CN106109600A - Nine Radix Polygoni Multiflori Preparata production technologies - Google Patents
Nine Radix Polygoni Multiflori Preparata production technologies Download PDFInfo
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- CN106109600A CN106109600A CN201610490263.4A CN201610490263A CN106109600A CN 106109600 A CN106109600 A CN 106109600A CN 201610490263 A CN201610490263 A CN 201610490263A CN 106109600 A CN106109600 A CN 106109600A
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- Prior art keywords
- polygoni multiflori
- radix polygoni
- block
- semen sojae
- sojae atricolor
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B21/00—Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
- F26B21/02—Circulating air or gases in closed cycles, e.g. wholly within the drying enclosure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B2200/00—Drying processes and machines for solid materials characterised by the specific requirements of the drying good
- F26B2200/02—Biomass, e.g. waste vegetative matter, straw
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Medical Informatics (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Mechanical Engineering (AREA)
- Medicinal Chemistry (AREA)
- Microbiology (AREA)
- General Engineering & Computer Science (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to nine Radix Polygoni Multiflori Preparata production technologies, comprise the following steps: prepared by decoction of black soybean；Radix Polygoni Multiflori Preparata block；Vexed Radix Polygoni Multiflori；Steam Radix Polygoni Multiflori；Dry Radix Polygoni Multiflori；Check vexed, steam, dry number of times；Nine Radix Polygoni Multiflori Preparatas；Inspection subpackage.The invention still further relates to a kind of drying room of nine Radix Polygoni Multiflori Preparata production processes, it is characterised in that drying room is provided with temperature inductor, drying room door forced locking device, and drying room realizes circulated air by arranging fan.The nine Radix Polygoni Multiflori Preparata production technologies that the present invention relates to adapt to modern pharmaceutical standard, compliant requirement completely, can produce stay-in-grade nine Radix Polygoni Multiflori Preparatas.
Description
Technical field
The present invention relates to pharmaceutical technology field, specifically refer to a kind of nine Radix Polygoni Multiflori Preparata production technologies.
Background technology
Chinese medicine is the treasure of the Chinese nation, is made that tremendous contribution for multiplying and being prosperous of the Chinese nation.Tradition doctor
The treatment concept learned the most gradually is accepted by the world, and traditional medicine is more and more paid close attention to by international community, in world wide
Growing to the demand of Chinese medicine, this is that the development of Chinese medicine provides wide space.1997, lead with the Ministry of Science and Technology
Head, is participated in by departments such as Ministry of Public Health, State Food and Drug Administration, State Administration of Traditional Chinese Medicines, has set up national new drug
Leading group, organizes national over hundreds of expert to propose the planning of modernization of Chinese medicine development, starts and implement modernization of Chinese medicine work
Make.The TCM Modernization work in the whole nation has been achieved for impressive progress: R&D mode is the most perfect, and the capability of independent innovation is notable
Strengthen；Successfully developing a collection of Chinese medicine new varieties, the important function of Chinese herb prevention disease is played further；Formulate one
The Chinese medicine basic standard that batch weight is wanted and meet the scientific and normal of character of traditional Chinese medicine, standards of Chinese traditional medicine industry normative construction wins initial success.With
Time, the modernization of Chinese medicine improve people's health level, increase farmers' income, the aspect such as preserve the ecological environment also has played notable work
With.Before in April, 2005, having established 448 Good Agricultural Practice bases, 18 province standardized planting areas reach interiorly
920000 hectares.Meanwhile, along with production technology and the breakthroughs of technique such as supercritical extraction, membrance separation, fluidized granulatings, Chinese medicine produces work
Technology, equipment are greatly improved, and Chinese medicine enterprise scale, benefit the most constantly promote.Contain medicinal plant farming, Chinese medicine industry, in
The modern TCM industry chain of pharmacist's industry constantly improves and development.
