CN105994775A - Dendrobium officinale Kimura et Migo-tea-vinegar beverage - Google Patents
Dendrobium officinale Kimura et Migo-tea-vinegar beverage Download PDFInfo
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- CN105994775A CN105994775A CN201610648035.5A CN201610648035A CN105994775A CN 105994775 A CN105994775 A CN 105994775A CN 201610648035 A CN201610648035 A CN 201610648035A CN 105994775 A CN105994775 A CN 105994775A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/14—Tea preparations, e.g. using additives
Abstract
The invention discloses a Dendrobium officinale Kimura et Migo-tea-vinegar beverage. The beverage comprises Dendrobium officinale Kimura et Migo fresh strips, Baimao tea, the root bark of the peony tree, pseudo-ginseng, herba eupatorii, divaricate saposhnikovia root, semen plantaginis, mint, fructus forsythia, root bark of white mulberry, rhizoma anemarrhenae, sweet osmanthus, malt vinegar, polyacryl pyrrolidone, hydroxypropyl methylcellulose sodium, potassium polyacrylate , sodium alginate, an American DuPont EEA2112AC compatilizer, a food-grade antioxidant potassium erythorbate, xanthan gum, carthamin yellow, nisin, maltose, starch sugar, acesulfame potassium, xylitol, vitamin E, vitamin K, vitamin PP, alanine, glutamic acid, aspartic acid, glycine, iron element, selenium element, cobalt element, zinc element, propyl-furfuryl fumarate, guanosine-5'-monophosphate disodium salt, glycine, carvone, dihydrojasmone, isoamyl acetate and 2-hexenol. The beverage can effectively treat or relieve halitosis symptoms.
Description
[technical field]
The invention belongs to technical field of agricultural product process, be specifically related to a kind of Herba Dendrobii tea vinegar drink.
[background technology]
Herba Dendrobii has the medical value of uniqueness, and the Shennong's Herbal of Qin Han dynasty records Herba Dendrobii " main damaging the spleen and stomach, eliminating impediment, the therapeutic method to keep the adverse QI flowing downwards, tonifying five ZANG-organs asthenia weakness and emaciation, the thick the intestines and stomach of reinforcing YIN-essence, for a long time clothes "；Herba Dendrobii was classified as first of " China's nine big Herba mesonae chinensis " by one-tenth book in more than 1,000 years front Taoist school's medical science classical " Taoist Scriptures "；Li Shizhen (1518-1593 A.D.) evaluates Herba Dendrobii " reinforcing YIN-essence benefit is smart, thick the intestines and stomach, never sufficient in benefit, flat gastric qi, long muscle, and Fructus Alpiniae Oxyphyllae, except frightened, made light of one's life by commiting suicide and prolonged life " in Compendium of Material Medica；Among the people it is called " help Herba mesonae chinensis ".
Implication, refers to inside of human body imbalance and smelly dirty a kind of disease of giving vent to anger in causing mouth.In daily contacts, implication often causes inconvenience and embarrassment.The reason causing implication has a lot, having plenty of because not focusing on oral hygiene, such as the most unclean tooth, causing food impaction teeth space；Having plenty of because there is oral disease, such as dental caries, dental calculus, periodontitis etc., easy breed bacteria, especially anaerobe in causing oral cavity, these bacterial decomposition food produces sulfide and easily causes implication；Have plenty of because of gastroenteropathy, such as chronic gastritis, dyspepsia etc.；Have plenty of because of daily smoking, drink or have a liking for the pungent stimulation food such as Herba Alii fistulosi, Bulbus Allii；Or because self endocrine disturbance, causing oral immunisation power to decline, easy bacteria infection causes implication.
For this phenomenon, occur in that a lot of the treatment medicine of implication, medicaments etc. on the market.As patent of invention " breath freshening Chinese medicine throat lozenge (application number: 201510073712.0) " discloses a kind of throat lozenge being made up of extracts such as Fructus Foeniculi extract, Radix Curcumae extract, Rhizoma Coptidis extracts, oral cavity gas can be effectively improved；Patent of invention " honeyed pill (application number: 201310459129.4) of a kind of fresh breath " disclose a kind of by Flos Caryophylli, Fructus Amomi Rotundus, Herba Asari, Herba Menthae etc. make can the honeyed pill of fresh breath；Patent " Chinese medicine for the treatment of implication and preparation method thereof (application number: 201510031046.4) " discloses a kind of Chinese medicine formula treating implication, Chinese medicine formula including Radix Scutellariae, Pericarpium Citri Reticulatae, Fructus Crataegi, Folium Nelumbinis, Herba Pogostemonis etc. and preparation method thereof, it is possible to alleviate implication symptom.Additionally occurring in that the teabag drink that can alleviate implication symptom in prior art, but it is long to there is the production cycle, the storage time is short, the problems such as mouthfeel is not good enough.
[summary of the invention]
The technical problem to be solved in the present invention is to provide a kind of Herba Dendrobii tea vinegar drink, and long to solve to produce the implication teabag drink production cycle of dispelling in prior art, the storage time is short, the problems such as mouthfeel is not good enough.The Herba Dendrobii tea vinegar drink of the present invention is nutritious, sour-sweet tasty and refreshing, and tea is aromatic strongly fragrant, and constitutive material source is easy to get, and preparation cost is low, it is easy to popularization and application.
