CN106093291A - A kind of clay Absorbance ratio-derivative method determinator - Google Patents
A kind of clay Absorbance ratio-derivative method determinator Download PDFInfo
- Publication number
- CN106093291A CN106093291A CN201610608320.4A CN201610608320A CN106093291A CN 106093291 A CN106093291 A CN 106093291A CN 201610608320 A CN201610608320 A CN 201610608320A CN 106093291 A CN106093291 A CN 106093291A
- Authority
- CN
- China
- Prior art keywords
- beaker
- clay
- burette
- absorbance ratio
- derivative method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/16—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using titration
Abstract
A kind of clay Absorbance ratio-derivative method determinator, including sample processing device, experimental determination device and control device, described sample processing device is mechanical shearing dispersal device；Described experimental determination device includes beaker, motor, burette and solution bottle, described beaker is placed in beaker torr, described beaker top arranges motor, for stirring the solution in beaker, described burette is placed in solution bottle top, titration piston is set between described burette and beaker, in the middle part of described burette, connects rubber bulbs,double by trachea；Described control device is connected with motor and mechanical shearing dispersal device, for controlling motor and the operation of mechanical shearing dispersal device.A kind of clay Absorbance ratio-derivative method determinator that the present invention provides uses ultra-sonic dispersion method, coordinates automatic burette and mechanical stirring device, can realize the mensuration of effective bentonite content in bentonite Absorbance ratio-derivative method and molding sand the most fast and accurately.
Description
Technical field
The present invention relates to a kind of clay determinator, be specifically related to a kind of clay Absorbance ratio-derivative method determinator.
Background technology
At present, in bentonite Absorbance ratio-derivative method and molding sand, the mensuration/detection of effective bentonite content is the most easy with some
Detecting instrument is produced error by manual operation titrimetry, such processing ease, it addition, system colors is stimulated by the eyes of people
Change insensitive, often result in last titrate the analysis result and differentiate unclear, make the data result accuracy detected relatively low, Er Qiejian
Survey process is time-consuming, laborious, and have large-scale, save time, detector laborsaving, standard expensive, the instrument that some are small-sized is added
Factory is not suitable for.
Summary of the invention
Not enough for prior art, the invention provides a kind of analysis and detect accurately for bentonite Absorbance ratio-derivative method and molding sand
In the determinator of effective bentonite content.
The present invention solves the technical scheme of above-mentioned technical problem employing: a kind of clay Absorbance ratio-derivative method determinator, including examination
Sample processing means, experimental determination device and control device, it is characterised in that: described sample processing device is mechanical shearing dispersion dress
Put；Described experimental determination device includes that beaker, motor, burette and solution bottle, described beaker are placed in beaker torr, described beaker
Top arranges motor, and for stirring the solution in beaker, described burette is placed in solution bottle top, described burette and beaker it
Between titration piston is set, in the middle part of described burette by trachea connect rubber bulbs,double；Described control device and motor and machinery
Shearing dispersal device is connected, for controlling motor and the operation of mechanical shearing dispersal device.
Further, described control device arranges digital time relay, timing reset switch, timing controller, choosing
Select switch and display lamp, for timing controlled motor and the operation of mechanical shearing dispersal device.
Further, described mechanical shearing dispersal device is batch (-type) high shear dispersion device.
Further, the content of described burette is 50mL.
Further, the timing controlled scope of described timing controller is 0-15min.
In clay, bentonite has the strongest absorbability to methylene blue dye.This device uses burette test method, measures
During sample Absorbance ratio-derivative method, process clay initially with mechanical shearing dispersal device, measure Absorbance ratio-derivative method and use titrimetry, and cooperative mechanical
Stirring makes clay sample and methylene blue be fully contacted to carry out adsorption reaction.According to whether sample suspension occurs free dye
Material, judges whether clay reaches saturated absorption, measures the Absorbance ratio-derivative method of the samples such as clay with this.
Compared with prior art, what the present invention possessed has the beneficial effect that
A kind of clay Absorbance ratio-derivative method determinator that the present invention provides uses ultra-sonic dispersion method, coordinates automatic burette and machinery
Agitating device, can realize the mensuration of effective bentonite content in bentonite Absorbance ratio-derivative method and molding sand the most fast and accurately.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention.
Detailed description of the invention
The present invention is described further below in conjunction with the accompanying drawings.
