CN106007787A - Environment-friendly inorganic spongy water storage material and preparation method thereof - Google Patents
Environment-friendly inorganic spongy water storage material and preparation method thereof Download PDFInfo
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- CN106007787A CN106007787A CN201610323603.4A CN201610323603A CN106007787A CN 106007787 A CN106007787 A CN 106007787A CN 201610323603 A CN201610323603 A CN 201610323603A CN 106007787 A CN106007787 A CN 106007787A
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- 239000011232 storage material Substances 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 22
- 239000010451 perlite Substances 0.000 claims abstract description 10
- 235000019362 perlite Nutrition 0.000 claims abstract description 10
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 23
- 239000002131 composite material Substances 0.000 claims description 18
- 239000000463 material Substances 0.000 claims description 11
- 239000011148 porous material Substances 0.000 claims description 10
- 235000019738 Limestone Nutrition 0.000 claims description 9
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 9
- 239000010436 fluorite Substances 0.000 claims description 9
- 239000006028 limestone Substances 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 9
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 9
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 7
- 238000010304 firing Methods 0.000 claims description 7
- 238000000465 moulding Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims 4
- 239000011521 glass Substances 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 230000008901 benefit Effects 0.000 abstract description 5
- 230000007613 environmental effect Effects 0.000 abstract description 5
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052750 molybdenum Inorganic materials 0.000 abstract description 2
- 239000011733 molybdenum Substances 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 abstract 1
- 239000011324 bead Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000003860 storage Methods 0.000 abstract 1
- 238000010276 construction Methods 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 206010000269 abscess Diseases 0.000 description 1
- 239000010242 baoji Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000009189 diving Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003673 groundwater Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 239000008239 natural water Substances 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/08—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by adding porous substances
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/1324—Recycled material, e.g. tile dust, stone waste, spent refractory material
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- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/36—Glass starting materials for making ceramics, e.g. silica glass
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/38—Non-oxide ceramic constituents or additives
- C04B2235/3817—Carbides
- C04B2235/3826—Silicon carbides
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/444—Halide containing anions, e.g. bromide, iodate, chlorite
- C04B2235/445—Fluoride containing anions, e.g. fluosilicate
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention relates to an environment-friendly inorganic spongy water storage material. The environment-friendly inorganic spongy water storage material is characterized by being prepared from, by mass, 10-35 parts of molybdenum tailings, 20-55 parts of loess in the Guanzhong basin, 10-30 parts of expanded perlite (glass beads), 2-5 parts of a compound additive and 0.5-2 parts of a pore-forming agent. The invention further discloses a preparation method of the environment-friendly inorganic spongy water storage material. The environment-friendly inorganic spongy water storage material has the advantages of being simple in composition, low in preparation cost, high in water storage capacity and high in environmental benefit. Industrial tailings and loess in the Guanzhong basin are selected as main raw materials, and thus secondary pollution is avoided in the production process.
Description
Technical field
The present invention relates to a kind of water-storage material and preparation method, specifically a kind of sponginess green phosphor water-storage material and preparation method, belong to inorganic material material manufacturing technology field.
Background technology
Inorganic water-storage material is wide, cheap because of saturated aqueous rate height, good endurance, use environmental field, is easily processed into the steps filtering material of different-grain diameter proportioning and comes into one's own, is preferred material and the basic material of sponge urban construction from now on.
The sunk type diving greenery patches built up with inorganic water-storage material, substitutes the greenery patches in existing city, greenery patches, residential quarters and lays roof, greenery patches, retaining rainwater from the charge for remittance source of Urban Rain.Inorganic water-storage material also can be widely used to multiple fields such as urban flowers and family's cultivation, environmental conservation, soil improvement, has market prospect widely.
Apply inorganic water-storage material to implement sponge urban engineering construction, be possible not only to realize Rainwater Resources in Urban Area, save the use after engineering is built up and management cost, but also engineering can be saved in a large number and build investment.Prove that the investment implementing Rainwater Resources management engineering will be saved about the half of engineering construction investment expense compared to traditional scheme drainage system and afforestation project implemented step by step according to related data introduction at the over thousands of case history that Germany is implemented.