Nine Radix Polygoni Multiflori Preparata successions, from the distinctive Chinese Traditional Medicine of China, invigorating the liver and kidney, benefiting essence-blood, crow beard and hair, bone and muscle strengthening, are changed turbid
Blood fat reducing.For blood deficiency and yellow complexion, vertigo and tinnitus. early whitening of beard and hair, soreness of the waist and knees, numb limbs and tense tendons, bleeding not during menses, hyperlipemia.But pass
Nine Radix Polygoni Multiflori Preparata preparation methods of system are numerous and diverse, are unfavorable for batch production, there is presently no a kind of adaptation modern pharmaceutical standard, compliant
Change requirement, stay-in-grade nine Radix Polygoni Multiflori Preparata production technologies.
Summary of the invention
The purpose of the present invention is contemplated to solve the above-mentioned problems in the prior art, it is provided that a kind of adaptation modern pharmaceutical
Standard, compliant requirement, stay-in-grade nine Radix Polygoni Multiflori Preparata production technologies.
The purpose of the present invention is achieved through the following technical solutions:
Nine Radix Polygoni Multiflori Preparata production technologies, comprise the following steps:
One, prepared by decoction of black soybean: quantitatively weigh Semen sojae atricolor, adds the water of 1.6 times of weight, after heated and boiled, keeps boiling 4 hours, stops
Heating, when solution temperature is down to below 35 DEG C, is collected by filtration Semen sojae atricolor filtered juice for the first time, and first collecting amount is about raw material Semen sojae atricolor weight
1.5 times, then the filtering residue that filters for the first time is added the water of raw material 1.2 times of weight of Semen sojae atricolor weight, after heated and boiled, keeps boiling 3 little
Time, stop heating, when solution temperature is down to below 35 DEG C, Semen sojae atricolor filtered juice be again collected by filtration, again collecting amount about with raw material
Semen sojae atricolor is equal in weight, and with the Semen sojae atricolor filtered juice being again collected by filtration, the Semen sojae atricolor filtered juice being collected by filtration for the first time is added rustless steel with cover
Bucket, mixing, standby as decoction of black soybean；
Two, Radix Polygoni Multiflori Preparata block: raw material Radix Polygoni Multiflori is cleaned, dry, cut into slices after standby as Radix Polygoni Multiflori block；
Three, vexed Radix Polygoni Multiflori: added by Radix Polygoni Multiflori block in vexed medicine pond, adds decoction of black soybean, Poria mixing, and decoction of black soybean addition is with dipped
Radix Polygoni Multiflori is as the criterion, and the weight of Poria is the half of decoction of black soybean weight, closes the lid after mixing, vexed medicine 3 hours；
Four, steam Radix Polygoni Multiflori: move in food steamer by Radix Polygoni Multiflori block vexed in step 3, open steamer and start to steam, treat that food steamer is
Last layer starts timing after starting vapour, closes steamer after steaming 6 hours；
Five, Radix Polygoni Multiflori is dried: after the Radix Polygoni Multiflori block cooling after steaming in step 3, Radix Polygoni Multiflori block is moved into drip pan, then by drip pan
Putting in baking car, car load pushes drying room, is then shut off drying room door, and arranging baking medicine temperature is 75 DEG C, opens heater switch, treats temperature
Reaching 75 DEG C and start timing, the baking medicine time is 4 hours, after drying the arrival of medicine time, closes heater, opens drying room door, treat
Temperature is down to when less than 30 DEG C collect Radix Polygoni Multiflori block；
Six, check vexed, steam, dry number of times: the Radix Polygoni Multiflori block in testing sequence five, if vexed, steam, dry number of times, then will collect less than 8 times
Radix Polygoni Multiflori block return to step 3, again check through step 3, after four, five, if vexed, steam, dry number of times and reach 8 times, then will
The sorting of Radix Polygoni Multiflori block is standby；
Seven, nine Radix Polygoni Multiflori Preparata: by step 6 vexed, steam, dry number of times and reach the Radix Polygoni Multiflori block of 8 times and add in vexed medicine pond, add
Decoction of black soybean, Poria mix, and decoction of black soybean addition is as the criterion with dipped Radix Polygoni Multiflori, closes the lid after mixing, and the weight of Poria is Semen sojae atricolor
The half of juice weight, vexed medicine 3 hours, then vexed Radix Polygoni Multiflori block is moved in food steamer, open steamer and start to steam, treat food steamer
Last layer starts timing after starting vapour, closes steamer after steaming 6 hours, after the Radix Polygoni Multiflori block cooling after steaming, by what
Radix Polygoni Multiflori block moves into drip pan, then is put into by drip pan in baking car, and car load pushes drying room, is then shut off drying room door, arranges baking medicine temperature and is
75 DEG C, opening heater switch, treat that temperature reaches 75 DEG C and starts timing, the baking medicine time is 8 hours, after drying the arrival of medicine time, closes
Close heater, open drying room door, when temperature is down to below 30 DEG C, collect Radix Polygoni Multiflori block；
Eight, inspection subpackage: according to packing instructions, the Radix Polygoni Multiflori block after nine systems in step 7 is carried out subpackage.
