CN106092792A - A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test - Google Patents

A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test Download PDF

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CN106092792A
CN106092792A CN201610580048.3A CN201610580048A CN106092792A CN 106092792 A CN106092792 A CN 106092792A CN 201610580048 A CN201610580048 A CN 201610580048A CN 106092792 A CN106092792 A CN 106092792A
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environment
fatigue test
pipe
liquid tank
horn
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刘永杰
杨昆
王清远
李久楷
何超
王聪
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Sichuan University
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Sichuan University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/32Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces
    • G01N3/34Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces generated by mechanical means, e.g. hammer blows
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N17/00Investigating resistance of materials to the weather, to corrosion, or to light
    • G01N17/006Investigating resistance of materials to the weather, to corrosion, or to light of metals
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/0069Fatigue, creep, strain-stress relations or elastic constants
    • G01N2203/0073Fatigue

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  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
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  • Biodiversity & Conservation Biology (AREA)
  • Ecology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Environmental Sciences (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention discloses a kind of physiological environment analog being applied to ultrasonic accelerated fatigue test, the environment pipe of simulated body fluid it is full of including horn and inside, described horn one end is placed in environment pipe, wherein, one end that horn is placed in environment pipe connects part to be measured, and the other end can be connected with ultrasonic accelerated fatigue test device.This device is by simulation human physiological environment, it is possible to accurately test out metal implant material Fatigue Life in Very High Cycle in human body environment.

Description

A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test
Technical field
The invention belongs to fatigue rig field, relate to a kind of ultrasonic accelerated fatigue test equipment, be related specifically to A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test.
Background technology
Metal implant stays in the body for a long time the most throughout one's life, human body when carrying out normal physiological activity, metal implant Mechanical behavior inherently dynamic, and the pulsating stress effect of higher cycle can be experienced, such as hip joint is wanted every year Experience about 3.5 × 106Secondary pulsating stress, heart to beat about 4 × 10 every year7Secondary, tooth implant to bear about 1 × 10 every year7 Secondary Cyclic Load.It addition, implant is in physiological environment, by the chemical attack of human body fluid, cause corrosion fatigue. The common effect of chemical attack and circulation machinery load is the main cause causing and implanting prosthese early fracture.Therefore, it is thus achieved that gold Genus embedded material Fatigue Life in Very High Cycle under physiological environment can be the design of embedded material and guarantees the reliable of embedded material Property, safety and to being estimated in implant under arms physiological environment and biometry provides favourable scientific basis and pass Key technology is supported.
The most conventional loading frequency for the fatigue test system of biomaterial test is below 100Hz, realize 108Super high cycle fatigue test more than cycle, according to traditional 20Hz electo hydraulic servocontrolled fatigue testing machine, tests 1 sample big About need 2 months, and use supersonic vibration accelerated fatigue test device, then have only to 1.4 hours, experiment can be greatly shortened In the cycle, reduce experimental cost.
Existing supersonic vibration accelerated fatigue test device can only test metal implant material in ordinary atmosphere Fatigue Life in Very High Cycle, and the Fatigue Life in Very High Cycle of metal implant in human body environment cannot be tested, therefore test out The Fatigue Life in Very High Cycle accuracy of metal implant is the highest, and reference value is relatively low, limits entering of metal implant material technology One step development.
Summary of the invention
In order to solve the problems referred to above, the present invention discloses a kind of physiological environment simulation dress being applied to ultrasonic accelerated fatigue test Putting, this device is by simulation human physiological environment, it is possible to accurately test out metal implant material Very High Cycle in human body environment Fatigue behaviour.
The technical problem to be solved realizes by the following technical solutions:
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test, is full of simulated body fluid including horn and inside Environment pipe, described horn one end is placed in environment pipe, and wherein, one end that horn is placed in environment pipe connects part to be measured, The other end can be connected with ultrasonic accelerated fatigue test device.
Described environment pipe is U-tube, is provided with lid in one end that environment pipe is connected with horn, and the other end is provided with pipe Plug, described horn is fixed in lid and one end is through lid, and described environment pipe is additionally provided with inlet and leakage fluid dram.Make Environment pipe is in sealing state, it is to avoid impurity or the interference of gas, is beneficial to the more real human body environment of simulation.
