CN106083220A - A kind of big tree nutritional solution compositing acid solution and processing technology thereof - Google Patents
A kind of big tree nutritional solution compositing acid solution and processing technology thereof Download PDFInfo
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Abstract
nullThe invention provides the present invention and a kind of big tree nutritional solution compositing acid solution and processing technology thereof are provided，Wherein，Big tree nutritional solution compositing acid solution includes following component in terms of mass parts: 1000 parts of deionized waters、0.20～0.30 part of tyrosine、4.80～5.00 parts of leucines、3.48～3.56 parts of isoleucine、3.50～3.70 parts of valines、2.21～2.29 parts of methionines、1.92～2.08 parts of alanine、5.23～5.43 parts of phenylalanine、0.71～0.79 part of glutamic acid、2.42～2.58 parts of Aspartic Acids、4.22～4.36 parts of lysine acetate、2.42～2.58 parts of threonine、7.54～7.66 parts of glycine、0.90～1.10 part of proline、0.90～1.10 part of serine、4.82～5.12 parts of arginine hydrochloride、2.41～2.62 parts of histidine monohydrochlorides、0.82～0.98 part of tryptophan and 0.007～0.012 part of cystine.Beneficial effects of the present invention: this aminoacids complex meets the growth demand of underfed big tree, the compositing acid solution sample that stability is higher has been obtained, it is to avoid a large amount of losses of the supplementary material of compositing acid solution in manufacturing process by the manufacturing process arranging this compositing acid solution.
Description
Technical field
The present invention relates to set greatly nutritional solution field, be specifically related to a kind of big tree nutritional solution compositing acid solution and system thereof
Make technique.
Background technology
Set greatly nutritional solution, be also big tree garter liquid, big tree Pig liquid.Along with people for fine, afforest, purify, sweetening treatment institute
Living environment, anti-season will transplant a lot of greening-trees every year in city, but the transplanting of big tree can make its root system sustain damage, and leads
Cause the indifferent of Root Absorption moisture and nutrient, add the evaporation of leaves portion of water, it is easy to make the trees just transplanted
Withered death, so beating this direct mode of transfusion bottle with big tree nutritional solution supplement the nutrients to trees to trees is good side
Method.
It is known that aminoacids complex is of many uses, human body, with strengthening immune function of human body, strengthens alimentation
Deng, and agriculturally can do concentration fertilizer, liquid fertilizer raw material, make an addition to fermented bean cake etc..Chinese patent discloses a kind of Shen
Please publication No. be the tree nutrient solution of CN 103641559 A, this nutritional solution includes: carbamide 35%, amino acid/11 5%, ammonium nitrate
20%, trace element 10%, potassium dihydrogen phosphate 10%, zinc sulfate 10%.Make although this nutritional solution discloses use aminoacid
For component, but the problem that this patent exists is: 1) amino acid whose of a great variety, then in order to adapt to the growth demand set greatly,
Various amino acid whose content are how many, and this patent is also not disclosed, it is impossible to realize；2) the most undisclosed how making of this patent is stablized
The aminoacid that property is good, also can being problem to be solved with longer-term storage.
Summary of the invention
For the deficiency in the presence of prior art, the invention provides a kind of big tree nutritional solution compositing acid solution
And processing technology, this aminoacids complex meets the growth demand of underfed big tree, molten by arranging this aminoacids complex
The manufacturing process of liquid obtained the compositing acid solution sample that stability is higher, it is to avoid aminoacids complex in manufacturing process
A large amount of losses of the supplementary material of solution.
For achieving the above object, present invention employs following technical scheme:
The present invention provides a kind of big tree nutritional solution compositing acid solution, it is characterised in that include following with mass parts
The component of meter:
1000 parts of deionized waters, 0.20～0.30 part of tyrosine, 4.80～5.00 parts of leucines, 3.48～3.56 parts different bright
Propylhomoserin, 3.50～3.70 parts of valines, 2.21～2.29 parts of methionines, 1.92～2.08 parts of alanine, 5.23～5.43 parts
Phenylalanine, 0.71～0.79 part of glutamic acid, 2.42～2.58 parts of Aspartic Acids, 4.22～4.36 parts of lysine acetate, 2.42
～2.58 parts of threonine, 7.54～7.66 parts of glycine, 0.90～1.10 part of proline, 0.90～1.10 part of serine, 4.82
～5.12 parts of arginine hydrochloride, 2.41～2.62 parts of histidine monohydrochlorides, 0.82～0.98 part of tryptophan and 0.07～0.12 part
Cystine.
Preferably, big tree nutritional solution compositing acid solution includes following component in terms of mass parts:
1000 parts of deionized waters, 0.25 part of tyrosine, 4.90 parts of leucines, 3.52 parts of isoleucine, 3.60 parts of valines,
2.25 parts of methionines, 2.00 parts of alanine, 5.33 parts of phenylalanine, 0.75 part of glutamic acid, 2.50 parts of Aspartic Acids, 4.30 parts
Lysine acetate, 2.50 parts of threonine, 7.60 parts of glycine, 1.00 parts of proline, 1.00 parts of serines, 5.00 parts of hydrochloric acid essence ammonia
Acid, 2.50 parts of histidine monohydrochlorides, 0.90 part of tryptophan and 0.1 part of cystine.
