CN106116505A - A kind of preparation method of seepage brick - Google Patents
A kind of preparation method of seepage brick Download PDFInfo
- Publication number
- CN106116505A CN106116505A CN201610484572.0A CN201610484572A CN106116505A CN 106116505 A CN106116505 A CN 106116505A CN 201610484572 A CN201610484572 A CN 201610484572A CN 106116505 A CN106116505 A CN 106116505A
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- Prior art keywords
- brick
- wood powder
- prepared
- mass ratio
- mould
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/1321—Waste slurries, e.g. harbour sludge, industrial muds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/06—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The present invention relates to the preparation method of a kind of seepage brick, belong to construction material preparing technical field.Discarded building flitch is mainly carried out basification by the present invention, obtain alkali and process wood powder, after itself and dry gelatinized starch are stirred mixing and ball milling, mix with poly-vinyl alcohol solution stirring, carry out fermentation process, it is placed in mould being dried, obtain the wood powder starch backbone that ferments, be then placed in brick mould, and its top layer is poured the mixture of mud and the water processed, carry out standing solidification, i.e. can get seepage brick.Seepage brick intensity prepared by the present invention is high, and intensity is up to 60～95MPa, not easy fracture；And water permeability is good, infiltration coefficient reaches 3.56 × 10‑2More than cm/s.
Description
Technical field
The present invention relates to the preparation method of a kind of seepage brick, belong to construction material preparing technical field.
Background technology
Seepage brick, is also water-permeable brick, Dutch brick, and the many employings of its raw material environment-friendly materials such as brick powder, slag, flyash that give up are
Primary low shapes, and its wearability is good, has good water penetration and water-retaining property, and antiskid function is strong, and it is not only with hard surface one
Sample can be beautified the environment, and has more preferable environment utilitarian function.When raining, rainwater can be penetrated into brick by seepage brick automatically
Beneath until earth's surface, recovery as far as possible, become subsoil water；When becoming a fine day, penetrate under brick or be retained in the water inside brick and can evaporate
In air, adjusting air humidity, reduces atmospheric temperature.
Traditional method uses bulky grain skeleton and cement composition or uses artificial treatment sand and high polymer binder to form.Water
Mud water-permeable brick or permeability rate is the highest, otherwise water permeability is permissible, but comprcssive strength is the highest, and this two aspects performance difficulty is taken into account；With
High polymer binder, artificial treatment sand water-permeable brick cost are high, it is impossible to promote on a large scale.And with flyash as primary raw material, preparation
Going out intensity is 30～90MPa, and porosity is the seepage brick of 40～50%.Although improve its intensity and increasing to a certain extent
Its porosity big, the problem solving grain composition, but this seepage brick porosity is high, intensity is low, infiltration coefficient is big, water conservation
Coefficient is little.
Summary of the invention
The technical problem to be solved: can not simultaneously hold concurrently for the seepage brick made with cement or bulky grain skeleton
Turning round and look at water permeability and comprcssive strength so that it is the problem that cannot promote on a large scale, discarded building flitch is mainly entered by the present invention
Row basification, obtains alkali and processes wood powder, after itself and dry gelatinized starch are stirred mixing and ball milling, with poly-vinyl alcohol solution
Stirring mixing, carries out fermentation process, is placed in mould being dried, and obtains the wood powder starch backbone that ferments, is then placed on
In brick mould, and its top layer is poured the mixture of mud and the water processed, carry out standing solidification, i.e. can be seeped water
Brick.The present invention is by by wood powder and starch blending and fermentation process, by microorganism to starch and the difference of wood powder corrosion rate,
Make wood powder remaining form micro hole structure, subsequently as skeleton, serosity is injected into skeletal internal, subsequently high temperature carbonization wood
Powder, after taking out carbon dust with oxygen reaction, can prepare simultaneously, and seepage brick intensity prepared by the present invention is high, and water permeability is good,
Can promote the use of on a large scale.