In above step one, when the first Semen sojae atricolor filtered juice amount collected is higher than 1.65 times of raw material Semen sojae atricolor weight, or again
When the Semen sojae atricolor filtered juice amount collected is higher than 1.2 times of raw material Semen sojae atricolor weight, check filter utility, to prevent filter utility holes.
In above step one, when the first Semen sojae atricolor filtered juice amount collected is less than 1.35 times of raw material Semen sojae atricolor weight, or again
When the Semen sojae atricolor filtered juice amount collected is less than 0.8 times of raw material Semen sojae atricolor weight, check filter utility, to prevent filter utility from blocking.
In above step one, the decoction of black soybean prepared needs to be finished in 8 hours.
In above step four, step 7, it is thick that the Radix Polygoni Multiflori tile height in every food steamer must not exceed 5cm.
In above step five, step 7, it is thick that the Radix Polygoni Multiflori tile height on drip pan must not exceed 5cm.
In above step five, step 7, dry temperature and control at 70 DEG C～80 DEG C.
In above step eight, loading amount should be no less than the 97% of mark amount.
The invention still further relates to a kind of drying room of nine Radix Polygoni Multiflori Preparata production processes, it is characterised in that drying room is provided with temperature sense
Device, drying room door forced locking device, drying room realizes circulated air by arranging fan.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further elaborated.
First 5kg Semen sojae atricolor is put in pot, add 8kg water, after heated and boiled, keep boiling 4 hours, stop heating, treat solution
When temperature is down to less than 35 DEG C, Semen sojae atricolor filtered juice is collected by filtration for the first time, by with cover not for the Semen sojae atricolor filtered juice addition being collected by filtration for the first time
Rust steel drum, then in filtering residue, add 6kg water, keep boiling 3 hours after heated and boiled, stop heating, treat that solution temperature is down to 35
Time below DEG C, Semen sojae atricolor filtered juice is again collected by filtration, is equipped with the Semen sojae atricolor filtered juice being again collected by filtration being collected by filtration for the first time
The stainless steel cask of Semen sojae atricolor filtered juice, mixing, standby as decoction of black soybean；
Raw material Radix Polygoni Multiflori is cleaned, dry, cut into slices after add in vexed medicine pond, add decoction of black soybean, Poria mixing, decoction of black soybean addition
It is as the criterion with dipped Radix Polygoni Multiflori, then regards the amount that decoction of black soybean adds, add the Poria of decoction of black soybean half weight, close the lid after mixing
Son, vexed medicine 3 hours, more vexed Radix Polygoni Multiflori block is moved in food steamer, open steamer and start to steam, treat that food steamer last layer starts
Start timing after going out vapour, after steaming 6 hours, close steamer, after the Radix Polygoni Multiflori block cooling after steaming, Radix Polygoni Multiflori block is moved into and dries
Dish, then drip pan is put in baking car, car load pushes drying room, is then shut off drying room door, and arranging baking medicine temperature is 75 DEG C, opens heating
Switch, treats that temperature reaches 75 DEG C and starts timing, and the baking medicine time is 4 hours, after drying the arrival of medicine time, closes heater, opens
Drying room door, collects Radix Polygoni Multiflori block when temperature is down to below 30 DEG C, then the Radix Polygoni Multiflori block collected is added decoction of black soybean mixing, weight
Multiple the most vexed, steam, dry step, when carrying out the 9th time and drying medicine, extend the baking medicine time to 8 hours, subpackage of then testing.
