CN106140045B - A kind of reactor for carrying filtering - Google Patents

A kind of reactor for carrying filtering Download PDF

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Publication number
CN106140045B
CN106140045B CN201610491661.8A CN201610491661A CN106140045B CN 106140045 B CN106140045 B CN 106140045B CN 201610491661 A CN201610491661 A CN 201610491661A CN 106140045 B CN106140045 B CN 106140045B
Authority
CN
China
Prior art keywords
filter
export
entrance point
port
negative pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201610491661.8A
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Chinese (zh)
Other versions
CN106140045A (en
Inventor
李德清
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ANHUI GUANGDE HUALIN PAINT FACTORY
Original Assignee
ANHUI GUANGDE HUALIN PAINT FACTORY
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Priority to CN201610491661.8A priority Critical patent/CN106140045B/en
Publication of CN106140045A publication Critical patent/CN106140045A/en
Application granted granted Critical
Publication of CN106140045B publication Critical patent/CN106140045B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/002Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D36/00Filter circuits or combinations of filters with other separating devices
    • B01D36/02Combinations of filters of different kinds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/04Feed or outlet devices; Feed or outlet control devices using osmotic pressure using membranes, porous plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/005Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the outlet side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00245Avoiding undesirable reactions or side-effects
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00245Avoiding undesirable reactions or side-effects
    • B01J2219/00252Formation of deposits other than coke

Abstract

The invention discloses a kind of reactor for carrying filtering, including reaction kettle body, also include being located at the negative-pressure cyclic filter that is filtered to raw material of being used on the reaction kettle body, the negative-pressure cyclic filter includes first filter connected with motor and the second filter being connected with first filter.The present invention can just filter before raw material is chemically reacted to the impurity in raw material, simple and convenient so that the product for reacting to obtain is purer.

