CN106147988A - A kind of healthy Oleum Brassicae campestris process for refining - Google Patents
A kind of healthy Oleum Brassicae campestris process for refining Download PDFInfo
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- CN106147988A CN106147988A CN201610463634.XA CN201610463634A CN106147988A CN 106147988 A CN106147988 A CN 106147988A CN 201610463634 A CN201610463634 A CN 201610463634A CN 106147988 A CN106147988 A CN 106147988A
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- oil
- refining
- raw material
- brassicae campestris
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
- C11B3/06—Refining fats or fatty oils by chemical reaction with bases
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to vegetable oil field, be specifically related to a kind of healthy Oleum Brassicae campestris process for refining, including following operation: prepared by (1), raw material；(2), raw material is pulverized；(3), crude rapeseed oil is produced；(4), refined rapeseed oil is produced.Producing of described refined rapeseed oil comprises the following steps: (1), aquation degumming；(2), alkali-refining deacidification；(3), washing；(4), adsorption bleaching；(5), vacuum distilling deodorization.Raw material type of the present invention is rich and varied, can promote the raw material of edibility containing the high Semen Pini of edibility, sunflower seed etc., and also added Folium acanthaceous indigo and the Rhizoma Atractylodis Macrocephalae etc. has the Chinese medicine of the effects such as spleen reinforcing stomach reinforcing, preventing cold, has the highest nutritive value；And Oleum Brassicae campestris has carried out the multiple working procedures such as degumming, deacidification, decolouring and deodorization in process for refining, it is effectively reduced the impurity of Oleum Brassicae campestris, it is ensured that the quality of Oleum Brassicae campestris.
Description
Technical field
The present invention relates to vegetable oil field, be specifically related to a kind of healthy Oleum Brassicae campestris process for refining.
Background technology
Oleum Brassicae campestris raw material is called: vegetable oil, rapeseed oil, Semen Brassicae Campestris oil, Oleum sesami, be the most also canola oil, main product in China
Southwest.
Oleum Brassicae campestris is exactly the vegetable oil that we are commonly called as, and is again Herba Coriandri oil, is with the kind of crucifer Semen Brassicae Campestris (i.e. Brassica campestris L)
Son presses the liquid of the transparent or semitransparent shape of gained.Oleum Brassicae campestris golden yellow color or pale brown, has certain penetrating odor, among the people cries
Make " blue or green abnormal smells from the patient ".This gas is wherein to contain caused by a certain amount of sinigrin, but the Semen Brassicae campestris of special quality product kind is then without this
Material, such as high gas oil ratio Oleum Brassicae campestris, double-low rapeseed oil etc..
Oleum Brassicae campestris is one of China's main edible oil, and main product is in the Yangtze river basin and the ground such as southwest, northwest, and it is first that yield occupies the world
Position.Human body is the highest to the absorbance of Oleum Brassicae campestris, up to 99%.Oleum Brassicae campestris has certain vessel softening, effect of slow down aging.
Raw material owing to extracting oil is that the kind of plant is real, typically can be containing certain seed phospholipid, to blood vessel, nerve, the growth ten of brain
Divide important, and the cholesterol of Oleum Brassicae campestris is with little or no containing, so the people controlling cholesterol intake can be with relieved edible.
The Oleum Brassicae campestris impurity produced through conventional press technique is more, and fluid is the most muddy, affects attractive in appearance and mouth
Sense.
Summary of the invention
The technical problem to be solved is to provide a kind of impurity content few and the most useful to health
Oleum sesami.
The technical problem to be solved realizes by the following technical solutions:
A kind of healthy Oleum Brassicae campestris process for refining, including following operation:
(1), prepared by raw material: divides by quality and takes Semen Sesami 1000, and Semen Pini 80, sunflower seed 55, the Rhizoma Atractylodis Macrocephalae 30 and Folium acanthaceous indigo 10 are carried out
It is mixed to get liquefaction raw material；
(2), pulverize raw material: by liquefaction raw material in 70 DEG C of freeze-day with constant temperature 4h, take out after drying, pulverize with pulverizer, then
Cross 30 mesh sieve screenings；
(3), crude rapeseed oil is produced；
(4), refined rapeseed oil is produced.
Take the liquefaction material powder after a certain amount of sieve, put into pressafiner, obtain crude rapeseed oil.
