class two.Lavender for essential oil mainly has 3 kinds, it may be assumed that 1. narrow-leaved lavender Lavandula angustifolia Mill,
Also known as lavandula angustifolia, real lavandula angustifolia；2. aspic L.latifolia Vill, also known as wide leaf lavandula angustifolia；3. lavandin L.hybrida
Rev, is the plant of lavandula angustifolia and aspic hybridization.Originate in Mediterranean, throughout Europe and Oceania archipelago, from last
Rise the sixties in century lavandula angustifolia successively in Henan, Shaanxi, the ground such as Gansu and Xinjiang carry out the regional cultivation test of larger area,
Through for many years it was verified that lavandula angustifolia because its happiness light, the habit that cools of happiness and the highest with the fitness of Xinjiang natural environmental condition.
At present, the planting area of Xinjiang lavandula angustifolia is concentrated mainly on Yi Li, and this area's essential oil yield can account for more than the 90% of the whole nation,
While meeting raw material and the perfumery oil market demand at home, even it is on sale in Europe and market, the Central Asia.It is referred to as " China's lavandula angustifolia
Township ".
Herba Lysimachiae foenum-graeci quintessence oil is to be formed by refinement in lavender flower, can be with heat-clearing and toxic substances removing, and cleaning skin controls oil and divides, freckle removing and whitening,
Wrinkle removal skin care, eye haustra-dsipelling black eye, may additionally facilitate the skin-protecting functions such as damaged tissues regeneration recovery.Heart is had by Herba Lysimachiae foenum-graeci quintessence oil
Sedation effect, it is possible to decrease hypertension, pacify cardiopalmus, helpful for insomnia.Along with people's quality of the life improve constantly and
The change of consumption idea, the demand of natural perfume material is grown with each passing day by people, objectively needs society to provide more more preferable natural perfume (or spice)
Material, this is that the development of lavandula angustifolia industry provides direction and power.
Present invention aim at providing a kind of technique simple, environmental protection, low cost, be applicable to produce and amplify, it is easy to promote and have
The method preparing Herba Lysimachiae foenum-graeci quintessence oil of the strongest practicality.
Chinese patent 201410296543.2 discloses the extracting method of a kind of Herba Lysimachiae foenum-graeci quintessence oil, and the method takes fresh lavandula angustifolia, clearly
Water is cleaned, and naturally dries, and adds sodium chloride solution, soaks；Proceed to distilling apparatus and carry out air-distillation, by condensed fluid by dress
The adsorption column of active charcoal；In active carbon adsorption column, add ethanol solution divide with the oil in extraction active carbon adsorption column；To obtain
Lixiviating solution carry out decompression distillation, obtain Herba Lysimachiae foenum-graeci quintessence oil.The method can produce substantial amounts of waste active carbon and pollute environment, is not suitable for
A large amount of productions.
Chinese patent 20131063072.3 discloses the extracting method of a kind of Herba Lysimachiae foenum-graeci quintessence oil.The method is by using supercritical extraction
Combining extraction with rectification and obtain lavandula angustifolia crude oil, lavandula angustifolia crude oil is purified and obtains lavandula angustifolia by recycling molecular distillation technique further
Quintessence oil.The method extracting pressure is very big, high to process specifications, and equipment investment is expensive, is not suitable for producing in a large number.
The invention have the advantages that the Herba Lysimachiae foenum-graeci quintessence oil that can obtain in Aromatic water by macroporous adsorbent resin column chromatography, and macroporous absorption
Resin column not only can save cost but also improve yield with Reusability.Organic solvent used by eluting is ethanol solution, through over subtraction
Pressure distillation, remains without ethanol in product, to human non-toxic's evil effect.This Herba Lysimachiae foenum-graeci quintessence oil can be used in preparing cosmetics, washing
Articles for use, medicine etc., tool has been widely used and market prospect.