For solving above-mentioned technical problem, the technical solution used in the present invention is:
(1) choose discarded building flitch, cleaned and naturally dry, subsequently comminution by gas stream sieving, prepare 65～70 mesh wooden
Powder, the most in mass ratio 1:3, mix wood powder with the stirring of mass concentration 20% sodium hydroxide solution, then water-bath at 65～80 DEG C
Heating 1～2h, filters subsequently and collects filter cake, is dried 6～8h at 130～150 DEG C, is prepared into alkali and processes wood powder；
(2) 1:5 in mass ratio, mixes corn starch with deionized water stirring and is placed in beaker, water-bath at 70～85 DEG C
Heating 25～30min, after its gelatinizing completes, continues Heat preservation rotary evaporated to dryness, collects and is dried gelatinized starch, subsequently
1:5 in mass ratio, processes wood powder by the alkali of dry gelatinized starch with above-mentioned preparation and is placed in ball grinder, 250～300r/min
Lower ball milling 1～2h, is prepared into ball milling mixed-powder；
(3) 1:5 in mass ratio, mixes the stirring of mass concentration 10% poly-vinyl alcohol solution and ball milling mixed-powder, 200～
After under 300W, sonic oscillation processes 10～15min, being placed in mould, under 5～10MPa after compacting, then sealing and fermenting processes 15
～20 days, after fermentation to be sealed completes, mould is placed at 85～100 DEG C and is dried 10～12h, be prepared into fermentation wood powder starch bone
Frame, standby；
(4) 1:10 in mass ratio, mixes the stirring of pond sludge and deionized water, under 200～300W ultrasonic disperse 20～
After 30min, sieve with the screen cloth of 60～80 mesh, collect lower floor mud and be placed at 95～100 DEG C being dried 6～8h, subsequently
Dry lower floor mud is placed in ball grinder, sieves after ball milling 3～5h under 650～700r/min, be prepared into 100～120 mesh
Mud granule；
(5) fermentation wood powder starch backbone prepared by step (3) is placed in rustless steel brick mould, 1:2 the most in mass ratio, will
Deionized water mixes with mud granule stirring and pours to fermentation wood powder starch backbone top layer, treats uniformly to be paved with rustless steel brick mould
After tool, more at room temperature standing solidification 20～24h, the demoulding subsequently is placed at 1000～1050 DEG C being fired into brick, natural cooling
A kind of seepage brick can be prepared into room temperature.
The seepage brick porosity prepared by the present invention reaches more than 75.6%, and intensity is up to 60～95MPa, and infiltration coefficient reaches
3.56×10-2More than cm/s, 25 freeze-thaw cycle, comprcssive strength loss rate≤16%, water-retaining property is more than 0.7g/cm3。
The present invention is compared with additive method, and Advantageous Effects is:
(1) the seepage brick intensity that prepared by the present invention is high, and intensity is up to 60～95MPa, not easy fracture；
(2) the seepage brick water permeability that prepared by the present invention is good, and infiltration coefficient reaches 3.56 × 10-2More than cm/s；
(3) present invention is raw material mainly by discarded building flitch, and preparation process is simple, required low cost.
Detailed description of the invention
First choose discarded building flitch, cleaned and naturally dry, subsequently comminution by gas stream sieving, preparation 65～70
Mesh wood powder, the most in mass ratio 1:3, mix wood powder with the stirring of mass concentration 20% sodium hydroxide solution, then at 65～80 DEG C
Heating in water bath 1～2h, filters subsequently and collects filter cake, is dried 6～8h at 130～150 DEG C, is prepared into alkali and processes wood powder；Again
1:5 in mass ratio, mixes the stirring of corn starch and deionized water and is placed in beaker, at 70～85 DEG C heating in water bath 25～
30min, after its gelatinizing completes, continues Heat preservation rotary evaporated to dryness, collects and is dried gelatinized starch, the most in mass ratio
1:5, processes wood powder by the alkali of dry gelatinized starch and above-mentioned preparation and is placed in ball grinder, under 250～300r/min ball milling 1～
2h, is prepared into ball milling mixed-powder；1:5 the most in mass ratio, by mass concentration 10% poly-vinyl alcohol solution and ball milling mixed-powder
Stirring mixing, after under 200～300W, sonic oscillation processes 10～15min, is placed in mould, under 5～10MPa after compacting,
Sealing and fermenting processes 15～20 days again, after fermentation to be sealed completes, is placed in by mould at 85～100 DEG C and is dried 10～12h, preparation
Must be fermented wood powder starch backbone, standby；1:10 the most in mass ratio, mixes the stirring of pond sludge and deionized water, 200～
Under 300W after ultrasonic disperse 20～30min, sieve with the screen cloth of 60～80 mesh, collect lower floor's mud and be placed in 95～100
It is dried 6～8h at DEG C, subsequently dry lower floor mud is placed in ball grinder, mistake after ball milling 3～5h under 650～700r/min
Sieve, is prepared into 100～120 mesh mud granules；Finally the fermentation wood powder starch backbone of preparation is placed in rustless steel brick mould,
1:2 the most in mass ratio, mixes deionized water with mud granule stirring and pours to fermentation wood powder starch backbone top layer, treating all
Even be paved with rustless steel brick mould after, more at room temperature stand solidification 20～24h, the demoulding subsequently is placed at 1000～1050 DEG C
It is fired into brick, naturally cools to room temperature and can be prepared into a kind of seepage brick.