Inorganic water-storage material is a kind of novel cystose ceramic material, has physical aspect stable under saturated aqueous or drying regime, physical strength.Its abscess dense distribution is uniform, is generally polygonal in shape, minority is circle, and most pores are hole of holding one's breath, and hole wall is thin, and water absorption rate is up to 70-110%.
The present invention uses industrial tailings and Central Shanxi Plain loess to be primary raw material.In succession there is mine tailing dam break serious accident in some province ground of China in recent years, causes serious personnel's property damage, and industrial tailings has become one of threat human health major hidden danger factor with safety.The only the most newly-increased mine tailing 13,500,000 tons of Shaanxi Jinduicheng Molybdenum Industry Corp one, current mine tailing stock 2.6 hundred million tons, floor space about 35 hectares.In Shanglou in Shaanxi, Baoji, Hanzhong, the safe and comfortable ground substantial amounts of metal mine of municipalization, a large amount of mine tailing of annual output.Central Shanxi Plain loess easily takes inexpensively, and stable components, clay sculpture physical and chemical performance is excellent.
Utilizing mine tailing raw material production to manufacture inorganic water-storage material is a green circulation economy industrial process.
Summary of the invention
The invention aims to solve rain water runoff and vegetation water shortage problem.Mining of groundwater is excessive now, and ground occurs that hollow is subsided, and city's green areas is not enough, and the natural water drain evaporations in vain such as nature sleet.The reality not corresponded with " naturally stockpile, the sponge city of naturally osmotic, self-purification function ", thus a kind of new technical scheme is provided.
For achieving the above object, the invention discloses following technical scheme:
A kind of sponginess green phosphor water-storage material, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 10～35 parts, Central Shanxi Plain loess 20～55 parts, expanded perlite (glass microballoon) 10～30 parts, composite assistant 2～5 parts, pore former 0.5～2 parts.
As a kind of preferred version, described composite assistant includes following raw material in terms of mass parts:
Carborundum powder 5～15 parts, limestone 70～85 parts, fluorite 5～15 parts.
As a kind of preferred version, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 30 parts, Central Shanxi Plain loess 45.5 parts, expanded perlite (glass microballoon) 20 parts, composite assistant 3 parts, pore former 1.5 parts, wherein, composite assistant includes following raw material in terms of mass parts: carborundum powder 10 parts, limestone 80 parts, 10 parts of fluorite.
The present invention also provides for the preparation method of a kind of sponginess green phosphor water-storage material as above, comprises the steps:
(1) ground and mixed: above-mentioned various component materials weigh in proportion, loads in ball mill, adds the water of 29%, grind；
(2) molding: going out the mud after mill and be dehydrated the moisture to 20% in Gypsum Fibrosum, mud cake shovel is divided into block, is dried in an oven；
(3) burn till: loading the block in step (2) in crucible to enter stove and burn till, temperature controls at 850～1180 DEG C, firing time 8～be prepared from for 10 hours.
As a kind of preferred version, in described step (1), grind to 250 mesh.
As a kind of preferred version, in described step (2), mud cake is divided into the block of a size of 20～30mm.
As a kind of preferred version, in described step (2), it is dried in an oven to moisture less than 2%.
A kind of sponginess green phosphor water-storage material disclosed by the invention and preparation method thereof, has the advantages that
Prescription is few, and low cost of manufacture, water-holding capacity are strong, and environmental benefit is high.Select industrial tailings and Central Shanxi Plain loess as primary raw material, production process does not exist secondary pollution.
Test proves, success integrated cost of the present invention is low, is a kind of novel green water-storage material.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
A kind of sponginess green phosphor water-storage material, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 32.5 parts, Central Shanxi Plain loess 42.5 parts, expanded perlite (glass microballoon) 22.5 parts, composite assistant 2 parts, pore former 0.5 part.
In the present embodiment, described composite assistant includes following raw material in terms of mass parts:
Carborundum powder 5 parts, limestone 70 parts, 5 parts of fluorite.
The present invention also provides for the preparation method of a kind of sponginess green phosphor water-storage material as above, comprises the steps:
(1) ground and mixed: above-mentioned various component materials weigh in proportion, loads in ball mill, adds the water of 29%, grind；
(2) molding: going out the mud after mill and be dehydrated the moisture to 20% in Gypsum Fibrosum, mud cake shovel is divided into block, is dried in an oven；
(3) burn till: entering stove in the block in step (2) is loaded crucible and burn till, temperature controls at 850 DEG C, and firing time is prepared from for 8 hours.
