CN106012514B - A kind of sizing afterwaxing agent and application thereof - Google Patents
A kind of sizing afterwaxing agent and application thereof Download PDFInfo
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- CN106012514B CN106012514B CN201610357459.6A CN201610357459A CN106012514B CN 106012514 B CN106012514 B CN 106012514B CN 201610357459 A CN201610357459 A CN 201610357459A CN 106012514 B CN106012514 B CN 106012514B
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- afterwaxing
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of sizing afterwaxing agent and application thereof, which is made of following raw material by weight percentage：50 58% paraffin, 19 25% rilanit special, 14 20% stearic acid, 8 10% emulsifier, and, 0.1 0.3% antistatic agent.The present invention uses the afterwaxing agent that wax is prepared as main material, has excellent lubricity, flexibility, emulsibility and antistatic property, is not easy to be layered, and it is good to print and dye, and solution generally believes the difficult point that follow-up printing quality can be influenced using paraffin both at home and abroad.Material proportion provided by the invention so that afterwaxing agent of the invention reaches sizing operation requirement, while meeting the dyeing quality requirement of printing and dyeing mill, is suitable for textile industry sizing operation.
Description
Technical field
The present invention relates to industrial wax products, it particularly relates to which a kind of being used for sizing of the textile mills in set-up procedure
Sizing afterwaxing agent used in process and application thereof.
Background technology
In fabrication processes, the quality of starching, efficiency and final product quality to loom all have a great impact.Foreign countries also have
The discussion of " on slurry good, be equal to cloth and be made into half ".Quality such as slurry is bad, is not waxed effectively to sizing
Processing can not only increase the end breakage rate of loom, reduce loom efficiency and final product quality, waste raw material.In recent years, the original of weaving loom
Material becomes complicated and diversified, and the speed of loom steps up, therefore new slurry, afterwaxing agent are as new research and development focus.
Waxing is to allow filoplume flattening on yarn is dry, to reduce abrasion of the yarn to yarn road, can also reduce woven fabric process
Middle filoplume blocks pin hole, and syringe causes the flaws such as rotten needle.The purpose of waxing is so that friction coefficient is low as far as possible, and waxes
It is uniformly correct to wax and spinning speed and knitting quality can be improved using high-quality wax and save cost.
Wax is used as yarn lubricant in knitting process, in order to reduce since a large amount of metals transmit point and needle contact generates
The influence of kinetic force of friction, yarn must wax while reduce and the abrasion of the metal parts of yarn contacts.In fact, yarn is wax
Carrier, Wax particles are brought to each contact point and are stored at this, formed coating of wax film at these, yarn is made to slide by yarn
It is dynamic that more i.e. friction is reduced, and frictional force is smaller, and tension suffered by yarn is more uniform, to reduce broken yarn, improve production efficiency and
The quality of production.Waxing amount is small, and friction coefficient also reduces, but yarn breakage increases；Best waxing is that friction coefficient and yarn are disconnected
Head rate is reduced to minimum, and not excessive waxing.
Afterwaxing agent is the compound of more complicated multiple material, is had based on wax, based on oil, with
And equal three types based on surfactant.The related document of Japan is thought：The afterwaxing agent of finish based on wax
It is R＆D direction from now on, it is usually required mainly for solve finish and adhere to uneven, easily emulsification（It is bad to move back wax）.
External most representational afterwaxing agent is the After Wax of Song Ben oil chemistries company of Japan（After waxing
Agent）；Domestic representational afterwaxing agent is water soluble wax BZW, solubilised textile wax SW, water-emulsifiable wax DHL etc..
But these afterwaxing agents there is a problem in that：Expensive, weaving use cost is high, and the fusing point of product is low, easily
It bonds, transport, storage and inconvenient to use, waste is big.
The excellent paraffin of conventionally used flatness as afterwaxing agent, exist follow-up printing and dyeing because move back wax it is bad due to influence cloth
Quality problems.
Therefore, there is an urgent need for researching and developing a kind of higher afterwaxing agent of cost performance, can sizing be had：It is good smooth
Property, flexibility and moves back the good completeness of wax at antistatic property（The emulsibility of cerate）.
