CN106084900A - A kind of preparation method of good dispersibility aluminum pigment - Google Patents
A kind of preparation method of good dispersibility aluminum pigment Download PDFInfo
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- CN106084900A CN106084900A CN201610469775.2A CN201610469775A CN106084900A CN 106084900 A CN106084900 A CN 106084900A CN 201610469775 A CN201610469775 A CN 201610469775A CN 106084900 A CN106084900 A CN 106084900A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/62—Metallic pigments or fillers
- C09C1/64—Aluminium
- C09C1/648—Aluminium treated with inorganic and organic, e.g. polymeric, compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses the preparation method of a kind of good dispersibility aluminum pigment, belong to aluminum pigment preparing technical field.The present invention takes the honed sieve of compost stalk grinding and sodium hydroxide solution mixing heating in water bath, centrifugal collection supernatant, after regulation pH, mixing heating in water bath with acrylamide etc., drip sodium hydroxide solution, filter cake is filtered to obtain in insulation, with dehydrated alcohol mixing ultrasonic disperse after washing freezing, mix heating in water bath again with aluminium powder etc., sucking filtration obtains filter cake, and washing is dried and prepares good dispersibility aluminum pigment.The invention has the beneficial effects as follows: preparation process of the present invention is simple, products obtained therefrom good hydrophilic property, during water paint uses, soilless sticking phenomenon occurs；Good with the Organic substance compatibility, long-time placement occurs without deposit clumps phenomenon.
Description
Technical field
The present invention relates to the preparation method of a kind of good dispersibility aluminum pigment, belong to aluminum pigment preparing technical field.
Background technology
Aluminum pigment is also called aluminium powder pigment, refers to have flakey particle structure and bright metallic luster and other face
The metallic aluminium powder (also referred to as aluminum argentum powder) of material characteristic or aluminum paste (also referred to as aluminum paste), it is a weight in metallic pigments
Want kind, be mainly used in the production of the products such as coating, printing-ink, plastic material, and in automobile, consumption electronic product, family
The fields such as electrical appliance, construction material, printing-ink, instrument and equipment, boats and ships, aircraft, plastic material and weaving obtain extensively application.
Major part aluminum pigment belongs to effect pigment category, can produce effect in its application system (such as film).Aluminum pigment
Mainly have powder (aluminum argentum powder) and slurry (aluminum paste) two kinds of forms, in addition with flake aluminum with Tissuemat E for mainly becoming
Point granule (strip or pellet) concentrate, it belongs to high-performance effect pigment, and its granule scale shape has flakes, Semen Maydis
Lamellar and silver dollar shape etc., feature is that aluminum flake surface is smooth, and particle size distribution is concentrated, regular shape, has the luminous reflectance of excellence
Ability and metallic luster, be used alone or be used in mixed way in coating with transparent coloured pigments, can make paint film produce significantly with
The heterochromatic effect in angle, decorative effect is the most magnificent and attractive in appearance.But owing to aluminum particle is smaller, specific surface area big, table in aluminum pigment
Face hydrophilic is poor, easily occurs agglomeration, most of aluminium powders not to can be uniformly dispersed in water during water paint uses,
With Organic substance poor compatibility, long-time placement there will be deposit clumps phenomenon.
Summary of the invention
The technical problem to be solved: in aluminum pigment owing to aluminum particle is smaller, specific surface area is big, table
Face hydrophilic is poor, during water paint uses, agglomeration easily occurs, with Organic substance poor compatibility, places meeting for a long time
The drawback of deposit clumps phenomenon occurs, it is provided that one takes the honed sieve of compost stalk grinding and adds with sodium hydroxide solution mixing water-bath
Heat, centrifugal supernatant of collecting, after regulation pH, mix heating in water bath with acrylamide etc., drip sodium hydroxide solution, insulation is filtered
Obtaining filter cake, with dehydrated alcohol mixing ultrasonic disperse after washing freezing, then mix heating in water bath with aluminium powder etc., sucking filtration obtains filter cake, washes
Wash and be dried the method preparing good dispersibility aluminum pigment.Preparation process of the present invention is simple, and products obtained therefrom good hydrophilic property, at water paint
During use, soilless sticking phenomenon occurs, and efficiently solves and Organic substance poor compatibility, and long-time placement there will be deposit clumps
Problem.
