CN105997675A - Mosquito repellent water containing green pepper extracts and preparation method of mosquito repellent water - Google Patents

Mosquito repellent water containing green pepper extracts and preparation method of mosquito repellent water Download PDF

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Publication number
CN105997675A
CN105997675A CN201610460260.6A CN201610460260A CN105997675A CN 105997675 A CN105997675 A CN 105997675A CN 201610460260 A CN201610460260 A CN 201610460260A CN 105997675 A CN105997675 A CN 105997675A
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China
Prior art keywords
extract
mosquito
plant extract
repellent water
mosquito repellent
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Pending
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CN201610460260.6A
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Chinese (zh)
Inventor
陈蕾
张锋伦
孙达锋
吴生高
张卫明
马仕宏
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Institution Of Comprehensive Utllization Of Wild Plants All China Federation Of Supply And Maketing C00peratives
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Institution Of Comprehensive Utllization Of Wild Plants All China Federation Of Supply And Maketing C00peratives
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Priority to CN201610460260.6A priority Critical patent/CN105997675A/en
Publication of CN105997675A publication Critical patent/CN105997675A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/02Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/81Preparation or application process involves irradiation

Abstract

The invention provides mosquito repellent water containing green pepper extracts and a preparation method of the mosquito repellent water. The mosquito repellent water is prepared from components in percentage by weight as follows: 1%-5% of plant extract, 40%-75% of ethanol and the balance of deionized water, wherein the plant extract is prepared from raw materials in parts by weight as follows: 25-40 parts of green pepper, 10-20 parts of lavender, 10-20 part of roses, 5-15 parts of wrinkled gianthyssop herbs and 5-15 parts of mint with a method shown as follows: the raw materials are mixed, cleaned, drained, dried and crushed, the crushed powder is added to the deionized water in a material-water ratio and extracted with a microwave-assisted extraction technology, an extracting solution is filtered, and filtrate is the plant extract. The mosquito repellent water has the mosquito repellent effect and further has the efficacy of refreshing, restoring consciousness, cooling, relieving itching, inhibiting and killing bacteria, protecting skin against bite by insects and the like; besides, raw materials of the product are from plants, and the mosquito repellent water is safe, non-toxic and applicable to various crowds and various skin.