Described inlet connects a delivery tube one, and leakage fluid dram connects a delivery tube two, and described delivery tube one connects one Individual water pump, delivery tube two connects a reserving liquid tank, and water pump is connected by delivery tube three with reserving liquid tank, described water pump also with one Flow speed controller is connected.Flow speed controller for regulation and coutroi velocity, make in environment pipe the flowing of simulated body fluid closer to The flowing of human body fluid, promotes the accuracy of test, avoids, because simulated body fluid flow velocity is excessive, part to be measured is caused an earnest simultaneously Reason impact, changes its motion mode, and interference test causes test result to produce deviation.
It is fixed with an automatic constant-temperature-heating rod on described reserving liquid tank, fixes near the side of water pump at reserving liquid tank upper surface One thermometer, this thermometer lower end is placed in reserving liquid tank, is used for observing liquid storage the temperature inside the box.
Described automatic constant-temperature-heating rod includes the thermal treatment zone and control zone, and control zone is placed in reserving liquid tank top, passes through control zone Can realize the setting to heating-up temperature and regulation, the described thermal treatment zone is placed in reserving liquid tank through reserving liquid tank outer wall, and heating-up temperature is 20~50 DEG C, preferably 36~37 DEG C, degree of regulation is ± 0.5 DEG C.
Described lid is connected by screw with horn, and environment pipe is connected with lid by screw thread.
Described delivery tube one, delivery tube two and delivery tube three are managed for PEX, and simulated body fluid will not be caused dirt by safety and environmental protection Contaminate and affect the accuracy of test.
It is equipped with steam vent on described pipe close and lid, in described steam vent, is provided with matched sealing-plug.Steam vent Be provided with and beneficially simulated body fluid be filled in environment pipe, after being full of simulated body fluid in environment pipe, utilize sealing-plug sealing ring Border is managed, it is to avoid simulated body fluid is by air pollution, and simulates the closed environment of real human body, promotes the accuracy of test.
All the time, for the test of metal implant Fatigue Life in Very High Cycle, directly test is all used in atmosphere to treat Survey the Fatigue Life in Very High Cycle of part, also have the test of only a few after being soaked in normal saline by part to be measured, to be placed in air survey again Examination, the result of test has greater difference with the fatigue behaviour in human body of actual metal implant, therefore, it is difficult to Accurate Prediction Metal implant is service life in human body, and the reference value of the selection for manufacturing and designing metal implant is relatively low, seriously Hinder the research and development of Artificial Intervention material.
Present invention applicant is for the purpose of raising metal implant fatigue property test accuracy, and devising one can Apply to the physiological environment analog of ultrasonic accelerated fatigue test, different from the past directly part to be measured is placed in air ambient Test, also different from part to be measured is soaked in re-test after normal saline, the part to be measured in the application can be placed in circulation all the time The simulated body fluid of flowing tests its Fatigue Life in Very High Cycle, owing to the many kinds of substance in human body fluid all can part to be measured to metal Causing chemical attack, this is a long-term and complex interaction process, and is not only the effect of Na+ and Cl-, utilizes this Physiological environment analog in application can effectively simulate the interior environment close to human body fluid, makes part to be measured be placed in one also Test its Fatigue Life in Very High Cycle, the fatigue behaviour of the metal implant that the result measured is more nearly in real human body and longevity Life.There is the highest reference value, the further research and development of metal implant material technology can be effectively facilitated.
The application of a kind of physiological environment analog being applied to ultrasonic accelerated fatigue test, comprises the steps:
(1) horn is connected with ultrasonic accelerated fatigue test device, then part to be measured is fixed in horn, described to be measured Part is Ti6Al7Nb alloy or Ti6Al4V alloy or TAMZ alloy or other metal materials, recycling pipe close and with horn Lid sealed environment pipe;
(2) environment pipe is connected with reserving liquid tank and water pump, sets the heating-up temperature of automatic constant-temperature-heating rod on reserving liquid tank, treat After reserving liquid tank temperature reaches setting value, set the flow velocity of flow speed controller, start water pump, make the simulated body fluid in reserving liquid tank fill Full whole environment pipe;
(3) start ultrasonic accelerated fatigue test device, test the part to be measured Fatigue Life in Very High Cycle in simulated body fluid environment.
