CN106118239A - A kind of preparation method of Novel black color ink juice - Google Patents
A kind of preparation method of Novel black color ink juice Download PDFInfo
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- CN106118239A CN106118239A CN201610044672.1A CN201610044672A CN106118239A CN 106118239 A CN106118239 A CN 106118239A CN 201610044672 A CN201610044672 A CN 201610044672A CN 106118239 A CN106118239 A CN 106118239A
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- China
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- prepared chinese
- black color
- chinese ink
- juice
- melanin
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
- C09D11/17—Writing inks characterised by colouring agents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention provides a kind of novel black prepared Chinese ink and preparation method thereof.This prepared Chinese ink mainly includes following dispensing: coloring agent, thickening agent, penetrating agent, preservative, aromatic and water.The coloring agent that the present invention uses is hair melanin, derives from the garbage produced during hair acid hydrolysis produces cystine, and through grinding with supper fine refined grinding machine, crosses the sieve of 2000 mesh, obtain melanin powder.Comparing common prepared Chinese ink, prepared Chinese ink firm coloration degree and writing light brightness that the inventive method prepares are improved, and too increase the stability of prepared Chinese ink simultaneously, originate with the melanin in garbage for coloring agent, it is achieved that the comprehensive utilization of refuse.
Description
(1) technical field
The present invention relates to the preparation method of a kind of Novel black color ink juice.
(2) background technology
Prepared Chinese ink is the Writing-painting articles for use that China is traditional, has long history.The quality of prepared Chinese ink is most important for painting and calligraphy.Mesh
The prepared Chinese ink used on front domestic market is made up of the raw material such as white carbon black cigarette, animal glue and anticorrosive additive mostly.Existing prepared Chinese ink also exists
Many shortcomings: brightness of painting on conventional writing paper or rice paper and fixing degree are inadequate；The prepared Chinese ink shelf-life is short, and time length there will be
Precipitation；The perishable phenomenon such as smelly.The invention discloses a kind of method utilizing discarded hair melanin to manufacture prepared Chinese ink, solve existing
Deficiency with the presence of prepared Chinese ink.At present utilization melanic in hair being also in the research and discovery stage, relevant report is less.
The manufacture that melanin is applied to prepared Chinese ink has no any report.
Melanin is insoluble in the amorphous little granule of water, is a kind of natural black pigment, is widely present in the hair of people and higher mammal
In Faing.Melanin in the present invention obtains from the garbage of commercial production cystine.Preparation method is with hair as raw material, logical
Cross acid hydrolysis to extract.Detailed process is, takes the hair 500g cleaning and drying and adds 30% (percentage by weight) concentrated hydrochloric acid 1000ml,
With the reflux of absorbing hydrogen chloride, under the conditions of 110～112 DEG C, it is heated to reflux 4 hours, obtains after cold filtration containing black
The filtering residue of pigment.Melanin is placed on porcelain hole funnel and uses water cyclic washing, during until filtrate pH value is 6, then with added with few
Amount ammonia scrubbing, filter, dry [Zhang Shayan, Hu Chunxia, melanic extraction and utilize [J] in hair. Liaoning Journal of Teachers College,
2003,5 (3): 95-96], obtain melanin crude product, dry.
(3) summary of the invention
Take dry melanin crude product, grind with supper fine refined grinding machine, cross the sieve of 2000 mesh, obtain melanin powder.Then with black
Pigment powder is that coloring agent configures Novel ink.The mass percent dispensing of Novel ink: coloring agent 15～20%, thickening agent 12
～18%, penetrating agent 2～4%, preservative 1～3%, aromatic 2～3%, surplus is water.
Novel black color ink juice preparation method, including step in detail below: 1. endure glue: add part water and thickening agent in a reservoir,
Heat and stir and be completely dissolved to it, infusion in boiling water bath, make glue；2. spice: glue is put in dasher,
Stir into ink cream with coloring agent, add penetrating agent and stir；3. grind: ink cream is put into grinder and grinds uniformly, with
Increasing the stability of prepared Chinese ink, grind the thinnest, the brightness of prepared Chinese ink and color and luster are the best；4. blending: be sequentially added into aromatic and prevent
Rotten agent, supplies 50 DEG C of hot water, stirs into juice and crosses the copper yarn gong sieve of 60 mesh；After cooling qualified through quality inspection, get final product filling bottle
Vanning.