The above-mentioned technology design merely illustrating the present invention and feature, its objective is to be to allow the ordinary skill in this area
Personnel will appreciate that the content of invention and implement according to this, can not limit the scope of the invention.Every according in the present invention
The change of the equivalence done by the essence held or modification, all should contain in protection scope of the present invention.
Claims (9)
1. nine Radix Polygoni Multiflori Preparata production technology, comprises the following steps:
One, prepared by decoction of black soybean: quantitatively weigh Semen sojae atricolor, adds the water of 1.6 times of weight, after heated and boiled, keeps boiling 4 hours, stops
Heating, when solution temperature is down to below 35 DEG C, is collected by filtration Semen sojae atricolor filtered juice for the first time, and first collecting amount is about raw material Semen sojae atricolor weight
1.5 times, then the filtering residue that filters for the first time is added the water of raw material 1.2 times of weight of Semen sojae atricolor weight, after heated and boiled, keeps boiling 3 little
Time, stop heating, when solution temperature is down to below 35 DEG C, Semen sojae atricolor filtered juice be again collected by filtration, again collecting amount about with raw material
Semen sojae atricolor is equal in weight, and with the Semen sojae atricolor filtered juice being again collected by filtration, the Semen sojae atricolor filtered juice being collected by filtration for the first time is added rustless steel with cover
Bucket, mixing, standby as decoction of black soybean；
Two, Radix Polygoni Multiflori Preparata block: raw material Radix Polygoni Multiflori is cleaned, dry, cut into slices after standby as Radix Polygoni Multiflori block；
Three, vexed Radix Polygoni Multiflori: added by Radix Polygoni Multiflori block in vexed medicine pond, adds decoction of black soybean, Poria mixing, and decoction of black soybean addition is with dipped
Radix Polygoni Multiflori is as the criterion, and the weight of Poria is the half of decoction of black soybean weight, closes the lid after mixing, vexed medicine 3 hours；
Four, steam Radix Polygoni Multiflori: move in food steamer by Radix Polygoni Multiflori block vexed in step 3, open steamer and start to steam, treat that food steamer is
Last layer starts timing after starting vapour, closes steamer after steaming 6 hours；
Five, Radix Polygoni Multiflori is dried: after the Radix Polygoni Multiflori block cooling after steaming in step 3, Radix Polygoni Multiflori block is moved into drip pan, then by drip pan
Putting in baking car, car load pushes drying room, is then shut off drying room door, and arranging baking medicine temperature is 75 DEG C, opens heater switch, treats temperature
Reaching 75 DEG C and start timing, the baking medicine time is 4 hours, after drying the arrival of medicine time, closes heater, opens drying room door, treat
Temperature is down to when less than 30 DEG C collect Radix Polygoni Multiflori block；
Six, check vexed, steam, dry number of times: the Radix Polygoni Multiflori block in testing sequence five, if vexed, steam, dry number of times, then will collect less than 8 times
Radix Polygoni Multiflori block return to step 3, again check through step 3, after four, five, if vexed, steam, dry number of times and reach 8 times, then will
The sorting of Radix Polygoni Multiflori block is standby；
Seven, nine Radix Polygoni Multiflori Preparata: by step 6 vexed, steam, dry number of times and reach the Radix Polygoni Multiflori block of 8 times and add in vexed medicine pond, add
Decoction of black soybean, Poria mix, and decoction of black soybean addition is as the criterion with dipped Radix Polygoni Multiflori, and the weight of Poria is the half of decoction of black soybean weight, mixed
Close the lid after even, vexed medicine 3 hours, then vexed Radix Polygoni Multiflori block is moved in food steamer, open steamer and start to steam, treat food steamer
Last layer starts timing after starting vapour, closes steamer after steaming 6 hours, after the Radix Polygoni Multiflori block cooling after steaming, by what
Radix Polygoni Multiflori block moves into drip pan, then is put into by drip pan in baking car, and car load pushes drying room, is then shut off drying room door, arranges baking medicine temperature and is
75 DEG C, opening heater switch, treat that temperature reaches 75 DEG C and starts timing, the baking medicine time is 8 hours, after drying the arrival of medicine time, closes
Close heater, open drying room door, when temperature is down to below 30 DEG C, collect Radix Polygoni Multiflori block；
Eight, inspection subpackage: according to packing instructions, the Radix Polygoni Multiflori block after nine systems in step 7 is carried out subpackage.
