CN106109255A - A kind of containing nano-graphene epithelium and preparation method thereof - Google Patents
A kind of containing nano-graphene epithelium and preparation method thereof Download PDFInfo
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- CN106109255A CN106109255A CN201610494191.0A CN201610494191A CN106109255A CN 106109255 A CN106109255 A CN 106109255A CN 201610494191 A CN201610494191 A CN 201610494191A CN 106109255 A CN106109255 A CN 106109255A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention provides a kind of containing nano-graphene epithelium and preparation method thereof, its epithelium includes by weight proportion: nano-graphene 0.03 ~ 0.1 part and plant enzyme 0.8 ~ 1.5 part.The present invention containing nano-graphene epithelium and preparation method thereof, with the addition of nano-graphene physical sterilization composition, allow antibacterial will not produce drug resistance, have skin good acne-removing inflammation-diminishing effect, comedo teen-age to chronic inflammation to have good effect.Use plant enzyme can repair the effect of small pox surrounding tissue simultaneously, its sterilization, effect of antiinflammatory, make chronic inflammatory disease heal, the most also there is the effect of whitening nutrition skin.Have again, the present invention containing nano-graphene epithelium solidify after epithelium shape, high adsorption capacity, self-cleaning ability by nanoscale graphite alkene, subcutaneous rubbish toxin is dissociated on the epithelium being adsorbed onto shaping, meanwhile, utilize far infrared merit effect of Graphene, reach antibacterial, antibacterial, antiinflammatory, the effect of enhancing blood.
Description
Technical field
The present invention relates to a kind of facial film and preparation method thereof, especially a kind of containing nano-graphene facial film and preparation side thereof
Method, described containing epithelium shape after the solidification of nano-graphene facial film.
Background technology
Mono-layer graphite, is also called Graphene (Graphene), is a kind of tight with graphite key (sp2) by monolayer carbon atom
Closs packing becomes the lattice structure of bi-dimensional cellular shape, the most only thickness of a carbon atom, and graphite key is covalent bond and metallic bond
Compound keys, can say to be insulator and the heaven-made match of electric conductor.Graphene be at present the thinnest be also the hardest material
Material, heat conductivity is higher than CNT and diamond, its electron mobility also ratio carbon nanotube or silicon wafer height, resistance under room temperature
Rate is lower than copper or silver, is the material that resistivity is minimum the most in the world, and the electric charge engineering properties of these uniquenesses makes to add stone
The composite more multifunction of ink alkene, not only shows mechanics and the electric property of excellence, also has excellent processing characteristics,
Broader practice field is provided for composite.But the Graphene of structural integrity is by the benzene without any labile bond
The two dimensional crystal that hexatomic ring combines, chemical stability is high, and the inert state in its surface, with other medium (such as solvent etc.
) interact more weak, and between the sheet of Graphene and sheet, there is stronger Fan get Wa Li, easily produce reunion so that it is be insoluble in
Water and other conventional organic solvent, thus limit research further and the application of Graphene.
Nano-graphene can kill 10 various bacteria such as bacillus pyocyaneus, escherichia coli, this is because nano-graphene this
Body is the carbon atom strung, and just as one layer of the most closely knit cloth the thinnest, they tackle the mode of antibacterial 3 kinds: the first is
Directly cutting, owing to Graphene is nano level, and antibacterial is micron order, and the former is less 1000 times than the latter, and Graphene is as same
The sharpest cutter, directly antibacterial is cut to death；The second is antibacterial hungry to death, and nano level Graphene can be by antibacterial as cloth
Wrap up closely, make antibacterial absorb less than nutrition, die of starvation；The third is slowly to wither away, owing to Graphene is the least, carefully
Graphene can be gulped down enter " tripe " inner by bacterium, can suffer from diarrhea uncomfortable just as people has eaten foreign body, cause antibacterial slowly to be withered away, exactly because
This physical sterilization method of Graphene, allows antibacterial will not produce drug resistance, has good acne-removing inflammation-diminishing effect to skin.
Acne-removing inflammation-diminishing product in the market often contains ethanol, salicylic acid or chloromycetin etc. illegally to be added antibiotic and swashs
Element situation, knows from experience generation drug resistance to people, insulting healthy.
Summary of the invention
For the shortcomings and deficiencies of prior art, the invention provides one and there is antibacterial effect, acne-removing inflammation-diminishing, skin protection effect
Fruit containing nano-graphene epithelium and preparation method thereof.
In order to realize the object of the invention, the present invention proposes a kind of epithelium Han nano-graphene, including by weight proportion: nanometer
Graphene 0.8 ~ 1.5 part and plant enzyme 0.8 ~ 1.5 part.