In order to solve above technical problem, the present invention by the following technical solutions:
nullA kind of Herba Dendrobii tea vinegar drink，In units of weight portion，Including following raw material: Herba Dendrobii fresh bar 155-196 part、Raw white tea 98-145 part、Cortex Moutan 9-14 part、Radix Notoginseng 7-10 part、Herba Eupatorii 6-8 part、Radix Saposhnikoviae 7-9 part、Semen Plantaginis 5-8 part、Herba Menthae 2-5 part、Fructus Forsythiae 4-6 part、Cortex Mori 4-9 part、Rhizoma Anemarrhenae 5-6 part、Flos Osmanthi Fragrantis 4-5 part、Malt vinegar 7-10 part、Carthamus yellow 2.5-6.2 part、Nisin 2.2-4.5 part、Maltose 7-9 part、Starch sugar 3-5 part、Acesulfame potassium 0.1-0.2 part、Xylitol 0.5-0.8 part、Vitamin E 0.6-1 part、Vitamin K 0.5-0.8 part、Vitamin PP 0.7-0.9 part、Alanine 0.5-0.7 part、Glutamic acid 0.3-0.5 part、Aspartic acid 0.4-0.6 part、Glycine 0.2-0.5 part、Ferrum element 0.07-0.22 part、Selenium element 0.12-0.2 part、Cobalt element 0.15-0.24 part、Zinc element 0.14-0.18 part、Polyvinyl pyrilodone 0.8-1.1 part、Hydroxypropyl methyl cellulose sodium 0.1-0.2 part、Polyacrylic acid potassium 0.14-0.25 part、Sodium alginate 0.14-0.22 part、Dupont EEA2112AC compatilizer 0.8-1.4 part、Food grade antioxidant different VC potassium 0.6-0.8 part、Xanthan gum 0.7-1.2 part、Fumaric acid furfuryl alcohol propyl ester 0.5-0.8 part、51-guanosine monophosphate disodium 0.08-0.18 part、51-disodium 5'-ribonucleotide 0.03-0.1 part、Glycine 0.05-0.07 part、Carvone 0.03-0.05 part，Dihydro jasmone 0.06-0.07 part、Isoamyl acetate 0.04-0.05 part、2-hexenol 0.07-0.09 part；
The preparation method of described Herba Dendrobii tea vinegar drink, comprises the following steps:
S1: the preparation of Herba Dendrobii juice, comprises the following steps；
S11: crushed by cleaned Herba Dendrobii fresh bar strand grinding machine, filters by 60-90 mesh sieve, and prepared Herba Dendrobii minces；
S12: the Herba Dendrobii that step S11 prepares is minced and mix loading extraction pot for the ratio of 1:2-4 in mass ratio with water, under pressure is 1-4MPa, by 5-6 layer filtered through gauze after decocting in water 0.5-1.5h, prepared filtrate A；
S13: filtrate A rotating speed step S12 prepared is the centrifuge of 2000-5000r/min, sucking filtration roguing under vacuum is 0.065-0.085MPa, prepares Herba Dendrobii juice；
S2, the preparation of raw white tea polyphenol, comprise the following steps:
S21: raw white tea is dried and pulverizes to water content≤9%, cross 60-80 mesh sieve, mix for 1:9-11 in mass ratio with the ethanol water that mass fraction is 75%-80%, being 100-160W at microwave power, temperature extracts 25-34min at being 40-42 DEG C, filters, concentrate, prepare tea polyphenols crude extract A；
S22: the tea polyphenols crude extract A that step S21 prepares is joined in the KCl solution that concentration is 12%-16%, pH regulator is to 5.2-6, impurity is removed under centrifugal rotational speed is 3500-4500r/min, using aperture is that the solution after being centrifuged is filtered at temperature is 29-36 DEG C by 0.03-0.1 μm filter membrane, prepares liquor B；
S23: liquor B propyl ether step S22 prepared extracts, prepared raw white tea polyphenol freezing, dried；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Radix Saposhnikoviae, Semen Plantaginis, Herba Menthae, Fructus Forsythiae, Cortex Mori, the Rhizoma Anemarrhenae, Flos Osmanthi Fragrantis are separately dried to water content≤8% co-grinding, add water, it is 1:10-14(W/V at solid-liquid ratio), microwave power is 120-180W, Extracting temperature is 85-92 DEG C, extraction time is 1.5-1.9h, then filtering residue, prepares medicinal liquid；
S4: by step S1 prepare Herba Dendrobii juice, step S2 prepare raw white tea polyphenol, step S3 prepare medicinal liquid, malt vinegar, polyvinyl pyrilodone, hydroxypropyl methyl cellulose sodium, polyacrylic acid potassium, sodium alginate, Dupont EEA2112AC compatilizer, food grade antioxidant different VC potassium, xanthan gum, 1200-1400 part water mixing after, it is 100-150W at microwave power, temperature is 55-60 DEG C, speed of agitator is stirring 0.5-0.8h under 200-300r/min, prepares uniform mixed liquor A；
S5: add Carthamus yellow in the uniform mixed liquor A that step S4 prepares, nisin, maltose, starch sugar, acesulfame potassium, xylitol, vitamin E, vitamin K, vitamin PP, alanine, glutamic acid, aspartic acid, glycine, ferrum element, selenium element, cobalt element, zinc element, fumaric acid furfuryl alcohol propyl ester, 51-guanosine monophosphate disodium, 51-disodium 5'-ribonucleotide, glycine, carvone, dihydro jasmone, isoamyl acetate, 2-hexenol, it is 80-120W at microwave power, temperature is 45-52 DEG C, speed of agitator is stirring 0.3-0.5h under 300-400r/min, prepare uniform mixed liquid B；
S6: uniform mixed liquor sterilizing step S5 prepared, prepares uniform mixed liquor C；
S7: the uniform mixed liquor C that step S6 prepares is carried out fill, sealing under negative pressure, then cools down, prepares Herba Dendrobii tea vinegar drink.
Further, the temperature of mixed liquor sterilizing described in step S6 is 134-136 DEG C.
Further, the pressure of described sterilizing is 210-230KPa.
Further, the time of described sterilizing is 2-4s.
Further, the vacuum of negative pressure described in step S7 is 0.088-0.091MPa.