Invention content
The afterwaxing agent prepared as main material present invention aim to address generally use wax is easily layered, and after easily leading to
Continuous printing and dyeing are difficult（Follow-up printing quality can be influenced using paraffin by generally believing both at home and abroad）The problem of, a kind of afterwaxing agent is provided,
It can meet that the lubricity of sizing after waxing, flexibility, emulsibility be excellent and the requirement of antistatic property.
In order to achieve the above objectives, the present invention provides a kind of sizing afterwaxing agent, which includes below with weight
The raw material of percentage meter：The paraffin of 50-58%, the rilanit special of 19-25%, the stearic acid of 14-20%, the emulsifier of 8-10%,
And the antistatic agent of 0.1-0.3%.
Above-mentioned sizing afterwaxing agent, wherein the emulsifier selects polyoxyethylene nonylphenol ether.
Such as above-mentioned sizing afterwaxing agent, wherein the paraffin is No. 58 paraffin, is semi-refined industrial paraffin, melts
Point is 58-60 DEG C.
Above-mentioned sizing afterwaxing agent, wherein the rilanit special selects S-185 rilanit specials.
Above-mentioned sizing afterwaxing agent, wherein the afterwaxing agent is prepared using four-part form mixing process, the four-part form
Mixing process includes：First segment concocts paraffin, stearic acid by emulsifier；Second segment, rilanit special and emulsifier tune
It closes；First segment blending solution is mixed with second segment blending solution, antistatic agent blending is added by third section；4th section, cooling is adjusted
It closes.
Above-mentioned sizing afterwaxing agent, wherein the first segment mixing process condition is：Concoct 100 DEG C of temperature, stirring
Speed 70r/min, mixing time 0.5 hour；Second segment mixing process condition is：Concoct 80 DEG C of temperature, mixing speed 40r/
Min, mixing time about 0.5 hour；Third section mixing process condition is：It is 90 DEG C, mixing speed 50r/min to concoct temperature,
Mixing time about 0.5 hour；4th section of mixing process condition be：It is 80-85 DEG C to concoct temperature, and does not select 80 DEG C and 85 DEG C,
Mixing speed is down to 20-25r/min, mixing time 0.5 hour.
The present invention also provides the purposes of above-mentioned sizing afterwaxing agent, the afterwaxing agent is used for sizing operation, adopts
Upper Lasaxing Oilfield is carried out to sizing with the afterwaxing agent.
The present invention, as principal ingredients, is reduced cost of material, improved using the rich paraffin of the excellent low price of flatness
The fusing point of afterwaxing agent product, solves the problems, such as that the transport, storage and use of existing similar product exist.Moreover, this hair
Compared with similar products, usage amount is few when waxing rate is identical for bright afterwaxing agent, and disconnected through several low when average platform, and printing and dyeing effect is good
It is good.
Description of the drawings
Fig. 1 is a kind of preparation process schematic diagram of sizing afterwaxing agent of the present invention.
Fig. 2 is the 4th section of blending result schematic diagram of the preparation process of sizing afterwaxing agent of the present invention a kind of.
Specific implementation mode
Below in conjunction with attached drawing, by specific embodiment, the invention will be further described, these embodiments are merely to illustrate
The present invention is not limiting the scope of the invention.
A kind of sizing afterwaxing agent provided by the invention includes following raw material by weight percentage：The stone of 50-58%
Wax, the rilanit special of 19-25%, the stearic acid of 14-20%, the emulsifier of 8-10%, and, the antistatic agent of 0.1-0.3%.
The present invention, which is incorporated, improves that lubricity, flexibility, emulsibility be excellent and the material of antistatic property, solves universal both at home and abroad
Think the difficult point for using paraffin that can influence follow-up printing quality.Material proportion provided by the invention so that after waxing of the invention
Agent reaches sizing operation requirement, while meeting the dyeing quality requirement of printing and dyeing mill.
The paraffin uses industrial paraffin, it is preferred to use No. 58 semi-refined industrial paraffins are that the high-melting-point of hydro carbons is solid
Shape substance, abundance and price is low, flatness is excellent, is the common material that conventional fabrics improve flatness.Its These characteristics
So that advantageously reducing cost, the guarantee of raw material supply is conducive to industrialize continuous production.