Summary of the invention
It is an object of the invention to provide a kind of method extracting Herba Lysimachiae foenum-graeci quintessence oil, use steam distillation and the method for column chromatography
Collect the Herba Lysimachiae foenum-graeci quintessence oil in Aromatic water, increase the yield of quintessence oil.
Comparison preferred embodiment according to the present invention, the preparation method extracting lavandula angustifolia comprises the steps:
(1) take a certain amount of lavandula angustifolia dry flower piece and put into distilling apparatus, be passed through steam and carry out air-distillation, to condensing droplet at glass
On plate, oil-free oozes and stops distillation now, cooling, oil-water separation；
(2) macroporous adsorptive resins on water intaking layer, after upper prop completes, after adding the water elution big polar impurity of removal, uses ethanol instead and washes
De-, without Herba Lysimachiae foenum-graeci quintessence oil to eluent, collect ethanol elution；
(3) ethanol elution carries out decompression distillation, and distillation Stress control is at-0.8Mpa～-1.0Mpa.
In above-mentioned steps (2), macroreticular resin used can be HPD-100, HPD-400, HPD-500, HPD-600,
Or D101, D1300, DM130, preferred resin model is the macroporous adsorbent resin of DM130；After upper prop completes, wash
Impurity, then with ethanol elution, the concentration of eluant can be 70%～95%, by containing eluting rate, sample yield, sample
Amount, the Integrated Selection of production cost, the concentration of eluting ethanol is preferably 95%；Eluting solvent consumption is the 0.1～1 of lavandula angustifolia amount
Again (m/V), preferably 0.5 times.
In above-mentioned steps (3), ethanol elution is recovered under reduced pressure at 60～70 DEG C, preferably 60 DEG C；
Detailed description of the invention
In following example, lavandula angustifolia used is purchased from Xinjiang Yili of China, and ethanol used is pharmaceutical grade, and water is purified water.
Embodiment one:
A: take 100Kg lavandula angustifolia dry flower piece and put into distilling apparatus, be passed through steam and carry out air-distillation, to condensing droplet at glass plate
On, oil-free oozes and stops distillation now, cooling, and oil-water separation obtains Herba Lysimachiae foenum-graeci quintessence oil 2.6L and water layer；
B: DM-130 macroporous adsorptive resins on water intaking layer, after upper prop completes, after adding the water elution big polar impurity of removal, uses instead
50L95% ethanol elution in eluent without Herba Lysimachiae foenum-graeci quintessence oil, collect eluent；By ethanol elution in-1.0Mpa 60 DEG C decompression
Distillation, obtains Herba Lysimachiae foenum-graeci quintessence oil 0.7L；
C: merge A and B gained Herba Lysimachiae foenum-graeci quintessence oil and obtain final Herba Lysimachiae foenum-graeci quintessence oil 3.3L.
Embodiment two:
A: take 50Kg lavandula angustifolia dry flower piece and put into distilling apparatus, be passed through steam and carry out air-distillation, to condensing droplet at glass plate
On, oil-free oozes and stops distillation now, cooling, and oil-water separation obtains Herba Lysimachiae foenum-graeci quintessence oil 1.3L and water layer；
B: HPD-100 macroporous resin column on water intaking layer, after upper prop completes, after adding the water elution big polar impurity of removal, uses 50L80% instead
Ethanol elution in eluent without Herba Lysimachiae foenum-graeci quintessence oil, collect eluent；By ethanol elution in-1.0Mpa 60 DEG C decompression distillation,
Obtain Herba Lysimachiae foenum-graeci quintessence oil 0.3L；
C: merge A and B gained Herba Lysimachiae foenum-graeci quintessence oil and obtain final Herba Lysimachiae foenum-graeci quintessence oil 1.6L.