For solving above-mentioned technical problem, the present invention uses the technical scheme as described below to be:
(1) choose compost straw, it is naturally dried and mills and sieves, be prepared into 70～80 mesh compost stalk particles, by quality
Ratio 1:10, mixes compost stalk particle with the stirring of mass concentration 30% sodium hydroxide solution, is placed in there-necked flask, to it
Logical nitrogen gets rid of air, subsequently at nitrogen atmosphere, heating in water bath 6～8h at 65～80 DEG C；
(2) to be heated complete after, stop heating and be placed in centrifugation 10～15min under 1200～1500r/min, collect upper strata
Clear liquid also regulates pH to 8.0 with 1mol/L hydrochloric acid solution, is prepared into sodium humate solution, counts by weight, weighs 45 respectively
～50 parts of sodium humate solutions, 5～10 parts of acrylamides, 3～5 parts of N, N '-methylene-bisacrylamides, 2～3 parts of Ammonium persulfate .s
Being placed in there-necked flask, stirring mixing is placed in heating in water bath 1～2h at 65～80 DEG C；
(3) after heating in water bath completes, its logical nitrogen being got rid of air, dropping mass concentration 30% sodium hydroxide solution is extremely subsequently
In there-necked flask, regulation pH to 8.5 after, Heat preservation 1～2h at 65～70 DEG C, to be heated complete after, filter and collect filter
Cake, after being washed with deionized 3～5 times, then processes 3～5h to its vacuum freezing, is prepared into modified xerogels；
(4) 1:5 in mass ratio, mixes the modified xerogels of above-mentioned preparation with absolute ethyl alcohol and stirring, ultrasonic under 200～300W
Dispersion processes 10～15min, is prepared into gel dispersion liquid, counts the most by weight, weighs 55～60 parts of gel dispersion respectively
Liquid, 20～25 parts of aluminium powders and 35～40 parts of mass concentration 10% ammonia spirits in there-necked flask, heating in water bath at 65～80 DEG C
After 2～3h, vacuum filtration also collects filter cake, is washed with deionized pH to 7.0, and vacuum lyophilization 6～8h is also milled,
It is prepared into a kind of good dispersibility aluminum pigment.
The application process of the present invention: the good dispersibility aluminum pigment present invention prepared adds to water paint, addition
It is 22～33g/kg, after being uniformly mixed.This aluminum pigment good dispersion in water paint, soilless sticking during use
Phenomenon occurs, and long-time placement occurs without deposit clumps phenomenon, is worthy to be popularized and uses.
The present invention is compared with additive method, and Advantageous Effects is:
(1) preparation process of the present invention is simple, products obtained therefrom good hydrophilic property, and during water paint uses, soilless sticking phenomenon is sent out
Raw；
(2) good with the Organic substance compatibility, long-time placement occurs without deposit clumps phenomenon.
