CN105994331A - Novel weeding composition and application thereof - Google Patents

Novel weeding composition and application thereof Download PDF

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Publication number
CN105994331A
CN105994331A CN201610441152.4A CN201610441152A CN105994331A CN 105994331 A CN105994331 A CN 105994331A CN 201610441152 A CN201610441152 A CN 201610441152A CN 105994331 A CN105994331 A CN 105994331A
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CN
China
Prior art keywords
effective ingredient
mixture
composition
heating
steps
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610441152.4A
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Chinese (zh)
Inventor
吴宏博
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HENAN ZHONG TIAN XIN BIOCHEMICAL TECHNOLOGY Co Ltd
Original Assignee
HENAN ZHONG TIAN XIN BIOCHEMICAL TECHNOLOGY Co Ltd
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Priority to CN201610441152.4A priority Critical patent/CN105994331A/en
Publication of CN105994331A publication Critical patent/CN105994331A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/36Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/16Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds
    • A01N33/18Nitro compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N35/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
    • A01N35/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical at least one of the bonds to hetero atoms is to nitrogen
    • A01N35/10Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical at least one of the bonds to hetero atoms is to nitrogen containing a carbon-to-nitrogen double bond
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647Triazoles; Hydrogenated triazoles
    • A01N43/6531,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/88Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms six-membered rings with three ring hetero atoms

Abstract

The invention discloses a novel weeding composition and application thereof. The novel weeding composition is prepared from a first effective ingredient, a second effective ingredient and a third effective ingredient, the first effective ingredient is a composition of pendimethalin, sulfentrazone and bentazone, the second effective ingredient is a composition of clethodim and halosulfuron-methyl, the third effective ingredient is a composition of a polar organic solvent, a defoaming agent, an anticorrosive agent, kaolin and deionized water, the weight ratio of the first effective ingredient to the second effective ingredient is 1:1-60:1, and the weight percentage of the sum of the first effective ingredient and the second effective ingredient in the composition is 15%-75%. The novel weeding composition is good in preventing and treating effect and weeding effect, free of pollution to the environment, capable of delaying the weed resistance, long in lasting period, capable of not harming crops and good in safe effect.