In the present embodiment, in described step (1), grind to 250 mesh.
In the present embodiment, in described step (2), mud cake is divided into the block of a size of 20mm.
In the present embodiment, in described step (2), it is dried in an oven to moisture less than 2%.
Embodiment 2
A kind of sponginess green phosphor water-storage material, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 35 parts, Central Shanxi Plain loess 50 parts, expanded perlite (glass microballoon) 25 parts, composite assistant 5 parts, pore former 2 parts.
In the present embodiment, described composite assistant includes following raw material in terms of mass parts:
Carborundum powder 15 parts, limestone 85 parts, 15 parts of fluorite.
The present invention also provides for the preparation method of a kind of sponginess green phosphor water-storage material as above, comprises the steps:
(1) ground and mixed: above-mentioned various component materials weigh in proportion, loads in ball mill, adds the water of 29%, grind；
(2) molding: going out the mud after mill and be dehydrated the moisture to 20% in Gypsum Fibrosum, mud cake shovel is divided into block, is dried in an oven；
(3) burn till: entering stove in the block in step (2) is loaded crucible and burn till, temperature controls at 1180 DEG C, and firing time is prepared from for 10 hours.
In the present embodiment, in described step (1), grind to 250 mesh.
In the present embodiment, in described step (2), mud cake is divided into the block of a size of 30mm.
In the present embodiment, in described step (2), it is dried in an oven to moisture less than 2%.
Embodiment 3
A kind of sponginess green phosphor water-storage material, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 30 parts, Central Shanxi Plain loess 45.5 parts, expanded perlite (glass microballoon) 20 parts, composite assistant 3 parts, pore former 1.5 parts, wherein, composite assistant includes following raw material in terms of mass parts: carborundum powder 10 parts, limestone 80 parts, 10 parts of fluorite.
The present invention also provides for the preparation method of a kind of sponginess green phosphor water-storage material as above, comprises the steps:
(1) ground and mixed: above-mentioned various component materials weigh in proportion, loads in ball mill, adds the water of 29%, grind；
(2) molding: going out the mud after mill and be dehydrated the moisture to 20% in Gypsum Fibrosum, mud cake shovel is divided into block, is dried in an oven；
(3) burn till: entering stove in the block in step (2) is loaded crucible and burn till, temperature controls at 1000 DEG C, and firing time is prepared from for 9 hours.
In the present embodiment, in described step (1), grind to 250 mesh.
In the present embodiment, in described step (2), mud cake is divided into the block of a size of 25mm.
In the present embodiment, in described step (2), it is dried in an oven to moisture less than 2%.
Embodiment 4
A kind of sponginess green phosphor water-storage material, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 10 parts, Central Shanxi Plain loess 20 parts, expanded perlite (glass microballoon) 10 parts, composite assistant 3 parts, pore former 1.5 parts, wherein, composite assistant includes following raw material in terms of mass parts: carborundum powder 10 parts, limestone 80 parts, 10 parts of fluorite.
The present invention also provides for the preparation method of a kind of sponginess green phosphor water-storage material as above, comprises the steps:
(1) ground and mixed: above-mentioned various component materials weigh in proportion, loads in ball mill, adds the water of 29%, grind；
(2) molding: going out the mud after mill and be dehydrated the moisture to 20% in Gypsum Fibrosum, mud cake shovel is divided into block, is dried in an oven；
(3) burn till: entering stove in the block in step (2) is loaded crucible and burn till, temperature controls at 1000 DEG C, and firing time is prepared from for 9 hours.
In the present embodiment, in described step (1), grind to 250 mesh.
In the present embodiment, in described step (2), mud cake is divided into the block of a size of 25mm.
In the present embodiment, in described step (2), it is dried in an oven to moisture less than 2%.
Embodiment 5
Embodiment 3
A kind of sponginess green phosphor water-storage material, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 35 parts, Central Shanxi Plain loess 55 parts, expanded perlite (glass microballoon) 30 parts, composite assistant 3 parts, pore former 1.5 parts, wherein, composite assistant includes following raw material in terms of mass parts: carborundum powder 10 parts, limestone 80 parts, 10 parts of fluorite.