A kind of clay Absorbance ratio-derivative method determinator as shown in Figure 1, including sample processing device, experimental determination device and control
Device, it is characterised in that: described sample processing device is mechanical shearing dispersal device 12；Described experimental determination device includes beaker
6, motor 7, burette 8 and solution bottle 10, described beaker 6 is placed in beaker torr 5, and described beaker 6 top arranges motor 7, is used for
Solution in stirring beaker 6, described burette 8 is placed in solution bottle 10 top, arranges titration between described burette 8 and beaker 6
Piston 9, connects rubber bulbs,double 11 by trachea in the middle part of described burette 8；Described control device and motor 7 and mechanical shear cutting
In bulk put 12 and be connected, for controlling motor 7 and the operation of mechanical shearing dispersal device 12.
Further, described control device is arranged digital time relay 1, timing reset switch 2, timing controller 3,
Select switch 13 and display lamp 4, for timing controlled motor 7 and the operation of mechanical shearing dispersal device 12.
Further, described mechanical shearing dispersal device 12 is batch (-type) high shear dispersion device.
Further, the content of described burette 8 is 50mL.
Further, the timing controlled scope of described timing controller 3 is 0-15min.
In clay, bentonite has the strongest absorbability to methylene blue dye.This device uses burette test method, measures
During sample Absorbance ratio-derivative method, process clay initially with mechanical shearing dispersal device, measure Absorbance ratio-derivative method and use titrimetry, and cooperative mechanical
Stirring makes clay sample and methylene blue be fully contacted to carry out adsorption reaction.According to whether sample suspension occurs free dye
Material, judges whether clay reaches saturated absorption, measures the Absorbance ratio-derivative method of the samples such as clay with this.A kind of clay that the present invention provides
Absorbance ratio-derivative method determinator can realize the survey of effective bentonite content in bentonite Absorbance ratio-derivative method and molding sand the most fast and accurately
Fixed.
Claims (5)
1. a clay Absorbance ratio-derivative method determinator, including sample processing device, experimental determination device and control device, its feature exists
In: described sample processing device is mechanical shearing dispersal device；Described experimental determination device include beaker, motor, burette and
Solution bottle, described beaker is placed in beaker torr, and described beaker top arranges motor, for stirring the solution in beaker, described
Fixed tube is placed in solution bottle top, arranges titration piston between described burette and beaker, in the middle part of described burette by trachea even
Connect rubber bulbs,double；Described control device is connected with motor and mechanical shearing dispersal device, is used for controlling motor and mechanical shearing
The operation of dispersal device.
A kind of clay Absorbance ratio-derivative method determinator the most according to claim 1, it is characterised in that: arrange on described control device
Digital time relay, timing reset switch, timing controller, selection switch and display lamp, for timing controlled motor and machine
The operation of dispersal device sheared by tool.
A kind of clay Absorbance ratio-derivative method determinator the most according to claim 1, it is characterised in that: described mechanical shearing dispersion dress
It is set to batch (-type) high shear dispersion device.
A kind of clay Absorbance ratio-derivative method determinator the most according to claim 1, it is characterised in that: the content of described burette is
50mL。
A kind of clay Absorbance ratio-derivative method determinator the most according to claim 2, it is characterised in that: determining of described timing controller
Time span of control be 0-15min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610608320.4A CN106093291A (en) | 2016-07-29 | 2016-07-29 | A kind of clay Absorbance ratio-derivative method determinator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610608320.4A CN106093291A (en) | 2016-07-29 | 2016-07-29 | A kind of clay Absorbance ratio-derivative method determinator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106093291A true CN106093291A (en) | 2016-11-09 |
Family
ID=57479220
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610608320.4A Pending CN106093291A (en) | 2016-07-29 | 2016-07-29 | A kind of clay Absorbance ratio-derivative method determinator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106093291A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112305154A (en) * | 2020-10-16 | 2021-02-02 | 中石化石油工程技术服务有限公司 | Automatic analysis detector for bentonite blue absorption amount and detection method thereof |