Producing of described refined rapeseed oil comprises the following steps:
(1), aquation degumming: weigh a certain amount of crude rapeseed oil, crude oil is heated to 80-85 DEG C, then the hot water with 90 DEG C
Being sufficiently mixed together, stir with 50r/min speed when adding water, amount of water is 2-3 times of colloid, then reacts in hydration tank
35min, finally enters butterfly centrifugal machine and separates, obtain degumming oil；
(2), alkali-refining deacidification: weighing a certain amount of degumming oil and add in water washing tank, selected initial temperature is 30 DEG C, and final temperature is 50
DEG C, programming rate is 1.5 DEG C/min, and the alkali liquor adding 2.50mol/L is stirred, and stir speed (S.S.) is 50r/min, and alkali liquor is at 5-
All adding in 10min, the most uniformly spray the temperature saline identical with oil temperature of 5%, adding the saline time controls
10min, is centrifuged separating alkali refining oil and soap stock afterwards；
(3), washing: being washed by the centrifugal alkali refining oil obtained, washing temperature is 90 DEG C, and each amount of water is oil weight
10%, to wash 2-3 time, after washing, carry out vacuum dehydration drying, vacuum drying temperature is 90 DEG C, and vacuum, at 0.1MPa, is dried
After obtain alkali refining oil；
(4), adsorption bleaching: the alkali refining oil after having washed adds active hargil under stirring and fine vacuum, and hargil adds
After under a high vacuum continue stirring 15-20min, obtain the bleached oil containing hargil, vacuum is at 0.2MPa, then through hargil
Filter, by contaminant filters such as active hargil, obtains final bleached oil.
(5), vacuum distilling deodorization: after the bleached oil filtered is got to deodorizing tank keep high vacuum state heat,
Vacuum, at 0.6MPa, opens steam during temperature to 150 DEG C, be incubated 2h after continuing to be warmed to 250 DEG C, and insulation cools to after terminating
Steam off when 120 DEG C, continues to cool to less than 70 DEG C, obtains the refined rapeseed oil after deodorization.
In above-mentioned Oleum sesami formula, effect of each composition is as follows:
Semen Pini: the seed of pinaster；Semen Pini is fatty, protein, carbohydrate etc., and the food body-building heart, skin care, prolong for a long time
Year lengthens one's life；
Sunflower seed: containing abundant fatty oil, protein, saccharide and citric acid etc., have pre-hyperlipidemia and hypercholesteremia
The effect of disease；
Folium acanthaceous indigo: influenza and upper respiratory tract infection can be prevented；
The Rhizoma Atractylodis Macrocephalae: spleen reinforcing, stomach reinforcing, dampness, and in, to controlling deficient QI of the spleen and stomach, anorexia, the few gas of asthenia, deficiency-distension, have loose bowels, expectorant
Drink, dizzy, spontaneous perspiration, the crowds such as nausea is uneasy have good therapeutic efficiency；
The beneficial effects of the present invention is, raw material type of the present invention is rich and varied, containing the high Semen Pini of edibility, sunflower
Seeds etc. can promote the raw material of edibility, also added Folium acanthaceous indigo and the Rhizoma Atractylodis Macrocephalae etc. and has the effects such as spleen reinforcing stomach reinforcing, preventing cold
Chinese medicine, has the highest nutritive value；And Oleum Brassicae campestris has carried out the multiple tracks such as degumming, deacidification, decolouring and deodorization in process for refining
Operation, is effectively reduced the impurity of Oleum Brassicae campestris, it is ensured that the quality of Oleum Brassicae campestris.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below knot
Close specific embodiment, the present invention is expanded on further.
A kind of healthy Oleum Brassicae campestris process for refining, including following operation:
(1), prepared by raw material: divides by quality and takes Semen Sesami 1000, and Semen Pini 80, sunflower seed 55, the Rhizoma Atractylodis Macrocephalae 30 and Folium acanthaceous indigo 10 are carried out
It is mixed to get liquefaction raw material；
(2), pulverize raw material: by liquefaction raw material in 70 DEG C of freeze-day with constant temperature 4h, take out after drying, pulverize with pulverizer, then
Cross 30 mesh sieve screenings；
(3), crude rapeseed oil is produced；
(4), refined rapeseed oil is produced.
Take the liquefaction material powder after a certain amount of sieve, put into pressafiner, obtain crude rapeseed oil.