Further, the temperature that fill described in step S7, sealing use is 87-91 DEG C.
Further, the temperature being cooled to described in step S7 is room temperature.
The method have the advantages that
(1) the Herba Dendrobii tea vinegar drink of the present invention is nutritious, sour-sweet tasty and refreshing, and tea is aromatic strongly fragrant, is a kind of novel Traditional Chinese medicine dendrobium candidum tea vinegar drink；
(2) the Herba Dendrobii tea vinegar drink of the present invention can effectively be treated or alleviate implication symptom；
(3) the Herba Dendrobii tea vinegar drink of the present invention is with short production cycle, and shelf life of products is long；
(4) present invention is compared with prior art: fill, sealing use higher temperature and vacuum, more can extend product and store the time；
(5) the Herba Dendrobii tea vinegar drink constitutive material source of the present invention is easy to get, and preparation method is uncomplicated, it is easy to popularization and application.
[detailed description of the invention]
For ease of being more fully understood that the present invention, being illustrated by following example, these embodiments belong to protection scope of the present invention, but are not intended to protection scope of the present invention.
nullIn an embodiment，Described Herba Dendrobii tea vinegar drink，It is characterized in that，In units of weight portion，Including following raw material: Herba Dendrobii fresh bar 155-196 part、Raw white tea 98-145 part、Cortex Moutan 9-14 part、Radix Notoginseng 7-10 part、Herba Eupatorii 6-8 part、Radix Saposhnikoviae 7-9 part、Semen Plantaginis 5-8 part、Herba Menthae 2-5 part、Fructus Forsythiae 4-6 part、Cortex Mori 4-9 part、Rhizoma Anemarrhenae 5-6 part、Flos Osmanthi Fragrantis 4-5 part、Malt vinegar 7-10 part、Carthamus yellow 2.5-6.2 part、Nisin 2.2-4.5 part、Maltose 7-9 part、Starch sugar 3-5 part、Acesulfame potassium 0.1-0.2 part、Xylitol 0.5-0.8 part、Vitamin E 0.6-1 part、Vitamin K 0.5-0.8 part、Vitamin PP 0.7-0.9 part、Alanine 0.5-0.7 part、Glutamic acid 0.3-0.5 part、Aspartic acid 0.4-0.6 part、Glycine 0.2-0.5 part、Ferrum element 0.07-0.22 part、Selenium element 0.12-0.2 part、Cobalt element 0.15-0.24 part、Zinc element 0.14-0.18 part、Polyvinyl pyrilodone 0.8-1.1 part、Hydroxypropyl methyl cellulose sodium 0.1-0.2 part、Polyacrylic acid potassium 0.14-0.25 part、Sodium alginate 0.14-0.22 part、Dupont EEA2112AC compatilizer 0.8-1.4 part、Food grade antioxidant different VC potassium 0.6-0.8 part、Xanthan gum 0.7-1.2 part、Fumaric acid furfuryl alcohol propyl ester 0.5-0.8 part、51-guanosine monophosphate disodium 0.08-0.18 part、51-disodium 5'-ribonucleotide 0.03-0.1 part、Glycine 0.05-0.07 part、Carvone 0.03-0.05 part，Dihydro jasmone 0.06-0.07 part、Isoamyl acetate 0.04-0.05 part、2-hexenol 0.07-0.09 part；
The preparation method of described Herba Dendrobii tea vinegar drink, comprises the following steps:
S1: the preparation of Herba Dendrobii juice, comprises the following steps；
S11: crushed by cleaned Herba Dendrobii fresh bar strand grinding machine, filters by 60-90 mesh sieve, and prepared Herba Dendrobii minces；
S12: the Herba Dendrobii that step S11 prepares is minced and mix loading extraction pot for the ratio of 1:2-4 in mass ratio with water, under pressure is 1-4MPa, by 5-6 layer filtered through gauze after decocting in water 0.5-1.5h, prepared filtrate A；
S13: filtrate A rotating speed step S12 prepared is the centrifuge of 2000-5000r/min, sucking filtration roguing under vacuum is 0.065-0.085MPa, prepares Herba Dendrobii juice；
S2, the preparation of raw white tea polyphenol, comprise the following steps:
S21: raw white tea is dried and pulverizes to water content≤9%, cross 60-80 mesh sieve, mix for 1:9-11 in mass ratio with the ethanol water that mass fraction is 75%-80%, being 100-160W at microwave power, temperature extracts 25-34min at being 40-42 DEG C, filters, concentrate, prepare tea polyphenols crude extract A；
S22: the tea polyphenols crude extract A that step S21 prepares is joined in the KCl solution that concentration is 12%-16%, pH regulator is to 5.2-6, impurity is removed under centrifugal rotational speed is 3500-4500r/min, using aperture is that the solution after being centrifuged is filtered at temperature is 29-36 DEG C by 0.03-0.1 μm filter membrane, prepares liquor B；
S23: liquor B propyl ether step S22 prepared extracts, prepared raw white tea polyphenol freezing, dried；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Radix Saposhnikoviae, Semen Plantaginis, Herba Menthae, Fructus Forsythiae, Cortex Mori, the Rhizoma Anemarrhenae, Flos Osmanthi Fragrantis are separately dried to water content≤8% co-grinding, add water, it is 1:10-14(W/V at solid-liquid ratio), microwave power is 120-180W, Extracting temperature is 85-92 DEG C, extraction time is 1.5-1.9h, then filtering residue, prepares medicinal liquid；
S4: by step S1 prepare Herba Dendrobii juice, step S2 prepare raw white tea polyphenol, step S3 prepare medicinal liquid, malt vinegar, polyvinyl pyrilodone, hydroxypropyl methyl cellulose sodium, polyacrylic acid potassium, sodium alginate, Dupont EEA2112AC compatilizer, food grade antioxidant different VC potassium, xanthan gum, 1200-1400 part water mixing after, it is 100-150W at microwave power, temperature is 55-60 DEG C, speed of agitator is stirring 0.5-0.8h under 200-300r/min, prepares uniform mixed liquor A；
S5: add Carthamus yellow in the uniform mixed liquor A that step S4 prepares, nisin, maltose, starch sugar, acesulfame potassium, xylitol, vitamin E, vitamin K, vitamin PP, alanine, glutamic acid, aspartic acid, glycine, ferrum element, selenium element, cobalt element, zinc element, fumaric acid furfuryl alcohol propyl ester, 51-guanosine monophosphate disodium, 51-disodium 5'-ribonucleotide, glycine, carvone, dihydro jasmone, isoamyl acetate, 2-hexenol, it is 80-120W at microwave power, temperature is 45-52 DEG C, speed of agitator is stirring 0.3-0.5h under 300-400r/min, prepare uniform mixed liquid B；
S6: being 134-136 DEG C by the uniform mixed liquor that step S5 prepares in temperature, pressure is sterilizing 2-4s under 210-230KPa, prepares uniform mixed liquor C；
S7: uniform mixed liquor C step S6 prepared is 0.089-0.093MPa in vacuum, and temperature carries out fill, sealing at being 88-92 DEG C, is then cooled to room temperature, prepares Herba Dendrobii tea vinegar drink.