Description

A kind of herbicide composition and application thereof
Technical field
The present invention relates to technical field of pesticide combination, be specially a kind of herbicide composition and application thereof.
Background technology
Chemical method weeding is agriculturally one of Main Means controlling weeds, in recent years, due to some herbicide kinds Large area is used alone, and already leads to a lot of weeds and develops immunity to drugs, and meanwhile, grass when weeds occur is mutually complicated, not only 1 year Weeds are mixed raw for many years, and draft, liana and shrub have concurrently, and weeds emerge uneven, and seed, low age, weeds at advanced age are handed over Wrong generation, during so herbicide kind is used alone, all can show defect in a certain respect and limitation.
Summary of the invention
It is an object of the invention to provide a kind of herbicide composition and application thereof, to solve above-mentioned background technology carries The problem gone out.
For achieving the above object, the present invention provides following technical scheme: a kind of herbicide composition, including effective ingredient A, effective ingredient b and effective ingredient c, described effective ingredient a is the compositions of pendimethalin, sulfentrazone and bentazone;Described Effective ingredient b is the compositions of clethodim and halosulfuronmethyl;Described effective ingredient c is polar organic solvent, defoamer, anticorrosion The compositions of agent, Kaolin and deionized water, described effective ingredient a, the ratio of weight and number of effective ingredient b are 1:1-60:1, And the percentage by weight that the summation of described effective ingredient a, effective ingredient b is in the composition is 15%-75%.
Preferably, the preparation method of described effective ingredient a comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
Preferably, the preparation method of described effective ingredient b comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
Preferably, the preparation method of described effective ingredient c comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
Compared with prior art, the invention has the beneficial effects as follows: the present invention prevents and treats, herbicidal effect is good, environmentally safe, Can delay Weed Resistance, the lasting period is long, does not injure crops simultaneously, and safe effect is good;The Herbicidal mixture that the present invention provides The single pesticide of life-time service can be overcome easily to produce the shortcoming of resistance, extend the service life of herbicide, its popularization and application There are huge economic benefit and social benefit.
Detailed description of the invention
Below the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment It is only a part of embodiment of the present invention rather than whole embodiments, based on the embodiment in the present invention, the common skill in this area The every other embodiment that art personnel are obtained under not making creative work premise, broadly falls into the model of present invention protection Enclose.
The present invention provides a kind of technical scheme: a kind of herbicide composition, including effective ingredient a, effective ingredient b with have Effect composition c, described effective ingredient a are the compositions of pendimethalin, sulfentrazone and bentazone;Described effective ingredient b is alkene grass Ketone and the compositions of halosulfuronmethyl;Described effective ingredient c is polar organic solvent, defoamer, preservative, Kaolin and goes The compositions of ionized water, described effective ingredient a, the ratio of weight and number of effective ingredient b are 1:1-60:1, and described effective ingredient a, The summation of effective ingredient b percentage by weight in the composition is 15%-75%.
Embodiment one: the composition proportion of employing is: 3% pendimethalin, 4% sulfentrazone, 2% bentazone, 2% clethodim, 4% Halosulfuronmethyl, 10% polar organic solvent, 5% defoamer, 5% preservative, 5% Kaolin and 60% deionized water.
The preparation method of the present embodiment effective ingredient a comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
The preparation method of the present embodiment effective ingredient b comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
The preparation method of the present embodiment effective ingredient c comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
Embodiment two:
Use composition proportion be: 4% pendimethalin, 5% sulfentrazone, 3% bentazone, 4% clethodim, 4% halosulfuronmethyl, 15% Polar organic solvent, 3% defoamer, 3% preservative, 4% Kaolin and 55% deionized water.
The preparation method of the present embodiment effective ingredient a comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
The preparation method of the present embodiment effective ingredient b comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
The preparation method of the present embodiment effective ingredient c comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
Embodiment three:
Use composition proportion be: 5% pendimethalin, 5% sulfentrazone, 6% bentazone, 7% clethodim, 7% halosulfuronmethyl, 15% Polar organic solvent, 5% defoamer, 2% preservative, 3% Kaolin and 45% deionized water.
The preparation method of the present embodiment effective ingredient a comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
The preparation method of the present embodiment effective ingredient b comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
The preparation method of the present embodiment effective ingredient c comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
Embodiment four:
The composition proportion used is: 10% pendimethalin, 10% sulfentrazone, 10% bentazone, 10% clethodim, the 10% phonetic sulphur of chlorine pyrrole Grand, 8% polar organic solvent, 6% defoamer, 4% preservative, 4% Kaolin and 28% deionized water.
The preparation method of the present embodiment effective ingredient a comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
The preparation method of the present embodiment effective ingredient b comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
The preparation method of the present embodiment effective ingredient c comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
Embodiment five:
The composition proportion used is: 15% pendimethalin, 10% sulfentrazone, 15% bentazone, 10% clethodim, the 25% phonetic sulphur of chlorine pyrrole Grand, 4% polar organic solvent, 6% defoamer, 2% preservative, 3% Kaolin and 10% deionized water.
The preparation method of the present embodiment effective ingredient a comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
The preparation method of the present embodiment effective ingredient b comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
The preparation method of the present embodiment effective ingredient c comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
Embodiment six:
Use composition proportion be: 10% pendimethalin, 15% sulfentrazone, 5% bentazone, 10% clethodim, 5% halosulfuronmethyl, 10% polar organic solvent, 5% defoamer, 5% preservative, 5% Kaolin and 30% deionized water.
The preparation method of the present embodiment effective ingredient a comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
The preparation method of the present embodiment effective ingredient b comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
The preparation method of the present embodiment effective ingredient c comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
Experimental example:
Choose one piece of corn field or Peanut Fields as experiment field, use common herbicide and various embodiments of the present invention on the market to prepare Herbicide is sprayed in experiment field, even spray 5 times, carry out effect research in after medicine 15 days, and experimental result is as shown in the table:
From above table data, the herbicide that embodiment six prepares can reach optimum efficiency.
Present invention preventing and treating, herbicidal effect are good, environmentally safe, can delay Weed Resistance, and the lasting period is long, does not hinders simultaneously Evil crops, safe effect is good;The Herbicidal mixture that the present invention provides can overcome the single pesticide of life-time service easily to produce anti- The shortcoming of property, extends the service life of herbicide, and its popularization and application have huge economic benefit and social benefit.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, permissible Understand and these embodiments can be carried out multiple change without departing from the principles and spirit of the present invention, revise, replace And modification, the scope of the present invention be defined by the appended.