The present invention using melanin powder as the coloring agent of prepared Chinese ink be a new invention.The prepared Chinese ink made by the inventive method is permissible
Solve the deficiency that existing prepared Chinese ink exists.Use this prepared Chinese ink writing light brightness and adhesion-tight degree to improve, too increase prepared Chinese ink simultaneously
Stability.Add plant gum and preservative, make prepared Chinese ink store for a long time be stale-proof the most smelly.Melanin powder is from discarding that cystine produces
Thing extracts, improves raw-material value, it is achieved that the comprehensive utilization of refuse.
(4) detailed description of the invention
Take the melanin crude product that 100g is dried, grind with supper fine refined grinding machine, cross the sieve of 2000 mesh, obtain the ultra-fine melanin of 95g
Powder, is applied in the following examples.
Being described in further detail the present invention below by specific embodiment, in the present embodiment, reagent is often if no special instructions
Rule commercial reagent or the reagent prepared according to a conventional method.
Embodiment 1
The dispensing of this prepared Chinese ink is: melanin powder 15.0g, thickening agent Resina persicae 12.0g, penetrating agent ethylene glycol 2.0g, preservative Camphora 1.0g,
Aromatic Flos Caryophylli 2.0g, supplies total amount 100g with water.
The preparation method of the present embodiment prepared Chinese ink is as follows:
1. glue is endured: adding 12.0g deionized water in water-bath, under agitation addition 12.0g Resina persicae is in pot, heats and stirs extremely
It is completely dissolved, and in boiling water bath, infusion becomes glue；2. spice: put into by glue in dasher, adds melanin powder
15.0g, adds 50 DEG C of water 30.0g, stirs into ink cream, adds 7 glycol 2.0g and stir；3. grind: ink cream is put
Levigate in entering grinder roll even 20 minutes, to increase the stability of prepared Chinese ink；4. blending: be sequentially added into the 2.0g fourth of hot water dissolving
Fragrant and 1.0g Camphora, supplies total amount as 100g with the water of 50 DEG C, stirs into juice and crosses the copper yarn gong of 60 mesh and sieve.Through inspection after cooling
Test up-to-standard, can filling bottle vanning.
Embodiment 2
The dispensing of this prepared Chinese ink is: melanin powder 16.2g, sizing material arabic gum 13.2g, penetrating agent glycerol 2.4g, preservative Borneolum Syntheticum 1.4g,
Aromatic Lignum Santali Albi 2.3g, supplies total amount 100g with water.
The preparation method of the present embodiment prepared Chinese ink is as follows:
1. glue is endured: adding 15.0g deionized water in water-bath, under agitation addition 13.2g arabic gum is in pot, heats and stirs
Being completely dissolved to it, in boiling water bath, infusion becomes glue；2. spice: put into by glue in dasher, adds melanin powder
End 16.2g, adds 50 DEG C of water 33.0g, stirs into ink cream, adds 2.4g glycerol and stir；3. grind: ink cream is put
Levigate in entering grinder roll even 30 minutes, to increase the stability of prepared Chinese ink；4. blending: be sequentially added into the 2.3g wingceltis of hot water dissolving
Fragrant and 1.4g Borneolum Syntheticum, supplies total amount as 100g with the water of 50 DEG C, stirs into juice and crosses the copper yarn gong of 60 mesh and sieve.Through inspection after cooling
Test up-to-standard, can filling bottle vanning.
Embodiment 3
The dispensing of this prepared Chinese ink is: melanin powder 17.6g, sizing material guar gum 14.8g, penetrating agent isobutanol 2.8g, preservative sorbic acid
1.8g, aromatic Herba Pogostemonis 2.5g, supply total amount 100g with water.