The present invention also provides for the processing technology of above-mentioned big tree nutritional solution compositing acid solution, comprises the following steps:
Add deionized water: according to compositing acid solution formula and the deionized water of the preset vol of compositing acid solution
Demand, toward preparation tank add demand deionized water；
To deionized water pretreatment: nitrogen charging limit, deionization waterside is heated；
Mixing deionized water and various aminoacid: after nitrogen charging 15 minutes, record according to compositing acid solution formula
Various aminoacid are put in deionized water by various amount of amino acid that every liter of water need to add successively, molten to obtain aminoacids complex
Liquid；
Moisturizing for the first time: after whole aminoacid dissolve, to the default body of moisturizing in preparation tank to compositing acid solution
Long-pending；
Regulation pH value: add glacial acetic acid in compositing acid solution, to regulate pH value to 7.2-7.4；
Desolventing technology: putting into activated carbon, quality of activated carbon is 0.04% with the ratio of the preset vol of compositing acid solution；
Preliminary filter: make the compositing acid solution containing activated carbon through 5 μm titanium core filters, compound tentatively to filter out
Activated carbon in Freamine Ⅲ, leaches the compositing acid solution after activated carbon and is recycled in preparation tank by titanium core filter；
Nitrogen filled protection: under the conditions of the temperature of compositing acid solution is 45-50 DEG C, to the compositing acid solution prepared
Nitrogen charging；
Moisturizing for the second time: to the preset vol of moisturizing in preparation tank to compositing acid solution；
Filter further: make the compositing acid solution containing activated carbon through 5 μm titanium core filters, to filter out further
Activated carbon in compositing acid solution, the compositing acid solution leaching activated carbon is recycled in preparation tank by titanium core filter.
Preferably, in mixing deionized water and various aminoacid step, various aminoacid are put into deionization successively
In water, add gauge with various aminoacid in every liter of deionized water, particularly as follows:
In 95 DEG C of deionized waters, put into 0.25 part of tyrosine, leucine 4.90 parts, isoleucine 3.52 parts, valine
3.60 parts and methionine 2.25 parts；
When deionized water is cooled to 70 DEG C, put into alanine 2.00 parts, phenylalanine 5.33 parts, 0.75 part of glutamic acid with
And Aspartic Acid 2.50 parts；
When deionized water is cooled to 65 DEG C, put into lysine acetate 4.30 parts, threonine 2.50 parts, glycine 7.60
Part, proline 1.00 parts, serine 1.00 parts and arginine hydrochloride 5.00 parts；
When deionized water is cooled to 60 DEG C, put into histidine monohydrochloride 2.50 parts, tryptophan 0.90 part and cystine 0.1
Part.
Preferably, also need to prepare front preparation before adding deionized water, comprising: supplementary material prepares, by compound ammonia
Base acid solution formula weighs each aminoacid；Glass bottle cleans, to obtain needing the clean glass bottle of quantity；Rubber plug cleaning, to obtain
Need the clean plug of quantity；Aluminium lid cleans, to obtain needing the clean aluminium lid of quantity；And preparation tank cleans, to obtain
Need to have and clean dense join cylinder, pipeline, filter and dilute preparation tank joining cylinder.
Preferably, supplementary material preparation concrete operations include: get each aminoacid according to compositing acid solution formula, respectively
The amino acid whose amount of weighing is: except tryptophan weighs by the 105% of compositing acid solution formula record amount, and other are all in accordance with compound
Freamine Ⅲ formula record amount weighs.
Preferably, glass bottle cleaning concrete operations include: get the glass bottle of specification quantity as desired, first, with drinking
Water cleans the glass bottle that visual inspection outward appearance is qualified；Then, it is the purified water of 40-65 DEG C by temperature in ultrasonic washing unit, with to glass
Bottle is slightly washed；Subsequently, glass bottle is rinsed outer 1 time and interior 2 times with the pure water after slightly washing in ultrasonic washing unit；After again, use
New purified water rinses glass bottle outer 1 time and interior 2 times；Finally, the temperature after filtering with 0.45 μm polypropylene filter is 40-65 DEG C
Deionized water rinsing glass bottle inside and outside the most once.
Preferably, rubber plug cleaning concrete operations include: get the butyl rubber plug of requirement as desired, take φ every time
It is not to be exceeded 22000 during 26 type plug, when taking φ 32 type plug, is not to be exceeded 7000, first, roll flushing 5 by purified water
Minute；Then, with ultrasonic washing unit, plug is rolled cleaning 5 minutes, and rinse 15 minutes；Finally, at ultrasonic washing unit
Interior use deionized water rolls rinsing 5 minutes to plug, and this cleaning drains the remaining water in ultrasonic washing unit after completing, clearly
Washed plug is airtight to be deposited, and should again clean more than 8 hours.