Description

A kind of mosquito-repellent water containing Zanthoxylum schinifolium extract and preparation method thereof
Technical field
The invention belongs to plant extract and daily-use chemical industry technical field, particularly to one with Zanthoxylum schinifolium extract be Mosquito-repellent water of main component and preparation method thereof.
Background technology
Mosquito bite not only can cause red swelling of the skin, pruritus and inflammation, it is also possible to spreads disease, as malaria, The diseases such as Gordon's heat, filaricide all can be sucked human blood by mosquito and be propagated, and serious threat human body is healthy.
Mosquito-repellent water in the market is varied, but main or the diethyltoluamide with synthetic, anophelifuge Ester and dimethyl phthalate are primary raw material, and these raw materials have certain toxicity to mammal, In use, people can absorb toxicant, the above anophelifuge of life-time service by respiratory tract, digestive tract etc. Water may induce the diseases such as asthma, the most also can teratogenesis, carcinogenic.Therefore, the material generation of plant origin is used Make mosquito-repellent water for synthesis material, prepare a kind of nontoxic, non-stimulated to human body mosquito-repellent water, will become a kind of New trend.
Zanthoxylum schinifolium (Zanthoxylum schinifolium Sieb.et Zucc) is distributed mainly on including China Asian countries, in America, African and Oceanian subtropical and tropical zones also have distribution.Due to Zanthoxylum schinifolium Containing compositions such as abundant volatile oil, alkaloid, amide, coumarin and lignanoids, have antibacterial, antiviral, Effects such as analgesia, raising immunity of organisms, protection cardiovascular so that it is at food, medicine, agricultural and daily use chemicals row Industry has huge application potential;But up to the present, market not yet occurs with Zanthoxylum schinifolium for the most former The mosquito-repellent water of material.
Summary of the invention
An object of the present invention is to provide a kind of mosquito-repellent water containing Zanthoxylum schinifolium extract, and this mosquito-repellent water predominantly contains Zanthoxylum schinifolium extract, it has safety non-toxic, can effectively prevent the effect of mosquito bite.
The two of the purpose of the present invention are to provide the preparation method of a kind of mosquito-repellent water containing Zanthoxylum schinifolium extract.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of mosquito-repellent water containing Zanthoxylum schinifolium extract, according to percentage by weight, its component and content is: plant carries Taking thing 1%-5%, ethanol 40%-75%, remaining is deionized water;Described plant extract is by following weight The raw material of part proportioning is prepared from: Zanthoxylum schinifolium 25-40 part, lavandula angustifolia 10-20 part, Flos Rosae Rugosae 10-20 part, the leaves of pulse plants Fragrant 5-15 part and Herba Menthae 5-15 part.
Further, described plant extract is to be prepared from by the raw material of following weight: Zanthoxylum schinifolium 35 parts, lavandula angustifolia 15 parts, 15 parts of Flos Rosae Rugosae, Herba Pogostemonis 7.5 parts and Herba Menthae 7.5 parts.
Further, according to percentage by weight, the component of described mosquito-repellent water and content it is: plant extract 1%-5%, ethanol 65%-75%, remaining is deionized water.
Further, described plant extract is to utilize microwave auxiliary extraction technology to extract to obtain.
The preparation method of a kind of mosquito-repellent water containing Zanthoxylum schinifolium extract, comprises the following steps:
(1) preparation of plant extract: Zanthoxylum schinifolium, lavandula angustifolia, Flos Rosae Rugosae, Herba Pogostemonis and Herba Menthae are entered in proportion Row mixing;The most cleaned, drain, be dried and pulverize, will pulverize after powder press solid-liquid ratio addition deionization Water, then use microwave auxiliary extraction technology to extract, filters extracting solution, the filtrate obtained be described in plant Thing extract;(2) by plant extract obtained above, ethanol and deionized water according to following percentage by weight Mix homogeneously: plant extract 1-5%, ethanol 40%-75%, remaining is deionized water;Canned, final To described mosquito-repellent water.
Further, the raw material of described plant extract mixes according to following weight: Zanthoxylum schinifolium 25-40 part, lavandula angustifolia 10-20 part, Flos Rosae Rugosae 10-20 part, Herba Pogostemonis 5-15 part, Herba Menthae 5-15 part.
Further, described raw material pulverizing is coarse pulverization, and the granularity of the described raw material of 90% is less than 20 mesh.Institute Stating solid-liquid ratio is 1:6-1:1.In described microwave auxiliary extraction technology, the power of microwave is 100W-300W, micro- The time of ripple is 1-2h, and Extracting temperature is 45-65 DEG C.
Plant extract of the present invention, choosing Zanthoxylum schinifolium is main anophelifuge raw material, add lavandula angustifolia, Flos Rosae Rugosae, Herba Pogostemonis and Herba Menthae, carry out mixed extraction, and the functional component obtained can be from antibacterial, sterilization, antipruritic, refrigerant etc. Each side reaches preferable repelling effect jointly;Effect of above material of vegetable origin is as follows:
Zanthoxylum schinifolium: warm in nature, acrid in the mouth, begins to be loaded in Shennong's Herbal.There is strong aromatic odor, have Anthelmintic, antibacterial, antiviral, ease pain, improve immunity of organisms isoreactivity.Cure mainly: Deficiency and coldness of spleen and stomach, gastral cavity abdomen are cold Bitterly, abdominal pain due to worm stagnation, vomiting are had loose bowels.
Lavandula angustifolia: have strong aromatic odor, has the merits such as sterilization, pain relieving, calmness, treatment mosquito bite Effect.
Flos Rosae Rugosae: sweet and slightly bitter taste, slightly warm in nature, returns liver, spleen, stomach warp;The most obvious effect regulate the flow of vital energy exactly resolving depression, Promoting blood circulation to remove blood stasis and menstruction regulating and pain relieving.
Herba Pogostemonis: acrid in the mouth, slightly warm in nature.There is the effect such as dispelling summer-heat from superficies of the body, removing dampness;Treatment anemopyretic cold, vomiting are let out Rush down.