Producing of described refined rapeseed oil comprises the following steps:
(1), aquation degumming: weigh a certain amount of crude rapeseed oil, crude oil is heated to 80-85 DEG C, then the hot water with 90 DEG C
Being sufficiently mixed together, stir with 50r/min speed when adding water, amount of water is 2-3 times of colloid, then reacts in hydration tank
35min, finally enters butterfly centrifugal machine and separates, obtain degumming oil；
(2), alkali-refining deacidification: weighing a certain amount of degumming oil and add in water washing tank, selected initial temperature is 30 DEG C, and final temperature is 50
DEG C, programming rate is 1.5 DEG C/min, and the alkali liquor adding 2.50mol/L is stirred, and stir speed (S.S.) is 50r/min, and alkali liquor is at 5-
All adding in 10min, the most uniformly spray the temperature saline identical with oil temperature of 5%, adding the saline time controls
10min, is centrifuged separating alkali refining oil and soap stock afterwards；
(3), washing: being washed by the centrifugal alkali refining oil obtained, washing temperature is 90 DEG C, and each amount of water is oil weight
10%, to wash 2-3 time, after washing, carry out vacuum dehydration drying, vacuum drying temperature is 90 DEG C, and vacuum, at 0.1MPa, is dried
After obtain alkali refining oil；
(4), adsorption bleaching: the alkali refining oil after having washed adds active hargil under stirring and fine vacuum, and hargil adds
After under a high vacuum continue stirring 15-20min, obtain the bleached oil containing hargil, vacuum is at 0.2MPa, then through hargil
Filter, by contaminant filters such as active hargil, obtains final bleached oil.
(5), vacuum distilling deodorization: after the bleached oil filtered is got to deodorizing tank keep high vacuum state heat,
Vacuum, at 0.6MPa, opens steam during temperature to 150 DEG C, be incubated 2h after continuing to be warmed to 250 DEG C, and insulation cools to after terminating
Steam off when 120 DEG C, continues to cool to less than 70 DEG C, obtains the refined rapeseed oil after deodorization.
Use the refined sesame correlation theory index such as following table obtained by the present invention
The ultimate principle of the present invention, principal character and advantage have more than been shown and described.The technical staff of the industry should
Understanding, the present invention is not restricted to the described embodiments, the simply explanation present invention's of the description in above-described embodiment and description
Principle, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these change and change
Enter to both fall within scope of the claimed invention.Claimed scope is by appending claims and equivalent thereof
Define.
Claims (3)
1. a healthy Oleum Brassicae campestris process for refining, it is characterised in that: include following operation:
(1), prepared by raw material: divides by quality and takes Semen Sesami 1000, and Semen Pini 80, sunflower seed 55, the Rhizoma Atractylodis Macrocephalae 30 and Folium acanthaceous indigo 10 mix
Obtain liquefaction raw material；
(2), pulverize raw material: by liquefaction raw material in 70 DEG C of freeze-day with constant temperature 4h, take out after drying, pulverize with pulverizer, then cross 30
Mesh sieve sieves；
(3), crude rapeseed oil is produced；
(4), refined rapeseed oil is produced.
A kind of healthy Oleum Brassicae campestris process for refining the most according to claim 1, it is characterised in that: take the liquefaction after a certain amount of sieve
Material powder, puts into pressafiner, obtains crude rapeseed oil.
A kind of healthy Oleum Brassicae campestris process for refining the most according to claim 1, it is characterised in that: the system of described refined rapeseed oil
Take and comprise the following steps:
(1), aquation degumming: weigh a certain amount of crude rapeseed oil, crude oil is heated to 80-85 DEG C, then together with the hot water of 90 DEG C
Being sufficiently mixed, stir with 50r/min speed when adding water, amount of water is 2-3 times of colloid, then reacts 35min in hydration tank,
Finally enter butterfly centrifugal machine to separate, obtain degumming oil；
(2), alkali-refining deacidification: weighing a certain amount of degumming oil and add in water washing tank, selected initial temperature is 30 DEG C, and final temperature is 50 DEG C,
Programming rate is 1.5 DEG C/min, and the alkali liquor adding 2.50mol/L is stirred, and stir speed (S.S.) is 50r/min, and alkali liquor is at 5-
All adding in 10min, the most uniformly spray the temperature saline identical with oil temperature of 5%, adding the saline time controls
10min, is centrifuged separating alkali refining oil and soap stock afterwards；
(3), washing: being washed by the centrifugal alkali refining oil obtained, washing temperature is 90 DEG C, and each amount of water is oil weight
10%, to wash 2-3 time, after washing, carry out vacuum dehydration drying, vacuum drying temperature is 90 DEG C, and vacuum, at 0.1MPa, is dried
After obtain alkali refining oil；
(4), adsorption bleaching: after having washed alkali refining oil stirring and fine vacuum under add active hargil, hargil add after
Continuing stirring 15-20min under fine vacuum, obtain the bleached oil containing hargil, vacuum, at 0.2MPa, filters then through hargil
Machine, by contaminant filters such as active hargil, obtains final bleached oil；
(5), vacuum distilling deodorization: keep high vacuum state to heat after the bleached oil filtered is got to deodorizing tank, vacuum
Degree, at 0.6MPa, opens steam during temperature to 150 DEG C, be incubated 2h after continuing to be warmed to 250 DEG C, and insulation cools to 120 after terminating
DEG C time steam off, continue to cool to less than 70 DEG C, obtain the refined rapeseed oil after deodorization.
