CN106118313A - The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings and preparation method - Google Patents
The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings and preparation method Download PDFInfo
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- CN106118313A CN106118313A CN201610458641.0A CN201610458641A CN106118313A CN 106118313 A CN106118313 A CN 106118313A CN 201610458641 A CN201610458641 A CN 201610458641A CN 106118313 A CN106118313 A CN 106118313A
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- mildew
- environmental protection
- coating material
- protection coating
- flame retarded
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/08—Homopolymers or copolymers of acrylic acid esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention belongs to functional environment-friendly paint field, be specifically related to formula and the preparation method of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings.The present invention is with acrylic acid ester emulsion as film forming matter, with glyoxaline compound as antifungus agent, halogen-free flame-retardant system is constituted with APP, tripolycyanamide and aluminium oxide, and add titanium dioxide, sericite, thickening agent, wetting agent, dispersant, defoamer and coalescents, it is prepared for may be used to the mildew-proof flame retarded environmental protection coating material of timber buildings.Prepared coating has mildew-resistant, the function such as fire-retardant, can be widely used for timber buildings, protects building, improves the live and work environment of people.
Description
Technical field
The invention belongs to field of functional coatings, be specifically related to a kind of mildew-proof flame retarded environmental protection coating material for timber buildings
Formula and preparation method.
Background technology
Timber has the features such as lightweight, intensity is high, attractive in appearance, good processability as construction material, is the most just subject to
Have a preference for people.Compared with the most a large amount of armored concrete used or brick structure house, wooden frame structure has following excellent
Gesture: (1) timber is a kind of natural, healthy material, wood materials is renewable, recoverable, environmental protection；(2) timber structure
Moment impact and Cyclic fatigue are destroyed there is good resistivity；(3) wooden frame structure is used can to protect soil；
(4) building timber buildings, the construction time is short, easy to maintenance, has layout and flexibly with moulding and keeps in repair and overhaul convenient spy
Point, and equipment required when timber keeps in repair or transforms is relatively easy, personnel are the most less.Timber buildings can be again because of it
Life, good processability, recoverable, meet the requirements of the times of low-carbon (LC), energy-saving and environmental protection, and demand increases the most year by year.But with
Time timber buildings there is also the defects such as inflammable, the most mouldy, the therefore fire prevention of wooden frame structure, mildew-resistant are the most necessary.Modern work
Cheng Zhong, most widely used, the suitability is the strongest, construction is fireproof coating the most easily.APP, tripolycyanamide, aluminium oxide structure
Become flame-retardant system to have good flameproof effect, hydrogen halide will not be released during burning simultaneously, such that it is able to provide for people
One safe and reliable living environment.Glyoxaline compound has good mildew-resistant, bactericidal property, and therefore adding to can in coating
To give the performance of coating mildew-resistant.It addition, Environmental Protective Water-paint is without low VOC (V DEG C), environmentally safe,
Health will not be damaged, green truly, environmental protection can be reached, increasingly liked by people and pay attention to.Wood
The complete composite green of the mildew-proof flame retarded coating of structural construction, the Times ' Demand of environmental protection, can be people provide one safe and healthy
Living environment.
Summary of the invention
It is an object of the invention to: formula and the preparation of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings are provided
Method.Using acrylic acid ester emulsion as film forming matter, using glyoxaline compound as antifungus agent, with APP, tripolycyanamide,
Aluminium oxide constitutes flame-retardant system, is compounded with the filler such as titanium dioxide, sericite, and adds thickening agent, wetting agent, dispersant, froth breaking
Agent, coalescents, be prepared for having mildew-resistant, anti-flaming function plate for timber-construction environmental protection coating material.
Technical scheme: the formula of the mildew-proof flame retarded environmental protection coating material for timber buildings that the present invention proposes:
Including following components and mass fraction:
| Acrylic acid ester emulsion | 35～50 |
| Antifungus agent | 0.2～1 |
| APP | 2～15 |
| Tripolycyanamide | 1～10 |
| Aluminium oxide | 1～5 |
| Titanium dioxide | 10～20 |
| Sericite | 2～10 |
| Thickening agent | 0.5～1 |
| Defoamer | 0.2～0.5 |
| Dispersant | 0.2～1 |
| Coalescents | 1～2 |
| Deionized water | 20～30 |
In the present invention, described antifungus agent is glyoxaline compound.
In the present invention, described fire retardant is that APP, tripolycyanamide and aluminium oxide constitute halogen-free flame-retardant system.
In the present invention, described thickening agent is hydroxyethyl cellulose.