Herba Menthae: there is sterilization, antipruritic and analgesia, effect of refrigerant heat radiation.
In this formula, formula based on Zanthoxylum schinifolium, there is effect of anophelifuge, with lavandula angustifolia, Flos Rosae Rugosae as tune Fragrant dispensing, Herba Pogostemonis is as the dispensing of bactericidal antiphlogistic, and Herba Menthae has refrigerant effect.
The mosquito-repellent water obtained by above-mentioned formula and technique, raw material employing natural green plant, aseptic, harmless, Nontoxic, there is anophelifuge, antipruritic, antibacterial, sterilization, the effect such as refrigerant, safe and reliable, it is adaptable to various people, Various skin quality.
The device have the advantages that as follows:
(1) present invention uses the material of plant origin to replace synthesis material to make mosquito-repellent water, prepares A kind of safe and nontoxic, non-stimulated to human body, can effectively prevent the mosquito-repellent water of mosquito bite, be suitable for various people, Various skin quality.
(2) mosquito-repellent water of the present invention contains Zanthoxylum schinifolium extract, also with the addition of lavandula angustifolia, Flos Rosae Rugosae, the leaves of pulse plants simultaneously Fragrant and Herba Menthae, has not only been in harmonious proportion the abnormal smells from the patient of mosquito-driving liquid, moreover it is possible to reach to strengthen antiinflammatory, antipruritic, the work of cooling effect With.
(3) the effective mosquito repellent time of the mosquito-repellent water of the present invention is long, and mosquito repellent function was lasting, up to 6-8 hour.
(4) raw material sources needed for the present invention prepares mosquito-repellent water is extensive, simple and easy to get, low price, suitable Close and promote.
(5) preparation method of mosquito-repellent water of the present invention is easy, and process step is few, is suitable to commercial production, has relatively High market value.
In a word, the present invention not only has an effect of anophelifuge, and have refreshment, refrigerant, antipruritic, antibacterial, Sterilize, protect the skin from the effects such as sting;Additionally, product raw material sources is in plant, safety non-toxic, It is applicable to various people, various skin quality;And the present invention is applicable not only to household, and be applicable to out on tours, The environment such as field work, carry more convenient.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.
The Zanthoxylum schinifolium that the present embodiment is selected is Zanthoxylum schinifolium;Lavandula angustifolia is Lavandula angustifolia;Flos Rosae Rugosae is Rosa rugosa;Herba Pogostemonis is Herba Pogostemonis;Herba Menthae is Herba Menthae。
One, embodiment is provided:
Embodiment 1
The preparation of plant extract: take Zanthoxylum schinifolium 25g, lavandula angustifolia 10g, Flos Rosae Rugosae 10g, Herba Pogostemonis 5g, Herba Menthae 5g, cleaned, drain, be dried, pulverize, it is thus achieved that powder cross 20 eye mesh screens after, add 55ml deionization Water, uses microwave auxiliary extraction technology, and control microwave power is 100W, microwave extraction 1h, Extracting temperature control System is between 45-65 DEG C.Extracting solution is crossed and is filtered to remove filtering residue, and filtrate is plant extract.
By plant extract obtained above, ethanol and deionized water according to following percentage by weight mix homogeneously: Plant extract 5%, ethanol (percent by volume of ethanol is 40%-75%) 40%, remaining is deionized water; Canned, finally give described mosquito-repellent water.
Embodiment 2
The preparation of plant extract: take Zanthoxylum schinifolium 40g, lavandula angustifolia 20g, Flos Rosae Rugosae 20g, Herba Pogostemonis 15g, Herba Menthae 15g, cleaned, drain, be dried, pulverize, it is thus achieved that powder cross 20 eye mesh screens after, add 110ml go from Sub-water, uses microwave auxiliary extraction technology, and control microwave power is 300W, microwave extraction 2h, Extracting temperature Control between 45-65 DEG C.Extracting solution is crossed and is filtered to remove filtering residue, and filtrate is plant extract.
By plant extract obtained above, ethanol and deionized water according to following percentage by weight mix homogeneously: Plant extract 1%, ethanol (percent by volume of ethanol is 40%-75%) 75%, remaining is deionized water; Canned, finally give described mosquito-repellent water.
Embodiment 3
The preparation of plant extract: take Zanthoxylum schinifolium 35g, lavandula angustifolia 15g, Flos Rosae Rugosae 15g, Herba Pogostemonis 7.5g, thin Lotus 7.5g, cleaned, drain, be dried, pulverize, it is thus achieved that powder cross 20 eye mesh screens after, add 80ml Deionized water, uses microwave auxiliary extraction technology, and control microwave power is 200W, and microwave extraction 1.5h carries Take temperature to control between 45-65 DEG C.Extracting solution is crossed and is filtered to remove filtering residue, and filtrate is plant extract.
By plant extract obtained above, ethanol and deionized water according to following percentage by weight mix homogeneously: Plant extract 2.5%, ethanol (percent by volume of ethanol is 40%-75%) 65%, remaining is deionization Water;Canned, finally give described mosquito-repellent water.
Two, using effect test:
Anophelifuge test is carried out according to GB/T17322.10-1998.Experimenter is 45 people, is divided into three groups, often Organize 15 people, respectively the mosquito-repellent water of the embodiment of the present invention 1,2,3 is tested.Everyone is blank on the other hand Comparison, another hands presses 1.5 μ l/cm2Dose uniformity smear 5cm × 5cm dorsal area, expose wherein 4cm × 4cm position, remainder tightly covers.Spread product 2 hours, proceeds by test.Experiment knot Fruit shows, the mosquito-repellent water of the embodiment of the present invention 1,2,3 is all combined B level to Aedes albopictus repellent effect, Mosquito repellent time reaches 6-8h.
The foregoing is only the preference embodiment of the present invention, be not intended that the limit to scope Fixed.Any any amendment, equivalent and improvement etc. made within the spirit and principles in the present invention, all should Within being included in the claims of the present invention.