The preparation method of the present embodiment prepared Chinese ink is as follows:
1. glue is endured: adding 18.0g deionized water in water-bath, under agitation addition guar gum 14.8g is in pot, heats and stirs extremely
It is completely dissolved, and in boiling water bath, infusion becomes glue；2. spice: put into by glue in dasher, adds melanin powder
17.6g, adds 50 DEG C of water 36.0g, stirs into ink cream, adds isobutanol 2.8g and stir；3. grind: ink cream is put
Levigate in entering grinder roll even 40 minutes, to increase the stability of prepared Chinese ink；4. blending: be sequentially added into the 2.5g leaves of pulse plants of hot water dissolving
Fragrant and 1.8g sorbic acid, supplies total amount as 100g with the water of 50 DEG C, stirs into juice and crosses the copper yarn gong of 60 mesh and sieve.Warp after cooling
Quality inspection is qualified, can filling bottle vanning.
Embodiment 4
The dispensing of this prepared Chinese ink is: melanin powder 18.9g, sizing material arabic gum 16.6g, 3.4g penetrating agent tween 80, preservative Pyrusussuriensis
Acid potassium 2.4g, aromatic Flos Caryophylli 2.7g, supply total amount 100g with water.
The preparation method of the present embodiment prepared Chinese ink is as follows:
1. glue is endured: adding 21.0g deionized water in water-bath, under agitation addition 16.6g arabic gum is in pot, heats and stirs
Being completely dissolved to it, in boiling water bath, infusion becomes glue；2. spice: put into by glue in dasher, adds melanin powder
End 18.9g, adds 50 DEG C of water 39.0g, stirs into ink cream, adds 3.4g tween 80 and stir；3. grind: by ink
Cream puts into that grinder is levigate to be rolled even 50 minutes, to increase the stability of prepared Chinese ink；4. blending: be sequentially added into the 2.7g of hot water dissolving
Flos Caryophylli and 2.4g potassium sorbate, supply total amount as 100g with the water of 50 DEG C, stirs into juice and crosses the copper yarn gong sieve of 60 mesh.Cooling
Qualified by quality inspection, can filling bottle vanning.
Embodiment 5
The dispensing of this prepared Chinese ink is: melanin powder 20.0g, sizing material guar gum 18.0g, penetrating agent sodium cetanesulfonate 4.0g, anticorrosion
Agent sodium benzoate 3.0g, aromatic Lignum Santali Albi 3.0g, supply total amount 100g with water.
The preparation method of the present embodiment prepared Chinese ink is as follows:
1. glue is endured: adding 21.0g water in water-bath, under agitation addition guar gum 18.0g is in pot, heats and stirs to it complete
Dissolving, in boiling water bath, infusion becomes glue；2. spice: put into by glue in dasher, adds melanin powder 20.0g,
Add 50 DEG C of water 42.0g, stir into ink cream, add sodium cetanesulfonate 4.0g and stir；3. grind: by ink cream
Put into that grinder is levigate to be rolled even 60 minutes, to increase the stability of prepared Chinese ink；4. blending: be sequentially added into hot water dissolving Herba Pogostemonis and
The each 3.0g of sodium benzoate, supplies total amount as 100g with the water of 50 DEG C, stirs into juice and crosses the copper yarn gong sieve of 60 mesh.Warp after cooling
Quality inspection is qualified, can filling bottle vanning.
Product of the present invention presses People's Republic of China's light industry standard QB/T2860-2007, detects physical and chemical index,
All can reach middle and high level product requirement.Test key data contrast is as follows:
The present invention is to be applied on prepared Chinese ink as coloring agent by melanin powder first.The prepared Chinese ink processing technology made in this way is simple,
Not precipitating, write smoothly, can arbitrarily allocate, painting and calligraphy suitable for four seasons, preferably book are preferably mounted, and can meet different levels painting and calligraphy fan and practice
Practise calligraphy, the demand of drawing.
Claims (8)
1. a Novel black color ink juice, it is characterised in that: include the dispensing of following mass percent, coloring agent 15～
20%, thickening agent 12～18%, penetrating agent 2～4%, preservative 1～3%, aromatic 2～3%, surplus
For water.
Novel black color ink juice the most according to claim 1, it is characterised in that: coloring agent source is, from hair
The melanin garbage that acid hydrolysis produces during producing cystine.