It is illustrated below by more specifically embodiment.
Embodiment 1
nullA kind of Herba Dendrobii tea vinegar drink，It is characterized in that，In units of weight portion，Including following raw material: the fresh bar of Herba Dendrobii 175 parts、Raw white tea 225 parts、Cortex Moutan 12 parts、9 parts of Radix Notoginseng、Herba Eupatorii 7 parts、Radix Saposhnikoviae 8 parts、Semen Plantaginis 7 parts、Herba Menthae 4 parts、Fructus Forsythiae 5 parts、Cortex Mori 7 parts、The Rhizoma Anemarrhenae 5 parts、Flos Osmanthi Fragrantis 4 parts、Malt vinegar 8 parts、Carthamus yellow 4.5 parts、Nisin 3.5 parts、Maltose 8 parts、Starch sugar 4 parts、Acesulfame potassium 0.1 part、Xylitol 0.7 part、Vitamin E 0.8 part、Vitamin K 0.7 part、Vitamin PP 0.8 part、Alanine 0.6 part、0.4 part of glutamic acid、Aspartic acid 0.5 part、Glycine 0.3 part、Ferrum element 0.15 part、Selenium element 0.16 part、Cobalt element 0.2 part、Zinc element 0.16 part、Polyvinyl pyrilodone 1 part、0.1 part of hydroxypropyl methyl cellulose sodium、Polyacrylic acid potassium 0.2 part、Sodium alginate 0.18 part、Dupont EEA2112AC compatilizer 1.2 parts、0.7 part of food grade antioxidant different VC potassium、Xanthan gum 1 part、Fumaric acid furfuryl alcohol propyl ester 0.7 part、51-guanosine monophosphate disodium 0.14 part、51-disodium 5'-ribonucleotide 0.07 part、Glycine 0.06 part、Carvone 0.04 part，Dihydro jasmone 0.06 part、Isoamyl acetate 0.04 part、2-hexenol 0.08 part；
The preparation method of described Herba Dendrobii tea vinegar drink, comprises the following steps:
S1: the preparation of Herba Dendrobii juice, comprises the following steps；
S11: crushed by cleaned Herba Dendrobii fresh bar strand grinding machine, filters by 80 mesh sieve, and prepared Herba Dendrobii minces；
S12: the Herba Dendrobii that step S11 prepares is minced and mix loading extraction pot for the ratio of 1:3 in mass ratio with water, under pressure is 3MPa, by 5 layers of filtered through gauze after decocting in water 0.9h, prepared filtrate A；
S13: filtrate A rotating speed step S12 prepared is the centrifuge of 3500r/min, sucking filtration roguing under vacuum is 0.075MPa, prepares Herba Dendrobii juice；
S2, the preparation of raw white tea polyphenol, comprise the following steps:
S21: raw white tea being dried to water content is to pulverize after 9%, crosses 70 mesh sieves, mix for 1:10 in mass ratio with the ethanol water that mass fraction is 78%, be 130W at microwave power, and temperature is extraction 30min at 41 DEG C, filters, concentration, prepared tea polyphenols crude extract A；
S22: the tea polyphenols crude extract A that step S21 prepares is joined in the KCl solution that concentration is 14%, pH regulator is to 5.8, removing impurity under centrifugal rotational speed is 4000r/min, using aperture is that the solution after being centrifuged is filtered at temperature is 32 DEG C by 0.07 μm filter membrane, prepares liquor B；
S23: liquor B propyl ether step S22 prepared extracts, prepared raw white tea polyphenol freezing, dried；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Radix Saposhnikoviae, Semen Plantaginis, Herba Menthae, Fructus Forsythiae, Cortex Mori, the Rhizoma Anemarrhenae, Flos Osmanthi Fragrantis are separately dried to water content be co-grinding after 8%, add water, it is 1:12(W/V at solid-liquid ratio), microwave power is 150W, Extracting temperature is 88 DEG C, extraction time is 1.7h, then filtering residue, prepares medicinal liquid；
After medicinal liquid that raw white tea polyphenol that S4: the Herba Dendrobii juice that step S1 prepared, step S2 prepare, step S3 prepare, malt vinegar, polyvinyl pyrilodone, hydroxypropyl methyl cellulose sodium, polyacrylic acid potassium, sodium alginate, Dupont EEA2112AC compatilizer, food grade antioxidant different VC potassium, xanthan gum, the mixing of 1300 parts of water, it is 130W at microwave power, temperature is 58 DEG C, speed of agitator is stirring 0.7h under 250r/min, prepares uniform mixed liquor A；
S5: add Carthamus yellow in the uniform mixed liquor A that step S4 prepares, nisin, maltose, starch sugar, acesulfame potassium, xylitol, vitamin E, vitamin K, vitamin PP, alanine, glutamic acid, aspartic acid, glycine, ferrum element, selenium element, cobalt element, zinc element, fumaric acid furfuryl alcohol propyl ester, 51-guanosine monophosphate disodium, 51-disodium 5'-ribonucleotide, glycine, carvone, dihydro jasmone, isoamyl acetate, 2-hexenol, it is 100W at microwave power, temperature is 48 DEG C, speed of agitator is stirring 0.4h under 350r/min, prepare uniform mixed liquid B；
S6: uniform mixed liquor step S5 prepared is 135 DEG C in temperature, and pressure is sterilizing 3s under 220KPa, prepares uniform mixed liquor C；
S7: uniform mixed liquor C step S6 prepared is 0.091MPa in vacuum, and temperature is to carry out fill, sealing at 90 DEG C, is then cooled to room temperature, prepares Herba Dendrobii tea vinegar drink.