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| CN201610463634.XA CN106147988A (en) | 2016-06-23 | 2016-06-23 | A kind of healthy Oleum Brassicae campestris process for refining |
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Family
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106635250A (en) * | 2016-12-08 | 2017-05-10 | 安徽凯奥新能源股份有限公司 | Method for preparing transformer oil from edible vegetable oil |
| CN106833868A (en) * | 2016-12-23 | 2017-06-13 | 庆阳敦博科技发展有限公司 | A kind of method that apple seed oil is extracted in pomace |
| CN106967504A (en) * | 2017-05-25 | 2017-07-21 | 国网河南省电力公司电力科学研究院 | A kind of natural esters insulating oil extracts alkali refining mixing acid stripping method |
| CN107245375A (en) * | 2017-07-21 | 2017-10-13 | 成都市新兴粮油有限公司 | Rapeseed oil aquation Degumming method |
| CN107307096A (en) * | 2017-07-07 | 2017-11-03 | 安徽省康龙农业开发有限公司 | A kind of stomach invigorating dispel cold type reconcile rapeseed oil |
| CN107557151A (en) * | 2017-09-08 | 2018-01-09 | 安徽赵老五油脂有限公司 | A kind of rapeseed oil processing process |
| CN109852472A (en) * | 2019-03-07 | 2019-06-07 | 四川德阳市年丰食品有限公司 | A kind of squeezing refining technique for manufacturing of rapeseed oil |
| CN109852471A (en) * | 2019-03-07 | 2019-06-07 | 四川德阳市年丰食品有限公司 | It is a kind of to refine the small manufacture craft for squeezing rapeseed oil |
| CN115926886A (en) * | 2022-12-29 | 2023-04-07 | 长寿花食品股份有限公司 | Corn oil refining process |
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| CN105132157A (en) * | 2015-08-28 | 2015-12-09 | 成都市新津迎先粮油有限公司 | Refining process for rapeseed oil |
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| CN1076589A (en) * | 1993-01-01 | 1993-09-29 | 吴宗民 | Nutrition oil |
| CN103168859A (en) * | 2013-04-10 | 2013-06-26 | 饶攀 | Oil composition and preparation method thereof |
| CN103636816A (en) * | 2013-12-06 | 2014-03-19 | 太和县庄老汉杂粮有限公司 | Sesame oil with functions of blood pressure lowering and health caring |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106635250A (en) * | 2016-12-08 | 2017-05-10 | 安徽凯奥新能源股份有限公司 | Method for preparing transformer oil from edible vegetable oil |
| CN106833868A (en) * | 2016-12-23 | 2017-06-13 | 庆阳敦博科技发展有限公司 | A kind of method that apple seed oil is extracted in pomace |
| CN106967504A (en) * | 2017-05-25 | 2017-07-21 | 国网河南省电力公司电力科学研究院 | A kind of natural esters insulating oil extracts alkali refining mixing acid stripping method |
| CN106967504B (en) * | 2017-05-25 | 2020-07-03 | 国网河南省电力公司电力科学研究院 | Natural ester insulating oil extraction-alkali refining mixed deacidification method |
| CN107307096A (en) * | 2017-07-07 | 2017-11-03 | 安徽省康龙农业开发有限公司 | A kind of stomach invigorating dispel cold type reconcile rapeseed oil |
| CN107245375A (en) * | 2017-07-21 | 2017-10-13 | 成都市新兴粮油有限公司 | Rapeseed oil aquation Degumming method |
| CN107557151A (en) * | 2017-09-08 | 2018-01-09 | 安徽赵老五油脂有限公司 | A kind of rapeseed oil processing process |
| CN109852472A (en) * | 2019-03-07 | 2019-06-07 | 四川德阳市年丰食品有限公司 | A kind of squeezing refining technique for manufacturing of rapeseed oil |
| CN109852471A (en) * | 2019-03-07 | 2019-06-07 | 四川德阳市年丰食品有限公司 | It is a kind of to refine the small manufacture craft for squeezing rapeseed oil |
| CN115926886A (en) * | 2022-12-29 | 2023-04-07 | 长寿花食品股份有限公司 | Corn oil refining process |
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