Detailed description of the invention
First choose compost straw, it is naturally dried and mills and sieves, be prepared into 70～80 mesh compost stalk particles, press
Mass ratio 1:10, mixes compost stalk particle with the stirring of mass concentration 30% sodium hydroxide solution, is placed in there-necked flask,
Its logical nitrogen is got rid of air, subsequently at nitrogen atmosphere, heating in water bath 6～8h at 65～80 DEG C；To be heated complete after, stop adding
Heat is placed in centrifugation 10～15min under 1200～1500r/min, collects the supernatant and regulates with 1mol/L hydrochloric acid solution
PH to 8.0, is prepared into sodium humate solution, counts by weight, weigh respectively 45～50 parts of sodium humate solutions, 5～10 parts
Acrylamide, 3～5 parts of N, N '-methylene-bisacrylamides, 2～3 parts of Ammonium persulfate .s are placed in there-necked flask, and stirring mixing is also
It is placed in heating in water bath 1～2h at 65～80 DEG C；Then, after heating in water bath completes, its logical nitrogen is got rid of air, drips subsequently
Mass concentration 30% sodium hydroxide solution is in there-necked flask, after regulation pH to 8.5, and Heat preservation 1～2h at 65～70 DEG C,
To be heated complete after, filter and collect filter cake, after being washed with deionized 3～5 times, then to its vacuum freezing process 3～5h, system
For obtaining modified xerogels；Last 1:5 in mass ratio, mixes the modified xerogels of above-mentioned preparation with absolute ethyl alcohol and stirring, 200
～under 300W ultrasonic disperse process 10～15min, be prepared into gel dispersion liquid, count the most by weight, respectively weigh 55～
60 parts of gel dispersion liquid, 20～25 parts of aluminium powders and 35～40 parts of mass concentration 10% ammonia spirits are in there-necked flask, 65～80
At DEG C after heating in water bath 2～3h, vacuum filtration also collects filter cake, is washed with deionized pH to 7.0, vacuum lyophilization 6～
8h also mills, and can be prepared into a kind of good dispersibility aluminum pigment.
Example 1
First choose compost straw, it is naturally dried and mills and sieves, be prepared into 70 mesh compost stalk particles, in mass ratio 1:
10, compost stalk particle is mixed with the stirring of mass concentration 30% sodium hydroxide solution, is placed in there-necked flask, to its logical nitrogen
Gas gets rid of air, subsequently at nitrogen atmosphere, heating in water bath 6h at 65 DEG C；To be heated complete after, stop heating being placed in 1200r/
Centrifugation 10min under min, collects the supernatant and regulates pH to 8.0 with 1mol/L hydrochloric acid solution, being prepared into sodium humate molten
Liquid, counts by weight, weighs 45 parts of sodium humate solutions, 5 parts of acrylamides, 3 parts of N, N '-methylene bisacrylamide acyls respectively
Amine, 2 parts of Ammonium persulfate .s are placed in there-necked flask, and stirring mixing is placed in heating in water bath 1h at 65 DEG C；Then treat that heating in water bath is complete
Cheng Hou, gets rid of air to its logical nitrogen, and dropping mass concentration 30% sodium hydroxide solution is in there-necked flask subsequently, and regulation pH is extremely
After 8.5, Heat preservation 1h at 65 DEG C, to be heated complete after, filter and collect filter cake, after being washed with deionized 3 times more right
Its vacuum freezing processes 3h, is prepared into modified xerogels；Last 1:5 in mass ratio, by modified xerogels and the nothing of above-mentioned preparation
Water-ethanol stirring mixing, under 200W, ultrasonic disperse processes 10min, is prepared into gel dispersion liquid, counts the most by weight, point
55 parts of gel dispersion liquid of another name amount, 20 parts of aluminium powders and 35 parts of mass concentration 10% ammonia spirits in there-necked flask, water at 65 DEG C
After bath heating 2h, vacuum filtration also collects filter cake, is washed with deionized pH to 7.0, vacuum lyophilization 6h and also mills,
It is prepared into a kind of good dispersibility aluminum pigment.
The good dispersibility aluminum pigment present invention prepared adds to water paint, and addition is 22g/kg, stirring mixing
After Jun Yun.This aluminum pigment good dispersion in water paint, during use, soilless sticking phenomenon occurs, and places nothing for a long time
Deposit clumps phenomenon occurs, is worthy to be popularized and uses.