Embodiment 2
nullA kind of Herba Dendrobii tea vinegar drink，It is characterized in that，In units of weight portion，Including following raw material: the fresh bar of Herba Dendrobii 155 parts、Raw white tea 98 parts、Cortex Moutan 9 parts、7 parts of Radix Notoginseng、Herba Eupatorii 6 parts、Radix Saposhnikoviae 7 parts、Semen Plantaginis 5 parts、Herba Menthae 2 parts、Fructus Forsythiae 4 parts、Cortex Mori 4 parts、The Rhizoma Anemarrhenae 5 parts、Flos Osmanthi Fragrantis 4 parts、Malt vinegar 7 parts、Carthamus yellow 2.5 parts、Nisin 2.2 parts、Maltose 7 parts、Starch sugar 3 parts、Acesulfame potassium 0.1 part、Xylitol 0.5 part、Vitamin E 0.6 part、Vitamin K 0.5 part、Vitamin PP 0.7 part、Alanine 0.5 part、0.3 part of glutamic acid、Aspartic acid 0.4 part、Glycine 0.2 part、Ferrum element 0.07 part、Selenium element 0.12 part、Cobalt element 0.15 part、Zinc element 0.14 part、Polyvinyl pyrilodone 0.8 part、0.1 part of hydroxypropyl methyl cellulose sodium、Polyacrylic acid potassium 0.14 part、Sodium alginate 0.14 part、Dupont EEA2112AC compatilizer 0.8 part、0.6 part of food grade antioxidant different VC potassium、Xanthan gum 0.7 part、Fumaric acid furfuryl alcohol propyl ester 0.5 part、51-guanosine monophosphate disodium 0.08 part、51-disodium 5'-ribonucleotide 0.03 part、Glycine 0.05 part、Carvone 0.03 part，Dihydro jasmone 0.06 part、Isoamyl acetate 0.04 part、2-hexenol 0.07 part；
The preparation method of described Herba Dendrobii tea vinegar drink, comprises the following steps:
S1: the preparation of Herba Dendrobii juice, comprises the following steps；
S11: crushed by cleaned Herba Dendrobii fresh bar strand grinding machine, filters by 60 mesh sieve, and prepared Herba Dendrobii minces；
S12: the Herba Dendrobii that step S11 prepares is minced and mix loading extraction pot for the ratio of 1:2 in mass ratio with water, under pressure is 1MPa, by 5 layers of filtered through gauze after decocting in water 1.5h, prepared filtrate A；
S13: filtrate A rotating speed step S12 prepared is the centrifuge of 2000r/min, sucking filtration roguing under vacuum is 0.065MPa, prepares Herba Dendrobii juice；
S2, the preparation of raw white tea polyphenol, comprise the following steps:
S21: raw white tea being dried to water content is to pulverize after 8%, crosses 60 mesh sieves, mix for 1:9 in mass ratio with the ethanol water that mass fraction is 75%, be 100W at microwave power, and temperature is extraction 34min at 40 DEG C, filters, concentration, prepared tea polyphenols crude extract A；
S22: the tea polyphenols crude extract A that step S21 prepares is joined in the KCl solution that concentration is 12%, pH regulator is to 5.2, removing impurity under centrifugal rotational speed is 3500r/min, using aperture is that the solution after being centrifuged is filtered at temperature is 29 DEG C by 0.03 μm filter membrane, prepares liquor B；
S23: liquor B propyl ether step S22 prepared extracts, prepared raw white tea polyphenol freezing, dried；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Radix Saposhnikoviae, Semen Plantaginis, Herba Menthae, Fructus Forsythiae, Cortex Mori, the Rhizoma Anemarrhenae, Flos Osmanthi Fragrantis are separately dried to water content be co-grinding after 7%, add water, it is 1:10(W/V at solid-liquid ratio), microwave power is 120W, Extracting temperature is 85 DEG C, extraction time is 1.9h, then filtering residue, prepares medicinal liquid；
After medicinal liquid that raw white tea polyphenol that S4: the Herba Dendrobii juice that step S1 prepared, step S2 prepare, step S3 prepare, malt vinegar, polyvinyl pyrilodone, hydroxypropyl methyl cellulose sodium, polyacrylic acid potassium, sodium alginate, Dupont EEA2112AC compatilizer, food grade antioxidant different VC potassium, xanthan gum, the mixing of 1200 parts of water, it is 100W at microwave power, temperature is 55 DEG C, speed of agitator is stirring 0.8h under 200r/min, prepares uniform mixed liquor A；
S5: add Carthamus yellow in the uniform mixed liquor A that step S4 prepares, nisin, maltose, starch sugar, acesulfame potassium, xylitol, vitamin E, vitamin K, vitamin PP, alanine, glutamic acid, aspartic acid, glycine, ferrum element, selenium element, cobalt element, zinc element, fumaric acid furfuryl alcohol propyl ester, 51-guanosine monophosphate disodium, 51-disodium 5'-ribonucleotide, glycine, carvone, dihydro jasmone, isoamyl acetate, 2-hexenol, it is 80W at microwave power, temperature is 45 DEG C, speed of agitator is stirring 0.5h under 300r/min, prepare uniform mixed liquid B；
S6: uniform mixed liquor step S5 prepared is 134 DEG C in temperature, and pressure is sterilizing 4s under 210KPa, prepares uniform mixed liquor C；
S7: uniform mixed liquor C step S6 prepared is 0.089MPa in vacuum, and temperature is to carry out fill, sealing at 88 DEG C, is then cooled to room temperature, prepares Herba Dendrobii tea vinegar drink.