Example 1
First choose discarded building flitch, cleaned and naturally dry, subsequently comminution by gas stream sieving, prepare 70 mesh wood powders,
1:3 the most in mass ratio, mixes wood powder with the stirring of mass concentration 20% sodium hydroxide solution, then heating in water bath 2h at 80 DEG C,
Filter subsequently and collect filter cake, at 150 DEG C, being dried 8h, being prepared into alkali and process wood powder；1:5 the most in mass ratio, by corn starch
Mix with deionized water stirring and be placed in beaker, heating in water bath 30min at 85 DEG C, after its gelatinizing completes, continues insulation
Heating rotary evaporated to dryness, collect and be dried gelatinized starch, the most in mass ratio 1:5, by dry gelatinized starch and above-mentioned preparation
Alkali process wood powder be placed in ball grinder, ball milling 2h under 300r/min, be prepared into ball milling mixed-powder；The most in mass ratio 1:
5, mass concentration 10% poly-vinyl alcohol solution is mixed with the stirring of ball milling mixed-powder, under 300W, sonic oscillation processes 15min
After, it is placed in mould, under 10MPa after compacting, then sealing and fermenting processes 20 days, after fermentation to be sealed completes, is placed in by mould
It is dried 12h at 100 DEG C, is prepared into fermentation wood powder starch backbone, standby；1:10 the most in mass ratio, by pond sludge and deionization
Water stirring mixing, under 300W after ultrasonic disperse 30min, sieves with the screen cloth of 80 mesh, collects lower floor's mud and is placed in 100
It is dried 8h at DEG C, subsequently dry lower floor mud is placed in ball grinder, sieves after ball milling 5h under 700r/min, be prepared into 120
Mesh mud granule；Finally the fermentation wood powder starch backbone of preparation is placed in rustless steel brick mould, 1:2 the most in mass ratio,
Deionized water mixed with mud granule stirring and pours to fermentation wood powder starch backbone top layer, treating uniformly to be paved with rustless steel brick
After mould, more at room temperature standing solidification 24h, the demoulding subsequently is placed at 1050 DEG C being fired into brick, naturally cools to room temperature i.e.
