CN106000257A - Rapid neutralization reaction tank in mica cladding work - Google Patents
Rapid neutralization reaction tank in mica cladding work Download PDFInfo
- Publication number
- CN106000257A CN106000257A CN201610367279.6A CN201610367279A CN106000257A CN 106000257 A CN106000257 A CN 106000257A CN 201610367279 A CN201610367279 A CN 201610367279A CN 106000257 A CN106000257 A CN 106000257A
- Authority
- CN
- China
- Prior art keywords
- kettle
- muscovitum
- retort
- shaft
- cladding
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
- C09C3/063—Coating
Abstract
The invention belongs to the technical field of mica processing, and relates to a rapid neutralization reaction tank in mica cladding work. The tank comprises a kettle body, a stirring mechanism is arranged in the kettle body, the inner wall of the kettle body is fixedly provided with a flow disturbing mechanism being able to collide with a liquid in the flowing process of the liquid in the kettle body in order to change the flow direction of the liquid, a hollow distribution disc is arranged in the kettle body, and the lower surface of the distribution disc is closely provided with discharging holes. The rapid neutralization reaction tank allows an acid and an alkali to be rapidly and uniformly mixed with a reaction solution in the acid and alkali neutralization process in order to realize rapid neutralization, so the mica cladding quality is improved.
Description
Technical field
The invention belongs to Muscovitum processing technique field, relate to a kind of Muscovitum cladding operation quick
Neutralize retort.
Background technology
Mica titanium nacreous material is with splitting as substrate, at smooth mica surface
Superscribe the titanium dioxide of transparent or relatively transparent high index of refraction and the thin of ferrum oxide composition
Layer.When fiber-optic illuminated to time on mica sheet, mica sheet is just as transparent small mirror, part
Light reflects away, and part fiber is transmissive in the way of refraction.Through the light gone
It is refracted on next interface, secondary partially reflective and fractional transmission occurs again, depends on
Secondary continue.Being known by physical optics, the light at two reflective surface can be mutually
Effect, the result of interaction depends on the factors such as phase contrast, angle of incidence, refractive index,
Thus form the pearly-lustre phenomenon interfering feature.
In encapsulation process, it is common that by Muscovitum and TiCl4、FeCl3Solution mixes, and adds
Acid adds alkali regulation pH value, makes TiCl4And FeCl3Change in TiCl2And Fe2O3, parcel
Outside Muscovitum, reach covered effect.During cladding, constant pH can improve
Cladding quality, but prior art is in the adition process of acid or alkali, tends not to realize
The effect of rapid dispersion, neutralizes speed slower.
Chinese patent literature discloses a kind of single coating cobalt titanate green/nacreous mica composite pigment
Preparation method [application number: 201310474467.5], use the sedimentation method, with pretreatment
Muscovitum is substrate, is configured to Muscovitum slurry with deionized water dispersion Muscovitum, adds a small amount of hydrochloric acid
Acidifying, under stirring at 80 DEG C, is slowly added dropwise TiCl4Acid solution and soluble cobalt
Mixed solution, is simultaneously added dropwise sodium hydroxide solution, drips complete regulation pH to 9, ripening,
Filtration washing is dried, and obtains yellow green composite pigment at 1000 DEG C of calcining 2h.Compound face
Material surface is nano grade titanium cobalt green particle, uniform in mica surface cladding densification, cladding
Lightness and the form and aspect of composite pigment are had an impact by rate.When material molar ratio Co/Ti >=2,
The characteristic diffraction peak of composite pigment surface spinel-type cobalt titanate green is notable.The cloud of different-grain diameter
Female covered effect is different, and particle diameter 20-100 μm Muscovitum is that the cobalt titanate green of substrate cladding is combined
The glittering pearl effect of pigment is notable.This is a kind of novel high-performance mica-based yellow green pearl
Photoreactivation pigment, performance is better than common nacreous mica pigment, and preparation technology is simple.