The present invention compared with prior art, has such advantages as and beneficial effect:
(1) by arranging environment pipe and horn, part to be measured is enable to test its super high cycle fatigue in simulated body fluid environment Can, the result of test, closer to metal implant fatigue life in human body, has higher reference value, promotees further Enter the development of metal implant material technology;
(2) by arranging reserving liquid tank and water pump, enable simulated body fluid to circulate, maintain the ion in environment pipe to be in balance State, more meets the interior environment of human body, improves the accuracy of test result;
(3) by arranging automatic constant-temperature-heating rod, make simulated body fluid maintain body temperature state, promote test result further Accuracy.
Accompanying drawing explanation
Accompanying drawing described herein is used for providing being further appreciated by the embodiment of the present invention, constitutes of the application Point, it is not intended that the restriction to the embodiment of the present invention.In the accompanying drawings:
Fig. 1 is present configuration schematic diagram;
Fig. 2 is the embodiment of the present invention 1 test result schematic diagram;
Fig. 3 is the embodiment of the present invention 2 test result schematic diagram;
The parts title of labelling and correspondence in accompanying drawing:
1-horn, 2-environment pipe, 21-lid, 22-pipe close, 23-inlet, 24-leakage fluid dram, 3-part to be measured, 4-delivery tube One, 5-delivery tube two, 6-water pump, 7-reserving liquid tank, 71-automatic constant-temperature-heating rod, 72-thermometer, the 73-thermal treatment zone, 74-controls District, 8-delivery tube three, 9-flow speed controller, 10-steam vent.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearer, below in conjunction with embodiment and accompanying drawing, to this Invention is described in further detail, and the exemplary embodiment of the present invention and explanation thereof are only used for explaining the present invention, do not make For limitation of the invention.
Embodiment 1
As it is shown in figure 1, a kind of physiological environment analog being applied to ultrasonic accelerated fatigue test, including horn 1 and inside Being full of the environment pipe 2 of simulated body fluid, described horn 1 one end is placed in environment pipe 2, and wherein, horn 1 is placed in environment pipe 2 One end connect part 3 to be measured, the other end can be connected with ultrasonic accelerated fatigue test device.
Described environment pipe 2 is U-tube, is provided with lid 21 with horn 1 in one end that environment pipe 2 is connected, and the other end is arranged There are pipe close 22, described horn 1 to be fixed in lid 21 and one end is through lid 21, described environment pipe 2 is additionally provided with feed liquor Mouth 23 and leakage fluid dram 24.
Described inlet 23 connects a delivery tube 1, and leakage fluid dram 24 connects a delivery tube 25, described delivery tube 1 Connecting a water pump 6, delivery tube 25 connects a reserving liquid tank 7, and water pump 6 is connected by delivery tube 38 with reserving liquid tank 7, described Water pump 6 is also connected with a flow speed controller 9.
An automatic constant-temperature-heating rod 71 it is fixed with, at reserving liquid tank 7 upper surface near the one of water pump 6 on described reserving liquid tank 7 A thermometer 72 is fixed in side, and this thermometer 72 lower end is placed in reserving liquid tank 7.
Described automatic constant-temperature-heating rod 71 includes the thermal treatment zone 73 and control zone 74, and control zone 74 is placed in reserving liquid tank 7 top, logical Crossing control zone 74 and can realize the setting to heating-up temperature and regulation, the described thermal treatment zone 73 is placed in reserving liquid tank 7 through reserving liquid tank 7 outer wall In, heating-up temperature is 20~50 DEG C, preferably 36~37 DEG C, and degree of regulation is ± 0.5 DEG C.
Described lid 21 is connected by screw with horn 1, and environment pipe 2 is connected with lid 21 by screw thread.
Described delivery tube 1, delivery tube 25 and delivery tube 38 are managed for PEX.
It is equipped with steam vent 10 on described pipe close 22 and lid 21, in described steam vent 10, is provided with matched sealing Plug.