Claims (9)

1. the mosquito-repellent water containing Zanthoxylum schinifolium extract, it is characterised in that: according to percentage by weight, its component And content is: plant extract 1%-5%, ethanol 40%-75%, remaining is deionized water;
Described plant extract is to be prepared from by the raw material of following weight: Zanthoxylum schinifolium 25-40 part, smokes Clothing grass 10-20 part, Flos Rosae Rugosae 10-20 part, Herba Pogostemonis 5-15 part and Herba Menthae 5-15 part.
A kind of mosquito-repellent water containing Zanthoxylum schinifolium extract the most according to claim 1, it is characterised in that: institute Stating plant extract is to be prepared from by the raw material of following weight: Zanthoxylum schinifolium 35 parts, lavandula angustifolia 15 Part, 15 parts of Flos Rosae Rugosae, Herba Pogostemonis 7.5 parts and Herba Menthae 7.5 parts.
A kind of mosquito-repellent water containing Zanthoxylum schinifolium extract the most according to claim 1 and 2, it is characterised in that: According to percentage by weight, the component of described mosquito-repellent water and content it is: plant extract 1%-5%, ethanol 65%-75%, remaining is deionized water.
A kind of mosquito-repellent water containing Zanthoxylum schinifolium extract the most according to claim 1 and 2, it is characterised in that: Described plant extract is to utilize microwave auxiliary extraction technology to extract to obtain.
5. the preparation method of the mosquito-repellent water containing Zanthoxylum schinifolium extract, it is characterised in that: described method includes Following steps:
(1) preparation of plant extract: Zanthoxylum schinifolium, lavandula angustifolia, Flos Rosae Rugosae, Herba Pogostemonis and Herba Menthae are entered in proportion Row mixing;The most cleaned, drain, be dried and pulverize, will pulverize after powder press solid-liquid ratio addition deionization Water, then use microwave auxiliary extraction technology to extract, filters extracting solution, the filtrate obtained be described in plant Thing extract;
(2) plant extract obtained above, ethanol and deionized water are mixed according to following percentage by weight Uniform: plant extract 1-5%, ethanol 40%-75%, remaining is deionized water;Canned, finally give institute State mosquito-repellent water.
Preparation method the most according to claim 5, it is characterised in that: the raw material of described plant extract Mix according to following weight: Zanthoxylum schinifolium 25-40 part, lavandula angustifolia 10-20 part, Flos Rosae Rugosae 10-20 Part, Herba Pogostemonis 5-15 part, Herba Menthae 5-15 part.
7. according to the preparation method described in claim 5 or 6, it is characterised in that: described raw material pulverizing is thick Pulverizing, the granularity of the described raw material of 90% is less than 20 mesh.
8. according to the preparation method described in claim 5 or 6, it is characterised in that: described solid-liquid ratio is 1:6-1:1.
9. according to the preparation method described in claim 5 or 6, it is characterised in that: described microwave radiation exaraction In technology, the power of microwave is 100W-300W, and the time of microwave is 1-2h, and Extracting temperature is 45-65 DEG C.
CN201610460260.6A 2016-06-22 2016-06-22 Mosquito repellent water containing green pepper extracts and preparation method of mosquito repellent water Pending CN105997675A (en)

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Application publication date: 20161012