Preferential as technique scheme, also includes part by weight: allantoin 0.1 ~ 0.5 part and deionized water 21 ~ 28
Part,
Preferential as technique scheme, also includes part by weight: the polyvinyl alcohol of 10% 55 ~ 75 parts, glycerol 8 ~ 14 parts, raw
Thing carbohydrate gum 5 ~ 8 parts.
Preferential as technique scheme, also includes part by weight: plant antiseptic agent 1 ~ 2 part.
A kind of preparation method containing nano-graphene epithelium, comprises the steps:
(1) weight ratio is divided into the deionized water of 21 ~ 28 parts, is heated to 88-92 DEG C, keep sterilizing in 30-40 minute, then add successively
Enter 0.8 ~ 1.5 part of nano-graphene, 0.1 ~ 0.5 part of allantoin, 0.8 ~ 1.5 part of plant enzyme mixing；
(2) successively polyvinyl alcohol, 8 ~ 14 parts of glycerol, 5 ~ 8 parts of biological carbohydrate gums of 55 ~ 75 part 10% are added step 1 gained solution
In, stir；
(3), by step 2 gained solution, when being cooled to 38-45 DEG C, add 1 ~ 2 part of plant antiseptic agent, stir；
(4) it is cooled to 30-40 DEG C, after waiting for 24 hours quietly, after checking every physical and chemical index qualified, can discharging fill.
The having the beneficial effect that containing nano-graphene epithelium and preparation method thereof of the present invention:
The present invention containing nano-graphene epithelium and preparation method thereof, with the addition of nano-graphene physical sterilization composition, allow antibacterial
Drug resistance will not be produced, skin is had good acne-removing inflammation-diminishing effect；Comedo teen-age to chronic inflammation (is also Cuo
Skin ulcer) there is good effect.
Use plant enzyme can repair the effect of small pox surrounding tissue simultaneously, its sterilization, effect of antiinflammatory, make chronic inflammatory disease
Healing, the most also has the effect of whitening nutrition skin.
The present invention containing nano-graphene epithelium solidify after epithelium shape, high adsorption capacity, by nanoscale graphite alkene from
Clean ability, dissociates on the epithelium being adsorbed onto shaping by subcutaneous rubbish toxin, meanwhile, utilizes far infrared merit effect of Graphene, reaches
To antibacterial, antibacterial, antiinflammatory, the effect of enhancing blood.
The present invention containing nano-graphene epithelium, to repair, whitening, water, antiinflammatory, defying age is integrated, due to nanometer stone
The miraculous effects of sterilization, inhibiting bacteria and diminishing inflammation and Low Temperature Far Infrared that ink alkene is natural, make skin adipose membrane balance, effectively control acne, pox
Pox, the generation of inflammation, little molecule surpasses permeance property, deep layer cleaning pore, gets through nutrition channel, and blood circulation promoting, rich in sky
So Moisture factor, lasting replenishing water and preserving moisture, repair skin barrier, nurse one's health sensitive substrate, alleviate skin sensitivity, promote skin keratin
The growth of layer, effectively decomposes melanin, due to the self-cleaning function of Graphene, skin can be made at rubbish toxin free discharge body interior
Outward, making skin the whitest, saturating, tender, bright, mottle is effectively decomposed, and thoroughly takes leave of lead mercurialism.
Epithelium shape after the solidification of this nano-graphene facial film, using method is simple, easily operates, can use whenever and wherever possible, take off
Need not clean after film and skin care item be can be used directly.This epithelium preparation method is simple, economical and efficient, manufacturing cycle are short, natural without dirty
Dye, product property is stable.
Detailed description of the invention
Embodiment 1
The preparation method containing nano-graphene epithelium of the present embodiment, comprises the following steps:
(1) weight ratio is divided into the deionized water of 21.7 parts, is heated to 90 DEG C, keep sterilizing in 30 minutes, sequentially add 1 part and receive
Rice Graphene, 0.3 part of allantoin, 1 part of plant enzyme mixing；
(2) successively 60 parts of polyvinyl alcohol, 10 parts of glycerol, 5 parts of biological carbohydrate gums are added in step 1 gained solution, stir (poly-
It is standby that vinyl alcohol is prepared as 10% aqueous solution in advance)；
(3), by step 2 gained solution, when being cooled to 40 DEG C, add 1 part of plant antiseptic agent, stir；
(4) temperature is down to 35 DEG C, after waiting for 24 hours quietly, after checking every physical and chemical index qualified, and can discharging fill.