But said method " is adding the acidifying of a small amount of hydrochloric acid, under stirring at 80 DEG C, slowly
Dropping TiCl4Acid solution and the mixed solution of soluble cobalt, be simultaneously added dropwise hydroxide
Sodium solution, drips complete regulation pH to 9 " problem that also do not addresses how quickly to neutralize.
Summary of the invention
It is an object of the invention to for the problems referred to above, it is provided that a kind of Muscovitum cladding operation is quick
Neutralize retort.
For reaching above-mentioned purpose, present invention employs following technical proposal: a kind of Muscovitum bag
Cover operation and quickly neutralize retort, including kettle, in described kettle, be provided with rabbling mechanism,
Described inner wall of kettle is fixed with one and can occur with liquid when the liquid in kettle flows
Collide thus change the flow-disturbing mechanism of liquid flow direction, in described kettle, be additionally provided with one
The individual cloth tray in hollow, the lower surface of described cloth tray is densely covered with discharge opening.
Quickly neutralize in retort in above-mentioned Muscovitum cladding operation, described flow-disturbing mechanism
Including at least one piece of spoiler being fixed on inner wall of kettle.
Quickly neutralize in retort in above-mentioned Muscovitum cladding operation, described flow-disturbing mechanism
The spoiler being fixed on inner wall of kettle including at least one row, described spoiler is along kettle
Circumferentially-spaced uniform setting.
Quickly neutralizing in retort in above-mentioned Muscovitum cladding operation, described spoiler is extremely
Rare two rows, and two adjacent row's spoilers are in being crisscross arranged.
Quickly neutralize in retort in above-mentioned Muscovitum cladding operation, described rabbling mechanism
Including driver and the shaft that is connected with driver, if being fixed with on described shaft
Dry stirring paddle, described cloth tray center has sealing ring ringwise, this sealing ring
Upper/lower terminal is connected, in sealing ring with upper and lower two face seals of cloth tray respectively
Between form resigning hole, described shaft passes resigning hole, and the aperture of resigning hole is more than stirring
Mix the diameter of axle.
Quickly neutralize in retort in above-mentioned Muscovitum cladding operation, described stirring paddle edge
The axially spaced-apart of shaft arranges uniformly.
Quickly neutralize in retort in above-mentioned Muscovitum cladding operation, described cloth tray position
Between two adjacent stirring paddles.
Compared with prior art, it is an advantage of the current invention that: during acid-base neutralization, it is possible to make
Soda acid is quickly mixed homogeneously with reactant liquor, thus quickly neutralizes, and improves the matter of Muscovitum cladding
Amount.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention；
Fig. 2 is the structural representation of shower tray；
Fig. 3 is the structural representation of shower tray lower surface；
Fig. 4 is the partial structurtes schematic diagram of reactor inwall.
In figure: kettle 1, rabbling mechanism 2, flow-disturbing mechanism 3, cloth tray 4, discharge opening
5, spoiler 6, driver 7, shaft 8, stirring paddle 9, sealing ring 10, step down
Hole 11, feeding engine 100, neutralizer storage tank 101.
Detailed description of the invention
With detailed description of the invention the present invention done further details of theory below in conjunction with the accompanying drawings
Bright.
As shown in figures 1 and 3, a kind of Muscovitum cladding operation quickly neutralizes retort, bag
Including kettle 1, autoclave body bottom is plane, is provided with rabbling mechanism 2 in described kettle 1,
Rabbling mechanism 2 includes driver 7 and the shaft 8 being connected with driver 7, described
Being fixed with some stirring paddles 9 on shaft 8, described kettle 1 inwall is fixed with one
Can collide with liquid when the liquid in kettle 1 flows thus change liquid flowing side
To flow-disturbing mechanism 3, be additionally provided with a cloth tray 4 in hollow in described kettle 1,
The lower surface of described cloth tray 4 is densely covered with discharge opening 5.