Embodiment three:
A: take 100Kg lavandula angustifolia dry flower and put into distilling apparatus, be passed through steam and carry out air-distillation, to condensing droplet on a glass,
Oil-free oozes and stops distillation now, cooling, and oil-water separation obtains Herba Lysimachiae foenum-graeci quintessence oil 2.6L and water layer；
B: D101 macroporous resin column on water intaking layer, after upper prop completes, after adding the water elution big polar impurity of removal, uses 100L95% instead
Ethanol elution in eluent without Herba Lysimachiae foenum-graeci quintessence oil, collect eluent；By ethanol elution in-8.0Mpa 70 DEG C decompression distillation,
Obtain Herba Lysimachiae foenum-graeci quintessence oil 0.5L；
C: merge A and B gained Herba Lysimachiae foenum-graeci quintessence oil and obtain final Herba Lysimachiae foenum-graeci quintessence oil 3.1L.
Claims (2)
1. a preparation method for Herba Lysimachiae foenum-graeci quintessence oil, its preparation method is made up of the following steps:
Step 1, take lavandula angustifolia dry flower piece and put into distilling apparatus, be passed through water vapour air-distillation, to condensing droplet on a glass,
Oil-free oozes and stops distillation now, cooling, oil-water separation；
The macroporous adsorptive resins of certain model on step 2, water layer, after upper prop completes, after adding the water elution big polar impurity of removal,
Use 95% ethanol elution of 0.1～1 times of (m/V) lavandula angustifolia amount instead, without Herba Lysimachiae foenum-graeci quintessence oil to eluent, collect eluent；
Step 3, eluent are at 60～70 DEG C of concentrating under reduced pressure, and wherein distillation pressure is-0.8～-1.0Mpa.
2. preparation method as claimed in claim 1, it is characterised in that the macroporous absorption tree of the certain model described in above-mentioned steps 2
The model of fat is HPD-100, HPD-400, HPD-500, HPD-600, or the macropore tree of D101, D1300, DM130
Fat.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107604655A (en) * | 2017-10-08 | 2018-01-19 | 安徽三宝棉纺针织投资有限公司 | A kind of antibiotic aromatic composite finishing method of polyester fabric |
| CN107778960A (en) * | 2017-11-24 | 2018-03-09 | 天长市天翔包装有限公司 | A kind of fragrant pearl ink composition |
| CN110055132A (en) * | 2019-03-28 | 2019-07-26 | 广州白云山维一实业股份有限公司 | The method of purification of plants essential oil |
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| CN102676299A (en) * | 2012-05-16 | 2012-09-19 | 沈阳化工大学 | Reinforced extraction method for lavender essential oil |
| CN102965198A (en) * | 2012-11-14 | 2013-03-13 | 陈和平 | Method for extracting and processing lavender essential oil |
| CN104031745A (en) * | 2014-06-27 | 2014-09-10 | 钟延华 | Method for extracting lavender essential oil |
| CN104173432A (en) * | 2014-09-08 | 2014-12-03 | 南京飞马食品有限公司 | Method for extracting lavender polyphenol |
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2015
- 2015-03-26 CN CN201510143664.8A patent/CN106148008A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102676299A (en) * | 2012-05-16 | 2012-09-19 | 沈阳化工大学 | Reinforced extraction method for lavender essential oil |
| CN102965198A (en) * | 2012-11-14 | 2013-03-13 | 陈和平 | Method for extracting and processing lavender essential oil |
| CN104031745A (en) * | 2014-06-27 | 2014-09-10 | 钟延华 | Method for extracting lavender essential oil |
| CN104173432A (en) * | 2014-09-08 | 2014-12-03 | 南京飞马食品有限公司 | Method for extracting lavender polyphenol |
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| 陈健等: "《食品化学原理》", 28 February 2015, 华南理工大学出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107604655A (en) * | 2017-10-08 | 2018-01-19 | 安徽三宝棉纺针织投资有限公司 | A kind of antibiotic aromatic composite finishing method of polyester fabric |
| CN107778960A (en) * | 2017-11-24 | 2018-03-09 | 天长市天翔包装有限公司 | A kind of fragrant pearl ink composition |
| CN110055132A (en) * | 2019-03-28 | 2019-07-26 | 广州白云山维一实业股份有限公司 | The method of purification of plants essential oil |
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Application publication date: 20161123 |