Description

A kind of reactor for carrying filtering
Technical field
The present invention relates to technical field of chemical, more specifically to a kind of reactor for carrying filtering.
Background technology
Chemical liquid reactor, reaction kettle body and stirring system are generally comprised, charge door is provided with the top of reaction kettle body, is reacted Autoclave body bottom is provided with drain hole, and stirring system includes the motor being arranged at the top of reaction kettle body and is arranged at stirring in reaction kettle body Device is mixed, agitator includes stirring shaft and stirring vane, stirring shaft and motor connection, and stirring vane is fixed with stirring shaft to be connected Connect;At present, raw material is directly directly added into by most of reactors from charge door, after stirring system stirs, passes through heating etc. Condition is reacted, and there is following hidden danger for the method:Impurity such as some Solid-state Chemistry particles in raw material can also participate in instead Should, raw material is both wasted, and other products are generated, the product with planning to obtain is not inconsistent, or the impurity in raw material is not joined With reaction, but impurity is adulterated in reacted product, leverage the quality of product.
The content of the invention
It is an object of the invention to provide a kind of reactor for carrying filtering, before raw material is chemically reacted, just to original Impurity in material is filtered, simple and convenient so that the product for reacting to obtain is purer.
The present invention above-mentioned technical purpose technical scheme is that:A kind of reaction for carrying filtering Kettle, including reaction kettle body, in addition to the negative-pressure cyclic for being filtered to raw material being located on the reaction kettle body filter dress Put, the second filtering dress that the negative-pressure cyclic filter includes the first filter and connected with first filter Put;First filter include being located at the rotation whipping screen pack of motor and the motor connection above reaction kettle body, Be located at it is described rotation whipping filtering sieve bottom impurity collecting box, be fixedly connected on reaction kettle body be used for store the rotation Whipping screen pack throws away the liquid holding tank of liquid and is located at the outlet at bottom of the liquid holding tank bottom, and the rotation is got rid of Dynamic screen pack is arranged on inside the liquid holding tank and can taken out from the liquid holding tank.
Preferably, the liquid holding tank and reaction kettle body junction be provided with it is convenient by the rotation whipping screen pack from The liquid holding tank takes out required hole.
Preferably, the rotation whipping screen pack includes and the connecting shaft of the motor connection, is fixedly connected on the company Cylinder type filter net in spindle and be set in outside the connecting shaft and the raw material that is communicated with the cylinder type filter net enter Enter passage, the uniform filter bores of cylinder type filter net, the cylinder type filter net does not have adhesiveness.
Preferably, the liquid holding tank bottom is in funnel-form.
Preferably, the impurity collecting box includes a collection entrance collapsed downwards.
Preferably, second filter includes liquid inlet tee joint pipe, goes out liquid threeway pipe, filtration members, negative pressure device, described Liquid inlet tee joint pipe includes entrance point a, entrance point b and port of export a, the goes out liquid threeway pipe include entrance point c, port of export b with And port of export c, the entrance point a connect with the outlet at bottom, the filtration members be located at the port of export a and entrance point c it Between, the negative pressure device is located between the port of export b and the entrance point b, the outlet at bottom, the entrance point a, described Port of export a, the filtration members, the entrance point c and the port of export c form passage by pipeline and note the raw material after filtering Enter in the reaction kettle body, the entrance point b, the port of export a, the filtration members, the entrance point c, the port of export b with And the negative pressure device forms negative-pressure cyclic filtration channel by pipeline.
Preferably, the filtration members include filtering body, the filter chamber being located inside the filtering body, are located at the filter chamber In the impurity discharging device discharged of screen pack and the impurity for being used to be filtered down the screen pack that is communicated with the filter chamber.
Preferably, the negative pressure device includes negative pressure body, the negative pressure cavity being located inside the negative pressure body, is located at the negative pressure Aspiration pump on body.
In summary, the invention has the advantages that:
Before raw material is chemically reacted, just the impurity in raw material is filtered, it is simple and convenient so that reaction obtains Product it is purer.
Brief description of the drawings
Fig. 1 is the structural representation of one embodiment of the invention;
Fig. 2 is the structural representation of the negative-pressure cyclic filter of the present invention;
Fig. 3 is the first filter apparatus configuration schematic diagram of the present invention;
Fig. 4 is the structural representation of filtration members;
Fig. 5 is the schematic top plan view of filtration members;
Fig. 6 is the sectional view at C-C in Fig. 5;
Fig. 7 is the schematic cross-sectional view of negative pressure device.
Embodiment
The present invention is described in further detail below in conjunction with accompanying drawing.
This specific embodiment is only explanation of the invention, and it is not limitation of the present invention, people in the art Member can make the modification of no creative contribution to the present embodiment as needed after this specification is read, but as long as at this All protected in the right of invention by Patent Law.
Embodiment:Shown in Fig. 1, Fig. 2, Fig. 3, Fig. 4, Fig. 5, Fig. 6, Fig. 7, a kind of reactor for carrying filtering, including reaction Kettle 1, in addition to be located on the reaction kettle body 1 for the negative-pressure cyclic filter 2 that is filtered to raw material, it is described negative Circulation filter 2 is pressed to include the first filter 201 and the second filter with first filter 201 connection 202;First filter 201 includes the motor 2011 for being located at the top of reaction kettle body 1 and the motor 2011 connects Rotation whipping screen pack 2012, be located at the impurity collecting box 2013 of the bottom of rotation whipping screen pack 2012, be fixedly connected On the reaction kettle body 1 be used to store the rotation whipping screen pack 2012 throw away liquid liquid holding tank 2014 and The outlet at bottom 2015 of the bottom of liquid holding tank 2014 is located at, the rotation whipping screen pack 2012 is arranged on the liquid It can take out inside holding tank 2014 and from the liquid holding tank 2014.