Flow-disturbing mechanism 3 includes at least one piece of spoiler 6 being fixed on kettle 1 inwall.
When liquid or Muscovitum collide with spoiler 6, flow direction changes, it is achieved turbulent flow or
Sinuous flow, it is thus possible to the mixing uniformity improved between Muscovitum and reactant liquor, carries further
High reaction efficiency and the quality of raising cladding.
Flow-disturbing mechanism 3 includes the spoiler 6 that at least one row is fixed on kettle 1 inwall,
Described spoiler 6 is along the circumferentially-spaced uniform setting of kettle 1.
Spoiler 6 at least two row, and two adjacent row's spoilers 6 are in being crisscross arranged.
Described cloth tray 4 center has sealing ring 10 ringwise, this sealing ring 10
Upper/lower terminal be connected with upper and lower two face seals of cloth tray 4 respectively, seal
Enclosing 10 intermediate formation resigning holes 11, described shaft 8, through resigning hole 11, is stepped down
The aperture in hole 11 is more than the diameter of shaft 8.When making resigning hole 11, Ke Yixian
Dig a hole at cloth tray 4 center, in hole, then insert circular sealing ring and cloth
Charging tray 4 seals, and sealing ring is ring-type, therefore can form resigning hole 11, or use metal
Band replacement seal circle, metal tape welds the structure that can form resigning hole 11 with cloth tray 4.
Stirring paddle 9 arrange uniformly along the axially spaced-apart of shaft 8.Cloth tray 4
Between two adjacent stirring paddles 9.When neutralizer discharging from cloth tray 4, can
Directly it is stirred oar 9 rapid dispersion, quickly mixes with the liquid in kettle 1 and neutralize
Reaction.
The operation principle of the present invention is: cloth tray 4 successively with feeding engine 100 and neutralizer
Storage tank 101 connects, and neutralizer can enter in kettle 1 by cloth tray 4, stirring paddle
9 rotations make the liquid in kettle 1 clash into the change flow direction with spoiler 6.When needs are to still
When body 1 adds acid or alkali liquor is neutralized, neutralizer overflows from discharge opening 5, by
It is positioned at cloth tray 4 lower surface in discharge opening 5, blocks thus without by Muscovitum, stirring paddle
9 rotate, and make neutralizer be quickly dispersed, and in dispersive process, liquid runs into spoiler 6
Produce sinuous flow and turbulent flow, improve mixing efficiency further, make neutralization reaction quickly carry out.
Specific embodiment described herein is only to present invention spirit theory for example
Bright.Those skilled in the art can be to described specific embodiment
Make various amendment or supplement or use similar mode to substitute, but without departing from
The spirit of the present invention or surmount scope defined in appended claims.
Although the most more employing kettle 1, rabbling mechanism 2, flow-disturbing mechanism 3, cloth
Charging tray 4, discharge opening 5, spoiler 6, driver 7, shaft 8, stirring paddle 9, close
The terms such as seal 10, resigning hole 11, feeding engine 100, neutralizer storage tank 101, but also
It is not excluded for using the probability of other term.These terms are used to be only used to more convenient
Describe and explain the essence of the present invention；It is construed as any additional restriction
It is all contrary with spirit of the present invention.
Claims (7)
1. the operation of Muscovitum cladding quickly neutralizes a retort, including kettle (1), described
Kettle (1) in be provided with rabbling mechanism (2), it is characterised in that described kettle (1)
Inwall be fixed with one when in kettle (1) liquid flow time can with liquid collide from
And change the flow-disturbing mechanism (3) of liquid flow direction, it is additionally provided with in described kettle (1)
One cloth tray (4) in hollow, the lower surface of described cloth tray (4) is densely covered with out
Material hole (5).
Muscovitum the most according to claim 1 cladding operation quickly neutralizes retort, its
Being characterised by, described flow-disturbing mechanism (3) includes that at least is fixed on a kettle (1)
Spoiler (6) on inwall.