Preferably, preparation tank cleans concrete operations and includes: first, adds deionized water 20-30 ten thousand ml and joins in cylinder to dense, then
Add sodium sulfite 150 parts, disodiumedetate (EDTA-2Na) 100 parts, be then turned on pump so that dense join cylinder in go from
Sub-water, sodium sulfite and disodiumedetate circulate 4 minutes, so that sodium sulfite and ethylenediaminetetraacetic acid two
Sodium is substantially dissolved in deionized water formation bottoming water；Then, use bottoming water rinse all pipelines of preparation tank, filter,
Pill tank and dilute join cylinder, subsequently enters dilute bottoming water joined in cylinder and cleans the fill structure of preparation tank, in last fill structure
Bottoming water through backflow pump dilute floor drain joining cylinder, to get rid of bottoming water；Finally, respectively distribution pipes dense, dilute is entered with activated carbon
Row bottoming processes, and makes the inner surface of titanium core filter form stable layer of charcoal, removes sodium sulfite and the second two of residual simultaneously
Amine tetraacethyl disodium.
Preferably, also needing to carry out canning operation after filtering further, canning operation includes:
Bottling operation: first pass through and compositing acid solution is sent in the fitting configuration in preparation tank, then will join
Compositing acid solution in assembling structure loads in glass bottle；Nitrogen charging evacuation plays plug: first empty glass bottle is carried out nitrogen charging；So
After, the compositing acid solution prepared is encased in glass bottle；After again, the glass bottle equipped with compositing acid solution is carried out
Nitrogen charging in airtight chamber；After again, the glass bottle equipped with compositing acid solution is carried out evacuation；After again, to equipped with compounded amino
The glass bottle of acid solution carries out playing plug, beats after plug completes and obtains semi-finished product；Finally, remaining oxygen in sampling observation glass bottle random to semi-finished product,
Under the semi-finished product entrance that remaining oxygen sampling observation is qualified, workshop section carries out rolling lid；And
Rolling lid, the qualified semi-finished product of remaining oxygen sampling observation, through vibration cover blanking machine upper cover, after cover lifter gland, rotate by bottle
Roll lid, roll the big tree nutritional solution compositing acid solution being finished product after covering lattice.
Compared to prior art, there is advantages that
Amino acid whose kind has multiple, and various amino acid whose function is different, specifically:
Glycine: increase the crops absorption to phosphorus potassium element；Improve stress resistance of plant；Growth particularly light to plant
Cooperation is with having unique facilitation, and it can increase chlorophyll content of plant, improves the activity of enzyme, promotes carbon dioxide
Infiltration, makes photosynthesis more vigorous, and to improving crop quality, the content increasing Vc and sugar suffers from important function；
Leucine: plant growth promoter；Crops are had peculiar photosynthesis and regulation effect；
Methionine: prevent the infringement of root fungus, kills many parasitic pathogenic bacterias；
Tyrosine: regulate and control the tip of a root, the maintenance of root cells in plant；
Alanine: resist and eliminate the effect of crops pathogenic bacteria；
Tryptophan: resist and eliminate the effect of crops pathogenic bacteria；Tryptophan, through decarboxylation, deamination, oxidation, generates indole second
Acid, the Endogenous auxin generally existed in plant；
Cystine: resist and eliminate the effect of crops pathogenic bacteria；
Lysine: crops are had peculiar photosynthesis and regulation effect；
Aspartic acid: the content of nitrate in reduction plant；
Phenylalanine: involved in plant disease resistance response；
Proline: under plant drouhgt stress, can cause osmotic pressure to decline；Play an important role at development of plants, with plant
Stage of development, organ type relevant；
Serine: involved in plant is old and feeble；Lignified synthesis；Germinate；Cell tissue is broken up；Programmed cell death；Letter
Number conduction；Protein degradation and processing；Suppression plant growing；
Glutamic acid: glutamic acid effect in light respiration nitrogen metabolism；The content of nitrate in reduction plant；To crops
There are peculiar photosynthesis and regulation effect；
Arginine: there is the function of storage nitrogen element nutrition；Generating the precursor substances such as PA and NO, involved in plant growth is sent out
Educate, the physiology process such as resistance.
Therefore the various aminoacid of rational allocation, with composition big tree nutritional solution aminoacids complex, it is possible to improve malnutrition and plant
The growth of thing so that it is trend is flourished.
The aminoacids complex that manufacturing process by arranging this compositing acid solution has obtained stability higher simultaneously is molten
Liquid sample, it is to avoid a large amount of losses of the supplementary material of compositing acid solution in manufacturing process.
Detailed description of the invention
The present invention provides a kind of big tree nutritional solution compositing acid solution, including following component in terms of mass parts:
1000 parts of deionized waters, 0.20～0.30 part of tyrosine, 4.80～5.00 parts of leucines, 3.48～3.56 parts different bright
Propylhomoserin, 3.50～3.70 parts of valines, 2.21～2.29 parts of methionines, 1.92～2.08 parts of alanine, 5.23～5.43 parts
Phenylalanine, 0.71～0.79 part of glutamic acid, 2.42～2.58 parts of Aspartic Acids, 4.22～4.36 parts of lysine acetate, 2.42
～2.58 parts of threonine, 7.54～7.66 parts of glycine, 0.90～1.10 part of proline, 0.90～1.10 part of serine, 4.82
～5.12 parts of arginine hydrochloride, 2.41～2.62 parts of histidine monohydrochlorides, 0.82～0.98 part of tryptophan and 0.07～0.12 part
Cystine.