A kind of seepage brick can be prepared into.After testing, seepage brick intensity prepared by the present invention is high, intensity up to 70MPa, not easy fracture；Ooze
Water brick water permeability is good, and infiltration coefficient reaches 3.78 × 10-2cm/s。
Example 2
First choose discarded building flitch, cleaned and naturally dry, subsequently comminution by gas stream sieving, prepare 65 mesh wood powders,
1:3 the most in mass ratio, mixes wood powder with the stirring of mass concentration 20% sodium hydroxide solution, then heating in water bath 1h at 65 DEG C,
Filter subsequently and collect filter cake, at 130 DEG C, being dried 6h, being prepared into alkali and process wood powder；1:5 the most in mass ratio, by corn starch
Mix with deionized water stirring and be placed in beaker, heating in water bath 25min at 70 DEG C, after its gelatinizing completes, continues insulation
Heating rotary evaporated to dryness, collect and be dried gelatinized starch, the most in mass ratio 1:5, by dry gelatinized starch and above-mentioned preparation
Alkali process wood powder be placed in ball grinder, ball milling 1h under 250r/min, be prepared into ball milling mixed-powder；The most in mass ratio 1:
5, mass concentration 10% poly-vinyl alcohol solution is mixed with the stirring of ball milling mixed-powder, under 200W, sonic oscillation processes 10min
After, it is placed in mould, under 5MPa after compacting, then sealing and fermenting processes 15 days, after fermentation to be sealed completes, mould is placed in 85
It is dried 10h at DEG C, is prepared into fermentation wood powder starch backbone, standby；1:10 the most in mass ratio, stirs pond sludge with deionized water
Mix mixing, under 300W after ultrasonic disperse 30min, sieve with the screen cloth of 60 mesh, collect lower floor's mud and be placed at 100 DEG C
It is dried 8h, subsequently dry lower floor mud is placed in ball grinder, sieves after ball milling 3h under 650r/min, be prepared into 100 mesh dirty
Mud granule；Finally the fermentation wood powder starch backbone of preparation is placed in rustless steel brick mould, 1:2 the most in mass ratio, will go
Ionized water mixes with mud granule stirring and pours to fermentation wood powder starch backbone top layer, treats uniformly to be paved with rustless steel brick mould
After, more at room temperature standing solidification 24h, the demoulding subsequently is placed at 1000 DEG C being fired into brick, and naturally cooling to room temperature can make
For obtaining a kind of seepage brick.After testing, seepage brick intensity prepared by the present invention is high, intensity up to 60MPa, not easy fracture；Seepage brick
Water permeability is good, and infiltration coefficient reaches 3.95 × 10-2cm/s。
Example 3
First choose discarded building flitch, cleaned and naturally dry, subsequently comminution by gas stream sieving, prepare 67 mesh wood powders,
1:3 the most in mass ratio, mixes wood powder with the stirring of mass concentration 20% sodium hydroxide solution, then heating in water bath 1h at 70 DEG C,
Filter subsequently and collect filter cake, at 140 DEG C, being dried 7h, being prepared into alkali and process wood powder；1:5 the most in mass ratio, by corn starch
Mix with deionized water stirring and be placed in beaker, heating in water bath 27min at 82 DEG C, after its gelatinizing completes, continues insulation
Heating rotary evaporated to dryness, collect and be dried gelatinized starch, the most in mass ratio 1:5, by dry gelatinized starch and above-mentioned preparation
Alkali process wood powder be placed in ball grinder, ball milling 2h under 270r/min, be prepared into ball milling mixed-powder；The most in mass ratio 1:
5, mass concentration 10% poly-vinyl alcohol solution is mixed with the stirring of ball milling mixed-powder, under 250W, sonic oscillation processes 12min
After, it is placed in mould, under 7MPa after compacting, then sealing and fermenting processes 17 days, after fermentation to be sealed completes, mould is placed in 90
It is dried 11h at DEG C, is prepared into fermentation wood powder starch backbone, standby；1:10 the most in mass ratio, stirs pond sludge with deionized water
Mix mixing, under 250W after ultrasonic disperse 25min, sieve with the screen cloth of 70 mesh, collect lower floor's mud and be placed at 97 DEG C
It is dried 7h, subsequently dry lower floor mud is placed in ball grinder, sieves after ball milling 4h under 670r/min, be prepared into 110 mesh dirty
Mud granule；Finally the fermentation wood powder starch backbone of preparation is placed in rustless steel brick mould, 1:2 the most in mass ratio, will go
Ionized water mixes with mud granule stirring and pours to fermentation wood powder starch backbone top layer, treats uniformly to be paved with rustless steel brick mould