Novel black color ink juice the most according to claim 1, it is characterised in that: take dry melanin crude product,
Grind with supper fine refined grinding machine, cross the sieve of 2000 mesh, obtain melanin powder, then with melanin powder be
Toner configuration Novel ink.
Novel black color ink juice the most according to claim 1, it is characterised in that: thickening agent is Resina persicae, Arab
One in glue and guar gum.
Novel black color ink juice the most according to claim 1, it is characterised in that: penetrating agent be ethylene glycol, glycerol,
One in isobutanol, tween 80 or sodium cetanesulfonate.
Novel black color ink juice the most according to claim 1, it is characterised in that: preservative be Camphora, Borneolum Syntheticum,
One in sorbic acid, potassium sorbate or sodium benzoate.
Novel black color ink juice the most according to claim 1, it is characterised in that: aromatic be Flos Caryophylli, Lignum Santali Albi or
One in Herba Pogostemonis.
8. the preparation method of the Novel black color ink juice described in claim 1-7, it is characterised in that comprise the following steps:
1. endure glue: add part water and thickening agent in a reservoir, heat and stir and be completely dissolved to it, at boiling water bath
Glue is made in middle infusion；2. spice: put into by glue in dasher, stirs into ink cream with coloring agent, then
Add penetrating agent to stir；3. grind: ink cream is put into grinder and grinds even, to increase stablizing of prepared Chinese ink
Property, grind the thinnest, the brightness of prepared Chinese ink and color and luster are the best；4. blending: be sequentially added into aromatic and anticorrosion
Agent, supplies 50 DEG C of hot water, stirs into juice and crosses the copper yarn gong sieve of 60 mesh, qualified through quality inspection after cooling,
Can filling bottle vanning.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610044672.1A CN106118239A (en) | 2016-01-19 | 2016-01-19 | A kind of preparation method of Novel black color ink juice |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610044672.1A CN106118239A (en) | 2016-01-19 | 2016-01-19 | A kind of preparation method of Novel black color ink juice |
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| Publication Number | Publication Date |
|---|---|
| CN106118239A true CN106118239A (en) | 2016-11-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201610044672.1A Pending CN106118239A (en) | 2016-01-19 | 2016-01-19 | A kind of preparation method of Novel black color ink juice |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883677A (en) * | 2017-03-01 | 2017-06-23 | 黄太海 | A kind of use natural plant gum substitutes the method that animal glue prepares prepared Chinese ink |
| CN108707367A (en) * | 2017-04-06 | 2018-10-26 | 上海大学 | A kind of prepared Chinese ink and preparation method thereof |
| CN110437673A (en) * | 2018-12-29 | 2019-11-12 | 江西滕王阁笔墨有限公司 | A kind of preparation method of writing brush ink |
| CN112226109A (en) * | 2020-11-05 | 2021-01-15 | 山西大学 | Plant calligraphy ink and preparation method thereof |
| WO2021235292A1 (en) * | 2020-05-18 | 2021-11-25 | 三菱鉛筆株式会社 | Ink composition for water-based ballpoint pen |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
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2016
- 2016-01-19 CN CN201610044672.1A patent/CN106118239A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 张沙艳等: "毛发中黑色素的提取和利用", 《辽宁师专学报》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883677A (en) * | 2017-03-01 | 2017-06-23 | 黄太海 | A kind of use natural plant gum substitutes the method that animal glue prepares prepared Chinese ink |
| CN108707367A (en) * | 2017-04-06 | 2018-10-26 | 上海大学 | A kind of prepared Chinese ink and preparation method thereof |
| CN110437673A (en) * | 2018-12-29 | 2019-11-12 | 江西滕王阁笔墨有限公司 | A kind of preparation method of writing brush ink |
| WO2021235292A1 (en) * | 2020-05-18 | 2021-11-25 | 三菱鉛筆株式会社 | Ink composition for water-based ballpoint pen |
| CN112226109A (en) * | 2020-11-05 | 2021-01-15 | 山西大学 | Plant calligraphy ink and preparation method thereof |
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20161116 |