| CN112305153A (en) * | 2020-10-16 | 2021-02-02 | 中石化石油工程技术服务有限公司 | Automatic analysis detector for bentonite content and detection method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003048000A (en) * | 2001-08-07 | 2003-02-18 | Kurita Water Ind Ltd | Treatment method for water-containing mud |
| JP2005006510A (en) * | 2003-06-16 | 2005-01-13 | Mizusawa Ind Chem Ltd | Silica-magnesia-based preparation excellent in base adsorptivity, and method for producing the same |
| CN101493451A (en) * | 2008-09-27 | 2009-07-29 | 辽宁工程技术大学 | Automatic analysis and detection instrument for bentonite blue suction quantity and detection method thereof |
| CN101806747A (en) * | 2010-03-05 | 2010-08-18 | 华中科技大学 | Methylene blue adsorption testing method of bentonite |
| CN201788154U (en) * | 2010-03-05 | 2011-04-06 | 华中科技大学 | Bentonite methylene blue absorption amount testing device |
| CN202947971U (en) * | 2012-12-07 | 2013-05-22 | 阜新市金地矿业有限公司 | Manual analyzing and detecting device for blue absorption power of bentonite |
-
2016
- 2016-07-29 CN CN201610608320.4A patent/CN106093291A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003048000A (en) * | 2001-08-07 | 2003-02-18 | Kurita Water Ind Ltd | Treatment method for water-containing mud |
| JP2005006510A (en) * | 2003-06-16 | 2005-01-13 | Mizusawa Ind Chem Ltd | Silica-magnesia-based preparation excellent in base adsorptivity, and method for producing the same |
| CN101493451A (en) * | 2008-09-27 | 2009-07-29 | 辽宁工程技术大学 | Automatic analysis and detection instrument for bentonite blue suction quantity and detection method thereof |
| CN101806747A (en) * | 2010-03-05 | 2010-08-18 | 华中科技大学 | Methylene blue adsorption testing method of bentonite |
| CN201788154U (en) * | 2010-03-05 | 2011-04-06 | 华中科技大学 | Bentonite methylene blue absorption amount testing device |
| CN202947971U (en) * | 2012-12-07 | 2013-05-22 | 阜新市金地矿业有限公司 | Manual analyzing and detecting device for blue absorption power of bentonite |
Non-Patent Citations (1)
| Title |
|---|
| 余笃武等: "《铸造测试仪器的原理及应用》", 30 June 1990, 机械工业出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112305154A (en) * | 2020-10-16 | 2021-02-02 | 中石化石油工程技术服务有限公司 | Automatic analysis detector for bentonite blue absorption amount and detection method thereof |
| CN112305153A (en) * | 2020-10-16 | 2021-02-02 | 中石化石油工程技术服务有限公司 | Automatic analysis detector for bentonite content and detection method thereof |
| CN112305153B (en) * | 2020-10-16 | 2022-09-23 | 中石化石油工程技术服务有限公司 | Automatic analysis detector for bentonite content and detection method thereof |
| CN112305154B (en) * | 2020-10-16 | 2022-09-23 | 中石化石油工程技术服务有限公司 | Automatic analysis detector for bentonite blue absorption amount and detection method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP2221622A3 (en) | Sample analyzer, sample analyzing method and computer program product | |
| CN106018674A (en) | Control device of methylene blue clay determination device | |
| EP2098868A3 (en) | Analyzer, sample transportation method, and computer program product | |
| CN106093029A (en) | A kind of methylene blue clay determinator | |
| CN106093291A (en) | A kind of clay Absorbance ratio-derivative method determinator | |
| CN105115472A (en) | Automatic flatness detection equipment | |
| CN102692200A (en) | Device for automatically detecting spool displacement of electromagnetic valve with high precision and method thereof | |
| CN102928424A (en) | Method and detection kit for detecting cervical fluid heme | |
| CN203376334U (en) | Automatic feeding device capable of automatically metering volume and mixing uniformly | |
| CN205593999U (en) | Water quality monitoring device | |
| Xie et al. | An efficient method for determining the acid value in edible oils by solvent-assisted headspace gas chromatography | |
| CN103901219B (en) | Suspension type gravimetric titrimetry device | |
| CN103293175A (en) | Method for measuring chemical components of liquid sodium silicate | |
| CN203572799U (en) | Device for quickly measuring content of hydrogen peroxide in hydrogen peroxide solution | |
| CN103512974B (en) | Method for rapidly determining contents of aureomycin for feed and impurities of aureomycin by HPLC | |
| CN105092306A (en) | Automatic sampling device and automatic sampling method | |
| CN104931521B (en) | Ternary system fluid mutual solubility assay method and its measurement system | |
| CN110716060A (en) | Novel material element detection and analysis system | |
| US8936765B2 (en) | Automatic analyzer | |
| CN206710192U (en) | A kind of seal wire performance comprehensive testing machine | |
| CN205280742U (en) | A spiral proportioning device for quick moisture meter | |
| CN106483037A (en) | A kind of device of real-time measurement rock water absorption | |
| CN104297295A (en) | Method for determining content of hydrogen peroxide in impurity-containing hydrogen peroxide solution | |
| CN204705534U (en) | A kind of material vestige tester | |
| CN202284938U (en) | Automatic thickness tester |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161109 |
|
| WD01 | Invention patent application deemed withdrawn after publication |