The rilanit special uses technical grade.Preferably, the S-185 rilanit specials that the present invention uses,
It is the excellent emulsifier of excellent auxiliary agent and paraffin for improving soft yarns and convergence in half solid fraction.
The stearic acid has surface-active and lubricating action, is conducive to the emulsibility and lubrication that improve afterwaxing agent
Property.Technical grade, the industrial stearic acid of 69 DEG C of preferably fusing point can be used in the stearic acid.
The emulsifier level dyeing, emulsibility and scourability are excellent, can protect cerate colloid, and with wetting and diffusion
The superfine feature of performance, the emulsification for not only improving wax are conducive to printing quality again.The emulsifier selects conventional wax breast
Agent, preferred emulsifier op.
Electrostatic is generated when the antistatic agent is for eliminating weaving, reduces the end breakage rate of yarn, avoids sucking when weaving yarn empty
Dust in gas, and can be good with the associativity of paraffin.Conventional wax antistatic agent can be selected in the antistatic agent, preferably anti-quiet
Electric agent SM.
Since the component of material is complicated, when the afterwaxing agent of the application is using existing various processing technology blending processing,
Finished laminar easily occurs because uneven, influences using effect.Through repetition test, inventor has found using point four sections of blendings, respectively
Heating temperatures different Duan Caiyong, different mixing speeds can complete production process in the shorter process-cycle.Contrast test is such as
Shown in table 1.
Table 1：Various processing technologys compare
| Project | One-part form | Two-period form | Three-stage | Four-part form |
| Quality | It is unqualified | It is unqualified | It is unqualified | It is qualified |
| Process-cycle, h | ＞ 4 | ＞ 4 | ＞ 3 | 1.5 |
Wherein, one-part form refers to all materials while adding, heating stirring blending.Through experiment, which no matter temperature,
How mixing speed changes, and the process-cycle extends, and concocts product after cooling and will produce different degrees of layering, does not meet matter
Figureofmerit requirement.
Two-period form includes：First segment is mixed together all raw materials in addition to antistatic agent；Second segment, supplying are antistatic
Agent is concocted.Through experiment, no matter how temperature, mixing speed change which, and the process-cycle extends, and blending is after cooling
Product will produce different degrees of layering, not meet quality index requirement.
Three-stage includes：First segment is mixed together all raw materials in addition to antistatic agent；Electrostatic agent is added in second segment
Blending；Third section, cooling blending.Through experiment, no matter how temperature, mixing speed change which, and the process-cycle extends, blending
Product after cooling will produce different degrees of layering, not meet quality index requirement.
As shown in Figure 1, the manufacturing technique of the present invention are as follows four sections of processing：
First segment is processed, and paraffin, stearic acid are concocted by emulsifier, concocts 100 DEG C, mixing speed 70r/min of temperature,
Mixing time 0.5 hour.There are two purposes for first segment processing：It is adjusted first, higher melt material is melted in higher temperature section
It closes, second is that supplying emulsifier 6-8%（The major part of total emulsifiers dosage）, Emulsification of Paraffin is concocted.Experiments have shown that when material is few
Emulsification blending effect is good, and can shorten total blending period.
Second segment is processed, by rilanit special and the remaining emulsifier of first segment（The use of the emulsifier of second segment processing
Amount and the dosage of the emulsifier of first segment processing add up the 8-10% for afterwaxing agent, are calculated in mass percent）Blending, blending
80 DEG C, mixing speed 40r/min of temperature, mixing time about 0.5 hour.The second segment processing purpose be two kinds of fusing points it is low and
Easily fused material blending, saving heat energy and mixing time.Second segment is concocted work and first segment blending work and can be carried out at the same time,
And then reduce blending total time.
Third section is concocted the blending liquid of the first blending kettle and the blending liquid of the second blending kettle after antistatic agent is added, into
The total blending of row.When sampling observes that mixed liquor is Clear ＆ Transparent, show mix homogenously.It is 90 DEG C that third section, which concocts temperature, stirring
Speed is 50r/min, mixing time about 0.5 hour.The third section is blending critical section.
