CN106047471A - Supercritical extraction process of walnut brain-nourishing tea oil - Google Patents

Supercritical extraction process of walnut brain-nourishing tea oil Download PDF

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Publication number
CN106047471A
CN106047471A CN201610618501.5A CN201610618501A CN106047471A CN 106047471 A CN106047471 A CN 106047471A CN 201610618501 A CN201610618501 A CN 201610618501A CN 106047471 A CN106047471 A CN 106047471A
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Prior art keywords
brain
tea oil
nourishing tea
semen
supplementing
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Pending
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CN201610618501.5A
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不公告发明人
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YUEXI COUNTY GLORIFIES SAGE TEA OIL Ltd
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YUEXI COUNTY GLORIFIES SAGE TEA OIL Ltd
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Priority to CN201610618501.5A priority Critical patent/CN106047471A/en
Publication of CN106047471A publication Critical patent/CN106047471A/en
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/42—Cucurbitaceae (Cucumber family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/52—Juglandaceae (Walnut family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/82—Theaceae (Tea family), e.g. camellia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0203—Solvent extraction of solids with a supercritical fluid
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/02—Pretreatment
    • C11B1/04—Pretreatment of vegetable raw material
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/005—Refining fats or fatty oils by wave energy or electric current, e.g. electrodialysis
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D2011/007—Extraction using a solvent in the gas phase

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
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  • Oil, Petroleum & Natural Gas (AREA)
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Abstract

The invention provides a supercritical extraction process of walnut brain-nourishing tea oil. The process is characterized by preparing the walnut brain-nourishing tea oil through the steps of CO2 supercritical extraction and ultra-micro filtration. Chemical reagents are not added in the production process, especially a refining process of the walnut brain-nourishing tea oil; a pure physical method is used for refining the walnut brain-nourishing tea oil; the prepared walnut brain-nourishing tea oil retains active materials, is free of solvent residues, free of pollution, high in safety and high in oil product quality. The chemical reagents are not added into the refining process, so that the walnut brain-nourishing tea oil is free of chemical residual reagents and can be used as excellent high-quality edible oil and cosmetic or a pharmaceutical additive; when the walnut brain-nourishing tea oil is eaten and is applied to the medicines, the walnut brain-nourishing tea oil has the effects of tonifying kidney and invigorating lung, absorbing qi and relieving asthma, relieving constipation with laxatives; the walnut brain-nourishing tea oil is thick in smell and special in flavor, can be widely used for cooking various foods and dishes, has a higher nutrition value and a healthcare effect, can guarantee active components with high resistance to oxidization, and is especially suitable for popularization in the technical field of production of small-batch special oil.

