CN106093029A - A kind of methylene blue clay determinator - Google Patents
A kind of methylene blue clay determinator Download PDFInfo
- Publication number
- CN106093029A CN106093029A CN201610608452.7A CN201610608452A CN106093029A CN 106093029 A CN106093029 A CN 106093029A CN 201610608452 A CN201610608452 A CN 201610608452A CN 106093029 A CN106093029 A CN 106093029A
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- Prior art keywords
- beaker
- burette
- determinator
- motor
- methylene blue
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
- G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
- G01N21/78—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour
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- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Plasma & Fusion (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)
Abstract
A kind of methylene blue clay determinator, including sample processing device, experimental determination device and control device, described sample processing device is ultrasonic disperse device；Described experimental determination device includes beaker, motor, burette and solution bottle, described beaker is placed in beaker torr, described beaker top arranges motor, for stirring the solution in beaker, described burette is placed in solution bottle top, titration piston is set between described burette and beaker, in the middle part of described burette, connects rubber bulbs,double by trachea；Described control device is connected with motor and ultrasonic disperse device, for controlling motor and the operation of ultrasonic disperse device.A kind of methylene blue clay determinator that the present invention provides uses ultra-sonic dispersion method, coordinates automatic burette and mechanical stirring device, can realize the mensuration of effective bentonite content in bentonite Absorbance ratio-derivative method and molding sand the most fast and accurately.
Description
Technical field
The present invention relates to a kind of clay determinator, be specifically related to a kind of methylene blue clay determinator.
Background technology
At present, in bentonite Absorbance ratio-derivative method and molding sand, the mensuration/detection of effective bentonite content is the most easy with some
Detecting instrument is produced error by manual operation titrimetry, such processing ease, it addition, system colors is stimulated by the eyes of people
Change insensitive, often result in last titrate the analysis result and differentiate unclear, make the data result accuracy detected relatively low, Er Qiejian
Survey process is time-consuming, laborious, and have large-scale, save time, detector laborsaving, standard expensive, the instrument that some are small-sized is added
Factory is not suitable for.
Summary of the invention
Not enough for prior art, the invention provides a kind of analysis and detect accurately for bentonite Absorbance ratio-derivative method and molding sand
In the determinator of effective bentonite content.
The present invention solves the technical scheme of above-mentioned technical problem employing: a kind of methylene blue clay determinator, including
Sample processing device, experimental determination device and control device, it is characterised in that: described sample processing device is ultrasonic disperse dress
Put；Described experimental determination device includes that beaker, motor, burette and solution bottle, described beaker are placed in beaker torr, described beaker
Top arranges motor, and for stirring the solution in beaker, described burette is placed in solution bottle top, described burette and beaker it
Between titration piston is set, in the middle part of described burette by trachea connect rubber bulbs,double；Described control device and motor and ultrasonic
Dispersal device is connected, for controlling motor and the operation of ultrasonic disperse device.
Further, described control device arranges digital time relay, timing reset switch, timing controller, choosing
Select switch and display lamp, for timing controlled motor and the operation of ultrasonic disperse device.
Further, the frequency of described ultrasonic disperse device is 40 ± 2KHz, and power is 50W.
Further, the content of described burette is 50mL.
Further, the timing controlled scope of described timing controller is 0-15min.
In clay, bentonite has the strongest absorbability to methylene blue dye.This device uses burette test method, measures
During sample Absorbance ratio-derivative method, process clay initially with ultrasonic disperse device, measure Absorbance ratio-derivative method and use titrimetry, and cooperative mechanical stirring
Make clay sample and methylene blue be fully contacted and carry out adsorption reaction.Whether free dye occurs according to in sample suspension,
Judge whether clay reaches saturated absorption, measure the Absorbance ratio-derivative method of the samples such as clay with this.
Compared with prior art, what the present invention possessed has the beneficial effect that
A kind of methylene blue clay determinator that the present invention provides uses ultra-sonic dispersion method, coordinates automatic burette and machine
Tool agitating device, can realize the mensuration of effective bentonite content in bentonite Absorbance ratio-derivative method and molding sand the most fast and accurately.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention.
Detailed description of the invention
The present invention is described further below in conjunction with the accompanying drawings.
A kind of methylene blue clay determinator as shown in Figure 1, including sample processing device, experimental determination device and control
Device processed, it is characterised in that: described sample processing device is ultrasonic disperse device 12；Described experimental determination device include beaker 6,
Motor 7, burette 8 and solution bottle 10, described beaker 6 is placed in beaker torr 5, and described beaker 6 top arranges motor 7, is used for stirring
Mixing the solution in beaker 6, described burette 8 is placed in solution bottle 10 top, arranges titration and live between described burette 8 and beaker 6
Plug 9, connects rubber bulbs,double 11 by trachea in the middle part of described burette 8；Described control device and motor 7 and ultrasonic disperse device
12 are connected, for controlling motor 7 and the operation of ultrasonic disperse device 12.
Further, described control device is arranged digital time relay 1, timing reset switch 2, timing controller 3,
Select switch 13 and display lamp 4, for timing controlled motor 7 and the operation of ultrasonic disperse device 12.
Further, the frequency of described ultrasonic disperse device 12 is 40 ± 2KHz, and power is 50W.
Further, the content of described burette 8 is 50mL.
Further, the timing controlled scope of described timing controller 3 is 0-15min.