Embodiment 1 to embodiment 3:
As shown in the table, each amino acid whose component that the compositing acid solution of embodiment 1 to embodiment 3 uses is different,
And each aminoacid is in terms of mass parts:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Deionized water | 1000 parts | 1000 parts | 1000 parts |
| Tyrosine | 0.20 part | 0.25 part | 0.30 part |
| Leucine | 4.80 part | 4.9 part | 5.00 part |
| Isoleucine | 3.48 part | 3.52 part | 3.56 part |
| Valine | 3.50 part | 3.60 part | 3.70 part |
| Methionine | 2.21 part | 2.25 part | 2.29 part |
| And propylhomoserin | 1.92 part | 2.00 part | 2.08 part |
| Phenylalanine | 5.23 part | 5.33 part | 5.43 part |
| Glutamic acid | 0.71 part | 0.75 part | 0.79 part |
| Aspartic Acid | 2.42 part | 2.50 part | 2.58 part |
| Lysine acetate | 4.22 part | 4.30 part | 4.36 part |
| Threonine | 2.42 part | 2.50 part | 2.58 part |
| Glycine | 7.54 part | 7.60 part | 7.66 part |
| Proline | 0.90 part | 1.00 part | 1.10 part |
| Serine | 0.91 part | 1.00 part | 1.10 part |
| Arginine hydrochloride | 4.82 part | 5.00 part | 5.12 part |
| Histidine monohydrochloride | 2.41 part | 2.50 part | 2.62 part |
| Tryptophan | 0.82 part | 0.90 part | 0.98 part |
| Cystine | 0.07 part | 0.10 part | 0.12 part |
By upper table it is recognised that the various amino acid whose component that uses of embodiment 1 is less, the various ammonia that embodiment 2 uses
The component of base acid is in medium, and the various amino acid whose component that embodiment 3 uses is most.
Use embodiment 1, embodiment 2 and embodiment 3 respectively with 12 Lignum cinnamomi camphoraes be randomly divided into three groups as subjects,
The situation of all Lignum cinnamomi camphoraes is: age of tree 10-20；After within 10 years, transplanting, growing way is bad for successive years；Young leaves is sprouted less and presents not
Healthy yellow.Use the big tree nutritional solution containing embodiment 1, embodiment 2 and embodiment 3 compositing acid solution to three groups
Lignum cinnamomi camphorae is infused, three kinds of big tree nutritional solutions in addition to compositing acid solution is different, other trace element and a great number of elements one
Sample, early Febuary uses then, and late May observes the situation of these 8 trees.Experiment effect contrast is as follows:
Embodiment 1 is compared with the big tree nutritional solution that embodiment 2 uses, in the complex amino acid aqueous solution that embodiment 1 uses
Various amino acid whose content on the low side, the leaves of acetonideexample 2 all change into health green, trunk surface has also sprouted one
The sprouting that sample is many, and the length of sprouting is longer, but the sprouting amount that embodiment 1 is sprouted is less, although leaf color and face before
Form and aspect are greener, but the color of leaves is more yellow compared with embodiment 2, and conclusion is: the only compositing acid solution of embodiment 2
In various amino acid whose content all meet the demand of the big tree of malnutrition, but each in the compositing acid solution of embodiment 1
Plant amino acid whose content on the low side, it is impossible to meet the demand of the big tree of malnutrition；
Embodiment 2 is compared with the big tree nutritional solution that embodiment 3 uses, in the complex amino acid aqueous solution that embodiment 2 uses
Various amino acid whose content on the low side, but the leaves of acetonideexample 2 and embodiment 3 all change into health green, trunk
As many sprouting has also been sprouted on surface, and the length of sprouting is longer, and conclusion is: embodiment 2 and the aminoacids complex of embodiment 3
In solution, various amino acid whose content all meet the demand of the big tree of malnutrition, but the aminoacids complex that embodiment 3 uses
In solution, various amino acid whose content are more, compare waste；
In sum, embodiment 1, embodiment 2 and embodiment 3 all can promote the growth of malnutrition Lignum cinnamomi camphorae, but implement
The promotion speed of example 1 is relatively slow, and effect does not has the good of embodiment 2 and embodiment 3, embodiment 3 as embodiment 2 effect, but
Amount of medicament uses more, more wastes, and embodiment 2 is that effect is best, is also that usage amount is most suitable.