Description

Semen Persicae supplementing the brain Oleum Camelliae supercritical extraction process
Technical field
A kind of method that the present invention relates to Semen Persicae supplementing the brain Oleum Camelliae supercritical extraction, art: biological and new medicine Technology, modern agricultural technology, agricultural product intensive processing and modern accumulating: agriculture and forestry product and extraordinary resource increment processing.
Background technology
Along with the raising of people's living standard, food, edible-flavouring industry also change occurring, flavored oils taste with And in product category, it is made that the biggest breakthrough, but seldom there is food to have special effect, this increasingly can not meet people To seasoning innage standard-required, the development in market of meeting the tendency, flavored oils's industry needs innovation and development.
Summary of the invention
It is an object of the invention to provide the Semen Persicae supplementing the brain tea of a kind of simplicity, nutritive value and health care, rational technology Oil producing method.
The technical scheme is that and be achieved in that, comprise the steps:
A, Semen Camelliae, Semen Juglandis, Semen Sesami Nigrum, sunflower seed, Fructus Cucurbitae moschatae, Fructus Maydis, Semen arachidis hypogaeae, Semen setariae are carried out dry in the sun, control moisture content 4%-8%；
B, the mixture core dried is put in the household freezer of-25 DEG C freezing 3～9 hours, be placed on-10 DEG C true In Altitude 3～8 hours, finally it is placed in 40～60 DEG C of vacuum environments dried 2～7 hours；
C, the mixture pulverizing that will obtain after B, process, sieve by 20～40 mesh sieve；
D、CO2 Supercritical extraction, fluid extraction pressure is 25～55MPa, extraction temperature 25～40 DEG C, CO2 Fluid stream Amount is 800～1000L/h, and extraction time is 60～120 minutes, obtains Semen Persicae supplementing the brain Oleum Camelliae crude oil；
E, hyperfiltration removing lipoxidase, select the hyperfiltration film of molecular cut off 80-120kD, after filtering Semen Persicae supplementing the brain Oleum Camelliae carries out hyperfiltration process；
F, ultra-vioket radiation, the irradiation unit by uviol lamp disposed above of the Semen Persicae supplementing the brain Oleum Camelliae flowing after filtration, exposure dose For 400-500J/m2, irradiation time is the 20-30 second,.
Compared with prior art the inventive method has the advantage that (1) present invention provides a kind of Semen Persicae supplementing the brain Oleum Camelliae Production technology, particularly in the refining process of Semen Persicae supplementing the brain Oleum Camelliae, does not add chemical reagent, uses pure physical method to carry out Refine, it is thus achieved that Semen Persicae supplementing the brain Oleum Camelliae remain active substance, no solvent residue, pollution-free, safety good, oil quality is high. Owing to not adding any chemical reagent in extractive process, without chemical residual reagent, can as fabulous high-end edible oil and Cosmetics or pharmacy additive.Eat and energy the kidney invigorating lung benefiting, helping inspiration to relieve asthma, loosening bowel to relieve constipation in medicine；(2) present invention Utilize Lyophilisation technique for making, be easy to mixture pulverize；(3) present invention utilizes CO2 Supercritical extraction technique so that Not having organic solvent residual in product, the crude oil color and luster simultaneously extracted is more shallow than squeezing Semen Persicae supplementing the brain Oleum Camelliae, it is not necessary to through de- Glue, alkali refining, decolouring, deodorize process, thus the loss such as natural nutrition VE is few, does not the most produce the harmful substances such as trans fatty acid and carries Supply；(4) present invention utilizes ultra micro membrane filtration technique, eliminates in Semen Persicae supplementing the brain Oleum Camelliae storage process and causes rotten biological factor ；Oxygenase in Semen Persicae supplementing the brain Oleum Camelliae, in storage process, in the unsaturated fatty acid in catalysis oxidation Semen Persicae supplementing the brain Oleum Camelliae Double bond ruptures, and produces the smell substances such as aldehyde ketone and produces, and makes Semen Persicae supplementing the brain Oleum Camelliae go bad；Tradition hot moulding is to utilize high temperature to make oxygen Synthase deactivation；Solvent extraction method, is to make oxygenase inactivate in refining process；The technique of the present invention is without heating Degenerative treatments, does not the most carry out refine, and uses ultra micro membrane filtration technique, and ultrafiltration removes the lipoxidase in Semen Persicae supplementing the brain Oleum Camelliae Enzyme, eliminates in Semen Persicae supplementing the brain Oleum Camelliae storage process and causes rotten biological factor, and the clarity simultaneously added；(5) The present invention utilizes ultra-vioket radiation technology, kills the activity of fatty oxygenase that is not completely removed during hyperfiltration processes, and goes forward side by side one Step destroys the structure of the aflatoxin of remaining, reaches the purpose eliminated further.In order to ensure the circulation of ultrafiltration, in technique The ultrafilter membrane of the 80-120KD selected, can remove most lipoxidase, but can not completely remove.Remaining fat Oxygenase, utilizes the ultra-vioket radiation of low dosage to process, and both can ensure that the quality of oil is not suffered a loss, can reduce again residual further Remaining activity of fatty oxygenase, it is ensured that the storage of oil.Meanwhile, the wavelength utilizing ultraviolet light is short, and energy is big, is irradiated to body surface Time, easily it is subsequently absorbed in the material, becomes the interior energy of material, destroy the characteristic of the chemical bond of material molecule, reduce Semen Persicae further and mend Aflatoxin content in brain Oleum Camelliae；Remove rapidly the aldehyde material letones wherein in abnormal flavour, and produce abnormal flavour Free fatty, and ensure nutrient substance therein loss seldom；(6) in the high-quality oils and fats that the present invention produces, because Rich in Natural antioxidants such as natural VEs, oils and fats storage process need not additionally add antioxidant.
The present invention provides the Semen Persicae supplementing the brain Production method of tea oil of a kind of simplicity, nutritive value and health care, rational technology, Can produce for small lot special oil and technical support is provided, be suitable to promote in edible fat production technical field.
Detailed description of the invention
A kind of Semen Persicae supplementing the brain Oleum Camelliae production technology:
A, Semen Camelliae, Semen Juglandis, Semen Sesami Nigrum, sunflower seed, Fructus Cucurbitae moschatae, Fructus Maydis, Semen arachidis hypogaeae, Semen setariae are carried out dry in the sun, control moisture content 4%；
B, the mixture core dried is put in the household freezer of-25 DEG C freezing 9 hours, the vacuum environment being placed on-10 DEG C In 3 hours, be finally placed in dried 2 hours in 40 DEG C of vacuum environments；
C, the mixture pulverizing that will obtain after B, process, sieve by 20 mesh sieve；
D、CO2Supercritical extraction, fluid extraction pressure is 55MPa, extraction temperature 40 DEG C, CO2Fluid flow is 1000L/h, Extraction time is 60 minutes, obtains Semen Persicae supplementing the brain Oleum Camelliae crude oil；
E, hyperfiltration removing lipoxidase, select the hyperfiltration film of molecular cut off 80kD, to the Semen Persicae after filtering Supplementing the brain Oleum Camelliae carries out hyperfiltration process；
F, ultra-vioket radiation, the irradiation unit by uviol lamp disposed above of the Semen Persicae supplementing the brain Oleum Camelliae flowing after filtration, exposure dose For 400-500J/m2, irradiation time is 30 seconds,.
The present invention can be used for special oil and produces, it is adaptable to nutritive value and health care's edible fat production, accomplishes pollution-free, low Energy consumption.