Claims (5)

1. a herbicide composition, it is characterised in that: include effective ingredient a, effective ingredient b and effective ingredient c, described in have Effect composition a is the compositions of pendimethalin, sulfentrazone and bentazone;Described effective ingredient b is clethodim and halosulfuronmethyl Compositions;Described effective ingredient c is the combination of polar organic solvent, defoamer, preservative, Kaolin and deionized water Thing, described effective ingredient a, the ratio of weight and number of effective ingredient b are 1:1-60:1, and described effective ingredient a, effective ingredient b Summation percentage by weight in the composition is 15%-75%.
A kind of herbicide composition the most according to claim 1, it is characterised in that: the preparation side of described effective ingredient a Method comprises the following steps:
A, pendimethalin and sulfentrazone are added in reactor and be heated to 45 DEG C, after heating 10min, adding bentazone;
B, mixture step A obtained use mechanical agitation, and mixing speed is 1000 revs/min, stand after stirring 20min, To effective ingredient a.
A kind of herbicide composition the most according to claim 1, it is characterised in that: the preparation side of described effective ingredient b Method comprises the following steps:
A, clethodim and halosulfuronmethyl are put into stirring container in, use mechanical agitation, speed of agitator is 1500 revs/min, stirs Stand after mixing 10min;
The mixture that step A is obtained by B heats, and heating-up temperature is 30 DEG C, stands and obtain effective ingredient b after heating 20min.
A kind of herbicide composition the most according to claim 1, it is characterised in that: the preparation side of described effective ingredient c Method comprises the following steps:
A, polar organic solvent, defoamer are put into stirring mixing in reactor;
B, in the mixture that step A obtains, add preservative and Kaolin, add post-heating to 55 DEG C, quiet after heating 10min Put;
C, in the mixture that step B obtains add deionized water, be cooled to room temperature afterwards, obtain mixture c.
On a kind of herbicide composition the most as claimed in claim 1 weeds in preventing and kill off corn field, Peanut Fields, Rapeseed Field Application.
CN201610441152.4A 2016-06-20 2016-06-20 Novel weeding composition and application thereof Pending CN105994331A (en)

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Application Number Priority Date Filing Date Title
CN201610441152.4A CN105994331A (en) 2016-06-20 2016-06-20 Novel weeding composition and application thereof

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Application Number Priority Date Filing Date Title
CN201610441152.4A CN105994331A (en) 2016-06-20 2016-06-20 Novel weeding composition and application thereof

Publications (1)

Publication Number Publication Date
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Country Status (1)

Country Link
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020102316A1 (en) * 2018-11-13 2020-05-22 Upl Limited Herbicidal combination

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1332608A (en) * 1998-11-10 2002-01-23 辛根塔参与股份公司 Herbicidal composition
CN104273167A (en) * 2014-09-19 2015-01-14 青岛蓝图文化传播有限公司市南分公司 Herbicide for tobacco farmland
CN105340917A (en) * 2015-12-04 2016-02-24 青岛钰兴石墨制品有限公司 Soybean field herbicide

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1332608A (en) * 1998-11-10 2002-01-23 辛根塔参与股份公司 Herbicidal composition
CN104273167A (en) * 2014-09-19 2015-01-14 青岛蓝图文化传播有限公司市南分公司 Herbicide for tobacco farmland
CN105340917A (en) * 2015-12-04 2016-02-24 青岛钰兴石墨制品有限公司 Soybean field herbicide

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020102316A1 (en) * 2018-11-13 2020-05-22 Upl Limited Herbicidal combination
CN114007424A (en) * 2018-11-13 2022-02-01 Upl有限公司 Herbicide combinations
US11311015B2 (en) * 2018-11-13 2022-04-26 Upl Limited Herbicidal combination

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