In the present invention, described defoamer is methyl-silicone oil.
In the present invention, described dispersant is carboxylic acid esters dispersant.
In the present invention, described coalescents is ethylene glycol phenyl ether.
The preparation method of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings that the present invention separately proposes, concrete steps
As follows:
(1) raw material of this coating includes following components and weight portion: acrylic acid ester emulsion 35～50；Titanium dioxide 10～20；
Sericite 2～10；Aluminium oxide: 1～5；Tripolycyanamide: 1～10；APP: 2～15；Thickening agent 0.5～1；Defoamer 0.2
～0.5；Dispersant 0.2～1；Antifungus agent 0.2～1；Coalescents 1～2；Deionized water 20～30；
(2) by the deionized water weighed, dispersant, defoamer, antifungus agent with the rotating speed of 400～700 revs/min 15～
10～20min are stirred at 40 DEG C；
(3) titanium dioxide, sericite, APP, tripolycyanamide, aluminium oxide are weighed again, with 5000～6000 revs/min
Rotating speed stirs 40～60min at 15～40 DEG C；
(4) reducing rotating speed to 400～700 revs/min, interpolation acrylic acid ester emulsion, coalescents stir at 20～40 DEG C
Mix 20～30min, add thickening agent and be stirred 10～20min, i.e. obtain the mildew-proof flame retarded environmental protection of described timber buildings and be coated with
Material.
It is an advantage of the current invention that:
(1) the Product Green environmental protection of the present invention.The product of this invention is adopted and is used water as solvent, does not use organic solvent,
The raw material used is all environment-friendly type.Environment and human body will not be impacted.
(2) product of the present invention has good mildew-resistant, flame retardant effect, can be widely used for timber buildings interior wall, thus
A safe and healthy living environment is provided for people.
Detailed description of the invention
Embodiment 1
A kind of formula for the mildew-proof flame retarded environmental protection coating material of timber buildings is as follows:
| Acrylic acid ester emulsion | 40 |
| Glyoxaline compound | 0.5 |
| APP | 5 |
| Tripolycyanamide | 4 |
| Aluminium oxide | 2 |
| Titanium dioxide | 20 |
| Sericite | 5 |
| Hydroxyethyl cellulose | 0.5 |
| Methyl-silicone oil | 0.4 |
| Carboxylic acid esters dispersant | 0.4 |
| Ethylene glycol phenyl ether | 1.5 |
| Deionized water | 20.7 |
The preparation method of above-mentioned coating, it comprises the following steps that:
Be that 100kg carries out dispensing by gross weight, the rotating speed of high speed dispersor be adjusted to 400 revs/min, be sequentially added into water,
Carboxylic acid esters dispersant, methyl-silicone oil, glyoxaline compound, stir 20min at 15 DEG C；After agitated, then add titanium dioxide,
Sericite, APP, tripolycyanamide, aluminium oxide, and high speed dispersor rotating speed is adjusted to 6000 revs/min, stir at 15 DEG C
Mix 60min；Reduce rotating speed to 400 revs/min, add acrylic acid ester emulsion, ethylene glycol phenyl ether, at 30 DEG C, stir 20min, then
Add hydroxyethyl cellulose stirring 10min.
Embodiment 2
A kind of material formula for the mildew-proof flame retarded environmental protection coating material of timber buildings is as follows:
The preparation method of above-mentioned coating, it comprises the following steps that:
Be that 100kg carries out dispensing by gross weight, the rotating speed of high speed dispersor be adjusted to 600 revs/min, be sequentially added into water,
Carboxylic acid esters dispersant, methyl-silicone oil, glyoxaline compound, stir 20min at 30 DEG C；After agitated, then add titanium dioxide,
Sericite, APP, tripolycyanamide, aluminium oxide, and high speed dispersor rotating speed is adjusted to 5000 revs/min, stir at 30 DEG C
Mix 50min；Reduce rotating speed to 600 revs/min, add acrylic acid ester emulsion, ethylene glycol phenyl ether, at 40 DEG C, stir 30min, then
Add hydroxyethyl cellulose stirring 20min.
Embodiment 3
A kind of formula for the mildew-proof flame retarded environmental protection coating material of timber buildings is as follows:
The preparation method of above-mentioned coating, it comprises the following steps that:
Be that 100kg carries out dispensing by gross weight, the rotating speed of high speed dispersor be adjusted to 700 revs/min, be sequentially added into water,
Carboxylic acid esters dispersant, methyl-silicone oil, glyoxaline compound, stir 10min at 40 DEG C；After agitated, then add titanium dioxide,
Sericite, APP, tripolycyanamide, aluminium oxide, and high speed dispersor rotating speed is adjusted to 5000 revs/min, stir at 40 DEG C
Mix 40min；Reduce rotating speed to 700 revs/min, add acrylic acid ester emulsion, ethylene glycol phenyl ether, at 40 DEG C, stir 20min, then
Add hydroxyethyl cellulose stirring 20min.