The application of a kind of physiological environment analog being applied to ultrasonic accelerated fatigue test, comprises the steps:
(1) horn is connected with ultrasonic accelerated fatigue test device, then part to be measured is fixed in horn, the present embodiment The part to be measured used is Ti6Al7Nb alloy or Ti6Al4V alloy, recycling pipe close and the lid sealed environment with horn Pipe;
(2) environment pipe is connected with reserving liquid tank and water pump, sets the heating-up temperature of automatic constant-temperature-heating rod on reserving liquid tank, this It is 37 DEG C that embodiment arranges heating-up temperature, after reserving liquid tank temperature reaches setting value, sets the flow velocity of flow speed controller, starts Water pump, makes the simulated body fluid in reserving liquid tank be full of whole environment pipe;
(3) start ultrasonic accelerated fatigue test device, test the part to be measured Fatigue Life in Very High Cycle in simulated body fluid environment.
The main component such as following table of step (2) described simulated body fluid:
Ion Na<sup>+</sup> K<sup>+</sup> Ca<sup>2+</sup> Mg<sup>2+</sup> HCO<sup>3-</sup> Cl<sup>-</sup> HPO4<sup>3-</sup> SO4<sup>2-</sup>
Simulated body fluid (Mmol/L) 142.0 5.0 2.5 1.5 4.2 148.5 1.0 0.5
Substantial amounts of Ti6Al7Nb alloy or Ti6Al4V alloy are the most each soaked by the present embodiment to be put at air ambient and simulated body fluid In environment, after ultrasonic accelerated fatigue test, record the Fatigue Life in Very High Cycle of each part to be measured, and draw out Ti6Al7Nb accordingly The S-N curve of matching in the most each comfortable air ambient and simulated body fluid environment distinguished by alloy and Ti6Al4V alloy.
Test result is as in figure 2 it is shown, Fig. 2 is specially Ti6Al7Nb alloy and the most each comfortable air of Ti6Al4V alloy S-N curve in environment and simulated body fluid environment, represent respectively stress in each comfortable air ambient and simulated body fluid environment with The curve of relation between fatigue life.
Wherein, l1For Ti6Al4V alloy S-N curve in air ambient, l2For Ti6Al4V alloy at analogue body pendular ring S-N curve in border, l3For Ti6Al7Nb alloy S-N curve in air ambient, l4For Ti6Al7Nb alloy at simulated body fluid S-N curve in environment, the vertical curve at abscissa 108 is scale line, is used for contrasting different materials in identical or different experiment Under environment, part to be measured reaches to specify fatigue strength during cycle that is 108 time, can intuitively and effectively contrast different materials of the same race Fatigue Life in Very High Cycle under environment, provides foundation and reference for selection when making metal implant.
From test result, Ti6Al4V alloy Fatigue Life in Very High Cycle in simulated body fluid environment is substantially less than it Fatigue Life in Very High Cycle in air ambient, Ti6Al7Nb alloy Fatigue Life in Very High Cycle in simulated body fluid environment is notable Less than its Fatigue Life in Very High Cycle in air ambient, this is due to Ti6Al4V alloy and Ti6Al7Nb alloy in atmosphere The most only acted on by circulation machinery load, and in simulated body fluid environment, Ti6Al4V alloy and Ti6Al7Nb alloy are not only Acted on by circulation machinery load, also by the chemical attack effect of simulated body fluid, accelerate its fatigue rupture, be therefore placed in mould Intend the metal part to be measured that the Fatigue Life in Very High Cycle of the metal part to be measured in fluid environment is substantially less than placed in air ambient.
S-N curve l2For having the broken line of a bending, occur that the place of bending is that fatigue rupture presents different mechanism Demarcation line.Owing to titanium alloy itself has stronger corrosion resistance, surface easily generates oxide-film, when Ti6Al4V alloy is placed in sky In compression ring border, its surface film oxide is not destroyed, so the Fatigue Life in Very High Cycle of titanium alloy is not affected, thus its S-N Curve l1For straight line.But when it is placed in simulated body fluid environment, due to the effect of mechanical load, may result in oxidation Film destroys, and material is acted on mechanical load by chemical attack simultaneously, causes tired just because of the interaction between them Labor performance significantly reduces, and occurs that the reason of flex point is because when load is reduced to certain value, and oxide-film becomes to be less susceptible to brokenly Bad, and along with the further reduction of load, the destructiveness of oxide-film is more and more lower, the metal material of oxide-film internal protection The chemical attack being subject to is more and more weak, thus the fatigue life of part to be measured is compared to just increasing before flex point, occurs in that approximation water Flat straightway.On the other hand, owing to oxide-film becomes increasingly difficult to destroy, simulated body fluid is to part super high cycle fatigue to be measured The impact of energy is more and more less, it is therefore envisaged, when load drops to of a sufficiently low, if oxide-film can not destroy completely, to be measured Part Fatigue Life in Very High Cycle in simulated body fluid is consistent with the result recorded in air ambient the most at last, l from Fig. 11And l2 The trend that will be intersected in any is measurable.