Embodiment 4:
The present embodiment provides the processing technology of a kind of big tree nutritional solution compositing acid solution, comprises the following steps:
Add deionized water: according to compositing acid solution formula and the deionized water of the preset vol of compositing acid solution
Demand, toward preparation tank add demand deionized water；
To deionized water pretreatment: nitrogen charging limit, deionization waterside is heated, to deionized water nitrogen charging to eliminate deionized water
Oxygen, prevent from adding after aminoacid oxidized, simultaneously to deionized water heating so that adding aminoacid below and can dissolving；
Mixing deionized water and various aminoacid: after nitrogen charging 15 minutes, record according to compositing acid solution formula
Various aminoacid are put in deionized water by various amount of amino acid that every liter of water need to add successively, molten to obtain aminoacids complex
Liquid, different due to every kind of amino acid whose fusing point during this, and also most of aminoacid is the most oxidized, therefore in this process
In each amino acid whose input order need strict control；
Moisturizing for the first time: after whole aminoacid dissolve, to the default body of moisturizing in preparation tank to compositing acid solution
Long-pending, owing to during heating and input aminoacid, the volume of deionized water easily loses, it is therefore desirable to moisturizing；
Regulation pH value: add glacial acetic acid in compositing acid solution, to regulate pH value to 5.0-7.0, through overtesting, when
When the pH value of compositing acid solution is 5.6-6.2, the light transmittance of compositing acid solution is best, and through 10 days hot environments
Zero difference front with placement after storage, when the pH value of compositing acid solution is 7.2 and 7.4, stores through 10 days hot environments
Slight difference is only had afterwards, therefore to ensure the stability of compositing acid solution, by compositing acid solution pH with before placing
Value regulates to 5.6-7.0；
Desolventing technology: putting into activated carbon, quality of activated carbon is 0.04% with the ratio of the preset vol of compositing acid solution,
In order to reduce rapidly compositing acid solution temperature, absorption compositing acid solution in pigment and other impurity, therefore need
Activated carbon to be put into, but the amount of activated carbon can not be too much, and the crude drug in compositing acid solution too much can be caused to lose, and
The two very few effects that can not reach again of activated carbon, therefore the ratio of design quality of activated carbon and the preset vol of compositing acid solution is
0.04%；
Preliminary filter: make the compositing acid solution containing activated carbon through 5 μm titanium core filters, compound tentatively to filter out
Activated carbon in Freamine Ⅲ, leaches the compositing acid solution after activated carbon and is recycled in preparation tank by titanium core filter, for
Remove the activated carbon in compositing acid solution, with prevent activated carbon affect the performance of function of compositing acid solution and its
Transparency；
Nitrogen filled protection: under the conditions of the temperature of compositing acid solution is 45-50 DEG C, to the compositing acid solution prepared
Nitrogen charging, owing to adding aminoacid, adding in regulation pH value, desolventing technology and preliminary filter process that many in solution I haven't seen you for ages there is oxygen
Gas, and the existence of oxygen has had influence on the stability of compositing acid solution, it is therefore desirable to nitrogen charging is to control dissolved oxygen and residual oxygen
Amount, adds, and when temperature is 45-50 DEG C, compositing acid solution will not seethe because of temperature overheating again, enters oxygen after nitrogen charging
Probability reduce, nitrogen charging the most at this temperature；
Moisturizing for the second time: to the preset vol of moisturizing in preparation tank to compositing acid solution, due to the most filtered
In journey, deionized water loss is more, it is therefore desirable to moisturizing；
Filter further: make the compositing acid solution containing activated carbon through 5 μm titanium core filters, to filter out further
Activated carbon in compositing acid solution, the compositing acid solution leaching activated carbon is recycled in preparation tank by titanium core filter,
In order to remove the activated carbon in compositing acid solution further, to prevent activated carbon from affecting the function of compositing acid solution
Play and its transparency.
In mixing deionized water and various aminoacid step, various aminoacid are put in deionized water successively, with often
Rise various aminoacid in deionized water and add gauge, particularly as follows:
In 95 DEG C of deionized waters, put into 0.25 part of tyrosine, leucine 4.90 parts, isoleucine 3.52 parts, valine
3.60 parts and methionine 2.25 parts；
When deionized water is cooled to 70 DEG C, put into alanine 2.00 parts, phenylalanine 5.33 parts, 0.75 part of glutamic acid with
And Aspartic Acid 2.50 parts；
When deionized water is cooled to 65 DEG C, put into lysine acetate 4.30 parts, threonine 2.50 parts, glycine 7.60
Part, proline 1.00 parts, serine 1.00 parts and arginine hydrochloride 5.00 parts；
When deionized water is cooled to 60 DEG C, put into histidine monohydrochloride 2.50 parts, tryptophan 0.90 part and cystine 0.1
Part.According to the compositing acid solution formula described in embodiment 1 to embodiment 3, put into each aggregate species aminoacid, to be needed
The compositing acid solution wanted.Simultaneously as the dissolubility of different material medicine is different, and water temperature also has certain shadow to it
Ringing, tyrosine, leucine, isoleucine, the valine dissolubility in water is poor, and tryptophan, cysteine are unstable,
The most oxidized, it is contemplated that fully to be dissolved by crude drug within the effective time, the crude drug avoiding instability again is oxidized, therefore
Need to feed intake at different temperatures, crude drug poor for dissolubility was fed intake when water temperature is higher, after being then placed on of instability
Face and temperature feed intake time relatively low.