Claims (3)

1. the processing method producing Semen Persicae supplementing the brain Oleum Camelliae, it is characterised in that comprise the steps:
A, Semen Camelliae, Semen Juglandis, Semen Sesami Nigrum, sunflower seed, Fructus Cucurbitae moschatae, Fructus Maydis, Semen arachidis hypogaeae, Semen setariae are carried out dry in the sun, control moisture content 4%-8%；
B, the mixture core dried is put in the household freezer of-25 DEG C freezing 3～9 hours, be placed on-10 DEG C true In Altitude 3～8 hours, finally it is placed in 40～60 DEG C of vacuum environments dried 2～7 hours；
C, the mixture pulverizing that will obtain after B, process, sieve by 20～40 mesh sieve；
D、CO 2Supercritical extraction, fluid extraction pressure is 25～55MPa, extraction temperature 25～40 DEG C, CO2Fluid Flow is 800～1000L/h, and extraction time is 60～120 minutes, obtains Semen Persicae supplementing the brain Oleum Camelliae crude oil；
E, hyperfiltration removing lipoxidase, select the hyperfiltration film of molecular cut off 80-120kD, after filtering East China Chinese walnut oil carries out hyperfiltration process；
F, ultra-vioket radiation, the irradiation unit by uviol lamp disposed above of the Semen Persicae supplementing the brain Oleum Camelliae flowing after filtration, exposure dose For 400-500J/m2, irradiation time is the 20-30 second,.
2. according to the Semen Persicae supplementing the brain Oleum Camelliae supercritical extraction process described in claim 1, it is characterized in that, C, step use 40 Mesh sieve is sieved.
3. according to the Semen Persicae supplementing the brain Oleum Camelliae supercritical extraction process described in claim 1 or 2, it is characterized in that, E, step are adopted The molecular cut off of hyperfiltration film be 110kD.
CN201610618501.5A 2016-08-01 2016-08-01 Supercritical extraction process of walnut brain-nourishing tea oil Pending CN106047471A (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107267279A (en) * 2017-06-20 2017-10-20 贵州祥驰农业开发有限公司 A kind of delicate fragrance camellia oil
CN107699342A (en) * 2017-11-27 2018-02-16 哈尔滨美森食品制造有限公司 A kind of method of supercritical carbon dioxide extraction walnut oil
CN112316484A (en) * 2020-10-31 2021-02-05 洞口县亿丰农林牧科技有限公司 Method for extracting camellia oleifera polyphenol from tea oil

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107267279A (en) * 2017-06-20 2017-10-20 贵州祥驰农业开发有限公司 A kind of delicate fragrance camellia oil
CN107699342A (en) * 2017-11-27 2018-02-16 哈尔滨美森食品制造有限公司 A kind of method of supercritical carbon dioxide extraction walnut oil
CN112316484A (en) * 2020-10-31 2021-02-05 洞口县亿丰农林牧科技有限公司 Method for extracting camellia oleifera polyphenol from tea oil

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Application publication date: 20161026