First segment blending solution is mixed with second segment blending solution, adds antistatic agent blending, temperature by the 4th section of blending
For degree at 80-85 DEG C, mixing speed is down to 20-25r/min, mixing time 0.5 hour or so, when forming mixed liquor, through naturally cold
But the bulk product formed afterwards is not stratified.The purpose of 4th section of blending is to ensure that the not stratified of finished product.Because the application it is rear on
The each component of cerate is not easy to fuse, and is easily layered.
Experiment shows when concocting temperature≤80 DEG C, no matter mixing speed how much, layering is all also easy to produce, when blending temperature
Also layering is generated at >=85 DEG C.Only 80-85 DEG C is being controlled when temperature（Not comprising 80 DEG C, 85 DEG C）And mixing speed control exists
When the section of 20-25r/min, product after cooling is not stratified（As shown in Figure 2）, meet quality index, illustrate to participate in reaction
Each group material has been concocted uniform completely, and sampling mixed liquor at this moment presents Clear ＆ Transparent, does not influence using effect.
Embodiment 1-4
Raw material is weighed by the formula of table 2, with above-mentioned four-part form blending method, prepares afterwaxing agent.
Table 2：The formula and waxing agent performance of embodiment 1-4
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Paraffin | 50 | 52 | 50 | 56 | 58 |
| Rilanit special | 25 | 23 | 21 | 20 | 19 |
| Stearic acid | 16.7 | 15 | 20 | 15.3 | 14 |
| Polyoxyethylene nonylphenol ether | 8 | 9.8 | 8.7 | 8.5 | 8.9 |
| Antistatic agent | 0.3 | 0.2 | 0.3 | 0.2 | 0.1 |
| Fusing point/ ASTMD127 ℃ | 54-56 | 54-56 | 54-56 | 54-56 | 54-56 |
| PH/1% aqueous solutions | 6-7 | 6-7 | 6-7 | 6-7 | 6-7 |
| Water solubility/range estimation | Stand 24 hours nothings point Layer and sediment | Stand 24 hours nothings point Layer and sediment | Stand 24 hours nothings Layering and sediment | Stand 24 hours nothings point Layer and sediment | Stand 24 hours nothings point Layer and sediment |
| Appearance/range estimation | Faint yellow solid is no different Taste, section is without layering | Faint yellow solid is no different Taste, section is without layering | Faint yellow solid without Peculiar smell, section without point Layer | Faint yellow solid is no different Taste, section is without layering | Faint yellow solid is no different Taste, section is without layering |
Sizing afterwaxing agent prepared by embodiment 1-5 and existing solubilised textile wax SW contrast tests waxing effect such as table
Shown in 3.
Table 3：Embodiment 1-5 sizing afterwaxing agent and existing solubilised textile wax SW contrast test situations
| Project | SW comparative examples 1 | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | SW comparative examples 2 |
| Experiment quantity, m | 36800 | 36800 | 36800 | 36800 | 36800 | 36800 | 36800 |
| Starch warp thread gross weight, kg | 3208 | 3206 | 3206 | 3206 | 3199 | 3199 | 3187 |
| The rotating ratio of sizing roller and waxing roller | 194:1 | 194:1 | 194:1 | 194:1 | 149:1 | 149:1 | 149:1 |
| Consume wax amount, kg | 3 | 3 | 3 | 3 | 4.6 | 4.6 | 6.8 |
| Waxing rate, % | 0.1 | 0.1 | 0.1 | 0.1 | 0.15 | 0. 15 | 0.22 |
| Wax liquor mean temperature, DEG C | 86 | 86 | 86 | 86 | 86 | 86.4 | 86.8 |
| Starch axis average weight, kg | 96.6 | 96.6 | 96.6 | 96.6 | 97.1 | 97.1 | 97.2 |
| Number when measuring cloth board | 137 | 117 | 117 | 117 | 184 | 184 | 145 |
| It is disconnected through number when average platform | 0.55 | 0.36 | 0.36 | 0.35 | 0.5 | 0.5 | 0.57 |
As shown in Table 3, identical in waxing rate, using the afterwaxing agent of the embodiment of the present invention 1-3 than present
It is disconnected through several low when the average platform of common SW class afterwaxing agents；Embodiment 4-5 is compared with comparative example 2, the afterwaxing agent of the application
Waxing rate is less than SW cerates, but disconnected through counting less than SW afterwaxing agents when average platform.Comparative test result show it is of the invention it is rear on
Cerate is than currently used domestic SW types sizing afterwaxing agent, disconnected to be greatly decreased through number in the case where waxing rate does not subtract, and has reached and had both dropped
It is low to use wax cost, and improve the effect of product quality.Through factory testing, after the embryo cloth using the afterwaxing agent of the present invention, dyeing
Quality is very good.