Embodiment 2
As it is shown in figure 1, a kind of physiological environment analog being applied to ultrasonic accelerated fatigue test, including horn 1 and inside Being full of the environment pipe 2 of simulated body fluid, described horn 1 one end is placed in environment pipe 2, and wherein, horn 1 is placed in environment pipe 2 One end connect part 3 to be measured, the other end can be connected with ultrasonic accelerated fatigue test device.
Described environment pipe 2 is U-tube, is provided with lid 21 with horn 1 in one end that environment pipe 2 is connected, and the other end is arranged There are pipe close 22, described horn 1 to be fixed in lid 21 and one end is through lid 21, described environment pipe 2 is additionally provided with feed liquor Mouth 23 and leakage fluid dram 24.
Described inlet 23 connects a delivery tube 1, and leakage fluid dram 24 connects a delivery tube 25, described delivery tube 1 Connecting a water pump 6, delivery tube 25 connects a reserving liquid tank 7, and water pump 6 is connected by delivery tube 38 with reserving liquid tank 7, described Water pump 6 is also connected with a flow speed controller 9.
An automatic constant-temperature-heating rod 71 it is fixed with, at reserving liquid tank 7 upper surface near the one of water pump 6 on described reserving liquid tank 7 A thermometer 72 is fixed in side, and this thermometer 72 lower end is placed in reserving liquid tank 7.
Described automatic constant-temperature-heating rod 71 includes the thermal treatment zone 73 and control zone 74, and control zone 74 is placed in reserving liquid tank 7 top, logical Crossing control zone 74 and can realize the setting to heating-up temperature and regulation, the described thermal treatment zone 73 is placed in reserving liquid tank 7 through reserving liquid tank 7 outer wall In, heating-up temperature is 20~50 DEG C, preferably 36~37 DEG C, and degree of regulation is ± 0.5 DEG C.
Described lid 21 is connected by screw with horn 1, and environment pipe 2 is connected with lid 21 by screw thread.
Described delivery tube 1, delivery tube 25 and delivery tube 38 are managed for PEX.
It is equipped with steam vent 10 on described pipe close 22 and lid 21, in described steam vent 10, is provided with matched sealing Plug.
The application of a kind of physiological environment analog being applied to ultrasonic accelerated fatigue test, comprises the steps:
(1) horn is connected with ultrasonic accelerated fatigue test device, then part to be measured is fixed in horn, described to be measured Part is Ti6Al7Nb alloy or Ti6Al4V alloy or TAMZ alloy, recycling pipe close and the lid sealed environment with horn Pipe;
(2) environment pipe is connected with reserving liquid tank and water pump, sets the heating-up temperature of automatic constant-temperature-heating rod on reserving liquid tank, this It is 36 DEG C that embodiment arranges heating-up temperature, after reserving liquid tank temperature reaches setting value, sets the flow velocity of flow speed controller, starts Water pump, makes the simulated body fluid in reserving liquid tank be full of whole environment pipe;
(3) start ultrasonic accelerated fatigue test device, test the part to be measured Fatigue Life in Very High Cycle in simulated body fluid environment.
The main component of described simulated body fluid such as following table:
Ion Na<sup>+</sup> K<sup>+</sup> Ca<sup>2+</sup> Mg<sup>2+</sup> HCO<sup>3-</sup> Cl<sup>-</sup> HPO4<sup>3-</sup> SO4<sup>2-</sup>
Simulated body fluid (Mmol/L) 142.0 5.0 2.5 1.5 4.2 148.5 1.0 0.5
Substantial amounts of TAMZ alloy is soaked by the present embodiment respectively to be put in air ambient and simulated body fluid environment, accelerates fatigue through ultrasonic After test, record the Fatigue Life in Very High Cycle of each part to be measured, and draw out TAMZ alloy accordingly at air ambient and simulated body fluid The S-N curve of matching in environment.