Nano-graphene physical sterilization composition, allows antibacterial will not produce drug resistance, has good acne-removing inflammation-diminishing to skin, takes out
Oily, sun-proof effect, plant enzyme has a whitening skin lightening, the anti-inflammatory analgetic effect that allantoin is good simultaneously, glycerol moisturizing,
Skin barrier effect repaired by biological carbohydrate gum.
Embodiment 2
The preparation method of the pectin mastic epithelium of the present embodiment, comprises the following steps:
(1) weight ratio is divided into the deionized water of 23 parts, is heated to 88 ~ 92 DEG C, sequentially add 1 part of nano-graphene, 0.3 part
Allantoin, 1.2 parts of plant enzyme mixings；
(2) adding in step 1 gained solution by polyvinyl alcohol, 10 parts of glycerol, 6 parts of biological carbohydrate gums of 65 part 10% successively, stirring is all
Even；
(3), by step 2 gained solution, when being cooled to 38-45 DEG C, add 1 part of plant antiseptic agent, stir；
(4) it is cooled to 30-40 DEG C, after waiting for 24 hours quietly, after checking every physical and chemical index qualified, can discharging fill.
Embodiment 2 ratio embodiment 1 good film-forming property, high adsorption capacity.
Embodiment 3
(1) weight ratio is divided into the deionized water of 24 parts, is heated to 88 ~ 92 DEG C, sequentially add 1 part of nano-graphene, 0.5 part
Allantoin, 1.3 parts of plant enzyme mixings；
(2) adding in step 1 gained solution by polyvinyl alcohol, 12 parts of glycerol, 8 parts of biological carbohydrate gums of 70 part 10% successively, stirring is all
Even；
(3), by step 2 gained solution, when being cooled to 38-45 DEG C, add 1.2 parts of plant antiseptic agents, stir；
(4) it is cooled to 30-40 DEG C, after waiting for 24 hours quietly, after checking every physical and chemical index qualified, can discharging fill.
Embodiment 3 ratio embodiment 2 good film-forming property, high adsorption capacity.
Use case:
The Contrast on effect case using embodiment 1 preparation method gained epithelium and commercially available facial film is as shown in the table: as shown in the table:
(commercially available facial film without the composition of stone nano-graphene, other all in the presence of)
Knowable to above concrete case, obvious containing nano-graphene epithelium anti-acne repairing effect, natural non-stimulated, it is possible to effectively to change
The skin problem that kind comedo brings, can play whitening anti-acne, nutrition skin, the effect of reparation skin simultaneously.
Nano-graphene can kill 10 various bacteria such as bacillus pyocyaneus, escherichia coli, this is because nano-graphene this
Body is the carbon atom strung, and just as one layer of the most closely knit cloth the thinnest, they tackle the mode of antibacterial 3 kinds: the first is
Directly cutting, owing to Graphene is nano level, and antibacterial is micron order, and the former is less 1000 times than the latter, and Graphene is as same
The sharpest cutter, directly antibacterial is cut to death；The second is antibacterial hungry to death, and nano level Graphene can be by antibacterial as cloth
Wrap up closely, make antibacterial absorb less than nutrition, die of starvation；The third is slowly to wither away, owing to Graphene is the least, carefully
Graphene can be gulped down enter " tripe " inner by bacterium, can suffer from diarrhea uncomfortable just as people has eaten foreign body, cause antibacterial slowly to be withered away, exactly because
This physical sterilization method of Graphene, allows antibacterial will not produce drug resistance, has good acne-removing inflammation-diminishing effect to skin.
Plant enzyme can repair the effect of small pox surrounding tissue, its sterilization, effect of antiinflammatory, makes chronic inflammatory disease heal, with
Time also there is the effect of whitening nutrition skin..
The present invention containing nano-graphene epithelium solidify after epithelium shape, high adsorption capacity, by nanoscale graphite alkene from
Clean ability, dissociates on the epithelium being adsorbed onto shaping by subcutaneous rubbish toxin, meanwhile, utilizes far infrared merit effect of Graphene, reaches
To antibacterial, antibacterial, antiinflammatory, the effect of enhancing blood.