The afterwaxing agent of the present invention and domestic and international main afterwaxing agent are more as shown in table 4.
Table 4：Main afterwaxing agent compares both at home and abroad
| Title | Main component | 1% aqueous solution pH | Fusing point DEG C | Shape |
| Japanese After Wax | Esters+ethers | \ | 50 | Sheet |
| Solubilised textile wax SW | Aliphatic acid+fatty alcohol+polyoxyethylene ether | 6-7 | 47.5 | Sheet |
| Water-emulsifiable wax DHL | Aliphatic acid+polyoxyethylene+polyethenoxy ether | 7-8 | 46-56 | Paste |
| The afterwaxing agent of the present invention | Paraffin+stearic acid+rilanit special | 6-7 | 54-56 | Small bulk |
The present invention, as principal ingredients, is reduced cost of material, improves production using the rich paraffin of the excellent low price of flatness
The fusing point of product solves the problems, such as that the transport, storage and use of existing similar product exist.
In conclusion the cost of the afterwaxing agent of the present invention is relatively low, usage amount is few when waxing rate is identical, and disconnected when average platform
Through several low, printing and dyeing work well, the advantages that transporting, store and is easy to use.
Although present disclosure is discussed in detail by above preferred embodiment, but it should be appreciated that above-mentioned
Description is not considered as limitation of the present invention.After those skilled in the art have read the above, for the present invention's
A variety of modifications and substitutions all will be apparent.Therefore, protection scope of the present invention should be limited to the appended claims.
Claims (5)
1. a kind of sizing afterwaxing agent, which is characterized in that the afterwaxing agent is made of following raw material by weight percentage：
The paraffin of 50-58%, the rilanit special of 19-25%, the stearic acid of 14-20%, the emulsifier of 8-10%, and, 0.1-0.3%
Antistatic agent；The afterwaxing agent is prepared using four-part form mixing process, which includes：First segment,
Paraffin, stearic acid are concocted by emulsifier, concoct 100 DEG C, mixing speed 70r/min of temperature, mixing time 0.5 hour；The
Two sections, rilanit special is concocted with emulsifier, concocts 80 DEG C, mixing speed 40r/min of temperature, mixing time about 0.5 hour；The
Three sections, first segment blending solution is mixed with second segment blending solution, antistatic agent blending is added, blending temperature is 90 DEG C, is stirred
It is 50r/min, mixing time about 0.5 hour to mix speed；4th section, cooling blending, blending temperature is 80-85 DEG C, and is not selected
80 DEG C and 85 DEG C, mixing speed is down to 20-25r/min, mixing time 0.5 hour.
2. sizing afterwaxing agent as described in claim 1, which is characterized in that the emulsifier selects polyoxyethylene nonylphenol ether.
3. sizing afterwaxing agent as described in claim 1, which is characterized in that the paraffin is No. 58 paraffin, for half essence
Industrial paraffin is refined, fusing point is 58-60 DEG C.
4. sizing afterwaxing agent as described in claim 1, which is characterized in that the rilanit special selection S-185 hydrogenations
Castor oil.
5. a kind of purposes of sizing afterwaxing agent according to claim 1, which is characterized in that the afterwaxing agent is used for
Sizing operation carries out upper Lasaxing Oilfield using the afterwaxing agent to sizing.
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| CN103147294A (en) * | 2013-03-26 | 2013-06-12 | 无锡嘉德纺织制品有限公司 | Textile wax auxiliary and preparation method thereof |
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2016
- 2016-05-26 CN CN201610357459.6A patent/CN106012514B/en active Active
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101050596A (en) * | 2007-04-24 | 2007-10-10 | 杨建� | Environment protection spinning thread wax ring and its producing method |
| CN101575803A (en) * | 2009-06-04 | 2009-11-11 | 浙江新澳纺织股份有限公司 | Wool worsted yarn wax and production method thereof |
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