Embodiment 3
nullA kind of Herba Dendrobii tea vinegar drink，It is characterized in that，In units of weight portion，Including following raw material: the fresh bar of Herba Dendrobii 196 parts、Raw white tea 145 parts、Cortex Moutan 14 parts、10 parts of Radix Notoginseng、Herba Eupatorii 8 parts、Radix Saposhnikoviae 9 parts、Semen Plantaginis 8 parts、Herba Menthae 5 parts、Fructus Forsythiae 6 parts、Cortex Mori 9 parts、The Rhizoma Anemarrhenae 6 parts、Flos Osmanthi Fragrantis 5 parts、Malt vinegar 10 parts、Carthamus yellow 6.2 parts、Nisin 4.5 parts、Maltose 9 parts、Starch sugar 5 parts、Acesulfame potassium 0.2 part、Xylitol 0.8 part、Vitamin e1 part、Vitamin K 0.8 part、Vitamin PP 0.9 part、Alanine 0.7 part、0.5 part of glutamic acid、Aspartic acid 0.6 part、Glycine 0.5 part、Ferrum element 0.22 part、Selenium element 0.2 part、Cobalt element 0.24 part、Zinc element 0.18 part、Polyvinyl pyrilodone 1.1 parts、0.2 part of hydroxypropyl methyl cellulose sodium、Polyacrylic acid potassium 0.25 part、Sodium alginate 0.22 part、Dupont EEA2112AC compatilizer 1.4 parts、0.8 part of food grade antioxidant different VC potassium、Xanthan gum 1.2 parts、Fumaric acid furfuryl alcohol propyl ester 0.8 part、51-guanosine monophosphate disodium 0.18 part、51-disodium 5'-ribonucleotide 0.1 part、Glycine 0.07 part、Carvone 0.05 part，Dihydro jasmone 0.07 part、Isoamyl acetate 0.05 part、2-hexenol 0.09 part；
The preparation method of described Herba Dendrobii tea vinegar drink, comprises the following steps:
S1: the preparation of Herba Dendrobii juice, comprises the following steps；
S11: crushed by cleaned Herba Dendrobii fresh bar strand grinding machine, filters by 90 mesh sieve, and prepared Herba Dendrobii minces；
S12: the Herba Dendrobii that step S11 prepares is minced and mix loading extraction pot for the ratio of 1:4 in mass ratio with water, under pressure is 4MPa, by 6 layers of filtered through gauze after decocting in water 0.5h, prepared filtrate A；
S13: filtrate A rotating speed step S12 prepared is the centrifuge of 5000r/min, sucking filtration roguing under vacuum is 0.085MPa, prepares Herba Dendrobii juice；
S2, the preparation of raw white tea polyphenol, comprise the following steps:
S21: raw white tea being dried to water content is to pulverize after 7%, crosses 80 mesh sieves, mix for 1:11 in mass ratio with the ethanol water that mass fraction is 80%, be 160W at microwave power, and temperature is extraction 25min at 42 DEG C, filters, concentration, prepared tea polyphenols crude extract A；
S22: the tea polyphenols crude extract A that step S21 prepares is joined in the KCl solution that concentration is 16%, pH regulator is to 6, removing impurity under centrifugal rotational speed is 4500r/min, using aperture is that the solution after being centrifuged is filtered at temperature is 36 DEG C by 0.1 μm filter membrane, prepares liquor B；
S23: liquor B propyl ether step S22 prepared extracts, prepared raw white tea polyphenol freezing, dried；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Radix Saposhnikoviae, Semen Plantaginis, Herba Menthae, Fructus Forsythiae, Cortex Mori, the Rhizoma Anemarrhenae, Flos Osmanthi Fragrantis are separately dried to water content be co-grinding after 6%, add water, it is 1:14(W/V at solid-liquid ratio), microwave power is 180W, Extracting temperature is 92 DEG C, extraction time is 1.5h, then filtering residue, prepares medicinal liquid；
After medicinal liquid that raw white tea polyphenol that S4: the Herba Dendrobii juice that step S1 prepared, step S2 prepare, step S3 prepare, malt vinegar, polyvinyl pyrilodone, hydroxypropyl methyl cellulose sodium, polyacrylic acid potassium, sodium alginate, Dupont EEA2112AC compatilizer, food grade antioxidant different VC potassium, xanthan gum, the mixing of 1400 parts of water, it is 150W at microwave power, temperature is 60 DEG C, speed of agitator is stirring 0.5h under 300r/min, prepares uniform mixed liquor A；
S5: add Carthamus yellow in the uniform mixed liquor A that step S4 prepares, nisin, maltose, starch sugar, acesulfame potassium, xylitol, vitamin E, vitamin K, vitamin PP, alanine, glutamic acid, aspartic acid, glycine, ferrum element, selenium element, cobalt element, zinc element, fumaric acid furfuryl alcohol propyl ester, 51-guanosine monophosphate disodium, 51-disodium 5'-ribonucleotide, glycine, carvone, dihydro jasmone, isoamyl acetate, 2-hexenol, it is 120W at microwave power, temperature is 52 DEG C, speed of agitator is stirring 0.3h under 400r/min, prepare uniform mixed liquid B；
S6: uniform mixed liquor step S5 prepared is 136 DEG C in temperature, and pressure is sterilizing 2s under 230KPa, prepares uniform mixed liquor C；
S7: uniform mixed liquor C step S6 prepared is 0.093MPa in vacuum, and temperature is to carry out fill, sealing at 92 DEG C, is then cooled to room temperature, prepares Herba Dendrobii tea vinegar drink.