The present invention also provides for the preparation method of a kind of sponginess green phosphor water-storage material as above, comprises the steps:
(1) ground and mixed: above-mentioned various component materials weigh in proportion, loads in ball mill, adds the water of 29%, grind；
(2) molding: going out the mud after mill and be dehydrated the moisture to 20% in Gypsum Fibrosum, mud cake shovel is divided into block, is dried in an oven；
(3) burn till: entering stove in the block in step (2) is loaded crucible and burn till, temperature controls at 1000 DEG C, and firing time is prepared from for 9 hours.
In the present embodiment, in described step (1), grind to 250 mesh.
In the present embodiment, in described step (2), mud cake is divided into the block of a size of 25mm.
In the present embodiment, in described step (2), it is dried in an oven to moisture less than 2%.
A kind of sponginess green phosphor water-storage material of disclosure of the invention, empirical tests,
Volume saturated water absorption ＞ 70%
Bulk density ＜ 300kg/m3
Comprcssive strength ＞ 2MPa.
Prescription is few, and low cost of manufacture, water-holding capacity are strong, and environmental benefit is high.
The above is only the preferred embodiment of the present invention, is not intended to limit；Should be understood that, although the present invention being described in detail with reference to the various embodiments described above, it will be understood by those within the art that, the technical scheme described in the various embodiments described above still can be modified by it, or the most some or all of technical characteristic is carried out equivalent；And these amendments and replacement, do not make the essence of corresponding technical scheme depart from the scope of various embodiments of the present invention technical scheme.
Claims (7)
1. a sponginess green phosphor water-storage material, it is characterised in that include by following with matter
The preparation that the raw material of amount part meter is made:
Molybdic tailing 10～35 parts, Central Shanxi Plain loess 25～55 parts, expanded perlite 10～30 parts,
Composite assistant 2～5 parts, pore former 0.5～2 parts.
A kind of sponginess green phosphor water-storage material the most according to claim 1, its feature
Being, described composite assistant includes following raw material in terms of mass parts:
Carborundum powder 5～15 parts, limestone 70～85 parts, fluorite 5～15 parts.
A kind of sponginess green phosphor water-storage material the most according to claim 2, its feature
It is, the preparation including being made up of following raw material in terms of mass parts:
Molybdic tailing 30 parts, Central Shanxi Plain loess 45.5 parts, expanded perlite 20 parts, composite assistant
3 parts, pore former 1.5 parts, wherein, composite assistant includes following raw material in terms of mass parts:
Carborundum powder 10 parts, limestone 80 parts, 10 parts of fluorite.
4. the preparation of the sponginess green phosphor water-storage material as described in claim 1-3
Method, it is characterised in that comprise the steps:
(1) ground and mixed: above-mentioned various component materials weigh in proportion, loads in ball mill,
Add the water of 29%, grind；
(2) molding: going out the mud after mill and be dehydrated the moisture to 20% in Gypsum Fibrosum, mud cake is used
Shovel is divided into block, is dried in an oven；
(3) burn till: enter stove in the block in step (2) is loaded crucible and burn till, temperature
Control at 850～1180 DEG C, firing time 8～be prepared from for 10 hours.
The preparation of a kind of sponginess green phosphor water-storage material the most according to claim 4
Method, it is characterised in that in described step (1), grind to 250 mesh.
The preparation of a kind of sponginess green phosphor water-storage material the most according to claim 4
Method, it is characterised in that in described step (2), is divided into a size of 20～30mm by mud cake
Block.
The preparation of a kind of sponginess green phosphor water-storage material the most according to claim 4
Method, it is characterised in that in described step (2), is dried to moisture in an oven less than 2%.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106747615A (en) * | 2017-03-09 | 2017-05-31 | 咸阳陶瓷研究设计院 | A kind of method that utilization molybdenum tailing produces ceramic thermal insulation plate |
| CN108947561A (en) * | 2018-09-18 | 2018-12-07 | 咸阳陶瓷研究设计院有限公司 | A kind of inorganic water-storage material multiple elements design pore-forming technique |
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| CN114409428A (en) * | 2021-12-08 | 2022-04-29 | 金堆城钼业股份有限公司 | Inorganic tailing-based liquid adsorption storage material and preparation method thereof |
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