Also need to prepare front preparation before adding deionized water, comprising: supplementary material prepares, join by compositing acid solution
Side weighs each aminoacid；Glass bottle cleans, to obtain needing the clean glass bottle of quantity；Rubber plug cleaning, to obtain needing quantity
Clean plug；Aluminium lid cleans, to obtain needing the clean aluminium lid of quantity；And preparation tank cleans, clean to obtain needing having
The denseest join cylinder, pipeline, filter and dilute preparation tank joining cylinder.In order to carry out the front preparation of preparation, compound to facilitate in preparation
Become with compositing acid solution tinning during Freamine Ⅲ in Finished product processThe and use.
Supplementary material prepares concrete operations and includes: get each aminoacid according to compositing acid solution formula, each amino acid whose
The amount of weighing is: except tryptophan weighs by the 105% of compositing acid solution formula record amount, other are molten all in accordance with aminoacids complex
Formula of liquid record amount weighs.Owing to tryptophan incurs loss because of the reason such as the most oxidized in process for preparation, and tryptophan
It is the precursor substance that auxin biosynthesis is important in plant, is to promote material necessary to malnutrition plant growing, therefore
Tryptophan need to weigh by the 105% of compositing acid solution formula record amount.
In order to obtain the glass bottle of cleaning, fill compositing acid solution in the inner to prevent glass bottle from the most totally making and damaged
Lose.Glass bottle cleans concrete operations and includes: gets the glass bottle of specification quantity as desired, first, cleans visual inspection outward appearance with drinking water
Qualified glass bottle；Then, it is the purified water of 40-65 DEG C by temperature in ultrasonic washing unit, so that glass bottle is slightly washed；With
After, rinse glass bottle outer 1 time and interior 2 times by the purified water after slightly washing in ultrasonic washing unit；After again, rinse glass by new purified water
Outer 1 time and interior 2 times of bottle；Finally, the deionized water rinsing that temperature is 40-65 DEG C after filtering with 0.45 μm polypropylene filter
Glass bottle is inside and outside the most once.
In order to obtain the plug of cleaning, fill compositing acid solution quilt in the inner preventing plug glass bottle from the most totally making
Loss rubber plug cleaning concrete operations include: get the butyl rubber plug of requirement as desired, when taking φ 26 type plug not every time
7000 should be not to be exceeded when taking φ 32 type plug more than 22000, first, roll by purified water and rinse 5 minutes；Then, use
Plug is rolled and cleans 5 minutes by ultrasonic washing unit, and rinses 15 minutes；Finally, spend in ultrasonic washing unit from
Sub-water rolls rinsing 5 minutes to plug, and this cleaning drains the remaining water in ultrasonic washing unit after completing, cleaned plug is close
Close and deposit, should again clean more than 8 hours.
In order to obtain the preparation tank of cleaning, fill compositing acid solution quilt in the inner to prevent preparation tank from the most totally making
Pollute.Preparation tank cleans concrete operations and includes: first, adds deionized water 20-30 ten thousand ml and joins in cylinder to dense, adds bisulfite
150 parts of sodium, disodiumedetate (EDTA-2Na) 100 parts, be then turned on pump so that dense joins deionized water, sulfurous acid in cylinder
Hydrogen sodium and disodiumedetate circulate 4 minutes, so that sodium sulfite and disodiumedetate fully dissolve
Form bottoming water in deionized water；Then, use bottoming water rinse all pipelines of preparation tank, filter, pill tank and
Dilute join cylinder, subsequently enter dilute bottoming water joined in cylinder and clean the fill structure of preparation tank, the bottoming water warp in last fill structure
Backflow pumps dilute floor drain joining cylinder, to get rid of bottoming water；Finally, respectively distribution pipes dense, dilute is carried out bottoming process with activated carbon,
The inner surface making titanium core filter forms stable layer of charcoal, removes sodium sulfite and the ethylenediaminetetraacetic acid two of residual simultaneously
Sodium.
Also needing to carry out canning operation after filtering further, canning operation includes:
Bottling operation: first pass through and compositing acid solution is sent in the fitting configuration in preparation tank, then will join
Compositing acid solution in assembling structure loads in glass bottle；
Nitrogen charging evacuation plays plug: first empty glass bottle is carried out nitrogen charging, prevents the empty glass bottle graft of oxygen from entering compounded amino
Acid solution is oxidized；Then, the compositing acid solution prepared is encased in glass bottle；After again, to molten equipped with aminoacids complex
The glass bottle of liquid carries out nitrogen charging in airtight chamber, eliminates the oxygen entered during compositing acid solution is encased in glass bottle；
After again, the glass bottle equipped with compositing acid solution is carried out evacuation, remove glass bottled enter residue sky after compositing acid solution
Oxygen between, to ensure the stability of compositing acid solution；After again, carry out the glass bottle equipped with compositing acid solution beating
Plug, beats after plug completes and obtains semi-finished product；Finally, remaining oxygen in sampling observation glass bottle random to semi-finished product, remaining oxygen inspects qualified half by random samples
Finished product enters lower workshop section to carry out rolling lid；And
Rolling lid, the qualified semi-finished product of remaining oxygen sampling observation, through vibration cover blanking machine upper cover, after cover lifter gland, rotate by bottle
Roll lid, roll the big tree nutritional solution compositing acid solution being finished product after covering lattice.