Example 2
First choose compost straw, it is naturally dried and mills and sieves, be prepared into 75 mesh compost stalk particles, in mass ratio 1:
10, compost stalk particle is mixed with the stirring of mass concentration 30% sodium hydroxide solution, is placed in there-necked flask, to its logical nitrogen
Gas gets rid of air, subsequently at nitrogen atmosphere, heating in water bath 7h at 72 DEG C；To be heated complete after, stop heating being placed in 1350r/
Centrifugation 13min under min, collects the supernatant and regulates pH to 8.0 with 1mol/L hydrochloric acid solution, being prepared into sodium humate molten
Liquid, counts by weight, weighs 48 parts of sodium humate solutions, 8 parts of acrylamides, 4 parts of N, N '-methylene bisacrylamide acyls respectively
Amine, 3 parts of Ammonium persulfate .s are placed in there-necked flask, and stirring mixing is placed in heating in water bath 2h at 72 DEG C；Then treat that heating in water bath is complete
Cheng Hou, gets rid of air to its logical nitrogen, and dropping mass concentration 30% sodium hydroxide solution is in there-necked flask subsequently, and regulation pH is extremely
After 8.5, Heat preservation 2h at 68 DEG C, to be heated complete after, filter and collect filter cake, after being washed with deionized 4 times more right
Its vacuum freezing processes 4h, is prepared into modified xerogels；Last 1:5 in mass ratio, by modified xerogels and the nothing of above-mentioned preparation
Water-ethanol stirring mixing, under 250W, ultrasonic disperse processes 13min, is prepared into gel dispersion liquid, counts the most by weight, point
58 parts of gel dispersion liquid of another name amount, 23 parts of aluminium powders and 38 parts of mass concentration 10% ammonia spirits in there-necked flask, water at 72 DEG C
After bath heating 3h, vacuum filtration also collects filter cake, is washed with deionized pH to 7.0, vacuum lyophilization 7h and also mills,
It is prepared into a kind of good dispersibility aluminum pigment.
The good dispersibility aluminum pigment present invention prepared adds to water paint, and addition is 28g/kg, stirring mixing
After Jun Yun.This aluminum pigment good dispersion in water paint, during use, soilless sticking phenomenon occurs, and places nothing for a long time
Deposit clumps phenomenon occurs, is worthy to be popularized and uses.
Example 3
First choose compost straw, it is naturally dried and mills and sieves, be prepared into 80 mesh compost stalk particles, in mass ratio 1:
10, compost stalk particle is mixed with the stirring of mass concentration 30% sodium hydroxide solution, is placed in there-necked flask, to its logical nitrogen
Gas gets rid of air, subsequently at nitrogen atmosphere, heating in water bath 8h at 80 DEG C；To be heated complete after, stop heating being placed in 1500r/
Centrifugation 15min under min, collects the supernatant and regulates pH to 8.0 with 1mol/L hydrochloric acid solution, being prepared into sodium humate molten
Liquid, counts by weight, weighs 50 parts of sodium humate solutions, 10 parts of acrylamides, 5 parts of N, N '-methylene bisacrylamide acyls respectively
Amine, 3 parts of Ammonium persulfate .s are placed in there-necked flask, and stirring mixing is placed in heating in water bath 2h at 80 DEG C；Then treat that heating in water bath is complete
Cheng Hou, gets rid of air to its logical nitrogen, and dropping mass concentration 30% sodium hydroxide solution is in there-necked flask subsequently, and regulation pH is extremely
After 8.5, Heat preservation 2h at 70 DEG C, to be heated complete after, filter and collect filter cake, after being washed with deionized 5 times more right
Its vacuum freezing processes 5h, is prepared into modified xerogels；Last 1:5 in mass ratio, by modified xerogels and the nothing of above-mentioned preparation
Water-ethanol stirring mixing, under 300W, ultrasonic disperse processes 15min, is prepared into gel dispersion liquid, counts the most by weight, point
60 parts of gel dispersion liquid of another name amount, 25 parts of aluminium powders and 40 parts of mass concentration 10% ammonia spirits in there-necked flask, water at 80 DEG C
After bath heating 3h, vacuum filtration also collects filter cake, is washed with deionized pH to 7.0, vacuum lyophilization 8h and also mills,
It is prepared into a kind of good dispersibility aluminum pigment.
The good dispersibility aluminum pigment present invention prepared adds to water paint, and addition is 33g/kg, stirring mixing
After Jun Yun.This aluminum pigment good dispersion in water paint, during use, soilless sticking phenomenon occurs, and places nothing for a long time
Deposit clumps phenomenon occurs, is worthy to be popularized and uses.