Second filter 202 is located at the left side of the reaction kettle body 1 and is fixedly mounted on institute by profile piece State on reaction kettle body 1, the motor 2011 is fixedly connected on mounting bracket 4, and mounting bracket 4 is profile piece, the He of motor 2011 The rotation whipping screen pack 2012 is connected by shaft coupling.
Further, the liquid holding tank 2014 is provided with convenient by the rotation with the junction of reaction kettle body 1 Whipping screen pack 2012 takes out required hole 20141 from the liquid holding tank 2014, and the rotation whipping screen pack 2012 wraps Include and the connecting shaft 20121 of the motor 2011 connection, the cylinder type filter net being fixedly connected in the connecting shaft 20121 20122 and be set in the outside of the connecting shaft 20121 and the raw material that is communicated with the cylinder type filter net 20122 enter it is logical Road 20123, the 20122 uniform filter bores of cylinder type filter net, the cylinder type filter net 20122 do not have adhesiveness.
Further, the bottom of liquid holding tank 2014 is in funnel-form, facilitates and is got rid of in the cylinder type filter net 20122 The raw material gone out more preferably enters the second filter 202.
Further, the impurity collecting box 2013 includes a collection entrance collapsed downwards, the rotation whipping mistake For filter screen 2012 in rotation, impurity enters impurity collecting box 2013 along the collection entrance collapsed downwards, and impurity is into impurity After collecting box 2013, due to collect entrance collapse downwards, impurity be not easy from impurity collecting box 2013 return to once again it is described rotation get rid of In dynamic screen pack 2012.
Further, second filter 202 includes liquid inlet tee joint pipe 2021, goes out liquid threeway pipe 2022, filtration members 2023rd, negative pressure device 2024, the liquid inlet tee joint pipe 2021 include entrance point a2021a, entrance point b2021b and the port of export A2021c, the goes out liquid threeway pipe 2022 include entrance point c2022a, port of export b2022b and port of export c2022c, it is described enter Mouth end a2021a connects with the outlet at bottom 2015, and the filtration members 2023 are located at the port of export a2021c and entrance point Between c2022a, the negative pressure device 2024 is located between the port of export b2022b and the entrance point b2021b, the bottom Portion outlet 2015, the entrance point a2021a, the port of export a2021c, the filtration members 2023, the entrance point c2022a And the port of export c2022c forms passage by pipeline and injects the raw material after filtering in the reaction kettle body 1, it is described enter Mouth end b2021b, the port of export a2021c, the filtration members 2023, the entrance point c2022a, the port of export b2022b And the negative pressure device 2024 forms negative-pressure cyclic filtration channel by pipeline.
The flow control valve for being used for adjusting flow, institute are provided with the port of export b2022b and port of export c2022c State and check valve is provided with entrance point b2021b, check valve control raw material can only flow into the port of export from the negative pressure device 2024 A2021c, adverse current will not be produced.
Further, the filtration members 2023 include filtering body 20231, the filtering being located inside the filtering body 20231 Chamber 20232, the screen pack 20233 being located in the filter chamber 20232 and and being used for institute of communicating of the filter chamber 20232 State the impurity discharging device 20234 for the impurity discharge that screen pack 20233 is filtered down.
Further, the negative pressure device 2024 includes negative pressure body 20241, is located at bearing inside the negative pressure body 20241 Pressure chamber 20242, the aspiration pump 20243 being located in the negative pressure body 20241, the bottom of negative pressure cavity 20242 is provided with negative pressure cavity liquid Import, the side wall of negative pressure cavity 20242 are provided with negative pressure cavity liquid outlet, the height of negative pressure cavity liquid outlet in the vertical direction be higher than into The height of mouthful end b2021b in the vertical directions, and pipeline between negative pressure cavity liquid outlet and entrance point b2021b it is curved to Under, the whole downward pipeline of arc is not at the pipeline in horizontal direction, further ensure that liquid from negative pressure cavity 20242 It will not be detained after into the downward pipeline of arc in the downward pipeline of arc.
The present invention specific implementation principle be:By the flow control valve at the port of export b2022b, the port of export The closed check valve at flow control valve and the entrance point b2021b at c2022c, with the aspiration pump 20243 by institute State the air in negative pressure cavity 20242 to detach to form negative pressure state, open motor 2011, it is logical to add the raw material into the raw material entrance In road 20123, raw material enters the second filter 202 after the rotation whipping screen pack 2012 tentatively filtering, opens institute The flow control valve at port of export b2022b is stated, raw material, which enters, to be in the negative pressure cavity 20242 under negative pressure state, when raw material covers After negative pressure cavity liquid outlet, continue to detach the air in negative pressure cavity 20242 with aspiration pump 20243, while open entrance point Check valve at b2021b, until raw material can be along the entrance point b2021b, the port of export a2021c, the filtration members 2023rd, the negative pressure that the entrance point c2022a, the port of export b2022b and the negative pressure device 2024 are formed by pipeline After the flowing of circulating filtration channel cycle, aspiration pump 20243 is closed, now the pressure in negative pressure device 2024 is kept constant, band mistake After the completion of filter, the check valve at flow control valve and entrance point b2021b at closing port of export b2022b, the port of export is opened Flow control valve at c2022c, the raw material after filtering enter in reaction kettle body 1.