Finally illustrating, above example is only in order to illustrate technical scheme and unrestricted, although with reference to relatively
The present invention has been described in detail by good embodiment, it will be understood by those within the art that, can be to the skill of the present invention
Art scheme is modified or equivalent, and without deviating from objective and the scope of technical solution of the present invention, it all should be contained at this
In the middle of the right of invention.
Claims (10)
1. a big tree nutritional solution compositing acid solution, it is characterised in that include following component in terms of mass parts:
1000 parts of deionized waters, 0.20～0.30 part of tyrosine, 4.80～5.00 parts of leucines, 3.48～3.56 parts of different bright ammonia
Acid, 3.50～3.70 parts of valines, 2.21～2.29 parts of methionines, 1.92～2.08 parts of alanine, 5.23～5.43 parts of benzene
Alanine, 0.71～0.79 part of glutamic acid, 2.42～2.58 parts of Aspartic Acids, 4.22～4.36 parts of lysine acetate, 2.42～
2.58 parts of threonine, 7.54～7.66 parts of glycine, 0.90～1.10 part of proline, 0.90～1.10 part of serine, 4.82～
5.12 parts of arginine hydrochloride, 2.41～2.62 parts of histidine monohydrochlorides, 0.82～0.98 part of tryptophan and 0.07～0.12 part of Guang
Propylhomoserin.
Big tree nutritional solution compositing acid solution the most according to claim 1, it is characterised in that include following with quality
The component of part meter:
1000 parts of deionized waters, 0.25 part of tyrosine, 4.90 parts of leucines, 3.52 parts of isoleucine, 3.60 parts of valines, 2.25
Part methionine, 2.00 parts of alanine, 5.33 parts of phenylalanine, 0.75 part of glutamic acid, 2.50 parts of Aspartic Acids, 4.30 parts of acetic acid
Lysine, 2.50 parts of threonine, 7.60 parts of glycine, 1.00 parts of proline, 1.00 parts of serines, 5.00 parts of arginine hydrochloride,
2.50 parts of histidine monohydrochlorides, 0.90 part of tryptophan and 0.1 part of cystine.
3. the biggest processing technology setting nutritional solution compositing acid solution, it is characterised in that include
Following steps:
Add deionized water: according to compositing acid solution formula and the need of the deionized water of the preset vol of compositing acid solution
The amount of asking, adds the deionized water of demand toward preparation tank；
To deionized water pretreatment: nitrogen charging limit, deionization waterside is heated；
Mixing deionized water and various aminoacid: after nitrogen charging 15 minutes, every liter recorded according to compositing acid solution formula
Various aminoacid are put in deionized water by various amount of amino acid that water need to add successively, to obtain compositing acid solution；
Moisturizing for the first time: after whole aminoacid dissolve, to the preset vol of moisturizing in preparation tank to compositing acid solution；
Regulation pH value: add glacial acetic acid in compositing acid solution, to regulate pH value to 5.0-7.0；
Desolventing technology: putting into activated carbon, quality of activated carbon is 0.04% with the ratio of the preset vol of compositing acid solution；
Preliminary filter: make the compositing acid solution containing activated carbon through 5 μm titanium core filters, tentatively to filter out compounded amino
Activated carbon in acid solution, leaches the compositing acid solution after activated carbon and is recycled in preparation tank by titanium core filter；
Nitrogen filled protection: under the conditions of the temperature of compositing acid solution is 45-50 DEG C, the compositing acid solution prepared is filled
Nitrogen；
Moisturizing for the second time: to the preset vol of moisturizing in preparation tank to compositing acid solution；
Filter further: make the compositing acid solution containing activated carbon through 5 μm titanium core filters, compound to filter out further
Activated carbon in Freamine Ⅲ, the compositing acid solution leaching activated carbon is recycled in preparation tank by titanium core filter.
The processing technology of big tree nutritional solution compositing acid solution the most according to claim 3, it is characterised in that mixed
Close in deionized water and various aminoacid step, various aminoacid are put in deionized water successively, with in every liter of deionized water
Various aminoacid add gauge, particularly as follows:
In 95 DEG C of deionized waters, put into 0.25 part of tyrosine, leucine 4.90 parts, isoleucine 3.52 parts, valine 3.60
Part and methionine 2.25 parts；
When deionized water is cooled to 70 DEG C, put into alanine 2.00 parts, phenylalanine 5.33 parts, 0.75 part of glutamic acid and
Winter propylhomoserin 2.50 parts；
When deionized water is cooled to 65 DEG C, put into lysine acetate 4.30 parts, threonine 2.50 parts, glycine 7.60 parts, dried meat
Propylhomoserin 1.00 parts, serine 1.00 parts and arginine hydrochloride 5.00 parts；
When deionized water is cooled to 60 DEG C, put into histidine monohydrochloride 2.50 parts, tryptophan 0.90 part and cystine 0.1 part.
The processing technology of big tree nutritional solution compositing acid solution the most according to claim 3, it is characterised in that adding
Also need before deionized water to prepare front preparation, comprising: supplementary material prepares, weigh each amino by compositing acid solution formula
Acid；Glass bottle cleans, to obtain needing the clean glass bottle of quantity；Rubber plug cleaning, to obtain needing the clean plug of quantity；Aluminum
Lid cleans, to obtain needing the clean aluminium lid of quantity；And preparation tank cleans, with obtain needs have clean dense join cylinder, pipeline,
Filter and dilute preparation tank joining cylinder.