Claims (1)
1. the preparation method of a good dispersibility aluminum pigment, it is characterised in that concrete preparation process is:
(1) choose compost straw, it is naturally dried and mills and sieves, be prepared into 70～80 mesh compost stalk particles, by quality
Ratio 1:10, mixes compost stalk particle with the stirring of mass concentration 30% sodium hydroxide solution, is placed in there-necked flask, to it
Logical nitrogen gets rid of air, subsequently at nitrogen atmosphere, heating in water bath 6～8h at 65～80 DEG C；
(2) to be heated complete after, stop heating and be placed in centrifugation 10～15min under 1200～1500r/min, collect upper strata
Clear liquid also regulates pH to 8.0 with 1mol/L hydrochloric acid solution, is prepared into sodium humate solution, counts by weight, weighs 45 respectively
～50 parts of sodium humate solutions, 5～10 parts of acrylamides, 3～5 parts of N, N '-methylene-bisacrylamides, 2～3 parts of Ammonium persulfate .s
Being placed in there-necked flask, stirring mixing is placed in heating in water bath 1～2h at 65～80 DEG C；
(3) after heating in water bath completes, its logical nitrogen being got rid of air, dropping mass concentration 30% sodium hydroxide solution is extremely subsequently
In there-necked flask, regulation pH to 8.5 after, Heat preservation 1～2h at 65～70 DEG C, to be heated complete after, filter and collect filter
Cake, after being washed with deionized 3～5 times, then processes 3～5h to its vacuum freezing, is prepared into modified xerogels；
(4) 1:5 in mass ratio, mixes the modified xerogels of above-mentioned preparation with absolute ethyl alcohol and stirring, ultrasonic under 200～300W
Dispersion processes 10～15min, is prepared into gel dispersion liquid, counts the most by weight, weighs 55～60 parts of gel dispersion respectively
Liquid, 20～25 parts of aluminium powders and 35～40 parts of mass concentration 10% ammonia spirits in there-necked flask, heating in water bath at 65～80 DEG C
After 2～3h, vacuum filtration also collects filter cake, is washed with deionized pH to 7.0, and vacuum lyophilization 6～8h is also milled,
It is prepared into a kind of good dispersibility aluminum pigment.
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| CN201610469775.2A CN106084900A (en) | 2016-06-26 | 2016-06-26 | A kind of preparation method of good dispersibility aluminum pigment |
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| CN201610469775.2A CN106084900A (en) | 2016-06-26 | 2016-06-26 | A kind of preparation method of good dispersibility aluminum pigment |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115820004A (en) * | 2022-12-21 | 2023-03-21 | 长沙族兴新材料股份有限公司 | PH response type water-based aluminum paste and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102604443A (en) * | 2012-02-15 | 2012-07-25 | 合肥旭阳铝颜料有限公司 | Preparation method of water-based high flash aluminum pigment for automobiles |
| CN103289493A (en) * | 2013-05-10 | 2013-09-11 | 舒城瑞宇涂料有限公司 | Preparation method of high-scrub-resistant water-based paint |
| CN103819947A (en) * | 2012-08-07 | 2014-05-28 | 江苏伊特复合新材料有限公司 | Preparation method of high-insulation aqueous aluminum paste |
-
2016
- 2016-06-26 CN CN201610469775.2A patent/CN106084900A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102604443A (en) * | 2012-02-15 | 2012-07-25 | 合肥旭阳铝颜料有限公司 | Preparation method of water-based high flash aluminum pigment for automobiles |
| CN103819947A (en) * | 2012-08-07 | 2014-05-28 | 江苏伊特复合新材料有限公司 | Preparation method of high-insulation aqueous aluminum paste |
| CN103289493A (en) * | 2013-05-10 | 2013-09-11 | 舒城瑞宇涂料有限公司 | Preparation method of high-scrub-resistant water-based paint |
Non-Patent Citations (1)
| Title |
|---|
| 生金峰: "腐植酸钠/丙烯酰胺接枝共聚物的合成与性能研究", 《东北石油大学硕士研究生学位论文》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115820004A (en) * | 2022-12-21 | 2023-03-21 | 长沙族兴新材料股份有限公司 | PH response type water-based aluminum paste and preparation method thereof |
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