Claims (5)

1. a kind of reactor for carrying filtering, including reaction kettle body(1), it is characterised in that also include being located at the reaction kettle body (1)On for the negative-pressure cyclic filter that is filtered to raw material(2), the negative-pressure cyclic filter(2)Including One filter(201)And with first filter(201)Second filter of connection(202);First mistake Filter device(201)Including being located at the reaction kettle body(1)The motor of top(2011)And the motor(2011)The rotation of connection Whipping screen pack(2012), be located at it is described rotation whipping screen pack(2012)The impurity collecting box of bottom(2013), be fixedly connected In the reaction kettle body(1)On be used for store it is described rotation whipping screen pack(2012)Throw away the liquid holding tank of liquid (2014)And it is located at the liquid holding tank(2014)The outlet at bottom of bottom(2015), the rotation whipping screen pack (2012)It is arranged on the liquid holding tank(2014)It is internal and can be from the liquid holding tank(2014)Middle taking-up;It is described Second filter(202)Including liquid inlet tee joint pipe(2021), goes out liquid threeway pipe(2022), filtration members(2023), negative pressure device (2024), the liquid inlet tee joint pipe(2021)Including entrance point a(2021a), entrance point b(2021b)And port of export a (2021c), the goes out liquid threeway pipe(2022)Including entrance point c(2022a), port of export b(2022b)And port of export c (2022c), the entrance point a(2021a)With the outlet at bottom(2015)Connection, the filtration members(2023)Go out described in being located at Mouth end a(2021c)With entrance point c(2022a)Between, the negative pressure device(2024)It is located at the port of export b(2022b)With institute State entrance point b(2021b)Between, the outlet at bottom(2015), the entrance point a(2021a), the port of export a (2021c), the filtration members(2023), the entrance point c(2022a)And the port of export c(2022c)Formed by pipeline Raw material after filtering is injected the reaction kettle body by passage(1)In, the entrance point b(2021b), the port of export a (2021c), the filtration members(2023), the entrance point c(2022a), the port of export b(2022b)And the negative pressure dress Put(2024)Negative-pressure cyclic filtration channel is formed by pipeline;The filtration members(2023)Including filtering body(20231), be located at institute State filtering body(20231)Internal filter chamber(20232), be located at the filter chamber(20232)In screen pack(20233)And With the filter chamber(20232)What is communicated is used for the screen pack(20233)The impurity discharging device of the impurity discharge filtered down (20234);The negative pressure device(2024)Including negative pressure body(20241), be located at the negative pressure body(20241)Internal negative pressure Chamber(20242), be located at the negative pressure body(20241)On aspiration pump(20243).
A kind of 2. reactor for carrying filtering according to claim 1, it is characterised in that the liquid holding tank(2014)With The reaction kettle body(1)Junction is provided with convenient by the rotation whipping screen pack(2012)From the liquid holding tank (2014)Hole needed for taking out(20141).
A kind of 3. reactor for carrying filtering according to claim 1, it is characterised in that the rotation whipping screen pack (2012)Including with the motor(2011)The connecting shaft of connection(20121), be fixedly connected in the connecting shaft (20121) Cylinder type filter net (20122) and be set in outside the connecting shaft (20121) and with the cylinder type filter net (20122) The raw material communicated enters passage(20123), the cylinder type filter net(20122)Uniform filter bores, the cylinder type filter net (20122)Without adhesiveness.
A kind of 4. reactor for carrying filtering according to claim 1, it is characterised in that the liquid holding tank(2014)Under End is in funnel-form.
A kind of 5. reactor for carrying filtering according to claim 1, it is characterised in that the impurity collecting box(2013)Bag Include the collection collapsed a downwards entrance.
CN201610491661.8A 2016-06-29 2016-06-29 A kind of reactor for carrying filtering Expired - Fee Related CN106140045B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610491661.8A CN106140045B (en) 2016-06-29 2016-06-29 A kind of reactor for carrying filtering

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610491661.8A CN106140045B (en) 2016-06-29 2016-06-29 A kind of reactor for carrying filtering

Publications (2)

Publication Number Publication Date
CN106140045A CN106140045A (en) 2016-11-23
CN106140045B true CN106140045B (en) 2017-11-24

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610491661.8A Expired - Fee Related CN106140045B (en) 2016-06-29 2016-06-29 A kind of reactor for carrying filtering

Country Status (1)

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Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201337902Y (en) * 2008-11-04 2009-11-04 无锡市张华医药设备有限公司 Filtering, washing and drying three-in-one device
CN201394388Y (en) * 2009-05-21 2010-02-03 赵恩 Circulation and filtration device
CN203763898U (en) * 2014-04-04 2014-08-13 佛山市海天(高明)调味食品有限公司 Raw material extraction tank
CN204710171U (en) * 2015-06-16 2015-10-21 李贞贞 A kind ofly stablize firm agitator tank
CN105413618A (en) * 2015-11-25 2016-03-23 郑臣钏 Chemical reaction device capable of detecting pH value of solution in real time and containing solution conveniently

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