Test result as it is shown on figure 3, Fig. 3 be specially TAMZ alloy respectively in air ambient and simulated body fluid environment S-N curve, represents TAMZ alloy test specimen stress in air ambient and simulated body fluid environment respectively and closes between fatigue life The curve of system.
Wherein, l5For TAMZ alloy S-N curve in air ambient, l6For TAMZ alloy in simulated body fluid environment S-N curve, abscissa 2 × 108The vertical curve at place is scale line, is used for contrasting different materials in identical or different experimental situation Under, part to be measured reaches to specify cycle that is 2 × 108Fatigue strength time secondary, can intuitively and effectively contrast different materials of the same race Fatigue Life in Very High Cycle under environment, provides foundation and reference for selection when making metal implant.
From test result, TAMZ alloy Fatigue Life in Very High Cycle in simulated body fluid environment is substantially less than it at sky Fatigue Life in Very High Cycle in compression ring border, this is owing to TAMZ alloy is the most only made by circulation machinery load in atmosphere With, and in simulated body fluid environment, TAMZ alloy is not only acted on by circulation machinery load, also by the chemistry of simulated body fluid Corrosiveness, accelerates its fatigue rupture, and the Fatigue Life in Very High Cycle of the metal part to be measured being therefore placed in simulated body fluid environment shows Write less than the metal part to be measured being placed in air ambient.
S-N curve l6For having the broken line of a bending, occur that the place of bending is that fatigue rupture presents different mechanism Demarcation line.Owing to TAMZ alloy itself has stronger corrosion resistance, surface easily generates oxide-film, when TAMZ alloy is placed in air In environment, its surface film oxide is not destroyed, so the Fatigue Life in Very High Cycle of TAMZ alloy is not affected, thus its S-N Curve l5For straight line.But when it is placed in simulated body fluid environment, due to the effect of mechanical load, may result in oxidation Film destroys, and material is acted on mechanical load by chemical attack simultaneously, causes tired just because of the interaction between them Labor performance significantly reduces, and occurs that the reason of flex point is because when load is reduced to certain value, and oxide-film becomes to be less susceptible to brokenly Bad, and along with the further reduction of load, the destructiveness of oxide-film is more and more lower, the metal material of oxide-film internal protection The chemical attack being subject to is more and more weak, thus the fatigue life of part to be measured is compared to just increasing before flex point, occurs in that approximation water Flat straightway.On the other hand, owing to oxide-film becomes increasingly difficult to destroy, simulated body fluid is to part super high cycle fatigue to be measured The impact of energy is more and more less, it is therefore envisaged, when load drops to of a sufficiently low, if oxide-film can not destroy completely, to be measured Part Fatigue Life in Very High Cycle in simulated body fluid is consistent with the result recorded in air ambient the most at last, l from Fig. 35And l6 The trend that will be intersected in any is measurable.
In sum, the physiological environment analog in the present invention is used in ultrasonic accelerated fatigue test, Ke Yi great The big accuracy improving metal implant Fatigue Life in Very High Cycle test in human body, the Very High Cycle promoting metal implant is tired The reference value of labor performance test, it is possible to effectively facilitate the further development of metal implant material technology.
Above-described detailed description of the invention, has been carried out the purpose of the present invention, technical scheme and beneficial effect further Describe in detail, be it should be understood that the detailed description of the invention that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. done, all should comprise Within protection scope of the present invention.

Claims (10)

1. the physiological environment analog being applied to ultrasonic accelerated fatigue test, it is characterised in that: include horn and ring Border is managed, and described horn one end is placed in environment pipe.
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 1, its feature It is: described environment pipe is U-tube, is provided with lid in one end that environment pipe is connected with horn, and the other end is provided with pipe close, institute State horn one end through lid.
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 1 and 2, it is special Levy and be: on described environment pipe, be additionally provided with inlet and leakage fluid dram.
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 3, its feature Being: described inlet connects a delivery tube one, leakage fluid dram connects a delivery tube two, and described delivery tube one connects a water Pump, delivery tube two connects a reserving liquid tank, and water pump is connected by delivery tube three with reserving liquid tank.
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 4, its feature It is: be fixed with an automatic constant-temperature-heating rod on described reserving liquid tank, fix one at reserving liquid tank upper surface near the side of water pump Individual thermometer, this thermometer lower end is placed in reserving liquid tank.