In clay, bentonite has the strongest absorbability to methylene blue dye.This device uses burette test method, measures
During sample Absorbance ratio-derivative method, process clay initially with ultrasonic disperse device, measure Absorbance ratio-derivative method and use titrimetry, and cooperative mechanical stirring
Make clay sample and methylene blue be fully contacted and carry out adsorption reaction.Whether free dye occurs according to in sample suspension,
Judge whether clay reaches saturated absorption, measure the Absorbance ratio-derivative method of the samples such as clay with this.A kind of methylene that the present invention provides
Blue clay determinator can realize the survey of effective bentonite content in bentonite Absorbance ratio-derivative method and molding sand the most fast and accurately
Fixed.
Claims (5)
1. a methylene blue clay determinator, including sample processing device, experimental determination device and control device, its feature
It is: described sample processing device is ultrasonic disperse device；Described experimental determination device includes beaker, motor, burette and molten
Liquid bottle, described beaker is placed in beaker torr, and described beaker top arranges motor, for stirring the solution in beaker, described titration
Pipe is placed in solution bottle top, arranges titration piston, connected by trachea in the middle part of described burette between described burette and beaker
Rubber bulbs,double；Described control device is connected with motor and ultrasonic disperse device, for controlling motor and ultrasonic disperse device
Run.
A kind of methylene blue clay determinator the most according to claim 1, it is characterised in that: set on described control device
Put digital time relay, timing reset switch, timing controller, selection switch and display lamp, for timing controlled motor and
The operation of ultrasonic disperse device.
A kind of methylene blue clay determinator the most according to claim 1, it is characterised in that: described ultrasonic disperse device
Frequency be 40 ± 2KHz, power is 50W.
A kind of methylene blue clay determinator the most according to claim 1, it is characterised in that: the content of described burette
For 50mL.
A kind of methylene blue clay determinator the most according to claim 2, it is characterised in that: described timing controller
Timing controlled scope is 0-15min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610608452.7A CN106093029A (en) | 2016-07-29 | 2016-07-29 | A kind of methylene blue clay determinator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610608452.7A CN106093029A (en) | 2016-07-29 | 2016-07-29 | A kind of methylene blue clay determinator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106093029A true CN106093029A (en) | 2016-11-09 |
Family
ID=57478444
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610608452.7A Pending CN106093029A (en) | 2016-07-29 | 2016-07-29 | A kind of methylene blue clay determinator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106093029A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110487675A (en) * | 2019-08-29 | 2019-11-22 | 新疆中泰纺织集团有限公司 | The method of viscose ripening degree detection device and detection viscose ripening degree |
| WO2020163971A1 (en) * | 2019-02-14 | 2020-08-20 | The Saskatchewan Research Council | Automated on-line active clay analyzer in mineral slurries |
| CN114924028A (en) * | 2022-04-29 | 2022-08-19 | 马鞍山钢铁股份有限公司 | Method for determining binder distribution uniformity in iron ore concentrate |
Citations (7)
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| JP2003048000A (en) * | 2001-08-07 | 2003-02-18 | Kurita Water Ind Ltd | Treatment method for water-containing mud |
| JP2005006510A (en) * | 2003-06-16 | 2005-01-13 | Mizusawa Ind Chem Ltd | Silica-magnesia-based preparation excellent in base adsorptivity, and method for producing the same |
| CN201266193Y (en) * | 2008-09-27 | 2009-07-01 | 辽宁工程技术大学 | Automatic analysis detector for alta-mud blue suction quantity |
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| CN101806747A (en) * | 2010-03-05 | 2010-08-18 | 华中科技大学 | Methylene blue adsorption testing method of bentonite |
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| CN202947971U (en) * | 2012-12-07 | 2013-05-22 | 阜新市金地矿业有限公司 | Manual analyzing and detecting device for blue absorption power of bentonite |
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2016
- 2016-07-29 CN CN201610608452.7A patent/CN106093029A/en active Pending
Patent Citations (7)
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| JP2003048000A (en) * | 2001-08-07 | 2003-02-18 | Kurita Water Ind Ltd | Treatment method for water-containing mud |
| JP2005006510A (en) * | 2003-06-16 | 2005-01-13 | Mizusawa Ind Chem Ltd | Silica-magnesia-based preparation excellent in base adsorptivity, and method for producing the same |
| CN201266193Y (en) * | 2008-09-27 | 2009-07-01 | 辽宁工程技术大学 | Automatic analysis detector for alta-mud blue suction quantity |
| CN101493451A (en) * | 2008-09-27 | 2009-07-29 | 辽宁工程技术大学 | Automatic analysis and detection instrument for bentonite blue suction quantity and detection method thereof |
| CN101806747A (en) * | 2010-03-05 | 2010-08-18 | 华中科技大学 | Methylene blue adsorption testing method of bentonite |
| CN201788154U (en) * | 2010-03-05 | 2011-04-06 | 华中科技大学 | Bentonite methylene blue absorption amount testing device |
| CN202947971U (en) * | 2012-12-07 | 2013-05-22 | 阜新市金地矿业有限公司 | Manual analyzing and detecting device for blue absorption power of bentonite |
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| 余笃武等: "《铸造测试仪器的原理及应用》", 30 June 1990, 机械工业出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020163971A1 (en) * | 2019-02-14 | 2020-08-20 | The Saskatchewan Research Council | Automated on-line active clay analyzer in mineral slurries |
| CN110487675A (en) * | 2019-08-29 | 2019-11-22 | 新疆中泰纺织集团有限公司 | The method of viscose ripening degree detection device and detection viscose ripening degree |
| CN114924028A (en) * | 2022-04-29 | 2022-08-19 | 马鞍山钢铁股份有限公司 | Method for determining binder distribution uniformity in iron ore concentrate |
| CN114924028B (en) * | 2022-04-29 | 2024-04-26 | 马鞍山钢铁股份有限公司 | Method for measuring binder distribution uniformity in iron ore concentrate |
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Application publication date: 20161109 |