CN106044829B8 - 一种白色纯氧化铈的制备方法 - Google Patents

一种白色纯氧化铈的制备方法 Download PDF

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CN106044829B8
CN106044829B8 CN201610351090.8A CN201610351090A CN106044829B8 CN 106044829 B8 CN106044829 B8 CN 106044829B8 CN 201610351090 A CN201610351090 A CN 201610351090A CN 106044829 B8 CN106044829 B8 CN 106044829B8
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ball milling
ball
preparation
room temperature
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CN106044829A (zh
CN106044829B (zh
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陈伟凡
卓明鹏
祝文才
高亮
任卫
方晓辰
周文威
郭兰玉
谢水军
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Ganzhou Zhanhai New Material Technology Co., Ltd.
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Ganzhou Zhanhai Industry And Trade Co ltd
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

一种白色纯氧化铈的制备方法，包括以下步骤：（1）按化学计量比称取氯化铈与碱金属碳酸盐、碱金属碳酸氢盐或者碱金属强碱；（2）将步骤（1）中称取的反应物放入球磨机中球磨0.5~2小时，取出球磨料和磨球，在40~60℃鼓风烘箱中干燥1~4小时后，再放入球磨机中球磨0.5~2小时；（3）将步骤（2）中球磨后的产物直接放入马弗炉，以1~15℃/min的升温速率从室温升至600~1000℃，保温1~8小时后随炉冷却至室温，再洗涤、过滤、干燥。本发明产物白度高、粒度小、分散性好、大小均匀；且设备要求低，合成产率高，无需添加任何添加剂等特点，合成过程绿色环保，生产成本低廉，非常适合于工业化生产。
CN201610351090.8A 2016-05-25 2016-05-25 一种白色纯氧化铈的制备方法 Active CN106044829B8 (zh)

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109928417B (zh) * 2019-02-28 2022-03-22 昆明理工大学 一种白色纯氧化铈的制备方法
CN110282651B (zh) * 2019-08-09 2021-09-14 赣州有色冶金研究所有限公司 一种利用复合沉淀剂制备高纯氧化稀土的方法
CN113233493A (zh) * 2021-05-31 2021-08-10 中南大学 一种批量化合成稀土纳米氧化物颗粒材料的方法
CN115724457A (zh) * 2022-12-05 2023-03-03 上海华明高纳稀土新材料有限公司 一种白色纳米氧化铈及其制备方法

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101372353A (zh) * 2008-06-12 2009-02-25 江苏工业学院 超声雾化工艺制备纳米CeO2粉体的方法
CN101709378A (zh) * 2009-11-23 2010-05-19 南昌大学 一种稀土铈(ⅳ)的沉淀方法
CN101879439A (zh) * 2009-05-08 2010-11-10 中国科学院兰州化学物理研究所 一种复合氧化物的制备方法
CN101891233A (zh) * 2010-07-12 2010-11-24 南昌大学 一种超细氧化铈的制备方法
CN101977873A (zh) * 2008-02-12 2011-02-16 圣戈本陶瓷及塑料股份有限公司 二氧化铈及其形成方法
CN102275971A (zh) * 2011-05-26 2011-12-14 哈尔滨工业大学 室温固相反应制备纳米二氧化铈的方法
CN102965026A (zh) * 2012-11-12 2013-03-13 上海华明高纳稀土新材料有限公司 稀土抛光粉及其制备方法
CN103288119A (zh) * 2013-06-17 2013-09-11 上海华明高纳稀土新材料有限公司 稀土抛光粉的制备方法
CN105565359A (zh) * 2015-12-22 2016-05-11 南昌大学 一种平均粒径可调的超细氧化铈抛光粉的制备方法

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101977873A (zh) * 2008-02-12 2011-02-16 圣戈本陶瓷及塑料股份有限公司 二氧化铈及其形成方法
CN101372353A (zh) * 2008-06-12 2009-02-25 江苏工业学院 超声雾化工艺制备纳米CeO2粉体的方法
CN101879439A (zh) * 2009-05-08 2010-11-10 中国科学院兰州化学物理研究所 一种复合氧化物的制备方法
CN101709378A (zh) * 2009-11-23 2010-05-19 南昌大学 一种稀土铈(ⅳ)的沉淀方法
CN101891233A (zh) * 2010-07-12 2010-11-24 南昌大学 一种超细氧化铈的制备方法
CN102275971A (zh) * 2011-05-26 2011-12-14 哈尔滨工业大学 室温固相反应制备纳米二氧化铈的方法
CN102965026A (zh) * 2012-11-12 2013-03-13 上海华明高纳稀土新材料有限公司 稀土抛光粉及其制备方法
CN103288119A (zh) * 2013-06-17 2013-09-11 上海华明高纳稀土新材料有限公司 稀土抛光粉的制备方法
CN105565359A (zh) * 2015-12-22 2016-05-11 南昌大学 一种平均粒径可调的超细氧化铈抛光粉的制备方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
"Preparation of nano-sized CeO2 by mechanochemical reaction of cerium carbonate with sodium hydroxide";Yongxiu Li et al.;《Mattericals Letters》;20031231;第58卷;第248页、图6 *

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CN106044829B (zh) 2018-03-23

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Inventor after: Chen Weifan

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Inventor after: Zhu Wencai

Inventor after: Gao Liang

Inventor after: Ren Wei

Inventor after: Fang Xiaochen

Inventor after: Zhou Wenwei

Inventor after: Guo Lanyu

Inventor after: Xie Shuijun

Inventor before: Chen Weifan

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Inventor before: Guo Lanyu

Inventor before: Xie Shuijun

CI03 Correction of invention patent
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Correction item: Inventor|Patentee|Address

Correct: Chen Weifan|Zhuo Mingpeng|Zhu Wencai|Gao Liang|Ren Wei|Fang Xiaochen|Zhou Wenwei|Guo Lanyu|Xie Shuijun|Ganzhou Zhanhai Industry Trade Co.,Ltd.|341000 Jiangxi province Ganzhou City Zhanggong District Water West Nonferrous Metallurgical base golden hair South Road

False: Chen Weifan|Zhuo Mingpeng|Fang Xiaochen|Zhou Wenwei|Guo Lanyu|Xie Shuijun|Nanchang University|330031 999, Xuefu Avenue, Nanchang, Jiangxi.

Number: 12-02

Page: The title page

Volume: 34

Correction item: Inventor|Patentee|Address

Correct: Chen Weifan|Zhuo Mingpeng|Zhu Wencai|Gao Liang|Ren Wei|Fang Xiaochen|Zhou Wenwei|Guo Lanyu|Xie Shuijun|Ganzhou Zhanhai Industry Trade Co.,Ltd.|341000 Jiangxi province Ganzhou City Zhanggong District Water West Nonferrous Metallurgical base golden hair South Road

False: Chen Weifan|Zhuo Mingpeng|Fang Xiaochen|Zhou Wenwei|Guo Lanyu|Xie Shuijun|Nanchang University|330031 999, Xuefu Avenue, Nanchang, Jiangxi.

Number: 12-02

Volume: 34

CP03 Change of name, title or address
CP03 Change of name, title or address

Address after: 341000 Jiangxi Ganzhou Shuixi Nonferrous Metallurgical Base

Patentee after: Ganzhou Zhanhai New Material Technology Co., Ltd.

Address before: 341000 Jiangxi province Zhanggong District of Ganzhou City, west of non-ferrous metallurgical base blonde Road

Patentee before: Ganzhou Zhanhai Industry Trade Co.,Ltd.