Embodiment 4
A kind of formula for the mildew-proof flame retarded environmental protection coating material of timber buildings is as follows:
The preparation method of above-mentioned coating, it comprises the following steps that:
Be that 100kg carries out dispensing by gross weight, the rotating speed of high speed dispersor be adjusted to 700 revs/min, be sequentially added into water,
Carboxylic acid esters dispersant, methyl-silicone oil, glyoxaline compound, stir 20min at 15 DEG C；After agitated, then add titanium dioxide,
Sericite, APP, tripolycyanamide, aluminium oxide, and high speed dispersor rotating speed is adjusted to 6000 revs/min, stir at 15 DEG C
Mix 60min；Reduce rotating speed to 700 revs/min, add acrylic acid ester emulsion, ethylene glycol phenyl ether, at 20 DEG C, stir 20min, then
Add hydroxyethyl cellulose stirring 20min.
Embodiment 5
A kind of formula for the mildew-proof flame retarded environmental protection coating material of timber buildings is as follows:
| Acrylic acid ester emulsion | 50 |
| Glyoxaline compound | 1 |
| APP | 2 |
| Tripolycyanamide | 2.5 |
| Aluminium oxide | 5 |
| Titanium dioxide | 10 |
| Sericite | 5 |
| Hydroxyethyl cellulose | 1 |
| Methyl-silicone oil | 0.5 |
| Carboxylic acid esters dispersant | 1 |
| Ethylene glycol phenyl ether | 2 |
| Deionized water | 20 |
The preparation method of above-mentioned coating, it comprises the following steps that:
Be that 100kg carries out dispensing by gross weight, the rotating speed of high speed dispersor be adjusted to 600 revs/min, be sequentially added into water,
Carboxylic acid esters dispersant, methyl-silicone oil, glyoxaline compound, stir 15min at 20 DEG C；After agitated, then add titanium dioxide,
Sericite, APP, tripolycyanamide, aluminium oxide, and high speed dispersor rotating speed is adjusted to 5500 revs/min, stir at 20 DEG C
Mix 40min；Reduce rotating speed to 600 revs/min, add acrylic acid ester emulsion, ethylene glycol phenyl ether, at 30 DEG C, stir 20min, then
Add hydroxyethyl cellulose stirring 10min.
Embodiment 6
A kind of formula for the mildew-proof flame retarded environmental protection coating material of timber buildings is as follows:
| Acrylic acid ester emulsion | 35 |
| Glyoxaline compound | 1 |
| APP | 5 |
| Tripolycyanamide | 10 |
| Aluminium oxide | 2 |
| Titanium dioxide | 10 |
| Sericite | 10 |
| Hydroxyethyl cellulose | 1 |
| Methyl-silicone oil | 0.5 |
| Carboxylic acid esters dispersant | 0.5 |
| Ethylene glycol phenyl ether | 1 |
| Deionized water | 24 |
The preparation method of above-mentioned coating, it comprises the following steps that:
Be that 100kg carries out dispensing by gross weight, the rotating speed of high speed dispersor be adjusted to 500 revs/min, be sequentially added into water,
Carboxylic acid esters dispersant, methyl-silicone oil, glyoxaline compound, stir 20min at 25 DEG C；After agitated, then add titanium dioxide,
Sericite, APP, tripolycyanamide, aluminium oxide, and high speed dispersor rotating speed is adjusted to 6000 revs/min, stir at 25 DEG C
Mix 50min；Reduce rotating speed to 500 revs/min, add acrylic acid ester emulsion, ethylene glycol phenyl ether, at 35 DEG C, stir 30min, then
Add hydroxyethyl cellulose stirring 10min.
Claims (8)
1. the formula for the mildew-proof flame retarded environmental protection coating material of timber buildings, it is characterised in that this kind is built for timber structure
The formula of the mildew-proof flame retarded environmental protection coating material built is calculated as with mass fraction:
The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings the most according to claim 1, its feature exists
In: antifungus agent is glyoxaline compound.
The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings the most according to claim 1, its feature exists
In: fire retardant is that APP, tripolycyanamide and aluminium oxide constitute halogen-free flame-retardant system.