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 5, its feature It is: the heating-up temperature of described automatic constant-temperature-heating rod is 20~50 DEG C, and degree of regulation is ± 0.5 ° of C.
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 5, its feature It is: described water pump is also connected with a flow speed controller.
A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 7, its feature It is: on described pipe close and lid, be equipped with steam vent, in described steam vent, is provided with matched sealing-plug.
9. a kind of physiological environment simulation dress being applied to ultrasonic accelerated fatigue test as according to any one of claim 1~8 The application put, it is characterised in that comprise the steps:
(1) horn is connected with ultrasonic accelerated fatigue test device, then part to be measured is fixed in horn, recycling pipe Plug and the lid sealed environment pipe with horn;
(2) environment pipe is connected with reserving liquid tank and water pump, sets the heating-up temperature of automatic constant-temperature-heating rod on reserving liquid tank, treat After reserving liquid tank temperature reaches setting value, set the flow velocity of flow speed controller, start water pump, make the simulated body fluid in reserving liquid tank fill Full whole environment pipe;
(3) start ultrasonic accelerated fatigue test device, test the part to be measured Fatigue Life in Very High Cycle in simulated body fluid environment.
The application of a kind of physiological environment analog being applied to ultrasonic accelerated fatigue test the most according to claim 9, It is characterized in that: described part to be measured is Ti6Al7Nb alloy or Ti6Al4V alloy or TAMZ alloy or other metal materials.
CN201610580048.3A 2016-07-22 2016-07-22 A kind of physiological environment analog being applied to ultrasonic accelerated fatigue test Pending CN106092792A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109549665A (en) * 2018-11-15 2019-04-02 青岛海信医疗设备股份有限公司 A kind of ultrasonic device detection system

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN200972450Y (en) * 2006-10-26 2007-11-07 中国船舶重工集团公司第七二五研究所 Salt air corrosion faigue test device
JP4817253B2 (en) * 2005-12-01 2011-11-16 独立行政法人物質・材料研究機構 Material testing equipment and material specimens
CN103308444A (en) * 2013-06-28 2013-09-18 重庆理工大学 Device for detecting service life of bone implantation metal and service life of metal material with coating layer
CN203745426U (en) * 2014-04-02 2014-07-30 四川大学 Ultra-long life corrosion fatigue experiment device adopting ultrasonically accelerated vibration
JP2014163779A (en) * 2013-02-25 2014-09-08 Yoshiharu Maruyama Environment resistance test method
CN205981950U (en) * 2016-07-22 2017-02-22 四川大学 Be applied to experimental physiology environmental simulation device of supersound accelerated fatigue

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4817253B2 (en) * 2005-12-01 2011-11-16 独立行政法人物質・材料研究機構 Material testing equipment and material specimens
CN200972450Y (en) * 2006-10-26 2007-11-07 中国船舶重工集团公司第七二五研究所 Salt air corrosion faigue test device
JP2014163779A (en) * 2013-02-25 2014-09-08 Yoshiharu Maruyama Environment resistance test method
CN103308444A (en) * 2013-06-28 2013-09-18 重庆理工大学 Device for detecting service life of bone implantation metal and service life of metal material with coating layer
CN203745426U (en) * 2014-04-02 2014-07-30 四川大学 Ultra-long life corrosion fatigue experiment device adopting ultrasonically accelerated vibration
CN205981950U (en) * 2016-07-22 2017-02-22 四川大学 Be applied to experimental physiology environmental simulation device of supersound accelerated fatigue

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
ASTM: "Standard Practice for Corrosion Fatigue Testing of Metallic Implant Materials", 《ASTM F1801-97(2004)》 *
M. PAPAKYRIACOU等: "Effects of surface treatments on high cycle corrosion fatigue of metallic implant materials", 《INTERNATIONAL JOURNAL OF FATIGUE》 *
曹小建等: "生理盐水浸泡对Ti-6Al-4V钛合金超高周疲劳性能的影响", 《西南科技大学学报》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109549665A (en) * 2018-11-15 2019-04-02 青岛海信医疗设备股份有限公司 A kind of ultrasonic device detection system
CN109549665B (en) * 2018-11-15 2021-06-22 青岛海信医疗设备股份有限公司 Ultrasonic equipment detection system

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