The present invention containing nano-graphene epithelium, to repair, whitening, water, antiinflammatory, defying age is integrated, due to nanometer stone
The miraculous effects of sterilization, inhibiting bacteria and diminishing inflammation and Low Temperature Far Infrared that ink alkene is natural, make skin adipose membrane balance, effectively control acne, pox
Pox, the generation of inflammation, little molecule surpasses permeance property, deep layer cleaning pore, gets through nutrition channel, and blood circulation promoting, rich in sky
So Moisture factor, lasting replenishing water and preserving moisture, repair skin barrier, nurse one's health sensitive substrate, alleviate skin sensitivity, promote skin keratin
The growth of layer, effectively decomposes melanin, due to the self-cleaning function of Graphene, skin can be made at rubbish toxin free discharge body interior
Outward, making skin the whitest, saturating, tender, bright, mottle is effectively decomposed, and thoroughly takes leave of lead mercurialism.
Epithelium shape after the solidification of this nano-graphene facial film, using method is simple, easily operates, can use whenever and wherever possible, take off
Need not clean after film and skin care item be can be used directly.This epithelium preparation method is simple, economical and efficient, manufacturing cycle are short, natural without dirty
Dye, product property is stable.
Embodiment described above is only to be described the preferred embodiment of the present invention, the not model to the present invention
Enclosing and be defined, under design spirit premise without departing from the present invention, this area ordinary skill technical staff is to the technology of the present invention side
Various deformation that case is made and improvement, all should fall in the protection domain that claims of the present invention determines.
Claims (5)
1. an epithelium Han nano-graphene, including by weight proportion: nano-graphene 0.8 ~ 1.5 part and plant enzyme 0.8 ~
1.5 part.
It is the most according to claim 1 containing nano-graphene epithelium, it is characterised in that: also include part by weight: allantoin 0.1
~ 0.5 part and deionized water 21 ~ 28 parts.
It is the most according to claim 1 and 2 containing nano-graphene epithelium, it is characterised in that: also include part by weight: 10%
Polyvinyl alcohol 55 ~ 75 parts, glycerol 8 ~ 14 parts, biological carbohydrate gum 5 ~ 8 parts.
It is the most according to claim 3 containing nano-graphene epithelium, it is characterised in that: also include part by weight: antiseptic
Agent 1 ~ 2 part.
5. the preparation method containing nano-graphene epithelium, comprises the steps:
(1) weight ratio is divided into the deionized water of 21 ~ 28 parts, is heated to 88-92 DEG C, keep sterilizing in 30-40 minute, then add successively
Enter 0.8 ~ 1.5 part of nano-graphene, 0.1 ~ 0.5 part of allantoin, 0.8 ~ 1.5 part of plant enzyme mixing；
(2) successively polyvinyl alcohol, 8 ~ 14 parts of glycerol, 5 ~ 8 parts of biological carbohydrate gums of 55 ~ 75 part 10% are added step 1 gained solution
In, stir；
(3), by step 2 gained solution, when being cooled to 38-45 DEG C, add 1 ~ 2 part of plant antiseptic agent, stir；
(4) it is cooled to 30-40 DEG C, after waiting for 24 hours quietly, after checking every physical and chemical index qualified, can discharging fill.
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| CN201610494191.0A CN106109255A (en) | 2016-06-30 | 2016-06-30 | A kind of containing nano-graphene epithelium and preparation method thereof |
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| CN201610494191.0A CN106109255A (en) | 2016-06-30 | 2016-06-30 | A kind of containing nano-graphene epithelium and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157654A (en) * | 2017-05-27 | 2017-09-15 | 中山市创思泰新材料科技股份有限公司 | Device and a kind of antibiotic skin-care film that a kind of humidity regulation and antibacterial for skin is nursed |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102600061A (en) * | 2012-03-06 | 2012-07-25 | 吉林敖东大高酵素有限公司 | Preparation method for plant enzyme skin care liquid |
| CN105287248A (en) * | 2015-11-18 | 2016-02-03 | 张建刚 | Graphene oxide mask and preparation method thereof |
| CN105380819A (en) * | 2015-11-18 | 2016-03-09 | 中山市艾丽意素生物科技有限公司 | Moisturized and compact basic essence and preparation method thereof |
-
2016
- 2016-06-30 CN CN201610494191.0A patent/CN106109255A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102600061A (en) * | 2012-03-06 | 2012-07-25 | 吉林敖东大高酵素有限公司 | Preparation method for plant enzyme skin care liquid |
| CN105287248A (en) * | 2015-11-18 | 2016-02-03 | 张建刚 | Graphene oxide mask and preparation method thereof |
| CN105380819A (en) * | 2015-11-18 | 2016-03-09 | 中山市艾丽意素生物科技有限公司 | Moisturized and compact basic essence and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157654A (en) * | 2017-05-27 | 2017-09-15 | 中山市创思泰新材料科技股份有限公司 | Device and a kind of antibiotic skin-care film that a kind of humidity regulation and antibacterial for skin is nursed |
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