The most according to claim 1, nine Radix Polygoni Multiflori Preparata production technology, it is characterised in that in described step one, that collects for the first time is black
When bean filtered juice amount is higher than 1.65 times of raw material Semen sojae atricolor weight, or the Semen sojae atricolor filtered juice amount again collected is higher than raw material Semen sojae atricolor weight
When 1.2 times, check filter utility, to prevent filter utility holes.
The most according to claim 1, nine Radix Polygoni Multiflori Preparata production technology, it is characterised in that in described step one, that collects for the first time is black
When bean filtered juice amount is less than 1.35 times of raw material Semen sojae atricolor weight, or the Semen sojae atricolor filtered juice amount again collected is less than raw material Semen sojae atricolor weight
When 0.8 times, check filter utility, to prevent filter utility from blocking.
Nine Radix Polygoni Multiflori Preparata production technology the most according to claim 1, it is characterised in that in described step one, the Semen sojae atricolor prepared
Juice needs to be finished in 8 hours.
Nine Radix Polygoni Multiflori Preparata production technology the most according to claim 1, it is characterised in that in described step 4, step 7, often steam
It is thick that Radix Polygoni Multiflori tile height in cage must not exceed 5cm.
Nine Radix Polygoni Multiflori Preparata production technology the most according to claim 1, it is characterised in that in described step 5, step 7, drip pan
On Radix Polygoni Multiflori tile height to must not exceed 5cm thick.
The most according to claim 1, nine Radix Polygoni Multiflori Preparata production technology, it is characterised in that in described step 5, step 7, dry
Temperature controls at 70 DEG C～80 DEG C.
The most according to claim 1, nine Radix Polygoni Multiflori Preparata production technology, it is characterised in that in described step 8, loading amount should be no less than
The 97% of mark amount.
9. the drying room used by a Radix Polygoni Multiflori Preparata production, it is characterised in that drying room is provided with temperature inductor, drying room door certainly
Dynamic locking device, drying room realizes circulated air by arranging fan.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610490263.4A CN106109600A (en) | 2016-06-29 | 2016-06-29 | Nine Radix Polygoni Multiflori Preparata production technologies |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610490263.4A CN106109600A (en) | 2016-06-29 | 2016-06-29 | Nine Radix Polygoni Multiflori Preparata production technologies |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107875203A (en) * | 2017-09-06 | 2018-04-06 | 上海德华国药制品有限公司 | Fleece-flower root Manufacture of medicinal slices of TCM technique |
| CN109999084A (en) * | 2019-04-19 | 2019-07-12 | 河南省青山药业股份有限公司 | A kind of preparation method of the fleece-flower root |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201344707Y (en) * | 2009-01-01 | 2009-11-11 | 蔡志鸿 | Heat pump drying room |
| CN105395623A (en) * | 2015-11-23 | 2016-03-16 | 北京康仁堂药业有限公司 | A processing technology of prepared fleeceflower root |
-
2016
- 2016-06-29 CN CN201610490263.4A patent/CN106109600A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201344707Y (en) * | 2009-01-01 | 2009-11-11 | 蔡志鸿 | Heat pump drying room |
| CN105395623A (en) * | 2015-11-23 | 2016-03-16 | 北京康仁堂药业有限公司 | A processing technology of prepared fleeceflower root |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107875203A (en) * | 2017-09-06 | 2018-04-06 | 上海德华国药制品有限公司 | Fleece-flower root Manufacture of medicinal slices of TCM technique |
| CN109999084A (en) * | 2019-04-19 | 2019-07-12 | 河南省青山药业股份有限公司 | A kind of preparation method of the fleece-flower root |
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Application publication date: 20161116 |