The processing technology of big tree nutritional solution compositing acid solution the most according to claim 5, it is characterised in that former auxiliary
Material prepares concrete operations and includes: getting each aminoacid according to compositing acid solution formula, each amino acid whose amount of weighing is: except color
Propylhomoserin weighs by the 105% of compositing acid solution formula record amount, and other are all in accordance with compositing acid solution formula record amount
Weigh.
The processing technology of big tree nutritional solution compositing acid solution the most according to claim 5, it is characterised in that glass bottle
Cleaning concrete operations include: get the glass bottle of specification quantity as desired, first, clean, with drinking water, the glass that visual inspection outward appearance is qualified
Bottle；Then, it is the purified water of 40-65 DEG C by temperature in ultrasonic washing unit, so that glass bottle is slightly washed；Subsequently, with ultrasonic
Pure water after slightly washing in ripple cleaning machine rinses glass bottle outer 1 time and interior 2 times；After again, with new purified water rinse glass bottle outer 1 time and
They interior 2 times；Finally, the deionized water rinsing glass bottle that temperature is 40-65 DEG C after filtering with 0.45 μm polypropylene filter is inside and outside
The most once.
The processing technology of big tree nutritional solution compositing acid solution the most according to claim 5, it is characterised in that plug
Cleaning concrete operations include: get the butyl rubber plug of requirement as desired, are not to be exceeded when taking φ 26 type plug every time
22000, when taking φ 32 type plug, it is not to be exceeded 7000, first, rolls by purified water and rinse 5 minutes；Then, ultrasound wave is used
Plug is rolled and cleans 5 minutes by cleaning machine, and rinses 15 minutes；Finally, use deionized water pair in ultrasonic washing unit
Plug rolls rinsing 5 minutes, and this cleaning drains the remaining water in ultrasonic washing unit after completing, cleaned plug is airtight to be deposited
Put, should again clean more than 8 hours.
The processing technology of big tree nutritional solution compositing acid solution the most according to claim 5, it is characterised in that preparation
Cylinder cleans concrete operations and includes: first, adds deionized water 20-30 ten thousand ml and joins in cylinder to the denseest, add sodium sulfite 150 parts,
Disodiumedetate (EDTA-2Na) 100 parts, is then turned on pump so that dense join deionized water in cylinder, sodium sulfite and
Disodiumedetate circulates 4 minutes, so that sodium sulfite and disodiumedetate are substantially dissolved in deionization
Water is formed bottoming water；Then, use bottoming water rinse all pipelines of preparation tank, filter, pill tank and dilute join cylinder, with
The dilute bottoming water joined in cylinder of rear entrance cleans the fill structure of preparation tank, and the bottoming water in last fill structure is dilute through backflow pumping
Join the floor drain of cylinder, to get rid of bottoming water；Finally, respectively distribution pipes dense, dilute is carried out bottoming process with activated carbon, make titanium core filter
The inner surface of device forms stable layer of charcoal, removes sodium sulfite and the disodiumedetate of residual simultaneously.
The processing technology of big tree nutritional solution compositing acid solution the most according to claim 3, it is characterised in that
Also needing to carry out canning operation after filtering further, canning operation includes:
Bottling operation: first pass through and compositing acid solution is sent in the fitting configuration in preparation tank, then by equipped knot
Compositing acid solution in structure loads in glass bottle；
Nitrogen charging evacuation plays plug: first empty glass bottle is carried out nitrogen charging；Then, the compositing acid solution prepared is encased in glass
In Ping；After again, the glass bottle equipped with compositing acid solution is carried out nitrogen charging in airtight chamber；After again, to equipped with compounded amino
The glass bottle of acid solution carries out evacuation；After again, carry out the glass bottle equipped with compositing acid solution playing plug, beat after plug completes and obtain
Semi-finished product；Finally, remaining oxygen in sampling observation glass bottle random to semi-finished product, under the semi-finished product entrance that remaining oxygen sampling observation is qualified, workshop section is carried out
Roll lid；And
Rolling lid, the qualified semi-finished product of remaining oxygen sampling observation, through vibration cover blanking machine upper cover, after cover lifter gland, carry out rotation by bottle and roll
Lid, rolls the big tree nutritional solution compositing acid solution being finished product after covering lattice.
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| CN107201230A (en) * | 2017-04-27 | 2017-09-26 | 广西棕海园林工程有限公司 | Soil moisturizing agent |
| CN109265229A (en) * | 2018-12-17 | 2019-01-25 | 河南省莱恩坪安园林植保有限公司 | A kind of amino acid fertilizer that can inhibit willow differentiation bud |
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Address after: 443100, No. 180 Yi Xing Road, Yiling District, Hubei, Yichang Applicant after: Hubei long Du Le Pharmaceutical Co. Ltd. Address before: 443100 No. 180 Yi Hing Road, Hubei, Yichang Applicant before: Hubei Aerodurer Medical Instrument Co., Ltd. |
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Application publication date: 20161109 |