Herba Dendrobii tea vinegar drink obtained by embodiment 1-3 carries out organoleptic quality, physical and chemical quality, preparation time mensuration, and result is as shown in table 1,2,3.
The organoleptic quality of table 1 Herba Dendrobii tea vinegar drink
| Embodiment | Color and luster | Mouthfeel | Fragrance |
| 1 | Limpid, golden yellow bright | Tea flavour is obvious, sour-sweet tasty and refreshing | Heavy flavour of vinegar fragrance, aobvious tea is fragrant |
| 2 | Limpid, golden yellow bright | Tea flavour is obvious, sour-sweet tasty and refreshing | Heavy flavour of vinegar fragrance, shows slightly tea fragrant |
| 3 | Limpid, golden yellow bright | Tea flavour is obvious, sour-sweet tasty and refreshing | Heavy flavour of vinegar fragrance, tea perfume (or spice) is more apparent |
As shown in Table 1, on the Herba Dendrobii tea vinegar drink color and luster that the present invention prepares limpid, golden yellow bright；Mouthfeel tea flavour is obvious, sour-sweet tasty and refreshing；Heavy flavour of vinegar fragrance on fragrance, has tea fragrant.
The physical and chemical quality of table 2 Herba Dendrobii tea vinegar drink
| Embodiment | Acetic acid content (g/L) | Polyphenol content (g/L) | PH value |
| 1 | 11.93 | 1.09 | 6.51 |
| 2 | 11.48 | 9.97 | 6.56 |
| 3 | 12.46 | 1.21 | 6.38 |
As shown in Table 2, the Herba Dendrobii tea vinegar drink acetic acid content that the present invention prepares is 11.48-12.46g/L, and polyphenol content is 9.97-1.21g/L, and pH value is 6.38-6.56.
The preparation time of table 3 Herba Dendrobii tea vinegar drink
| Embodiment | 1 | 2 | 3 | Prior art preparation time |
| Preparation time (h) | Less than 24h | Less than 24h | Less than 24h | More than 500h |
As shown in Table 3, the preparation time of the Herba Dendrobii tea vinegar drink that the present invention prepares is more shorter than the preparation time of prior art, thus shortens the production cycle, reduces cost.
The Herba Dendrobii tea vinegar drink of the present invention is dispelled implication effect test
Choose 67 people with implication symptom, the maleest 34 people, female 33 people.Drink the Herba Dendrobii tea vinegar drink 3 glasss of the present invention, every glass of 300mL every day, obtain result of the test after 5 days as shown in table 4.
Table 4 is dispelled implication effect test result
| Sex | Total number of persons | Implication transference cure | Implication symptom alleviates | Implication symptom is constant |
| Man | 34 | 30 | 4 | 0 |
| Female | 33 | 31 | 2 | 0 |
As shown in Table 4, the Herba Dendrobii tea vinegar drink of the present invention can effectively be treated or alleviate implication symptom.
Above content it cannot be assumed that the present invention be embodied as be confined to these explanations; for general technical staff of the technical field of the invention; without departing from the inventive concept of the premise; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by the claims submitted to.
Claims (7)
- null1. a Herba Dendrobii tea vinegar drink，It is characterized in that，In units of weight portion，Including following raw material: Herba Dendrobii fresh bar 155-196 part、Raw white tea 98-145 part、Cortex Moutan 9-14 part、Radix Notoginseng 7-10 part、Herba Eupatorii 6-8 part、Radix Saposhnikoviae 7-9 part、Semen Plantaginis 5-8 part、Herba Menthae 2-5 part、Fructus Forsythiae 4-6 part、Cortex Mori 4-9 part、Rhizoma Anemarrhenae 5-6 part、Flos Osmanthi Fragrantis 4-5 part、Malt vinegar 7-10 part、Carthamus yellow 2.5-6.2 part、Nisin 2.2-4.5 part、Maltose 7-9 part、Starch sugar 3-5 part、Acesulfame potassium 0.1-0.2 part、Xylitol 0.5-0.8 part、Vitamin E 0.6-1 part、Vitamin K 0.5-0.8 part、Vitamin PP 0.7-0.9 part、Alanine 0.5-0.7 part、Glutamic acid 0.3-0.5 part、Aspartic acid 0.4-0.6 part、Glycine 0.2-0.5 part、Ferrum element 0.07-0.22 part、Selenium element 0.12-0.2 part、Cobalt element 0.15-0.24 part、Zinc element 0.14-0.18 part、Polyvinyl pyrilodone 0.8-1.1 part、Hydroxypropyl methyl cellulose sodium 0.1-0.2 part、Polyacrylic acid potassium 0.14-0.25 part、Sodium alginate 0.14-0.22 part、Dupont EEA2112AC compatilizer 0.8-1.4 part、Food grade antioxidant different VC potassium 0.6-0.8 part、Xanthan gum 0.7-1.2 part、Fumaric acid furfuryl alcohol propyl ester 0.5-0.8 part、51-guanosine monophosphate disodium 0.08-0.18 part、51-disodium 5'-ribonucleotide 0.03-0.1 part、Glycine 0.05-0.07 part、Carvone 0.03-0.05 part，Dihydro jasmone 0.06-0.07 part、Isoamyl acetate 0.04-0.05 part、2-hexenol 0.07-0.09 part；The preparation method of described Herba Dendrobii tea vinegar drink, comprises the following steps:S1: the preparation of Herba Dendrobii juice, comprises the following steps；S11: crushed by cleaned Herba Dendrobii fresh bar strand grinding machine, filters by 60-90 mesh sieve, and prepared Herba Dendrobii minces；S12: the Herba Dendrobii that step S11 prepares is minced and mix loading extraction pot for