After, more at room temperature standing solidification 22h, the demoulding subsequently is placed at 1055 DEG C being fired into brick, and naturally cooling to room temperature can make
For obtaining a kind of seepage brick.After testing, seepage brick intensity prepared by the present invention is high, intensity up to 65MPa, not easy fracture；Seepage brick
Water permeability is good, and infiltration coefficient reaches 4.02 × 10-2cm/s。
Claims (1)
1. the preparation method of a seepage brick, it is characterised in that concrete preparation process is:
(1) choose discarded building flitch, cleaned and naturally dry, subsequently comminution by gas stream sieving, prepare 65～70 mesh wooden
Powder, the most in mass ratio 1:3, mix wood powder with the stirring of mass concentration 20% sodium hydroxide solution, then water-bath at 65～80 DEG C
Heating 1～2h, filters subsequently and collects filter cake, is dried 6～8h at 130～150 DEG C, is prepared into alkali and processes wood powder；
(2) 1:5 in mass ratio, mixes corn starch with deionized water stirring and is placed in beaker, water-bath at 70～85 DEG C
Heating 25～30min, after its gelatinizing completes, continues Heat preservation rotary evaporated to dryness, collects and is dried gelatinized starch, subsequently
1:5 in mass ratio, processes wood powder by the alkali of dry gelatinized starch with above-mentioned preparation and is placed in ball grinder, 250～300r/min
Lower ball milling 1～2h, is prepared into ball milling mixed-powder；
(3) 1:5 in mass ratio, mixes the stirring of mass concentration 10% poly-vinyl alcohol solution and ball milling mixed-powder, 200～
After under 300W, sonic oscillation processes 10～15min, being placed in mould, under 5～10MPa after compacting, then sealing and fermenting processes 15
～20 days, after fermentation to be sealed completes, mould is placed at 85～100 DEG C and is dried 10～12h, be prepared into fermentation wood powder starch bone
Frame, standby；
(4) 1:10 in mass ratio, mixes the stirring of pond sludge and deionized water, under 200～300W ultrasonic disperse 20～
After 30min, sieve with the screen cloth of 60～80 mesh, collect lower floor mud and be placed at 95～100 DEG C being dried 6～8h, subsequently
Dry lower floor mud is placed in ball grinder, sieves after ball milling 3～5h under 650～700r/min, be prepared into 100～120 mesh
Mud granule；
(5) fermentation wood powder starch backbone prepared by step (3) is placed in rustless steel brick mould, 1:2 the most in mass ratio, will
Deionized water mixes with mud granule stirring and pours to fermentation wood powder starch backbone top layer, treats uniformly to be paved with rustless steel brick mould
After tool, more at room temperature standing solidification 20～24h, the demoulding subsequently is placed at 1000～1050 DEG C being fired into brick, natural cooling
A kind of seepage brick can be prepared into room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610484572.0A CN106116505A (en) | 2016-06-28 | 2016-06-28 | A kind of preparation method of seepage brick |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610484572.0A CN106116505A (en) | 2016-06-28 | 2016-06-28 | A kind of preparation method of seepage brick |
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| CN106116505A true CN106116505A (en) | 2016-11-16 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002241176A (en) * | 2001-02-13 | 2002-08-28 | Minebea Co Ltd | Ceramic material, producing method therefor and molding thereof |
| CN102826868A (en) * | 2012-08-27 | 2012-12-19 | 中南大学 | Foaming agent for tailing sintering perforated brick and application thereof |
| CN103553698A (en) * | 2013-10-18 | 2014-02-05 | 苏州大学 | Porous material and preparation method thereof |
| CN103922784A (en) * | 2014-03-25 | 2014-07-16 | 西安理工大学 | Method for preparing porous ceramic by microbial fermentation and low-temperature forming |
| CN105330318A (en) * | 2015-10-29 | 2016-02-17 | 合肥正拓装饰材料有限公司 | Multi-pore high-strength sintering permeable floor brick |
-
2016
- 2016-06-28 CN CN201610484572.0A patent/CN106116505A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002241176A (en) * | 2001-02-13 | 2002-08-28 | Minebea Co Ltd | Ceramic material, producing method therefor and molding thereof |
| CN102826868A (en) * | 2012-08-27 | 2012-12-19 | 中南大学 | Foaming agent for tailing sintering perforated brick and application thereof |
| CN103553698A (en) * | 2013-10-18 | 2014-02-05 | 苏州大学 | Porous material and preparation method thereof |
| CN103922784A (en) * | 2014-03-25 | 2014-07-16 | 西安理工大学 | Method for preparing porous ceramic by microbial fermentation and low-temperature forming |
| CN105330318A (en) * | 2015-10-29 | 2016-02-17 | 合肥正拓装饰材料有限公司 | Multi-pore high-strength sintering permeable floor brick |
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Application publication date: 20161116 |