Muscovitum the most according to claim 1 cladding operation quickly neutralizes retort, its
Being characterised by, described flow-disturbing mechanism (3) includes that at least one row is fixed on kettle (1)
Spoiler (6) on inwall, described spoiler (6) is along between the circumference of kettle (1)
Arrange every uniform.
Muscovitum the most according to claim 3 cladding operation quickly neutralizes retort, its
It is characterised by, described spoiler (6) at least two row, and two adjacent row's spoilers
(6) in being crisscross arranged.
Muscovitum the most according to claim 1 cladding operation quickly neutralizes retort, its
Be characterised by, described rabbling mechanism (2) include driver (7) and with driver (7)
The shaft (8) connected, described shaft (8) is fixed with some stirring paddles (9),
Described cloth tray (4) center has sealing ring (10) ringwise, this sealing ring (10)
Upper/lower terminal be connected with upper and lower two face seals of cloth tray (4) respectively, close
Seal (10) intermediate formation resigning hole (11), described shaft (8) is through stepping down
Hole (11), the aperture of resigning hole (11) is more than the diameter of shaft (8).
Muscovitum the most according to claim 5 cladding operation quickly neutralizes retort, its
Being characterised by, described stirring paddle (9) is uniform along the axially spaced-apart of shaft (8)
Arrangement.
Muscovitum the most according to claim 5 cladding operation quickly neutralizes retort, its
Being characterised by, described cloth tray (4) is positioned between two adjacent stirring paddles (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610367279.6A CN106000257A (en) | 2016-05-30 | 2016-05-30 | Rapid neutralization reaction tank in mica cladding work |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610367279.6A CN106000257A (en) | 2016-05-30 | 2016-05-30 | Rapid neutralization reaction tank in mica cladding work |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106000257A true CN106000257A (en) | 2016-10-12 |
Family
ID=57092582
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610367279.6A Pending CN106000257A (en) | 2016-05-30 | 2016-05-30 | Rapid neutralization reaction tank in mica cladding work |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106000257A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115193387A (en) * | 2022-07-22 | 2022-10-18 | 诸城泰盛化工股份有限公司 | Trichloroisocyanuric acid removing device |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3865910A (en) * | 1971-05-20 | 1975-02-11 | Shoichiro Hori | Apparatus and method for causing contact between gas and liquid |
| CN204544172U (en) * | 2015-01-06 | 2015-08-12 | 天津市浩宇助剂有限公司 | A kind of reactor with three layers of baffle arrangement |
| CN104955774A (en) * | 2012-12-11 | 2015-09-30 | 住友金属矿山株式会社 | Processing device and processing method for hydrogen-sulphide-containing barren solution |
| CN204911499U (en) * | 2015-08-24 | 2015-12-30 | 成都杰晟蜀邦新材料科技有限公司 | Auxiliary agent adds distribution apparatus |
-
2016
- 2016-05-30 CN CN201610367279.6A patent/CN106000257A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3865910A (en) * | 1971-05-20 | 1975-02-11 | Shoichiro Hori | Apparatus and method for causing contact between gas and liquid |
| CN104955774A (en) * | 2012-12-11 | 2015-09-30 | 住友金属矿山株式会社 | Processing device and processing method for hydrogen-sulphide-containing barren solution |
| CN204544172U (en) * | 2015-01-06 | 2015-08-12 | 天津市浩宇助剂有限公司 | A kind of reactor with three layers of baffle arrangement |
| CN204911499U (en) * | 2015-08-24 | 2015-12-30 | 成都杰晟蜀邦新材料科技有限公司 | Auxiliary agent adds distribution apparatus |
Non-Patent Citations (1)
| Title |
|---|
| 陈志平等: "《搅拌与混合设备设计选用手册》", 31 May 2004, 化学工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115193387A (en) * | 2022-07-22 | 2022-10-18 | 诸城泰盛化工股份有限公司 | Trichloroisocyanuric acid removing device |
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| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161012 |