the ratio of 1:2-4 in mass ratio with water, under pressure is 1-4MPa, by 5-6 layer filtered through gauze after decocting in water 0.5-1.5h, prepared filtrate A；S13: filtrate A rotating speed step S12 prepared is the centrifuge of 2000-5000r/min, sucking filtration roguing under vacuum is 0.065-0.085MPa, prepares Herba Dendrobii juice；S2, the preparation of raw white tea polyphenol, comprise the following steps:S21: raw white tea is dried and pulverizes to water content≤9%, cross 60-80 mesh sieve, mix for 1:9-11 in mass ratio with the ethanol water that mass fraction is 75%-80%, being 100-160W at microwave power, temperature extracts 25-34min at being 40-42 DEG C, filters, concentrate, prepare tea polyphenols crude extract A；S22: the tea polyphenols crude extract A that step S21 prepares is joined in the KCl solution that concentration is 12%-16%, pH regulator is to 5.2-6, impurity is removed under centrifugal rotational speed is 3500-4500r/min, using aperture is that the solution after being centrifuged is filtered at temperature is 29-36 DEG C by 0.03-0.1 μm filter membrane, prepares liquor B；S23: liquor B propyl ether step S22 prepared extracts, prepared raw white tea polyphenol freezing, dried；S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Radix Saposhnikoviae, Semen Plantaginis, Herba Menthae, Fructus Forsythiae, Cortex Mori, the Rhizoma Anemarrhenae, Flos Osmanthi Fragrantis are separately dried to water content≤8% co-grinding, add water, it is 1:10-14(W/V at solid-liquid ratio), microwave power is 120-180W, Extracting temperature is 85-92 DEG C, extraction time is 1.5-1.9h, then filtering residue, prepares medicinal liquid；S4: by step S1 prepare Herba Dendrobii juice, step S2 prepare raw white tea polyphenol, step S3 prepare medicinal liquid, malt vinegar, polyvinyl pyrilodone, hydroxypropyl methyl cellulose sodium, polyacrylic acid potassium, sodium alginate, Dupont EEA2112AC compatilizer, food grade antioxidant different VC potassium, xanthan gum, 1200-1400 part water mixing after, it is 100-150W at microwave power, temperature is 55-60 DEG C, speed of agitator is stirring 0.5-0.8h under 200-300r/min, prepares uniform mixed liquor A；S5: add Carthamus yellow in the uniform mixed liquor A that step S4 prepares, nisin, maltose, starch sugar, acesulfame potassium, xylitol, vitamin E, vitamin K, vitamin PP, alanine, glutamic acid, aspartic acid, glycine, ferrum element, selenium element, cobalt element, zinc element, fumaric acid furfuryl alcohol propyl ester, 51-guanosine monophosphate disodium, 51-disodium 5'-ribonucleotide, glycine, carvone, dihydro jasmone, isoamyl acetate, 2-hexenol, it is 80-120W at microwave power, temperature is 45-52 DEG C, speed of agitator is stirring 0.3-0.5h under 300-400r/min, prepare uniform mixed liquid B；S6: uniform mixed liquor sterilizing step S5 prepared, prepares uniform mixed liquor C；S7: the uniform mixed liquor C that step S6 prepares is carried out fill, sealing under negative pressure, then cools down, prepares Herba Dendrobii tea vinegar drink.
- Herba Dendrobii tea vinegar drink the most according to claim 1, it is characterised in that the temperature of mixed liquor sterilizing described in step S6 is 134-136 DEG C.
- Herba Dendrobii tea vinegar drink the most according to claim 2, it is characterised in that the pressure of described sterilizing is 210-230KPa.
- Herba Dendrobii tea vinegar drink the most according to claim 3, it is characterised in that the time of described sterilizing is 2-4s.
- Herba Dendrobii tea vinegar drink the most according to claim 1, it is characterised in that the vacuum of negative pressure described in step S7 is 0.088-0.091MPa.
- Herba Dendrobii tea vinegar drink the most according to claim 1, it is characterised in that the temperature that fill described in step S7, sealing use is 87-91 DEG C.
- Herba Dendrobii tea vinegar drink the most according to claim 1, it is characterised in that the temperature being cooled to described in step S7 is room temperature.
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| US11731948B2 (en) | 2016-09-21 | 2023-08-22 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
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| US11724993B2 (en) | 2016-09-21 | 2023-08-15 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
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| CN106562143A (en) * | 2016-10-20 | 2017-04-19 | 广西好青春醋业有限公司 | Sugar cane flavored vinegar drink and preparation method thereof |
| CN106562142A (en) * | 2016-10-20 | 2017-04-19 | 广西好青春醋业有限公司 | New sugar cane vinegar drink and preparation method thereof |
| CN106566767A (en) * | 2016-10-20 | 2017-04-19 | 广西好青春醋业有限公司 | Sugarcane fruit vinegar drink and preparation method thereof |
| CN106578750A (en) * | 2016-10-20 | 2017-04-26 | 广西好青春醋业有限公司 | Sugarcane vinegar beverage and making method thereof |
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