The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings the most according to claim 1, its feature exists
In: thickening agent is hydroxyethyl cellulose.
The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings the most according to claim 1, its feature exists
In: defoamer is methyl-silicone oil.
The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings the most according to claim 1, its feature exists
In: dispersant is carboxylic acid esters dispersant.
The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings the most according to claim 1, its feature exists
In: coalescents is ethylene glycol phenyl ether.
The preparation method of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings the most according to claim 1, it is special
Levy and be: specifically comprise the following steps that
(1) each raw material is weighed according to the parts by weight required by right 1；
(2) deionized water that step (1) weighed, dispersant, defoamer, antifungus agent exist with the rotating speed of 400～700 revs/min
10～20min are stirred at 15～40 DEG C；
(3) APP that weighs according still further to step (1), tripolycyanamide, aluminium oxide, titanium dioxide, sericite, with 5000～6000
Rev/min rotating speed at 15～40 DEG C, stir 40～60min；
(4) reduce rotating speed to 400～700 revs/min, add acrylic acid ester emulsion that step (1) weighs, coalescents 20～
Stir 20～30min at 40 DEG C, add the thickening agent that step (1) weighs and be stirred 10～20min, i.e. obtain described wood knot
The mildew-proof flame retarded environmental protection coating material of structure.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610458641.0A CN106118313A (en) | 2016-06-22 | 2016-06-22 | The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610458641.0A CN106118313A (en) | 2016-06-22 | 2016-06-22 | The formula of a kind of mildew-proof flame retarded environmental protection coating material for timber buildings and preparation method |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106810976A (en) * | 2017-01-24 | 2017-06-09 | 安徽华晟涂料有限公司 | A kind of water proof fire retardant water paint |
| CN106833197A (en) * | 2017-01-24 | 2017-06-13 | 安徽华晟涂料有限公司 | A kind of water paint with water proofing property |
| CN107312403A (en) * | 2017-08-11 | 2017-11-03 | 苏州金螳螂园林绿化景观有限公司 | Historic building structure anti-corrosion moisture-proof coating |
| CN109054539A (en) * | 2018-07-26 | 2018-12-21 | 合肥欧仕嘉机电设备有限公司 | A kind of mildew-proof flame retarded coating and preparation method thereof for timber buildings |
| CN112831235A (en) * | 2021-01-06 | 2021-05-25 | 浙江海悦绿建科技有限公司 | Wood structure flame-retardant coating and preparation method thereof |
| CN116515357A (en) * | 2023-02-06 | 2023-08-01 | 广州大学 | Preparation method of amphiphobic flame-retardant coating for wood surface |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1824716A (en) * | 2005-12-22 | 2006-08-30 | 北京首创纳米科技有限公司 | Aqueous environmental protection ultration expansion type steel structure fireproof paint and its preparation method |
| CN101671523A (en) * | 2009-10-01 | 2010-03-17 | 厦门大学 | Aqueous flame-retardant and thermal-insulated coating and preparation method thereof |
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2016
- 2016-06-22 CN CN201610458641.0A patent/CN106118313A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1824716A (en) * | 2005-12-22 | 2006-08-30 | 北京首创纳米科技有限公司 | Aqueous environmental protection ultration expansion type steel structure fireproof paint and its preparation method |
| CN101671523A (en) * | 2009-10-01 | 2010-03-17 | 厦门大学 | Aqueous flame-retardant and thermal-insulated coating and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106810976A (en) * | 2017-01-24 | 2017-06-09 | 安徽华晟涂料有限公司 | A kind of water proof fire retardant water paint |
| CN106833197A (en) * | 2017-01-24 | 2017-06-13 | 安徽华晟涂料有限公司 | A kind of water paint with water proofing property |
| CN107312403A (en) * | 2017-08-11 | 2017-11-03 | 苏州金螳螂园林绿化景观有限公司 | Historic building structure anti-corrosion moisture-proof coating |
| CN109054539A (en) * | 2018-07-26 | 2018-12-21 | 合肥欧仕嘉机电设备有限公司 | A kind of mildew-proof flame retarded coating and preparation method thereof for timber buildings |
| CN112831235A (en) * | 2021-01-06 | 2021-05-25 | 浙江海悦绿建科技有限公司 | Wood structure flame-retardant coating and preparation method thereof |
| CN116515357A (en) * | 2023-02-06 | 2023-08-01 | 广州大学 | Preparation method of amphiphobic flame-retardant coating for wood surface |
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Application publication date: 20161116 |